CN108486295A - A kind of surface peculiar smell removing care agent of leather furniture - Google Patents
A kind of surface peculiar smell removing care agent of leather furniture Download PDFInfo
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- CN108486295A CN108486295A CN201810305637.XA CN201810305637A CN108486295A CN 108486295 A CN108486295 A CN 108486295A CN 201810305637 A CN201810305637 A CN 201810305637A CN 108486295 A CN108486295 A CN 108486295A
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- peculiar smell
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- C—CHEMISTRY; METALLURGY
- C14—SKINS; HIDES; PELTS; LEATHER
- C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
- C14C11/00—Surface finishing of leather
- C14C11/003—Surface finishing of leather using macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C14—SKINS; HIDES; PELTS; LEATHER
- C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
- C14C11/00—Surface finishing of leather
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention discloses a kind of surface peculiar smell removing care agent of leather furniture, including following component：3~10 parts of Asiatic plantain extract；10 8~15 parts of alkyl phenol polyether OP；3~10 parts of spice slow-releasing body；Acrylic resin modified 8~15 parts of water-soluble organic silicon；1~3 part of taste removal enzyme；4~10 parts of system stabilizers；5~30 parts of deionized water；In terms of parts by weight.The peculiar smell that product of the present invention is exclusively used in leather furniture surface is removed; with good cleaning effect; by the way that this product is applied to leather products surface; can quickly absorb and decompose leather surface has the gas of peculiar smell; it simultaneously can be in the protective film of leather fabric surface travel densification, to leather product surface into the good protection of progress after invention product use.
Description
Technical field
The invention belongs to cleaning-nursing technical fields, and in particular to a kind of surface peculiar smell removing care agent of leather furniture.
Background technology
As the improvement of people's living standards, the health degree requirement to living environment is also higher and higher, with leather-like man
Tool is widely used, and Peculiar Smell existing for leather-like furniture is also increasingly concerned, and people also remove leather in continuous develop
The product of furniture peculiar smell.Mainly there are physical absorption class, fragrance masking class, chemistry for the currently used eliminating smell agent of leather-like furniture
React class and enzyme preparation；Physical absorption class relies primarily on the influence that peculiar smell is eliminated in physical absorption, and logical the most commonly used is activated carbon, activity
Carclazyte, diatomite etc., such eliminating smell agent taste removal effect is insufficient, and efficiency is low, and is inhaled as the raising of temperature can discharge part
Addendum, therefore, such product cannot be satisfied the demand of people；Fragrance covers the fragrance covering smell that class product relies on fragrance, and
Peculiar smell cannot fundamentally be removed；What is relatively favored at present is the product for chemically reacting class and enzyme preparation class, however, current city
On field it is existing go out with ineffective for product taste removal, efficiency is low, and different degrees of damage is easy tod produce to leather furniture surface,
Therefore it also needs to be improved.
Invention content
Goal of the invention：It is good and to leather present invention aims at a kind of taste removal effect in view of the deficiencies of the prior art, is provided
The surface peculiar smell of the good leather furniture of furniture surface protective effect removes care agent.
Technical solution：A kind of surface peculiar smell of leather furniture of the present invention removes care agent, including following component：
Further, it is the preferable taste removal effect of guarantee, the preparation method of the Asiatic plantain extract includes the following steps：
(11) fresh Herba Plantaginis extract at 35~45 DEG C is soaked in 12~30h in saturated salt solution, then taken out, 40
Ventilation bakes drying at~50 DEG C, obtains dry Herba Plantaginis extract；
(12) the drying Herba Plantaginis extract obtained in step (11) is crushed, and its powder is immersed in deionized water, big fire
It boils rear small fire and decocts 1~3h, Herba Plantaginis extract level-one extracting solution is then obtained by filtration；
(13) the Herba Plantaginis extract level-one extracting solution reduced pressure 0.0035MPa~0.0045MPa that will be obtained in step (12)
Lower carry out rectifying extracts the fraction of 60~70 DEG C of boiling ranges, obtains Herba Plantaginis extract extracting solution.
Further, spice slow-releasing body includes matrix and fragrance, and described matrix is porous load, and the fragrance includes thin
Lotus essential oil, Rosa Damascana and sandalwood essential oil.
Further, as preferred embodiment, the preparation method of the spice slow-releasing body includes the following steps：
(21) it is for use to prepare mesoporous silicon oxide skeleton；
(22) thickener is added into fragrance to appropriate viscosity, the mesoporous silicon oxide that then will be obtained in step (21)
Skeleton immerses in fragrance viscous fluid, 2~6h of stir process under centrifugal condition；
(23) aqueous acetic acid is added into the viscous chitosan of height, stirs evenly, two urethanes two is then added into the system
Alcohol and initiator system are warming up to 150~170 DEG C under nitrogen environment, and decompression is stirred at reflux 3~8h of reaction, obtain modified high viscous
Chitosan；Reflux system is removed, is cooled to 80~95 DEG C, the system that step (22) obtains is added under heat-retaining condition, and then add
Enter sodium bicarbonate and ethyl alcohol mixed system, stops stirring after stirring evenly under nitrogen environment, it is under ultrasonic environment that system is gradual
Be cooled to 80~100 DEG C, 2~5h, rear system bubble-free kept to emerge, system is continued to be cooled to room temperature, after to system filtering,
Washing, dry, grinding, obtain spice slow-releasing body.
Further, to improve the stability of system, preventing flocculation the generation of the problems such as, the system stabilizers include such as
Lower component：
The present invention also provides the preparation methods that the surface peculiar smell of above-mentioned leather furniture removes care agent, including walk as follows
Suddenly：
(31) it is spare to prepare Asiatic plantain extract；
(32) alkyl phenol polyether OP-10 and taste removal enzyme is added under room temperature in Asiatic plantain extract obtained into step (31)
And it stirs evenly；
(33) temperature of step (32) system is warming up to 30~45 DEG C with 2~5 DEG C/min, is then added under stirring condition
Water-soluble organic silicon is acrylic resin modified and system stabilizers, constant temperature stir 1~3h；
(34) 30~45 DEG C are maintained, and spice slow-releasing body is added into step (33) system, 2~5h is stirred, is cooled to room
Temperature obtains peculiar smell and removes care agent.
Further, it avoids damaging taste removal enzyme while mixed effect to improve, the stirring speed in step (32)
Degree is 100~150r/min.
Further, it avoids damaging taste removal enzyme while mixed effect to improve, the stirring speed in step (33)
Degree first half term is that 70~100r/min at the uniform velocity increases to 200~250r/min, and the second half is at the uniform velocity decreased to by 200~250r/min
50~80r/min.
Advantageous effect：(1) product of the present invention is exclusively used in the peculiar smell removing on leather furniture surface, has good cleaning effect
Fruit, by the way that this product is applied to leather products surface, can quickly absorb and decompose leather surface has the gas of peculiar smell, together
Fine and close protective film can be formed after Shi Faming product uses on leather and fur products surface, good protection is carried out to leather product surface；
(2) by adding special spice slow-releasing body in product of the present invention, the matrix of spice slow-releasing body is porous material, can not only be controlled
Fragrance slow release additionally aids absorption gas with foreign flavor, achievees the effect that quickly to remove smell pollution, by porous matrix absorption
Gas with foreign flavor is eliminated by going out taste enzyme fast decoupled；(3) product of the present invention makes product have by coordinating specific system stabilizers
Good stability is applied to leather furniture surface and preferable perception is presented.
Specific implementation mode
Technical solution of the present invention is described in detail below by embodiment, but protection scope of the present invention is not limited to
In the embodiment.The drug used in the present invention, not specified is conventional commercial product.
Embodiment 1：A kind of surface peculiar smell removing care agent of leather furniture, including following component：
Further, it is the preferable taste removal effect of guarantee, the preparation method of the Asiatic plantain extract includes the following steps：
(11) fresh Herba Plantaginis extract at 40 DEG C is soaked in 25h in saturated salt solution, then taken out, divulged information at 45 DEG C
Drying is baked, dry Herba Plantaginis extract is obtained；
(12) the drying Herba Plantaginis extract obtained in step (11) is crushed, and its powder is immersed in deionized water, big fire
It boils rear small fire and decocts 2.5h, Herba Plantaginis extract level-one extracting solution is then obtained by filtration；
(13) rectifying will be carried out under the Herba Plantaginis extract level-one extracting solution reduced pressure 0.004MPa obtained in step (12), carried
The fraction for taking 65 DEG C of boiling ranges obtains Herba Plantaginis extract extracting solution.
Spice slow-releasing body includes matrix and fragrance, and described matrix is porous load, and the fragrance includes Peppermint essential oil, rose
Rare essential oil and sandalwood essential oil；The preparation method of the spice slow-releasing body includes the following steps：
(21) it is for use to prepare mesoporous silicon oxide skeleton；
(22) thickener is added into fragrance to appropriate viscosity, the mesoporous silicon oxide that then will be obtained in step (21)
Skeleton immerses in fragrance viscous fluid, stir process 4h under centrifugal condition；
(23) aqueous acetic acid is added into the viscous chitosan of height, stirs evenly, two urethanes two is then added into the system
Alcohol and initiator system are warming up to 160 DEG C under nitrogen environment, and decompression is stirred at reflux reaction 5h, obtain modified high viscous chitosan；It removes
Fall reflux system, be cooled to 90 DEG C, the system that step (22) obtains is added under heat-retaining condition, and sodium bicarbonate and second is then added
Alcohol mixed system stops stirring, system is gradually cooled to 90 DEG C under ultrasonic environment, keeps after stirring evenly under nitrogen environment
4h, rear system bubble-free are emerged, and system is continued to be cooled to room temperature, after system be filtered, washed, dry, grinding, obtain fragrance
Sustained release.
Further, to improve the stability of system, preventing flocculation the generation of the problems such as, the system stabilizers include such as
Lower component：
The present invention also provides the preparation methods that the surface peculiar smell of above-mentioned leather furniture removes care agent, including walk as follows
Suddenly：
(31) it is spare to prepare Asiatic plantain extract；
(32) alkyl phenol polyether OP-10 and taste removal enzyme is added under room temperature in Asiatic plantain extract obtained into step (31)
And it stirs evenly；
(33) temperature of step (32) system is warming up to 40 DEG C with 3 DEG C/min, is then added under stirring condition water-soluble
Organosilicon modified crylic acid resin and system stabilizers, constant temperature stir 2.5h；
(34) 43 DEG C are maintained, and spice slow-releasing body is added into step (33) system, 24.5h is stirred, is cooled to room temperature, obtains
Care agent is removed to peculiar smell.
Mixing speed in step (32) is 135r/min.
Mixing speed first half term in step (33) is that 85r/min at the uniform velocity increases to 220r/min, and the second half is by 220r/
Min is at the uniform velocity decreased to 75r/min.
Embodiment 2：A kind of surface peculiar smell removing care agent of leather furniture, including following component：
Further, it is the preferable taste removal effect of guarantee, the preparation method of the Asiatic plantain extract includes the following steps：
(11) fresh Herba Plantaginis extract at 35 DEG C is soaked in 12h in saturated salt solution, then taken out, divulged information at 40 DEG C
Drying is baked, dry Herba Plantaginis extract is obtained；
(12) the drying Herba Plantaginis extract obtained in step (11) is crushed, and its powder is immersed in deionized water, big fire
It boils rear small fire and decocts 1h, Herba Plantaginis extract level-one extracting solution is then obtained by filtration；
(13) rectifying will be carried out under the Herba Plantaginis extract level-one extracting solution reduced pressure 0.0035MPa obtained in step (12),
The fraction for extracting 65 DEG C of boiling ranges, obtains Herba Plantaginis extract extracting solution.
Spice slow-releasing body includes matrix and fragrance, and described matrix is porous load, and the fragrance includes Peppermint essential oil, rose
Rare essential oil and sandalwood essential oil；The preparation method of the spice slow-releasing body includes the following steps：
(21) it is for use to prepare mesoporous silicon oxide skeleton；
(22) thickener is added into fragrance to appropriate viscosity, the mesoporous silicon oxide that then will be obtained in step (21)
Skeleton immerses in fragrance viscous fluid, stir process 2h under centrifugal condition；
(23) aqueous acetic acid is added into the viscous chitosan of height, stirs evenly, two urethanes two is then added into the system
Alcohol and initiator system are warming up to 150 DEG C under nitrogen environment, and decompression is stirred at reflux reaction 3h, obtain modified high viscous chitosan；It removes
Fall reflux system, be cooled to 80 DEG C, the system that step (22) obtains is added under heat-retaining condition, and sodium bicarbonate and second is then added
Alcohol mixed system stops stirring, system is gradually cooled to 80 DEG C under ultrasonic environment, keeps after stirring evenly under nitrogen environment
2h, rear system bubble-free are emerged, and system is continued to be cooled to room temperature, after system be filtered, washed, dry, grinding, obtain fragrance
Sustained release.
The system stabilizers include following component：
The present invention also provides the preparation methods that the surface peculiar smell of above-mentioned leather furniture removes care agent, including walk as follows
Suddenly：
(31) it is spare to prepare Asiatic plantain extract；
(32) alkyl phenol polyether OP-10 and taste removal enzyme is added under room temperature in Asiatic plantain extract obtained into step (31)
And it stirs evenly；
(33) temperature of step (32) system is warming up to 30 DEG C with 2 DEG C/min, is then added under stirring condition water-soluble
Organosilicon modified crylic acid resin and system stabilizers, constant temperature stir 1h；
(34) 30 DEG C are maintained, and spice slow-releasing body is added into step (33) system, 2h is stirred, is cooled to room temperature, obtains
Peculiar smell removes care agent.
Further, it avoids damaging taste removal enzyme while mixed effect to improve, the stirring speed in step (32)
Degree is 100r/min.
Further, it avoids damaging taste removal enzyme while mixed effect to improve, the stirring speed in step (33)
Degree first half term is that 70r/min at the uniform velocity increases to 200r/min, and the second half is at the uniform velocity decreased to 50r/min by 200r/min.
Embodiment 3：A kind of surface peculiar smell removing care agent of leather furniture, including following component：
The preparation method of the Asiatic plantain extract includes the following steps：
(11) fresh Herba Plantaginis extract at 45 DEG C is soaked in 30h in saturated salt solution, then taken out, divulged information at 50 DEG C
Drying is baked, dry Herba Plantaginis extract is obtained；
(12) the drying Herba Plantaginis extract obtained in step (11) is crushed, and its powder is immersed in deionized water, big fire
It boils rear small fire and decocts 3h, Herba Plantaginis extract level-one extracting solution is then obtained by filtration；
(13) rectifying will be carried out under the Herba Plantaginis extract level-one extracting solution reduced pressure 0.0045MPa obtained in step (12),
The fraction for extracting 70 DEG C of boiling ranges, obtains Herba Plantaginis extract extracting solution.
Spice slow-releasing body includes matrix and fragrance, and described matrix is porous load, and the fragrance includes Peppermint essential oil, rose
Rare essential oil and sandalwood essential oil；The preparation method of the spice slow-releasing body includes the following steps：
(21) it is for use to prepare mesoporous silicon oxide skeleton；
(22) thickener is added into fragrance to appropriate viscosity, the mesoporous silicon oxide that then will be obtained in step (21)
Skeleton immerses in fragrance viscous fluid, stir process 6h under centrifugal condition；
(23) aqueous acetic acid is added into the viscous chitosan of height, stirs evenly, two urethanes two is then added into the system
Alcohol and initiator system are warming up to 170 DEG C under nitrogen environment, and decompression is stirred at reflux reaction 8h, obtain modified high viscous chitosan；It removes
Fall reflux system, be cooled to 95 DEG C, the system that step (22) obtains is added under heat-retaining condition, and sodium bicarbonate and second is then added
Alcohol mixed system stops stirring, system is gradually cooled to 100 DEG C under ultrasonic environment, protects after stirring evenly under nitrogen environment
Hold 5h, rear system bubble-free is emerged, and system is continued to be cooled to room temperature, after system be filtered, washed, dry, grinding, obtain perfume (or spice)
Expect sustained release.
The system stabilizers include following component：
The present invention also provides the preparation methods that the surface peculiar smell of above-mentioned leather furniture removes care agent, including walk as follows
Suddenly：
(31) it is spare to prepare Asiatic plantain extract；
(32) alkyl phenol polyether OP-10 and taste removal enzyme is added under room temperature in Asiatic plantain extract obtained into step (31)
And it stirs evenly；
(33) temperature of step (32) system is warming up to 45 DEG C with 5 DEG C/min, is then added under stirring condition water-soluble
Organosilicon modified crylic acid resin and system stabilizers, constant temperature stir 3h；
(34) 45 DEG C are maintained, and spice slow-releasing body is added into step (33) system, 5h is stirred, is cooled to room temperature, obtains
Peculiar smell removes care agent.
Mixing speed in step (32) is 150r/min.
Mixing speed first half term in step (33) is that 100r/min at the uniform velocity increases to 250r/min, and the second half is by 250r/
Min is at the uniform velocity decreased to 80r/min.
Invention product is sprayed on leather furniture surface, can quickly and effectively eliminate the peculiar smell of leather surface, Er Qie
Leather surface formed one layer of flexible protective film, protective film can rapid draing, have preferable taste removal, protecting effect, specifically make
It is as shown in table 1 with effect data：
The using effect data of the product of 1 Examples 1 to 3 of table
| Product | Eliminate the peculiar smell time (hour) | Product effective time (moon) | It forms a film drying time (minute) |
| Embodiment 1 | 2 | 6 | 5 |
| Embodiment 2 | 2.5 | 6 | 6 |
| Embodiment 3 | 3 | 6 | 6.5 |
As seen from the above table, there is peculiar smell elimination effect faster using product of the present invention, film forming is rapid, does not influence furniture
Normal use, keeping life is long, reduce use cost.
As described above, although the present invention has been indicated and described with reference to specific preferred embodiment, must not explain
For the limitation to invention itself.It without prejudice to the spirit and scope of the invention as defined in the appended claims, can be right
Various changes can be made in the form and details for it.
Claims (8)
1. a kind of surface peculiar smell of leather furniture removes care agent, it is characterised in that including following component：
In terms of parts by weight.
2. the surface peculiar smell of leather furniture according to claim 1 removes care agent, it is characterised in that：The Asiatic plantain carries
The preparation method of liquid is taken to include the following steps：
(11) fresh Herba Plantaginis extract at 35~45 DEG C is soaked in 12~30h in saturated salt solution, then taken out, 40~50
Ventilation bakes drying at DEG C, obtains dry Herba Plantaginis extract；
(12) the drying Herba Plantaginis extract obtained in step (11) is crushed, and its powder is immersed in deionized water, be boiled by fire
Small fire decocts 1~3h afterwards, and Herba Plantaginis extract level-one extracting solution is then obtained by filtration；
(13) by under the Herba Plantaginis extract level-one extracting solution reduced pressure 0.0035MPa~0.0045MPa obtained in step (12) into
Row rectifying extracts the fraction of 60~70 DEG C of boiling ranges, obtains Herba Plantaginis extract extracting solution.
3. the surface peculiar smell of leather furniture according to claim 1 removes care agent, it is characterised in that：Spice slow-releasing body packet
Matrix and fragrance are included, described matrix is porous load, and the fragrance includes Peppermint essential oil, Rosa Damascana and sandalwood essential oil.
4. the surface peculiar smell of leather furniture according to claim 3 removes care agent, it is characterised in that：The spice slow-releasing
The preparation method of body includes the following steps：
(21) it is for use to prepare mesoporous silicon oxide skeleton；
(22) thickener is added into fragrance to appropriate viscosity, the mesoporous silicon oxide skeleton that then will be obtained in step (21)
It immerses in fragrance viscous fluid, 2~6h of stir process under centrifugal condition；
(23) aqueous acetic acid is added into the viscous chitosan of height, stirs evenly, be then added into the system two urethane diols and
Initiator system is warming up to 150~170 DEG C under nitrogen environment, and decompression is stirred at reflux 3~8h of reaction, and it is poly- to obtain modified high viscous shell
Sugar；Reflux system is removed, is cooled to 80~95 DEG C, the system that step (22) obtains is added under heat-retaining condition, and carbon is then added
Sour hydrogen sodium and ethyl alcohol mixed system stop stirring after stirring evenly under nitrogen environment, system gradually cool down under ultrasonic environment
To 80~100 DEG C, keep 2~5h, rear system bubble-free emerges, system continued to be cooled to room temperature, after to system filtering, wash
It washs, dry, grinding, obtaining spice slow-releasing body.
5. the surface peculiar smell of leather furniture according to claim 1 removes care agent, it is characterised in that：The stable system
Agent includes following component：
In terms of weight fraction.
6. a kind of surface peculiar smell of leather furniture described in claim 1 removes the preparation method of care agent, it is characterised in that including
Following steps：
(31) it is spare to prepare Asiatic plantain extract；
(32) alkyl phenol polyether OP-10 and taste removal enzyme is added under room temperature in Asiatic plantain extract obtained into step (31) and stirs
It mixes uniformly；
(33) temperature of step (32) system is warming up to 30~45 DEG C with 2~5 DEG C/min, is then added under stirring condition water-soluble
Property organosilicon modified crylic acid resin and system stabilizers, constant temperature stirs 1~3h；
(34) 30~45 DEG C are maintained, and spice slow-releasing body is added into step (33) system, 2~5h is stirred, is cooled to room temperature, obtains
Care agent is removed to peculiar smell.
7. preparation method according to claim 6, it is characterised in that：Mixing speed in step (32) is 100~150r/
min。
8. preparation method according to claim 6, it is characterised in that：Mixing speed first half term in step (33) is 70~
100r/min at the uniform velocity increases to 200~250r/min, and the second half is at the uniform velocity decreased to 50~80r/min by 200~250r/min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810305637.XA CN108486295A (en) | 2018-04-08 | 2018-04-08 | A kind of surface peculiar smell removing care agent of leather furniture |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810305637.XA CN108486295A (en) | 2018-04-08 | 2018-04-08 | A kind of surface peculiar smell removing care agent of leather furniture |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106834567A (en) * | 2015-12-04 | 2017-06-13 | 青岛华南盛源果业有限公司 | Leather eliminating smell agent |
| CN107159150A (en) * | 2017-06-30 | 2017-09-15 | 上海睿沁环保科技有限公司 | A kind of indoor air purification article and preparation method thereof |
| CN107326126A (en) * | 2017-06-23 | 2017-11-07 | 宁波市海曙区伊万卡农业科技有限公司 | A kind of Chinese herbal medicine leather and fur conditioning liquid and preparation method thereof |
-
2018
- 2018-04-08 CN CN201810305637.XA patent/CN108486295A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106834567A (en) * | 2015-12-04 | 2017-06-13 | 青岛华南盛源果业有限公司 | Leather eliminating smell agent |
| CN107326126A (en) * | 2017-06-23 | 2017-11-07 | 宁波市海曙区伊万卡农业科技有限公司 | A kind of Chinese herbal medicine leather and fur conditioning liquid and preparation method thereof |
| CN107159150A (en) * | 2017-06-30 | 2017-09-15 | 上海睿沁环保科技有限公司 | A kind of indoor air purification article and preparation method thereof |
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Application publication date: 20180904 |
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