CN108484259A - The method for improving filter mud of sugarcane fertilizer backward production facilities using disc granulation technique - Google Patents

The method for improving filter mud of sugarcane fertilizer backward production facilities using disc granulation technique Download PDF

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Publication number
CN108484259A
CN108484259A CN201810296825.0A CN201810296825A CN108484259A CN 108484259 A CN108484259 A CN 108484259A CN 201810296825 A CN201810296825 A CN 201810296825A CN 108484259 A CN108484259 A CN 108484259A
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fertilizer
sugarcane
internal diameter
machine
production capacity
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CN108484259B (en
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苏天明
何铁光
李琴
苏利荣
秦芳
曾成城
李卓勇
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Guangxi Zhuang Nationality Autonomous Region Academy of Agricultural Sciences
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Agricultural Resource and Environment Research Institute of Guangxi Academy of Agricultural Sciences
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/14Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic in rotating dishes or pans
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12Granules or flakes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses the methods for improving filter mud of sugarcane fertilizer backward production facilities using disc granulation technique, include the following steps:(1) the fertilizer production capacity functional equation high with granulating disc interior diameter, granulation drying all-in-one machine internal diameter is worked out;(2) fertilizer production capacity target is set, granulating disc interior diameter is calculated separately out according to functional equation and granulation drying all-in-one machine internal diameter is high;(3) high according to calculated granulating disc interior diameter and granulation drying all-in-one machine internal diameter, it selects to be suitble to model, specification, the equipment of material;(4) composition of raw materials is worked out, addition sugarcane alcohol Fermented Condensed liquid is binder;(5) scheduling and planning is carried out, determines optimum operation parameter.The method of the present invention can be used for producing using filter mud of sugarcane as the organic fertilizer of primary raw material, biological organic fertilizer, compound organic and inorganic fertilizer; by improving crucial corollary equipment (granulating disc, granulation drying all-in-one machine) internal diameter specification and reducing rotating speed to improve fertilizer production capacity; simultaneously by add sugarcane alcohol Fermented Condensed liquid be binder to improve fertilizer balling ratio and production capacity; fertilizer efficiency is high, and crop yield is notable.

Description

The method for improving filter mud of sugarcane fertilizer backward production facilities using disc granulation technique
Technical field
The invention belongs to Production of manure technology fields more particularly to a kind of utilization disc granulation technique to improve filter mud of sugarcane fertilizer Expect the method for backward production facilities.
Background technology
Currently, the technique and technique study about filter mud Production of manure have obtained certain achievement.Such as patent CN91102320.8 discloses the method for manufacturing fertilizer using filtrated sludge of cane sugar refinery, and this method is to the wet of undried processing Conditioner is added in filter mud, it is in powdery or granular mixed fertilizer, Jin Ertian that it is splendid that physical behavior is made in agitated hybrid reaction Add suitable nitrogen, potassium, rare earth element, plant growth regulator that binary containing rare earth element or plant growth regulator, three are made Component composite fertilizer.
Patent CN200710009153.2 discloses the side that compound organic and inorganic fertilizer is produced with molasses fermented waste liquid and filter mud Method, the filter mud of this method biological humic pair 65%~68% of 0.4%~0.6% bagasse of weight percent, 10% ~12% bagasse powder and 1.5%~2.5% wheat bran and 16%~25% materials such as regulator fill within a short period of time Divide and continuously ferment, is dried after reactor startup and obtain aqueous 10%~12% fermentation materials, be ground into filter mud organic fertilizer.Aqueous 90% molasses fermented waste liquid is condensed into aqueous 26%~28% hyper-concentration liquid, by weight percentage 30%~33% it is super Concentrate and 9%~10% above-mentioned biological humic be uniformly mixed after be added 32%~34% chemical fertilizer and 25%~ 27% filter mud organic fertilizer stirring, through dry type extruder grain at compound organic and inorganic fertilizer.
Patent CN201610999641.1 is disclosed prepares organic/inorganic mixed active composite fertilizer side using alcohol filter mud Method, this method mainly by preparing introduction agent, biofermentation, condiment granulation step, take seawall mud, alcohol effluent, biogas slurry fertile, ripe Lime retting ferments to obtain introduction agent;It is stirred using starter agent and boiler slag, alcohol filter mud, humic acid, probiotics Level-one biofermentation obtains biofermentation fertilizer;It is mixed that generation organic/inorganic in rotary drum granulator is sprayed into after fermentation fertilizer is adjusted Close active composite fertilizer.
Fan protects paper Jie that peaceful develops organic-inorganic compound fertilizer for sugarcane material [J] phosphate fertilizer with compound fertilizer .2007.3 using filter mud The graininess that continued filter mud organic-inorganic compound mixed fertilizer (9-4-7, OM >=20%) disc granulation production technology by filter mud fermentation, is shone Dry, broken, granulation, drying, cooling, screening, packaging, granulating disc specification are 3.5m*0.45m, and power is controllable for 7.5KW 30% physical granularity reaches 5mm in basin, and the specification of rotary drum dryer is 2m*22m, power 15KW, and gas inlet temperature is 150 DEG C, gas outlet temperature is 30 DEG C.
Above-mentioned patent, paper relate generally to powdery filter mud Production of manure technique, and graininess filter mud Production of manure technique compared with Few, it is extruder grain, disc granulation or drum granulating to only disclose its granulation mode about graininess filter mud granulation of fertilizer technique, Matching relationship between its specific prilling, production capacity and equipment is not disclosed, and its production capacity and balling ratio are relatively low.
Invention content
The technical problem to be solved by the present invention is to overcome existing prilling production capacity and the low defect of balling ratio, one is provided The method that kind improves filter mud of sugarcane fertilizer backward production facilities using disc granulation technique utilizes disc granulation technology generations for the crowded of backwardness Prilling is pressed, the fertilizer production capacity functional equation high with granulating disc interior diameter, granulation drying all-in-one machine internal diameter is worked up, leads to It crosses crucial corollary equipment (granulating disc, granulation drying all-in-one machine) the internal diameter specification of raising and reduces rotating speed to improve filter mud of sugarcane Fertilizer production capacity, while being the present situation that binder overcomes highly effective binder to lack by adding sugarcane alcohol Fermented Condensed liquid, simultaneously Improve filter mud of sugarcane fertilizer balling ratio and production capacity.
In order to solve the above technical problems, the present invention uses following technical scheme:
The method for improving filter mud of sugarcane fertilizer backward production facilities using disc granulation technique, includes the following steps:
Step 1:Work out the fertilizer production capacity functional equation high with granulating disc interior diameter, granulation drying all-in-one machine internal diameter Respectively:
Y1 (m)=2.0509e0.0482X (6t/h≤X≤16t/h)
Y2 (m)=0.9461e0.0706X (6t/h≤X≤16t/h)
Wherein, Y1 indicates granulating disc interior diameter, and unit is rice;Y2 indicates that granulation drying all-in-one machine internal diameter is high, unit For rice;X indicates disc granulation technique fertilizer production capacity, and unit is ton hour;
Step 2:Fertilizer production capacity target is set, is calculated separately out in granulating disc according to functional equation described in step 1 Diameter and granulation drying all-in-one machine internal diameter are high;
Step 3:High, the selection according to the calculated granulating disc interior diameter of step 2 and granulation drying all-in-one machine internal diameter It is suitble to model, specification, the equipment of material;
Step 4:Composition of raw materials is worked out, addition sugarcane alcohol Fermented Condensed liquid is binder;
Step 5:Scheduling and planning is carried out, determines optimum operation parameter.
Equipment includes cast hopper, pulverizer, screening machine, mixing and blending machine, beater, granulating disc, makes in step 3 Grain drying integral machine, cooler, exhaust fan, polishing machine, packing machine and idler wheel transmission platform.
The addition manner of sugarcane alcohol Fermented Condensed liquid is to carry out sprinkling addition in granulating disc feed end in step 4, Fountain height is 4%~10%.
A concentration of 55BX °~65BX ° of sugarcane alcohol Fermented Condensed liquid in step 4.
The technical principle of the present invention:
Extruder grain technique is relatively backward production technology, and production efficiency and balling ratio are low, and fertilizer balling-up condition Mixed material type and moisture content of material are required very high;Disc granulation is relatively advanced production technology, production efficiency and Balling ratio is higher than extruder grain technique;Granulating disc, the internal diameter of granulation drying all-in-one machine are higher, it is desirable that mating rotating speed get over Low, fertilizer production capacity is higher.
The technical principle of the fertilizer production capacity functional equation high with granulating disc interior diameter, granulation drying all-in-one machine internal diameter is such as Under:
Through investigation, disc granulation technique is maximum in the market, intermediate, minimum production capacity is respectively 16t/h, 10t/h, 6t/h, right The granulating disc interior diameter answered is respectively 4.5m, 3.2m, 2.8m, and corresponding granulation drying all-in-one machine internal diameter height is respectively 3.0m、1.8m、1.5m.According to investigation result obtain maximum, intermediate, the minimum production capacity value of disc granulation technique currently on the market and its Mating granulating disc interior diameter and granulation drying all-in-one machine internal diameter is high, it can be deduced that, production capacity is higher, and internal diameter is bigger.For circle Relationship that may be present between disk prilling, fertilizer production capacity, granulating disc interior diameter, granulation drying all-in-one machine internal diameter height, A large amount of repetition tests are carried out, finally obtain fertilizer production capacity with granulating disc interior diameter, granulation drying all-in-one machine internal diameter height in finger Number functional relation finally obtains the fertilizer production capacity functional equation high with granulating disc interior diameter, granulation drying all-in-one machine internal diameter. After setting fertilizer production capacity target, it can be calculated according to the functional equation in granulating disc interior diameter and granulation drying all-in-one machine Diameter is high, and selects to be suitble to model, specification, the equipment of material on this basis.
The invention has the advantages that:
(1) present invention works up fertilizer production capacity and disk using disc granulation technology generations for backward extruder grain technique The high functional equation of comminutor interior diameter, granulation drying all-in-one machine internal diameter can be according to the function after setting fertilizer production capacity target Equation calculation goes out granulating disc interior diameter and granulation drying all-in-one machine internal diameter is high, and on this basis come select to be suitble to model, Specification, the equipment of material, by improving crucial corollary equipment (granulating disc, granulation drying all-in-one machine) internal diameter specification and reduction Rotating speed improves filter mud of sugarcane fertilizer production capacity.
(2) humic acid containing high concentration in sugarcane alcohol Fermented Condensed liquid, humic acid have stronger viscous at high concentrations Property, it is binder that the present invention, which adds sugarcane alcohol Fermented Condensed liquid, is greatly improved fertilizer balling ratio and production capacity.Sugarcane alcohol is sent out Ferment concentrate contains trace element and organic matter in abundant N P and K, Ca, Mg and Fe zinc etc. simultaneously, can be provided for Production of manure compared with More nutrients and organic matter, reduces the additive amount of other materials;Its organic matter main component is humic acid, and humic acid is plant life Long irritation active constituent can promote plant growth after using in farmland, utilization rate of fertilizer be improved, to improve fertilizer efficiency and work Produce amount.
(3) present invention using disc granulation technique improve filter mud of sugarcane fertilizer backward production facilities method, it can be achieved that fertilizer at Ball rate reaches 78% or more, and fertilizer production capacity mentions 200% or more compared to the extruder grain technique used before improving.
Specific implementation mode
Embodiment 1
Guangxi karst bio-fertilizer industry Co., Ltd positioned at Guangxi Zhuang Autonomous Region economic and technological development zones Huan Jiangxian, profit It is applicable in organic-inorganic compound mixed fertilizer (15-5-7, organic matter >=15%) with the decomposed filter mud production graininess mulberry tree of sugarcane.It adopts within 2014 Prilling is extruder grain technique, and the high 1m of Squeezinggranulator internal diameter, long 6m, rotating speed 3r/min, binder is kaolinite Soil, fertilizer production capacity are 3t/h, balling ratio 30%.It is changed within 2015 improve filter mud of sugarcane fertilizer backwardness using disc granulation technique The method of production capacity specifically carries out according to the following steps:
Step 1:Work out the fertilizer production capacity functional equation high with granulating disc interior diameter, granulation drying all-in-one machine internal diameter Respectively:
Y1 (m)=2.0509e0.0482X (6t/h≤X≤16t/h)
Y2 (m)=0.9461e0.0706X (6t/h≤X≤16t/h)
Wherein, Y1 indicates granulating disc interior diameter, and unit is rice;Y2 indicates that granulation drying all-in-one machine internal diameter is high, unit For rice;X indicates disc granulation technique fertilizer production capacity, and unit is ton hour.
Step 2:Fertilizer production capacity target is set as 9.5t/h, disk is calculated separately out according to the functional equation of step 1 and is made Grain machine interior diameter is the 3.24m and a height of 1.85m of granulation drying all-in-one machine internal diameter.
Step 3:High, the selection according to the calculated granulating disc interior diameter of step 2 and granulation drying all-in-one machine internal diameter It is suitble to model, specification, the equipment of material, equipment includes cast hopper, pulverizer, screening machine, mixing and blending machine, beater, disk Comminutor, granulation drying all-in-one machine, cooler, exhaust fan, polishing machine, packing machine and idler wheel transmission platform.Existing equipment is removed, New equipment is installed.
Step 4:Composition of raw materials is worked out, as described in Table 1, sugarcane alcohol is added on the basis of using kaolin as binder Fermented Condensed liquid is binder, and the addition manner of sugarcane alcohol Fermented Condensed liquid is to carry out sprinkling in granulating disc feed end to add Add, fountain height 6.5%, a concentration of 63BX °.
Step 5:Scheduling and planning is carried out, determines optimum operation parameter.Main equipment specification and operating parameters are as follows:(1) circle Disk comminutor interior diameter 3.24m, the high 0.6m in side, rotating speed 16r/min;(2) the high 1.85m of granulation drying all-in-one machine internal diameter, it is long 18.5m, rotating speed 3.5r/min, 550 DEG C of hot blast temperature.
The fertilizer balling ratio obtained according to the method described above is increased to 78%, and the extruder grain technique than being used before improvement improves 160%;Fertilizer production capacity is increased to 9.35t/h, and the extruder grain technique than being used before improvement improves 211.67%.Add sugarcane Smart Fermented Condensed liquid is the utilization rate of fertilizer higher that binder obtains, and fertilizer efficiency is more preferable, and crop yield is more notable.
Embodiment 2
Guangxi karst bio-fertilizer industry Co., Ltd positioned at Guangxi Zhuang Autonomous Region economic and technological development zones Huan Jiangxian, profit It is applicable in organic-inorganic compound mixed fertilizer (16-7-11, organic matter >=15%) with the decomposed filter mud production graininess eucalyptus of sugarcane.2014 The prilling used is extruder grain technique, Squeezinggranulator internal diameter high 1m, long 6m, rotating speed 3r/min, and binder is height Ridge soil, fertilizer production capacity are 3t/h, balling ratio 30%.It is changed within 2015 fall using disc granulation technique raising filter mud of sugarcane fertilizer The method of production capacity afterwards specifically carries out according to the following steps:
Step 1:Work out the fertilizer production capacity functional equation high with granulating disc interior diameter, granulation drying all-in-one machine internal diameter Respectively:
Y1 (m)=2.0509e0.0482X (6t/h≤X≤16t/h)
Y2 (m)=0.9461e0.0706X (6t/h≤X≤16t/h)
Wherein, Y1 indicates granulating disc interior diameter, and unit is rice;Y2 indicates that granulation drying all-in-one machine internal diameter is high, unit For rice;X indicates disc granulation technique fertilizer production capacity, and unit is ton hour.
Step 2:Fertilizer production capacity target is set as 9.5t/h, disk is calculated separately out according to the functional equation of step 1 and is made Grain machine interior diameter is the 3.24m and a height of 1.85m of granulation drying all-in-one machine internal diameter.
Step 3:High, the selection according to the calculated granulating disc interior diameter of step 2 and granulation drying all-in-one machine internal diameter It is suitble to model, specification, the equipment of material, equipment includes cast hopper, pulverizer, screening machine, mixing and blending machine, beater, disk Comminutor, granulation drying all-in-one machine, cooler, exhaust fan, polishing machine, packing machine and idler wheel transmission platform.Existing equipment is removed, New equipment is installed.
Step 4:Composition of raw materials is worked out, as described in Table 2, sugarcane alcohol is added on the basis of using kaolin as binder Fermented Condensed liquid is binder, and the addition manner of sugarcane alcohol Fermented Condensed liquid is to carry out sprinkling in granulating disc feed end to add Add, fountain height 6%, a concentration of 65BX °.
Step 5:Scheduling and planning is carried out, determines optimum operation parameter.Main equipment specification and operating parameters are as follows:(1) circle Disk comminutor interior diameter 3.24m, the high 0.6m in side, rotating speed 16r/min;(2) the high 1.85m of granulation drying all-in-one machine internal diameter, it is long 18.5m, rotating speed 3.5r/min, 550 DEG C of hot blast temperature.
The fertilizer balling ratio obtained according to the method described above is increased to 81.5%, and the extruder grain technique than being used before improvement carries It is high by 171.67%;Fertilizer production capacity is increased to 9.7t/h, and the extruder grain technique than being used before improvement improves 223.33%.It adds sweet Sugarcane alcoholic fermentation concentrate is the utilization rate of fertilizer higher that binder obtains, and fertilizer efficiency is more preferable, and crop yield is more notable.
1 mulberry tree of table is applicable in filter mud organic-inorganic compound mixed fertilizer (15-5-7) composition of raw materials table
2 eucalyptus of table is applicable in filter mud organic-inorganic compound mixed fertilizer (16-7-11) composition of raw materials table

Claims (4)

1. the method for improving filter mud of sugarcane fertilizer backward production facilities using disc granulation technique, which is characterized in that include the following steps:
Step 1:Fertilizer production capacity is worked out with the high functional equation of granulating disc interior diameter, granulation drying all-in-one machine internal diameter to distinguish For:
Y1=2.0509e0.0482X
Y2=0.9461e0.0706X
Wherein, Y1 indicates granulating disc interior diameter, and unit is rice;Y2 indicates that granulation drying all-in-one machine internal diameter is high, and unit is rice; X indicates disc granulation technique fertilizer production capacity, and 6≤X≤16, unit is ton hour;
Step 2:Fertilizer production capacity target is set, granulating disc interior diameter is calculated separately out according to functional equation described in step 1 It is high with granulation drying all-in-one machine internal diameter;
Step 3:High according to the calculated granulating disc interior diameter of step 2 and granulation drying all-in-one machine internal diameter, selection is suitble to Model, specification, the equipment of material;
Step 4:Composition of raw materials is worked out, addition sugarcane alcohol Fermented Condensed liquid is binder;
Step 5:Scheduling and planning is carried out, determines optimum operation parameter.
2. according to the method described in claim 1, it is characterized in that, equipment includes cast hopper, pulverizer, sieve in the step 3 Extension set, mixing and blending machine, beater, granulating disc, granulation drying all-in-one machine, cooler, exhaust fan, polishing machine, packing machine With idler wheel transmission platform.
3. according to the method described in claim 1, it is characterized in that, in the step 4 sugarcane alcohol Fermented Condensed liquid addition Mode is to carry out sprinkling addition in granulating disc feed end, and fountain height is 4%~10%.
4. according to the method described in claim 1, it is characterized in that, in the step 4 sugarcane alcohol Fermented Condensed liquid concentration It is 55BX °~65BX °.
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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3362809A (en) * 1965-02-03 1968-01-09 Continental Oil Co Apparatus for granulating fertilizer
US3577223A (en) * 1969-08-11 1971-05-04 Flour Corp Slurry distributor
CN1055351A (en) * 1991-03-31 1991-10-16 福建省化学工业科学技术研究所 Utilize filtrated sludge of cane sugar refinery to make the method for fertilizer
CN101108779A (en) * 2007-06-20 2008-01-23 福建省诏安县绿洲生化有限公司 Method of manufacturing organic, inorganic compound fertilizer with molasses zymolysis waste liquor and lime sludge
CA2845656A1 (en) * 2011-08-26 2013-03-07 Ekompany Agro B.V. Process for producing a coated fertilizer
CN104030768A (en) * 2014-07-01 2014-09-10 广西力源宝科技有限公司 Method for fertilizer granulation through molasses alcohol fermentation liquor
CN106518397A (en) * 2016-11-14 2017-03-22 广西新天德能源有限公司 Method for preparing organic/inorganic mixed activated compound fertilizer from ethyl alcohol filter mud

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3362809A (en) * 1965-02-03 1968-01-09 Continental Oil Co Apparatus for granulating fertilizer
US3577223A (en) * 1969-08-11 1971-05-04 Flour Corp Slurry distributor
CN1055351A (en) * 1991-03-31 1991-10-16 福建省化学工业科学技术研究所 Utilize filtrated sludge of cane sugar refinery to make the method for fertilizer
CN101108779A (en) * 2007-06-20 2008-01-23 福建省诏安县绿洲生化有限公司 Method of manufacturing organic, inorganic compound fertilizer with molasses zymolysis waste liquor and lime sludge
CA2845656A1 (en) * 2011-08-26 2013-03-07 Ekompany Agro B.V. Process for producing a coated fertilizer
CN104030768A (en) * 2014-07-01 2014-09-10 广西力源宝科技有限公司 Method for fertilizer granulation through molasses alcohol fermentation liquor
CN106518397A (en) * 2016-11-14 2017-03-22 广西新天德能源有限公司 Method for preparing organic/inorganic mixed activated compound fertilizer from ethyl alcohol filter mud

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