CN108497417A - A kind of compound buccal tablet of matrimony vine royal jelly and preparation method thereof - Google Patents
A kind of compound buccal tablet of matrimony vine royal jelly and preparation method thereof Download PDFInfo
- Publication number
- CN108497417A CN108497417A CN201810343026.4A CN201810343026A CN108497417A CN 108497417 A CN108497417 A CN 108497417A CN 201810343026 A CN201810343026 A CN 201810343026A CN 108497417 A CN108497417 A CN 108497417A
- Authority
- CN
- China
- Prior art keywords
- mass parts
- royal jelly
- matrimony vine
- xeraphium
- celery
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229940109850 royal jelly Drugs 0.000 title claims abstract description 104
- 244000241838 Lycium barbarum Species 0.000 title claims abstract description 79
- 235000015459 Lycium barbarum Nutrition 0.000 title claims abstract description 79
- 150000001875 compounds Chemical class 0.000 title claims abstract description 28
- 229940046011 buccal tablet Drugs 0.000 title claims abstract description 27
- 239000006189 buccal tablet Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 238000001035 drying Methods 0.000 claims abstract description 62
- 240000007087 Apium graveolens Species 0.000 claims abstract description 47
- 235000015849 Apium graveolens Dulce Group Nutrition 0.000 claims abstract description 47
- 235000010591 Appio Nutrition 0.000 claims abstract description 47
- 241000220225 Malus Species 0.000 claims abstract description 42
- 235000011430 Malus pumila Nutrition 0.000 claims abstract description 42
- 235000015103 Malus silvestris Nutrition 0.000 claims abstract description 42
- 240000008067 Cucumis sativus Species 0.000 claims abstract description 39
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 claims abstract description 39
- 239000000843 powder Substances 0.000 claims abstract description 30
- 238000000034 method Methods 0.000 claims abstract description 26
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 22
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims abstract description 18
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 11
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 11
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims abstract description 9
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims abstract description 9
- 235000019359 magnesium stearate Nutrition 0.000 claims abstract description 9
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims abstract description 9
- 239000008108 microcrystalline cellulose Substances 0.000 claims abstract description 9
- 229940016286 microcrystalline cellulose Drugs 0.000 claims abstract description 9
- 229910021487 silica fume Inorganic materials 0.000 claims abstract description 9
- 229930006000 Sucrose Natural products 0.000 claims abstract description 7
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 7
- 239000005720 sucrose Substances 0.000 claims abstract description 7
- 238000004108 freeze drying Methods 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 15
- 238000012545 processing Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 13
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 11
- 239000004471 Glycine Substances 0.000 claims description 8
- 238000005292 vacuum distillation Methods 0.000 claims description 5
- 241000219112 Cucumis Species 0.000 claims description 3
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims description 3
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 3
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims description 3
- 239000012153 distilled water Substances 0.000 claims description 3
- 230000007935 neutral effect Effects 0.000 claims description 3
- 230000001954 sterilising effect Effects 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000003826 tablet Substances 0.000 claims description 3
- 235000002710 Ilex cornuta Nutrition 0.000 claims 1
- 241001310146 Ilex cornuta Species 0.000 claims 1
- 235000010326 Osmanthus heterophyllus Nutrition 0.000 claims 1
- 239000002002 slurry Substances 0.000 claims 1
- 239000007937 lozenge Substances 0.000 abstract description 10
- 150000004676 glycans Chemical class 0.000 abstract description 8
- 229920001282 polysaccharide Polymers 0.000 abstract description 8
- 239000005017 polysaccharide Substances 0.000 abstract description 8
- 238000010298 pulverizing process Methods 0.000 abstract description 8
- 235000016709 nutrition Nutrition 0.000 abstract description 7
- 230000035764 nutrition Effects 0.000 abstract description 7
- 238000005260 corrosion Methods 0.000 abstract description 6
- 230000007797 corrosion Effects 0.000 abstract description 6
- 238000007710 freezing Methods 0.000 description 9
- 230000008014 freezing Effects 0.000 description 9
- 238000005516 engineering process Methods 0.000 description 7
- 235000013305 food Nutrition 0.000 description 7
- 239000012071 phase Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- QHBZHVUGQROELI-SOFGYWHQSA-N (E)-10-hydroxydec-2-enoic acid Chemical compound OCCCCCCC\C=C\C(O)=O QHBZHVUGQROELI-SOFGYWHQSA-N 0.000 description 4
- QHBZHVUGQROELI-UHFFFAOYSA-N Royal Jelly acid Natural products OCCCCCCCC=CC(O)=O QHBZHVUGQROELI-UHFFFAOYSA-N 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- 235000013399 edible fruits Nutrition 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 150000007524 organic acids Chemical class 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 239000011521 glass Substances 0.000 description 3
- 235000013311 vegetables Nutrition 0.000 description 3
- 239000004677 Nylon Substances 0.000 description 2
- 240000000111 Saccharum officinarum Species 0.000 description 2
- 235000007201 Saccharum officinarum Nutrition 0.000 description 2
- 230000036772 blood pressure Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 235000013402 health food Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 235000015110 jellies Nutrition 0.000 description 2
- 239000008274 jelly Substances 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 229920001778 nylon Polymers 0.000 description 2
- 235000013324 preserved food Nutrition 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000000859 sublimation Methods 0.000 description 2
- 230000008022 sublimation Effects 0.000 description 2
- 235000015468 Lycium chinense Nutrition 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000012907 honey Nutrition 0.000 description 1
- 235000008446 instant noodles Nutrition 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000008194 pharmaceutical composition Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- 238000009777 vacuum freeze-drying Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/09—Mashed or comminuted products, e.g. pulp, purée, sauce, or products made therefrom, e.g. snacks
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Botany (AREA)
- Mycology (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The application provides a kind of compound buccal tablet of matrimony vine royal jelly and preparation method thereof, wherein method includes：Royal jelly xeraphium is prepared, matrimony vine, apple and cucumber combination drying powder is prepared, prepares celery xeraphium, dispensing, tabletting.It solves the problems, such as that the sour corrosion of royal jelly in royal jelly pulverizing process is brought, solves the problems, such as that polysaccharides in matrimony vine pulverizing process brought sticks together.Compound buccal tablet includes：200 400 mass parts of royal jelly xeraphium；600 800 mass parts of matrimony vine, apple and cucumber combination drying powder；400 600 mass parts of celery xeraphium；20 40 mass parts of sucrose；5 20 mass parts of D-sorbite；13 mass parts of glycine；5 10 mass parts of magnesium stearate；15 mass parts of micro- silica white；5 20 mass parts of sodium bicarbonate；15 25 mass parts of microcrystalline cellulose.The compound buccal tablet of matrimony vine royal jelly provided by the present application, a piece of lozenge is combined by royal jelly, matrimony vine, cucumber, apple and celery, keeps the healthcare function of the compound buccal tablet abundant, and nutrition is balanced, in good taste, easily absorbs.
Description
Technical field
This application involves technical field of food healthcare more particularly to a kind of compound buccal tablet of matrimony vine royal jelly and its preparation sides
Method.
Background technology
In many countries, nutrient and healthcare products industry has become new industry mutually accelerate development unexpectedly, important and economy
Increase bright spot.Honey increasingly has been favored by people as the outstanding person in current health food.Though fresh royal jelly product is
The traditional tonic food in China, but also have inconvenience when edible.For example, the activity due to fresh royal jelly is extremely strong, normal
It cannot keep its quality under temperature, it is necessary to which cryogenic freezing preserves.And the royal jelly freezed is very inconvenient when daily edible, it can not
Travelling carries, and is increasingly not suitable with the requirement of human lives' tempo increase.
It is quick freezing that frozen dried food, which is frozen dried food, the dehydration of vacuum ice-like, save original color, nutrition at
Divide the appearance with original material, and there is good rehydration, and be free of any additive, is ideal naturally hygienic food
Product.The time that freeze drying technology rises in China is not grown also, has been mainly used on pharmaceutical formulations field and instant noodles dewatered vegetables.
Freeze-dried powder is made in fresh royal jelly using freeze-drying, its can be kept activity stabilized and stores 3 years mass conservations, and
It can be restored to original state after adding water to restore, the indexs such as color are similar with fresh royal jelly, are ideal royal jelly manufactured goods.
However, in the preparation method of existing royal jelly product, there are problems that.For example, being isolated from royal jelly
A kind of organic acid royal jelly acid, be one of important component of royal jelly, be a kind of special unsaturated organic acid, royal jelly is permitted
More properties such as smell, pH value etc. are all related with it.The pure white crystal of royal jelly acid, in fresh royal jelly mostly in a free form
In the presence of Nature comparison is stablized, and causes royal jelly to have certain corrosivity since its acidity exists, influences preparation manipulation.
Royal jelly has huge resource and the market demand, the research and development and application of New Processing that can make this in China
One product is more easily supplied to domestic and international consumer.
Invention content
A kind of compound buccal tablet of matrimony vine royal jelly of the application offer and preparation method thereof.
In a first aspect, this application provides a kind of preparation method of the compound buccal tablet of matrimony vine royal jelly, this method includes：
(1) royal jelly xeraphium is prepared：
Fresh royal jelly is taken, with distilled water with volume ratio for 1:1 ratio mixing, stirs evenly, filters, obtain pure bee
Royal jelly；
Sodium bicarbonate is added into pure royal jelly, it is neutrality to be neutralized to pH value；
Neutral pure royal jelly is put into precooling under (- 30) DEG C-(- 35) DEG C environment and handles 1h-3h；
It will be put into less than -50 DEG C drying boxes of temperature by the pure royal jelly of precooling processing, vacuum and low temperature freezing is dry
Dry 40h, then drying box temperature is risen to 30 DEG C -40 DEG C, heated drying 1h-2h；
The royal jelly after drying is crushed, royal jelly xeraphium is obtained；
(2) matrimony vine, apple and cucumber combination drying powder are prepared：
High-quality matrimony vine, apple and cucumber are taken, clean respectively, peeling, remove seed, slice；
By the matrimony vine of sheet, apple and cucumber, it is respectively put into precooling processing 3h- under (- 30) DEG C-(- 35) DEG C environment
5h；
It takes out, is put into less than -50 DEG C drying boxes of temperature, vacuum and low temperature is freeze-dried 48h, then drying box temperature is risen to
30 DEG C -40 DEG C, heated drying 1h-2h；
It takes out, is crushed under the conditions of cryogenic vacuum, obtain matrimony vine, apple and cucumber combination drying powder；
(3) celery xeraphium is prepared：
High-quality celery is taken, cleans, squeeze the juice, obtain Celery Juice；
Celery Juice vacuum distillation is condensed into celery stiff paste；
Celery stiff paste is dry, crushing, obtains celery xeraphium；
(4) dispensing：
Take respectively the matrimony vine, apple that royal jelly xeraphium 200-400 mass parts, step (2) that step (1) obtains obtain with
And cucumber combination drying powder 600-800 mass parts, step (3) obtain celery xeraphium 400-600 mass parts, sucrose 20-40
Mass parts, D-sorbite 5-20 mass parts, glycine 1-3 mass parts, magnesium stearate 5-10 mass parts, micro- silica white 1-5 mass
Part and sodium bicarbonate 5-20 mass parts, mixing cross 100-200 mesh sieve, obtain mixture；
Microcrystalline cellulose 15-25 mass parts are added into the mixture, mixing crushes, and crosses 80-120 mesh sieve, is pressed
Piece materials；
(5) tabletting：
The tabletting materials are fitted into tablet press machine, tabletting, sterilizing, obtain the compound buccal tablet of matrimony vine royal jelly.
Further, in the matrimony vine, apple and cucumber combination drying powder, matrimony vine xeraphium, apple xeraphium and Huang
The ratio of melon xeraphium is 10:13:12.
Further, in step (1), by the vacuum degree control of drying box in 0.01MPa or less；In step (2), it will do
The vacuum degree control of dry case is in 0.009MPa or less.
Further, in step (1), after the vacuum and low temperature freeze-drying 40h, by the temperature of drying box in 3h-4h
Rise to 30 DEG C -40 DEG C.
Further, in step (4), 300 mass parts of royal jelly xeraphium, step (2) that step (1) obtains is taken to obtain respectively
To 700 mass parts of matrimony vine, apple and cucumber combination drying powder, step (3) obtain 500 mass parts of celery xeraphium, sugarcane
Sugared 30 mass parts, 10 mass parts of D-sorbite, 2 mass parts of glycine, 7 mass parts of magnesium stearate, 3 mass parts of micro- silica white and
10 mass parts of sodium bicarbonate, mixing cross 100-200 mesh sieve, obtain mixture；
20 mass parts of microcrystalline cellulose are added into the mixture, mixing crushes, and crosses 80-120 mesh sieve, obtains tabletting
Materials.
By above technical scheme it is found that the application provides a kind of preparation method of the compound buccal tablet of matrimony vine royal jelly, including：
Royal jelly xeraphium is prepared, matrimony vine, apple and cucumber combination drying powder is prepared, prepares celery xeraphium, dispensing, tabletting five
Step.In step (1), the impurity in fresh royal jelly is first removed, and is handled to neutrality, then pre-cooled jelly is handled, vacuum is low
Temperature freeze-drying and heated drying, are made royal jelly xeraphium；In step (2), to pretreated matrimony vine, apple and cucumber
Precooling processing, vacuum and low temperature freeze-drying and heated drying processing are carried out, matrimony vine, apple and cucumber combination drying powder is made；
In step (3), vacuum distillation is carried out to Celery Juice and is condensed into celery stiff paste, then is dried, crushes, obtains celery drying
Powder；Through step (4) blending process, tabletting materials are obtained, through step (5), obtain the compound buccal tablet of matrimony vine royal jelly.The application system
Preparation Method solves the problems, such as that the sour corrosion of royal jelly in royal jelly pulverizing process is brought, solves in matrimony vine pulverizing process
What polysaccharides was brought sticks together problem, and royal jelly, matrimony vine, cucumber, apple and celery are combined into a piece of lozenge, keep this compound
The healthcare function of buccal tablet is abundant, and nutrition is balanced, in good taste, easily absorbs.
Second aspect, the application provide a kind of compound buccal tablet of matrimony vine royal jelly, including：Royal jelly xeraphium 200-400
Mass parts；Matrimony vine, apple and cucumber combination drying powder 600-800 mass parts；Celery xeraphium 400-600 mass parts；Sucrose
20-40 mass parts；D-sorbite 5-20 mass parts；Glycine 1-3 mass parts；Magnesium stearate 5-10 mass parts；Micro- silica white 1-5
Mass parts；Sodium bicarbonate 5-20 mass parts；Microcrystalline cellulose 15-25 mass parts.
The compound buccal tablet of matrimony vine royal jelly provided by the present application, royal jelly, matrimony vine, cucumber, apple and celery is compound
At a piece of lozenge, keep the healthcare function of the compound buccal tablet abundant, nutrition is balanced, in good taste, easily absorbs.
Description of the drawings
In order to illustrate more clearly of the technical solution of the application, letter will be made to attached drawing needed in the embodiment below
Singly introduce, it should be apparent that, for those of ordinary skills, without having to pay creative labor,
Other drawings may also be obtained based on these drawings.
Fig. 1 is a kind of preparation method of matrimony vine royal jelly compound buccal tablet of the application shown according to an exemplary embodiment
Flow chart；
Fig. 2 is the thinning method flow chart of step S110 in embodiment illustrated in fig. 1 method；
Fig. 3 is the thinning method flow chart of step S120 in embodiment illustrated in fig. 1 method；
Fig. 4 is the thinning method flow chart of step S130 in embodiment illustrated in fig. 1 method.
Specific implementation mode
Referring to Fig. 1 to Fig. 4, wherein Fig. 1 is multiple for a kind of matrimony vine royal jelly of the application shown according to an exemplary embodiment
It heals up the preparation method flow chart of lozenge, Fig. 2 is the thinning method flow chart of step S110 in embodiment illustrated in fig. 1 method, Fig. 3
For the thinning method flow chart of step S120 in embodiment illustrated in fig. 1 method, Fig. 4 is step in embodiment illustrated in fig. 1 method
The thinning method flow chart of S130.
A kind of preparation method of compound buccal tablet of matrimony vine royal jelly provided by the present application, including：
Step S110 prepares royal jelly xeraphium；
Specifically include following sub-steps：
Step S111, takes fresh royal jelly, with distilled water with volume ratio for 1:1 ratio mixing, stirs evenly, filters,
Obtain pure royal jelly；
There are a small amount of wax bits and larva, the presence of these impurity in fresh royal jelly, is unfavorable for the long-term storage of royal jelly
And processing, it is therefore necessary to remove it.The application is preferably filtered using brush worry method, and specific practice is first in thickness 1cm
The nylon leaching net of a 80-100 mesh is fixed in the glass drum bottom of left and right, and hairbrush, hairbrush are made with the nylon yarn rich in toughness
Backboard is made with 1cm with fixed organic glass, and there is fixing axle at middle part, which is connected with machine shaft.Then with distillation
Water is with royal jelly with volume ratio for 1:1 ratio mixed diluting pours into filter glass bucket refined filtration, obtains pure royal jelly.
Sodium bicarbonate is added into pure royal jelly in step S112, and it is neutrality to be neutralized to pH value；
A kind of organic acid royal jelly acid isolated in royal jelly, is one of important component of royal jelly, is a kind of special
Unsaturated organic acid, many properties such as smell, pH value of royal jelly etc. are all related with it.The pure white crystal of royal jelly acid, new
More in fresh royal jelly to exist in a free form, Nature comparison is stablized, and due to its presence, royal jelly is caused to have certain corruption
Corrosion influences preparation manipulation.
Based on this, the application is neutralized to neutrality by the way that sodium bicarbonate is added into pure royal jelly, by royal jelly, eliminates bee
The sour corrosion of royal jelly is convenient for subsequent preparation manipulation.
Neutral pure royal jelly is put into precooling under (- 30) DEG C-(- 35) DEG C environment and handles 1h-3h by step S113；
Preferably, cryogenic freezing is carried out using low temperature refrigerator, temperature controls between -30 to -35 DEG C, chilling rate control
In 2-3 DEG C/min, cooling time is controlled in 2h.
Step S114 will be put by the pure royal jelly of precooling processing in less than -50 DEG C drying boxes of temperature, and vacuum is low
Temperature freeze-drying 40h, then drying box temperature is risen to 30 DEG C -40 DEG C, heated drying 1h-2h；
Freeze-drying is that is, under cryogenic a kind of novel dried technology is freezed wet stock, then in higher vacuum
Lower heating, makes solid ice distil, and sloughs the moisture in material, and full name is Vacuum Freezing ＆ Drying Technology, abbreviation freeze drying technology.
Vacuum freeze drying basic principle is three phase changes based on water.With the reduction of pressure, the freezing point variation of water is not
Greatly, and boiling point constantly declines, and moves closer to freezing point.When the boiling point of water, which is down to, to be overlapped with freezing point, gas, liquid, solid three-phase water coexists,
Corresponding othermohygrometer value claims three phase point at this time, and the three phase point of pure water is (610.5Pa, 0.01 DEG C).In triple point and pressure
Power referred to as distils hereinafter, ice is directly translated into gas phase by solid phase.Under high vacuum state, using sublimation principle, make to freeze in advance
Moisture in the food of knot is directly removed with the distillation of ice state for vapor, to obtain freeze-drying and dehydrating food.It was lyophilized
Journey needs, in freeze-drying stage additional heat, frozen fraction constantly to be passed to by drying layer, at distillation interface since distillation is absorbed heat
On, hydrone enters in ambient enviroment along capillary after being heated and is captured and excluded by condenser, avoids the reduction of vacuum degree.
In the drying process, material necessarily is in vacuum refrigeration state, and temperature of charge need to be maintained to be less than triple point.
In the application step S114, the refrigeration equipment of condenser is opened, its temperature is made to be maintained at -50 DEG C hereinafter, being put into
The good queen bee lumps of pre-freeze；Open vacuum pump, make drying box formed negative pressure of vacuum, using physics sublimation principle to royal jelly into
Row freeze-drying, vacuum degree general control is in 0.01MPa or less.
After vacuum and low temperature freeze-drying, product still have 10% or so do not freeze and the water that is firmly adsorbed by product, at this moment
It needs the temperature of drying box to be increased to 30 DEG C -40 DEG C, the time control of heating is in 3-4h, heated drying 1h-2h.
Step S115 crushes the royal jelly after drying, obtains royal jelly xeraphium；
After above-mentioned steps S114, dried royal jelly material is taken out, processing is crushed with pulverizer, obtains queen bee
Starch xeraphium.
In the above embodiments of the present application, the pH value of fresh royal jelly is adjusted by sodium bicarbonate, solves royal jelly powder
The problem of sour corrosion of royal jelly is brought in the process, convenient for the progress of powder operation subsequently processed.
The preparation method of a kind of compound buccal tablet of matrimony vine royal jelly provided by the present application, after above-mentioned steps S110, in step
In rapid S120, matrimony vine, apple and cucumber combination drying powder are prepared.
Matrimony vine is a kind of health food with medical value being popular, and one of main component is polysaccharides,
Polysaccharides is a kind of water-soluble polysaccharide, is most important active constituent in matrimony vine, relative molecular mass 68-200.In matrimony vine
Drying pulverizing process in, due to the presence of polysaccharides, easily make Walfberry fruit particle generation stick together, the application using low temperature cold freeze-drying
Dry crushing technology solves the problems, such as the adhesion of polysaccharides in matrimony vine pulverizing process brought.
Cucumber, apple and celery are common acquired fruit or vegetable type foods, have cosmetic slimming, it is clearing heat and detoxicating and
Reduce blood pressure equal health-care effects.Royal jelly, matrimony vine, cucumber, apple and celery are combined into a piece of lozenge by the application, keep this multiple
Heal up lozenge healthcare function it is abundant, nutrition is balanced, in good taste, easily absorbs.
Based on this, above-mentioned steps S120 specifically includes following steps：
Step 121, high-quality matrimony vine, apple and cucumber are taken, clean respectively, peeling, remove seed, slice；
There are a small amount of matrimony vine leaf, mouldy little particle matrimony vine etc. in the matrimony vine of common procurement, the presence of these impurity, no
Conducive to the long-term storage and processing of matrimony vine, it is therefore necessary to be gone out.In general, by large fan, the leaf in matrimony vine is removed,
Then particle sieve is used, mouldy little particle, the fragment etc. in matrimony vine is removed, finally also needs to clean by artificial screening,
It can obtain high-quality matrimony vine.
The matrimony vine of sheet, apple and cucumber are respectively put under (- 30) DEG C-(- 35) DEG C environment and are pre-chilled by step S122
Freeze processing 3h-5h；
Preferably, cryogenic freezing is carried out using low temperature refrigerator, temperature controls between -30 to -35 DEG C, chilling rate control
In 2-3 DEG C/min, cooling time is controlled in 4h.
Step S123 takes out, and is put into less than -50 DEG C drying boxes of temperature, vacuum and low temperature is freeze-dried 48h, then will dry
Box temperature degree rises to 30 DEG C -40 DEG C, heated drying 1h-2h；
Preferably, in step S123, by the vacuum degree control of drying box in 0.009MPa or less.
Step S124 takes out, and is crushed under the conditions of cryogenic vacuum, obtains matrimony vine, apple and cucumber combination drying powder；
Containing a large amount of sugar in matrimony vine, when ambient ground, is easy caking, is unfavorable for crushing.The application uses cryogenic vacuum powder
Broken technology handles it, obtains wolfberry fruit powder in bulk.Specific treatment temperature and vacuum degree, the visual specific feelings of those skilled in the art
Condition voluntarily adjusts setting.
Preferably, in the matrimony vine, apple and cucumber combination drying powder, matrimony vine xeraphium, apple xeraphium and Huang
The ratio of melon xeraphium is 10:13:12.
The preparation method of a kind of compound buccal tablet of matrimony vine royal jelly provided by the present application, after above-mentioned steps S120, in step
In rapid S130, celery xeraphium is prepared, following step is specifically included：
Step S131 takes high-quality celery, cleans, squeezes the juice, obtains Celery Juice；
Celery Juice vacuum distillation is condensed into celery stiff paste by step S132；
Step S133, celery stiff paste is dry, crushing, obtains celery xeraphium；
After above-mentioned steps S130, in step S140, dispensing is carried out as steps described below：
The matrimony vine, apple that the royal jelly xeraphium 200-400 mass parts that step S110 obtains, step S120 obtain are taken respectively
And cucumber combination drying powder 600-800 mass parts, step S130 obtain celery xeraphium 400-600 mass parts, sucrose 20-
40 mass parts, D-sorbite 5-20 mass parts, glycine 1-3 mass parts, magnesium stearate 5-10 mass parts, micro- silica white 1-5 matter
Part and sodium bicarbonate 5-20 mass parts are measured, mixing crosses 100-200 mesh sieve, obtains mixture；
Microcrystalline cellulose 15-25 mass parts are added into the mixture, mixing crushes, and crosses 80-120 mesh sieve, is pressed
Piece materials.
Preferably, take respectively matrimony vine that 300 mass parts of royal jelly xeraphium that step S110 obtains, step S120 obtain,
500 mass parts of celery xeraphium, 30 mass of sucrose that 700 mass parts of apple and cucumber combination drying powder, step S130 are obtained
Part, 10 mass parts of D-sorbite, 2 mass parts of glycine, 7 mass parts of magnesium stearate, 3 mass parts of micro- silica white and sodium bicarbonate 10
Mass parts, mixing cross 100-200 mesh sieve, obtain mixture；20 mass parts of microcrystalline cellulose are added into the mixture, mix
It is even, it crushes, crosses 80-120 mesh sieve, obtain tabletting materials.
In step S150, the tabletting materials are fitted into tablet press machine, it is compound to obtain matrimony vine royal jelly for tabletting, sterilizing
Buccal tablet.
By above-described embodiment it is found that the application provides a kind of preparation method of the compound buccal tablet of matrimony vine royal jelly, including：System
Standby royal jelly xeraphium prepares matrimony vine, apple and cucumber combination drying powder, prepares five celery xeraphium, dispensing, tabletting steps
Suddenly.In step s 110, the impurity in fresh royal jelly is first removed, and is handled to neutrality, then the processing of pre-cooled jelly, vacuum and low temperature
Royal jelly xeraphium is made in freeze-drying and heated drying；In the step s 120, to pretreated matrimony vine, apple and cucumber
Precooling processing, vacuum and low temperature freeze-drying and heated drying processing are carried out, matrimony vine, apple and cucumber combination drying powder is made；
In step s 130, vacuum distillation is carried out to Celery Juice and is condensed into celery stiff paste, then be dried, crush, obtain celery drying
Powder；Through step S140 blending processes, tabletting materials are obtained, through step S150, obtain the compound buccal tablet of matrimony vine royal jelly.The application
Preparation method solves the problems, such as that the sour corrosion of royal jelly in royal jelly pulverizing process is brought, solves matrimony vine pulverizing process
What middle polysaccharides was brought sticks together problem, and royal jelly, matrimony vine, cucumber, apple and celery are combined into a piece of lozenge, keeps this multiple
Heal up lozenge healthcare function it is abundant, nutrition is balanced, in good taste, easily absorbs.
The embodiment of the present application also provides a kind of compound buccal tablet of matrimony vine royal jelly, including：Royal jelly xeraphium 200-
400 mass parts；Matrimony vine, apple and cucumber combination drying powder 600-800 mass parts；Celery xeraphium 400-600 mass parts；Sugarcane
Sugared 20-40 mass parts；D-sorbite 5-20 mass parts；Glycine 1-3 mass parts；Magnesium stearate 5-10 mass parts；Micro- silica white
1-5 mass parts；Sodium bicarbonate 5-20 mass parts；Microcrystalline cellulose 15-25 mass parts.
Cucumber, apple and celery are common acquired fruit or vegetable type foods, have cosmetic slimming, it is clearing heat and detoxicating and
Reduce blood pressure equal health-care effects.Royal jelly, matrimony vine, cucumber, apple and celery are combined into a piece of lozenge by the application, keep this multiple
Heal up lozenge healthcare function it is abundant, nutrition is balanced, in good taste, easily absorbs.
The same or similar parts between the embodiments can be referred to each other in this specification.Especially for embodiment
Speech, since it is substantially similar to the method embodiment, so description is fairly simple, related place is referring to saying in embodiment of the method
It is bright.
Invention described above embodiment is not intended to limit the scope of the present invention..
Claims (6)
1. a kind of preparation method of the compound buccal tablet of matrimony vine royal jelly, which is characterized in that the method includes：
(1) royal jelly xeraphium is prepared：
Fresh royal jelly is taken, with distilled water with volume ratio for 1:1 ratio mixing, stirs evenly, filters, obtain pure queen bee
Slurry；
Sodium bicarbonate is added into pure royal jelly, it is neutrality to be neutralized to pH value；
Neutral pure royal jelly is put into precooling under (- 30) DEG C-(- 35) DEG C environment and handles 1h-3h；
It will be put into less than -50 DEG C drying boxes of temperature by the pure royal jelly of precooling processing, vacuum and low temperature freeze-drying
40h, then drying box temperature is risen to 30 DEG C -40 DEG C, heated drying 1h-2h；
The royal jelly after drying is crushed, royal jelly xeraphium is obtained；
(2) matrimony vine, apple and cucumber combination drying powder are prepared：
High-quality matrimony vine, apple and cucumber are taken, clean respectively, peeling, remove seed, slice；
By the matrimony vine of sheet, apple and cucumber, it is respectively put into precooling processing 3h-5h under (- 30) DEG C-(- 35) DEG C environment；
It takes out, is put into less than -50 DEG C drying boxes of temperature, vacuum and low temperature is freeze-dried 48h, then drying box temperature is risen to 30
DEG C -40 DEG C, heated drying 1h-2h；
It takes out, is crushed under the conditions of cryogenic vacuum, obtain matrimony vine, apple and cucumber combination drying powder；
(3) celery xeraphium is prepared：
High-quality celery is taken, cleans, squeeze the juice, obtain Celery Juice；
Celery Juice vacuum distillation is condensed into celery stiff paste；
Celery stiff paste is dry, crushing, obtains celery xeraphium；
(4) dispensing：
Matrimony vine, apple and the Huang that royal jelly xeraphium 200-400 mass parts, step (2) that step (1) obtains obtain are taken respectively
Celery xeraphium 400-600 mass parts, the sucrose 20-40 mass that melon combination drying powder 600-800 mass parts, step (3) obtain
Part, D-sorbite 5-20 mass parts, glycine 1-3 mass parts, magnesium stearate 5-10 mass parts, micro- silica white 1-5 mass parts with
And sodium bicarbonate 5-20 mass parts, mixing, 100-200 mesh sieve is crossed, mixture is obtained；
Microcrystalline cellulose 15-25 mass parts are added into the mixture, mixing crushes, and crosses 80-120 mesh sieve, obtains tabletting use
Material；
(5) tabletting：
The tabletting materials are fitted into tablet press machine, tabletting, sterilizing, obtain the compound buccal tablet of matrimony vine royal jelly.
2. according to the method described in claim 1, it is characterized in that, in the matrimony vine, apple and cucumber combination drying powder, Chinese holly
The ratio of Qi xeraphium, apple xeraphium and cucumber xeraphium is 10:13:12.
3. according to the method described in claim 1, it is characterized in that, in step (1), the vacuum degree control of drying box is existed
0.01MPa or less；In step (2), by the vacuum degree control of drying box in 0.009MPa or less.
4. according to the method described in claim 1, it is characterized in that, in step (1), the vacuum and low temperature is freeze-dried 40h
Afterwards, the temperature of drying box is risen to 30 DEG C -40 DEG C in 3h-4h.
5. according to the method described in claim 1, it is characterized in that, in step (4), the queen bee that takes step (1) to obtain respectively
300 mass parts of xeraphium, 700 mass parts of matrimony vine, apple and cucumber combination drying powder that step (2) obtains, step (3) is starched to obtain
500 mass parts of celery xeraphium that arrive, 30 mass parts of sucrose, 10 mass parts of D-sorbite, 2 mass parts of glycine, magnesium stearate 7
10 mass parts of mass parts, 3 mass parts of micro- silica white and sodium bicarbonate, mixing cross 100-200 mesh sieve, obtain mixture；
20 mass parts of microcrystalline cellulose are added into the mixture, mixing crushes, and crosses 80-120 mesh sieve, obtains tabletting materials.
6. a kind of compound buccal tablet of matrimony vine royal jelly, which is characterized in that including：
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810343026.4A CN108497417A (en) | 2018-04-17 | 2018-04-17 | A kind of compound buccal tablet of matrimony vine royal jelly and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810343026.4A CN108497417A (en) | 2018-04-17 | 2018-04-17 | A kind of compound buccal tablet of matrimony vine royal jelly and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108497417A true CN108497417A (en) | 2018-09-07 |
Family
ID=63382264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810343026.4A Pending CN108497417A (en) | 2018-04-17 | 2018-04-17 | A kind of compound buccal tablet of matrimony vine royal jelly and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108497417A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3123542A1 (en) * | 2021-06-04 | 2022-12-09 | Laboratoires Super Diet | NEW FLUIDIFIED COMPOSITION CONTAINING ROYAL JELLY |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1466983A (en) * | 2003-05-22 | 2004-01-14 | 四川省辰龙股份有限公司 | Matrimony vine royal jelly capsule and method for preparing the same |
| CN105962237A (en) * | 2016-05-09 | 2016-09-28 | 武汉思维特食品有限公司 | Royal jelly-propolis-momordica charantia lozenges and preparation method thereof |
| CN106962909A (en) * | 2017-03-14 | 2017-07-21 | 福建省神蜂科技开发有限公司 | A kind of matrimony vine royal jelly complex capsule and preparation method thereof |
-
2018
- 2018-04-17 CN CN201810343026.4A patent/CN108497417A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1466983A (en) * | 2003-05-22 | 2004-01-14 | 四川省辰龙股份有限公司 | Matrimony vine royal jelly capsule and method for preparing the same |
| CN105962237A (en) * | 2016-05-09 | 2016-09-28 | 武汉思维特食品有限公司 | Royal jelly-propolis-momordica charantia lozenges and preparation method thereof |
| CN106962909A (en) * | 2017-03-14 | 2017-07-21 | 福建省神蜂科技开发有限公司 | A kind of matrimony vine royal jelly complex capsule and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 张裕中: "《食品制造成套装备》", 31 March 2010 * |
| 王强虎等: "《糖尿病绿色疗法》", 31 August 2014, 人民军医出版社 * |
| 蔡向红: "《生活中来的10000个窍门 上》", 31 March 2014, 中国三峡出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3123542A1 (en) * | 2021-06-04 | 2022-12-09 | Laboratoires Super Diet | NEW FLUIDIFIED COMPOSITION CONTAINING ROYAL JELLY |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102132906B (en) | Method for producing instant leisure peeled prawn food | |
| TWI637693B (en) | Coniferous cherry fruit powder and manufacturing method thereof | |
| CN103431331A (en) | Preparation method of actinidia arguta freeze-dried fruit powder | |
| CN105029274A (en) | Preparation method of convenient fruit crisp | |
| Umesh Hebbar et al. | Properties of dried and intermediate moisture honey products: A review | |
| KR101743141B1 (en) | Oriental melon grain syrup with contains ginger, and manufacturing method thereof | |
| CN104982861A (en) | Production method of instant fruit and vegetable shortcakes | |
| CN103610203A (en) | Method for preparing instant actinidia arguta powder through vacuum freeze drying | |
| CN109090524A (en) | Giving off a strong fragrance coconut powder and preparation method thereof | |
| CN108077824A (en) | A kind of blueberry freeze-dried powder and its production technology | |
| CN104286757A (en) | Heat-clearing pear powder and preparation method thereof | |
| CN108497417A (en) | A kind of compound buccal tablet of matrimony vine royal jelly and preparation method thereof | |
| CN1235515C (en) | Process for producing natural fruit-juice perfume synergist using passion flower as raw material | |
| CN105361027A (en) | Kiwi berry leisure food preparation method | |
| CN102987493A (en) | Method for reducing content of natural pectin in fructus rhodomyrti and improving juice yield | |
| CN107821699A (en) | A kind of processing method of Exocarpium Citri Grandis flower health tea | |
| EP2734061A1 (en) | Dried pulp preparation from unprocessed raw materials | |
| CN111887408A (en) | Preparation method of low-nitrite pickled radishes | |
| CN104996937A (en) | Preparation method of convenient vegetable crisps | |
| CN108967869A (en) | A kind of processing method reducing fresh edible maize color change | |
| CN102511578B (en) | Grosvenor momordica persimmon leaf tea and preparation method thereof | |
| CN104839724A (en) | Ginseng and red date compound health-care buccal tablet and preparation method thereof | |
| CN103875798A (en) | Freeze drying processing method of raspberries | |
| CN107996805A (en) | A kind of preparation process of wax gourd preserved fruit | |
| CN105969607A (en) | Raspberry fruit wine and method for preparing same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180907 |
|
| RJ01 | Rejection of invention patent application after publication |