CN108477385A - A kind of microbe additive - Google Patents

Abstract

A kind of microbe additive disclosed by the invention, it is characterized in that being uniformly mixed by bacillus, lactic acid bacteria, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder, the charing egg-shell meal for adding surplus again is uniformly mixed, and composite packaging is made：Bacillus 5000 100,000,000 hundred million in every 1000g additives, lactic acid bacteria 5000 100,000,000 hundred million, 5 50g of sea-buckthorn freeze-dried powder, 5 50g of Rosa roxburghii freeze-dried powder, 3 30g of wintercherry freeze-dried powder, 3 30g of blackcurrant freeze-dried powder, 50 150g of cactus freeze-dried powder, remaining is charing egg-shell meal.Viable bacteria contained by the present invention is clear, application conducive to user and Quantitatively Selecting, using sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus freeze-dried powder and charing egg-shell meal as the matrix of additive, stability, trophism and the adsorptivity of additive institute mycetome can not only be improved, the nutritive value for promoting product simultaneously promotes the metabolism of animal, improves body resistance against diseases, promote growth of animal, the final economic benefit for improving aquaculture.

Description

A kind of microbe additive

Technical field

The invention belongs to feed additive fields, are related to a kind of microbial bacteria feed addition of the work for cultivated animals Agent.More particularly to a kind of microbe additive.

Background technology

Probiotics is a kind of probiotics, also known as live bacteria agent or bacteria-promoting agent.This is a more comprehensive concept.It is Refer in animal body normal beneficial microbe through special process manufactured active bacteria formulation.The range of this concept includes micro- life Object growth promotion and probiotic, therewith it is similar be a more popular concept be microorganism fodder additive and one compared with For comprehensive concept.For microbial bacteria, one is microorganism growth promoters, then refer to the microorganism training for the work being added in feed Object is supported, effect is to participate in the balance of microorganism in enteron aisle, directly improves the efficiency of feed utilization and the speed of growth of animal.Such as gemma Bacillus class additive mainly generates enzyme, vitamin, amino acid and growth-stimulating factor etc. by living microorganism in enteron aisle, It directly reaches growth promotion and improves the purpose of efficiency of feed utilization.The other is probiotics, also referred to as regulator, are also added to feed In work culture of microorganism, it also assists in the balance of microorganism in enteron aisle, but effect is to increase micropopulation in animal intestine The inhibition fallen（I.e. dominant population acts on）, or by enhancing non-specific immune function prevent disease, and pick up To the effect for promoting growth and raising food utilization efficiency.If Bacillus acidi lactici class additive is not directly to play growth promoting function, But by improving body non-specific immune function, the enteron aisle sense with or without clinical symptom is reduced, to having grown indirectly product Pole acts on.Currently, there are many composite viable bacteria preparations in the market, both contains lactic acid bacteria, also there is bacillus, through Market Feedback, and Feeding effect is good.With regard to the dosage form that current microorganism fodder is used as additive, there are aqua and pulvis two major classes, aqueous solution Dosage form is because thalline is easy to continue to be metabolized using the nutritional substance in aqua, and growth fermentation, therefore, the thalline of this dosage form is in Unstable state, storage life are shorter.Powder formulation is then that the thalline lived is utilized the drying means such as low temperature hot wind, freezing, by bacterium Body or gemma are dehydrated at a slow speed, so that thalline or gemma is in stable drying dormant state, are recycled substance that can be feeding It is uniformly mixed as filler and relatively stable powder-type biological feed additive is made.But current manufacturing enterprise is considered Raw material be easy to get and processing cost, often select rice bran, wheat bran, corn flour, maize cob meal, peanut shell powder, oyster shell whiting, vermiculite One or more of powder, mountain flour, calcium carbonate, medical stone, zeolite powder mixture, some also use plant straw powder or grass meal to make For filler material.The considerations of these are in line with production cost then has ignored the stability of microbial bacteria and the trophism of feed addictive Value.

In order in use, have certain adhesion, make in microbial bacteria additive microbe additive admix it is dynamic When being mixed in object feed, can be adsorbed on animal feed, convenient in animal feeding uniformity and be fed into the maximum of bacterium amount Change, some products take pains a certain amount of binder of addition.

In order to make the relative constant of raising animal stomach inner pH value, acid is continued up to after so that the foodstuff being fed into is entered small intestine The effect of change, in the product often simultaneously using acidulants such as citric acid, lactic acid, hydrochloric acid, fumaric acid, but these acidulants are not only straight It connects and locally causes acidity too strong microbial bacteria contained by additive, influence the survival of thalline, meanwhile, these acidifying substances are to cultivation Animal also without the nutritive value directly utilized, meanwhile, there is prodigious irritation to the gastrointestinal tract of the cubs of livestock and poultry, young fowl, Compatibility is using not ideal enough.

Exploitation one kind can overcome above-mentioned deficiency, can either keep stability, the trophism of institute's mycetome, have again to thalline There is adhesion, while the filler to using has the microbe additive that nutritive value is provided to cultivated animals again, is to promote The basis of feed additive industry long-term stability development.

Invention content

The purpose of the present invention is to provide a kind of microbe additive, which not only there is thalline to stablize, and thalline is deposited Live time is long, plays the Overlay of use in conjunction, and used auxiliary agents have certain adhesiveness and adsorptivity, Thalline can be made preferably to be bonding on one with auxiliary agents, meanwhile, complementary additive has certain acidity, is raised to animal After food, abundant nutriment can not only be provided, while its acidic materials can keep stomach inner pH value relative constant, into after small intestine The effect of continuing up to acidification.The purpose is to provide a kind of microbe additive of more stability and trophism.

A kind of microbe additive of the present invention, it is characterized in that by bacillus, lactic acid bacteria and a certain amount of seabuckthorn fruit powder, Rosa roxburghii Tratt Powder, wintercherry powder, blackcurrant powder, cactus powder and charing egg-shell meal uniformly mix, and obtain a kind of new microbe additive, this adds The thalline of agent is added to stablize, the thalline time-to-live is long, and seabuckthorn fruit powder, Ribes burejense powder, wintercherry powder, blackcurrant powder sugar content are high, especially Being cactus powder, all there is preferable Adhesion property, charing egg-shell meal also to have preferable adsorptivity.Wherein sea-buckthorn, Rosa roxburghii Tratt, acid Slurry, blackcurrant are the ascorbic fruits of high-content, and acidity is extremely strong, and abundant vitamin etc. is not only provided to cultivated animals Nutriment, the acidic materials after feeding play the effect for promoting digestion well, to highlight the purpose of the present invention.

In order to realize the present invention, the following technical solutions are specifically adopted：

A kind of microbe additive, feature it be first by bacillus, lactic acid bacteria, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, acid It starches freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder to be uniformly mixed, then adds the charing egg-shell meal of surplus and be uniformly mixed, it is multiple Packaging is closed to be made：Bacillus 5000 hundred million -60000 hundred million in every 1000g additives, lactic acid bacteria 5000 hundred million -60000 Hundred million, sea-buckthorn freeze-dried powder 5-50g, Rosa roxburghii freeze-dried powder 5-50g, wintercherry freeze-dried powder 3-30g, blackcurrant freeze-dried powder 3-30g, cactus are frozen Dry powder 50-150g, remaining is charing egg-shell meal.

Bacillus described above is bacillus dry powder product；The lactic acid bacteria is dry powder of lactic acid bacteria product.

The bacillus dry powder product and dry powder of lactic acid bacteria product can be used as feed using commercially available respectively Every gram of preparation that 200 hundred million are no less than containing viable bacteria concentration of additive, the bacillus dry powder product, dry powder of lactic acid bacteria product It is determined by the thalline content of thalline dry powder and final products with the weight proportion of the filler material in formula.

The bacillus dry powder product and dry powder of lactic acid bacteria product can also utilize existing method to select corresponding optimization Culture medium then the thalline in zymotic fluid is separated with high speed centrifugation mode respectively by liquid fermentation equipment culture, It is placed in dry indoor cold wind or bacterium mud drying is made, every gram of the viable bacteria concentration obtained respectively with vacuum freeze drying mode No less than 200 hundred million bacillus thalline dry powder products and the lactic acid bacteria thalline of every gram of viable bacteria concentration no less than 200 hundred million are dry Powder product.

Bacillus described above is bacillus licheniformis, bacillus lentus, bacillus cereus, withered grass gemma Appointing in bacillus, bacillus coagulans, Japan bacillus, bacillus laterosporus, bacillus pumilus, bafillus natto Meaning is a kind of.

Lactic acid bacteria described above is lactobacillus lactis, streptococcus lactis, lactobacillus acidophilus, lactobacillus plantarum, acidified milk Bacillus, propionibacterium freudenreichii, Pediococcus acidilactici, Lactobacillus helveticus, Xie Shi Propionibacteriums, Pediococcus pentosaceus, does streptococcus thermophilus Any one in junket lactic acid bacteria, lactobacillus plantarum, German-style lactobacillus, lactobacillus cellobiosas, Bifidobacterium.

Sea-buckthorn freeze-dried powder described above, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder, It being made by following methods, technical process is that fresh sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus is taken to remove carpopodium respectively, The impurity such as rotten fruit, rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, remove seed step；Rinsing condition described above is The citric acid of weight 0.1% is added with 40 DEG C of water, rinses 15min, and be stirred continuously, and is pulled out to be put into pure water and is rinsed 3 times；On It is that will be cooled to -45 DEG C or less rapidly after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot respectively to state freezing；Above-mentioned distillation Dry process conditions are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is dry until moisture is less than 6%/w；It is above-mentioned Low-temperature grinding is the crushing that temperature of charge is in 0 DEG C or less progress, 100 mesh of grinding particle size ＞.

Composite packaging described above uses interior outer bag composite packaging, inner bag that polypropylene plastics pocket, outer packing is used to use aluminium Foil bag is filled with silica-gel desiccant between interior outer bag.

Charing egg-shell meal described above is made by following methods：

（1）Dry, dipping first cleans up eggshell, dries moisture, is dried 1-2 hours in advance, then pulverizes into 20- 30 mesh coarse powder, by weight 1:0.5 sprays the salt that prepared weight fraction is 25% on eggshell coarse powder（Sodium chloride）It is molten Liquid is mixed in sprinkling, is placed after mixing 6-7 hours, then uniformly mixing is primary again, then places 6-7 hours；The purpose is to allow Salt effectively penetrates into eggshell organization internal gap；

（2）The eggshell powder raw material impregnated is put into rotary carbonizing pot by charing, and charing is rotated at a temperature of 420-450 DEG C 70-80 minutes, until observing the complete blackening of raw material（Carbonization process should have corresponding scraping blade, to prevent raw material in carbonization process viscous Pot and caking）；

（3）The raw material carbonized is rapidly moved in activation furnace by activation, is closed fire door, is passed through carbon dioxide gas, is caught up with to the greatest extent wherein Air, at 720-800 DEG C anoxybiotic activate 55-85 minutes（Corresponding turning mechanism is set in activation furnace, keeps activation raw material every It can be stirred within 10 minutes once, to ensure activation fully and uniformly）；

（4）After activated material is taken out in cleaning, it is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, until Until basic inspection does not measure sodium chloride；After having cleaned sodium chloride, it is small that the hydrochloric acid for being 12% with mass ratio submerges activated material 2.5-3 When, it waits after impregnating, with 95 DEG C of pure water washing activated materials, is floated after material grain is there is no white, then with room temperature pure water It is washed till neutrality（PH value is about in 6.9-7.1）, filter, obtain rinse activator material；

（5）Dry and screening, which dries the activated material of rinsed clean at 115-120 DEG C to water content, is less than 6%（w）, cross 60 mesh Sieve, the coarse grain after screening are pulverized again, make all to sieve to get charing egg-shell meal product by 60 mesh.

Drying described above uses heated-air drying or far-infrared ray drying；Dry condition is 180 DEG C -300 DEG C.It is dried Purpose be that can make the crisp matter of eggshell, increase eggshell hole be conducive to sprinkling saline solution effectively penetrate eggshell internal voids In.

Eggshell described above is the mixed of any one or a few in egg shell, Ovum Anas domestica putamina, goose egg-shell and quail eggshell Close eggshell.

A kind of prioritization scheme of microbe additive of the present invention is, first by bacillus, lactic acid bacteria, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing eggshell of surplus Powder is uniformly mixed, and composite packaging is made：Bacillus 7000 hundred million -60000 hundred million, lactic acid bacteria in every 1000g additives 7000 hundred million -60000 hundred million, sea-buckthorn freeze-dried powder 10-50g, Rosa roxburghii freeze-dried powder 8-50g, wintercherry freeze-dried powder 5-30g, blackcurrant freeze Dry powder 5-30g, cactus freeze-dried powder 70-150g, remaining is charing egg-shell meal.

The further prioritization scheme of the present invention is a kind of microbe additive, it is characterized in that first by bacillus, lactic acid Bacterium, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add The charing egg-shell meal of surplus is uniformly mixed, and composite packaging is made：Bacillus 9000 hundred million -60000 in every 1000g additives A hundred million, lactic acid bacteria 9000 hundred million -60000 hundred million, sea-buckthorn freeze-dried powder 15-50g, Rosa roxburghii freeze-dried powder 12-50g, wintercherry freeze-dried powder 8- 30g, blackcurrant freeze-dried powder 8-30g, cactus freeze-dried powder 85-150g, remaining is charing egg-shell meal.

The further prioritization scheme of the present invention is a kind of microbe additive, it is characterized in that first by bacillus, breast Sour bacterium, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add The charing egg-shell meal of surplus is added to be uniformly mixed, composite packaging is made：The bacillus 10000 hundred million-in every 1000g additives 60000 hundred million, lactic acid bacteria 10000 hundred million -60000 hundred million, sea-buckthorn freeze-dried powder 20-50g, Rosa roxburghii freeze-dried powder 15-50g, wintercherry are frozen Dry powder 10-30g, blackcurrant freeze-dried powder 10-30g, cactus freeze-dried powder 100-150g, remaining is charing egg-shell meal.

Bacillus mainly takes oxygen by force by biology in the gastrointestinal tract and maintains intestinal eubiosis, it is colonized in short-term in enteron aisle Afterwards, a large amount of oxygen can be consumed and maintain enteron aisle anaerobic environment, field planting power of the enhancing enteron aisle to anaerobic bacteria.In addition, bacillus It can be monosaccharide by Starch Conversion in enteron aisle, then these monosaccharide are converted to lactic acid by other strains in enteron aisle, reduce enteron aisle PH, to play the role of inhibit pathogen.

Probiotic composition made of bacillus and other microorganisms has a significant difference, bacillus can condition not Gemma is formed in the case of profit, will be protected self, and resurrection rate is high.Raw spore form exists within such product, have compared with More advantages：1. acidproof, salt tolerant, high temperature resistant（100℃）And anti-extrusion, thus the processing of feed granulation, pass through animal hydrochloric acid in gastric juice There is higher stability during environment etc.；2. the activity with very strong protease, lipase, amylase, to vegetalitas Carbohydrate has stronger degradation capability, can in degrading plant feed certain complexity compound, generate with antagonism The polypeptides matter of pathogenic entero becteria ability.This bacteroid has drop to the carbohydrate of many complexity of plant component part Solution ability, the substance that can be degraded have triglycerides, protein, starch, xylan, β-Isosorbide-5-Nitrae-galactan, pectin, carboxymethyl Cellulose, polygalacturonase, araban, glucose, p-nitrophenyl-glucopyranoside, p-nitrophenyl-Arab Furanoside, lichenin and p-nitrophenyl-furyl xylose etc..

The lactic acid bacteria being currently known has more than 100 kind.The applicating history of lactic acid bacteria is very long, such as dairy products, pickles, blueness Store the making and production of feed etc..There is a large amount of lactic acid bacterias in the enteron aisle of humans and animals.Lactobacillus preparation is that one kind contains The preparation of live lactobacillus, entitled alctasin.Lactic acid bacteria growth and development in enteron aisle decomposes carbohydrate and generates lactic acid and form acyclic acidic Border to inhibit the proliferation of harmful bacteria in intestinal canal, and prevents production malicious and pathogenic.The strain for preparing lactobacillus preparation has acidophilus newborn Bacillus, lactobacillus bulgaricus, streptococcus lactis and streptococcus fecalis etc..Leading at present to be applied has lactobacillus acidophilus, bifid breast bar Bacterium and enterococcus.

Lactobacillus is animal（Especially poultry）The normal settler of enteron aisle.Poultry went out after shell in a few hours can be The streptococcus fecalis, the enterobacteria that are dispersed in are found in enteron aisle（) and clostridium Enterobateria（Clostridia), with Bacillus acidi lactici just starts to settle down in alimentary canal in a couple of days afterwards.Lactobacillus is the main Pseudomonas of fowl crop flora, with large intestine Bacillus, streptococcus（Streptococci it) compares and occupies advantage.Bacillus acidi lactici is adhered to fowl crop epithelium, and this adhesion has kind Specificity.Fowl crop Bacillus acidi lactici is the Bacillus acidi lactici source that poultry maintains intestinal bacteria balance.Bacillus acidi lactici is maintaining to digest The aspect of stablizing of the normal microflora system in road plays conclusive effect.Most probiotic products be Lactobacillus or other Lactic acid-producing bacteria.

Lactic acid bacteria anaerobism or amphimicrobian growth, still are able to survive under the acid conditions of pH3.0 ~ 4.5.It is in animal intestinal tract Middle by monosaccharide, especially Lactose conversion is lactic acid, to reduce intestinal pH, prevents foreign bacteria in the field planting of enteron aisle, inhibits large intestine The growth of the pathogens such as bacillus, detection of Salmonella, and the growth of final lactic acid bacteria inhibiting itself.Lactic acid bacteria also can be by adjusting enteron aisle PH promotes gastrointestinal peristalsis to activate pepsin, helps the digestion of food, absorbs, mitigate flatulence and promote liver function etc.. Lactic acid bacteria is acted on by competitive exclusion（Competitive binding site）Inhibit the growth of pathogen.Lactic acid bacteria can also stimulate siberian crabapple System improves immunity of organisms, improves resistivity of the intestinal tissue to bacteria attack.Some Bacillus acidi lacticis can neutralize certain toxin, As lactobacillus bulgaricus can neutralize escherichia coli enterotoxin, but precise mechanism is unclear.Bacillus acidi lactici itself can also generate Some digestive ferments, such as invertase, lactase and peptase, help to improve animal digestion function.Sawada reports, certain lactic acid Contain a kind of safe and effective natural anti-hypertension compound SG-1 in bacilli-cell wall.Lang Zhongwu is equal to 1994 in egg young bird Brood of layers chichen is added in daily grain of chicken, as a result feed efficiency improves 8.73% ~ 11.23%；Xiao Zhenduo etc. (1995) is tried Verify bright, Brood of layers chichen is compared compared with antibiotic control group, improves feed efficiency 4.6%.In addition Bacillus acidi lactici can The digestive function of small intestine is improved by increasing surface area.Animal is in stress（As birth, wean, daily ration variation, intestinal pH are abnormal Increase) during, total variation tendency is that pathogen is increased, and Bacillus acidi lactici quantity is reduced.Lactobacillus is successfully established in enteron aisle PH can be made to become stable.

Sea-buckthorn（Hippophae rhamnoides Linn.）, fruit contains abundant nutriment and biological active matter Matter can be widely applied to many fields of the national economy such as food, medicine, light industry, space flight, agriculture and animal husbandry fishery.Fructus hippophae and oil With very high medical value, there is a cough-relieving apophlegmatic, relieving dyspepsia, promoting blood circulation to remove blood stasis effect, can treat gastric duodenal ulcer with And indigestion etc..

Sea buckthorn fruit is full of nutrition, according to surveying and determination in its fruit containing multivitamin, aliphatic acid, trace element, sub- oil element, The various amino acid of Hippophate flavone, superoxides isoreactivity substance and needed by human body.Wherein Vitamin C content is high, every 100 grams In fruit juice, Vitamin C content can reach 825-1100 milligrams, be 2-3 times of Kiwi berry, be known as the laudatory title of the king of vitamin C.Contain Sugared 7.5%-10%, the 3%-5% containing acid.

Rosa roxburghii Tratt（Rosa roxbunghii）For the fruit of the perennial machaka rosa roxburghii of the rose family also known as mountain king fruit, thorn Certain kind of berries fruit, thatch pears etc..With clearing heat and promoting fluid, stomach strengthening and digestion promoting, relieving summer-heat and other effects.Rosa roxburghii Tratt contains abundant vitamin B, C, carrotene, The ingredients such as malic acid, citric acid are usually used in deficiency of stomach-Yin, anorexia, indigestion or eating accumulation, glutted full bored, diarrhea Loose stool；Pyreticosis or hot summer weather hinder Tianjin, thirsty, scanty drak urine.

Ripe Rosa roxburghii Tratt is fleshy hypertrophy, sweet and sour, fruit are rich in sugar, vitamin, carrotene, organic acid and more than 20 kinds of ammonia Base acid, more than 10 the kinds trace element and superoxide dismutase, especially Vitamin C content beneficial to human body are high, are to work as Highest in preceding fruit, 841.58 milligrams -3541.13 milligrams of content in every 100 grams of fresh fruits is 50 times of citrus, Kiwi berry 10 times, the laudatory title with " king of vitamin C ".Fruit of Grossularia burejensis Berger has very high nutritive value and medical value, sour, puckery, flat, Digestion-promoting spleen-invigorating restrains stopping leak, for treating having indigestion abdominal distension, dysentery, enteritis, vitamin C deficiency etc..

Wintercherry（Physali alkekengiL.）Also known as groundcherry, franchet groundcherry persistent calyx or fruit, cape gooseberry etc..Containing more in Fruit of Physalis Kind of nutritional ingredient, the content of wherein calcium is 73.1 times of tomato, 13.8 times of carrot, and ascorbic content is tomato 6.4 times, 5.4 times of carrot.With unique flavor and abundant nutrition.Fruit of Physalis aromatic flavour, delicious.Berry is rich Containing vitamin C, beta carotene, more than 20 kinds of mineral element and 18 kinds of amino acid, there is heat-clearing, removing toxic substances, diuresis effect to be usually used in It controls in heat-syndrome cough, pharyngalgia, jaundice, dysentery, water, the treatment of furunculosis, erysipelas etc..

Blackcurrant scientific name elements of black currant（Ribes nigrum L.）Also known as currant, purple plum etc., ripening fruits are black Small berries, it is interior rich in vitamin C, anthocyanidin.Blackcurrant is not only a kind of delicious flavour, fruit full of nutrition, and has Good medicinal efficacy.Blackcurrant fruit is rich in mineral matter element, and the Zn content in mineral matter element is high, can be used as and comes for zinc Source；Ascorbic content is high, hence it is evident that higher than citrus, hawthorn, also contains phosphorus, magnesium, potassium, calcium, anthocyanidin, aldehydes matter.Seed Linoleic acid content is high.Ascorbic content is very abundant in blackcurrant, it is often more important that also contains a large amount of antioxygen and is melted into Point, this assures ascorbic function and effect.Blackcurrant is rich in such as anthocyanidin, vitamin C, flavones, Quercetin, red bayberry The substances such as alcohol, phenolic acid, catechin and blackcurrant polysaccharide, these are all the bioactive substances with good anti-oxidation function.

Cactus（Scientific name：Opuntia stricta(Haw.)Haw.var.dillenii(Ker-Gawl.) Benson）, It is a kind of plant of Opuntia.Alias celestial being palm, kwan-yin palm etc..Cactus is the meat shrub that grows thickly, the wide ovum of top branch Shape, obovate elliptic or subcircular；Flower spoke shape, holder obovate.It is used as medicine with complete stool.The four seasons can adopt.

Cactus is cool in nature, sour, nontoxic.Have the promoting flow of qi and blood circulation, heat-clearing toxin-expelling functions.Mainly have clearing heat and detoxicating, eliminating stasis to subdue swelling, The functions such as the promoting flow of qi and blood circulation, benefiting stomach and stopping pain.Cactus contains amino acid and various trace elements in needed by human 8, and embraces green The preciousness ingredient such as lotus, Kok Beattie cents, cholla stem, starches through cactus crude drug and analyzes, contain pectin, polysaccharide and glue exudate.From herb point From extracting to obtain freidelin ketone（friedelin）, -3 α -ol of freidelin（friedelan-3-α-ol）, taraxerone （taraxerone）And taraxerol（taraxerol）.

Eggshell, what quantity was larger in China's poultry farming has chicken, duck, goose and quail etc., using egg, duck's egg, As in food processing process, the useless eggshell enormous amount generated is provided according to existing disclosed report for goose egg and quail egg Material display, the eggshell total amount that a medium-sized city is monthly discarded reach 60-100 tons, and account for egg size by Eggshell weight 11% calculates, The eggshell that about 1,500,000 tons of the daily output in China, not only pollutes environment, but also waste of resource in this way.Discarded eggshell is integrated It utilizes, resource utilization can not only be improved and avoids environmental pollution, and be greatly improved the economic benefit and social benefit of enterprise.

Wherein egg shell is in China's yield maximum, and egg shell accounts for the 10-12% in entire egg, by under film, shell on shell Film and eggshell three parts composition, eggshell is a kind of calcareous hard shell, is located on shell between film and shell lower film.In the change of egg shell In studying point, minerals account for 95%, and protein 3.3%, moisture 1%, fat 0.03%, remaining is carbohydrate and other have Machine substance（Certainly, a large amount of remaining egg white in eggshell in the above ingredient are not included）.Eggshell mineral ingredient is mainly Calcium carbonate accounts for 94% or so, remaining is magnesium carbonate and calcium phosphate, and calcium, phosphorus content account for 34.9% and of eggshell dry matter respectively 0.2%.In eggshell, seven kinds of vitamins and various trace elements and some important enzyme, peptide matters can be measured, he Although content it is seldom, be all the substance needed in human body or animal body.

In the prior art, it is replenished the calcium with egg-shell meal, has the product of the grinds after sterilization by eggshell in people's product, also have The application of organic calcium is prepared into using primary or secondary clacining method.It is at present most widely in drug, food and nutriment In preparation, micron order, submicron order and nano level superfine powder are mostly used, is added to various food, nutrition kind, has reached very Good effect.Application of the eggshell in China's animal-breeding is taken mostly by eggshell cleaning, drying, and milling makes an addition in feed The method of feeding, since grinding particle size is larger, being absorbed and utilized for animal is poor, can't reach good application effect.

The present invention is to clean eggshell, after high temperature drying, then be made one through spice, charing, activation, cleaning, drying, screening The adsorbent of kind function admirable, the program not only remains the nutrition that eggshell utilizes, while making the abundant carbonaceous of eggshell, not only right It is contained it is calcareous form organic calcium, and form the filling substrate with adsorption capacity.

The beneficial effects of the invention are as follows：

（1）Product of the present invention can highlight the viable bacteria content of bacillus and lactic acid bacteria, be obviously improved bacillus and lactic acid bacteria The more preferably effect of use in conjunction significantly improves survival rate and stability of the thalline in closed composite packaging.

（2）Pass through sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder and bud Spore bacillus and lactic acid bacteria mixing, due to the stickum in the colloidal substance that these dry powder formulations are rich in, especially cactus, energy The adhesive effect between additive and feed is preferably increased, and improves the utilization rate of additive；

（3）By sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus freeze-dried powder high-content amino acid, vitamin, mineral element, more Sugar.The nutritional ingredients such as the vitamin C of organic acid, especially high-content and various bioactivators, to improving animal immune energy Power is simultaneously obviously improved meat, Egg Quality, the acidic materials in especially above-mentioned dry powder, utilization, promotion to contained complex microorganism Animal digestion all has significant effect；

（4）Due to using Freeze Drying Technique means, enable sea-buckthorn obtained, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus freeze-dried powder Its active constituent is maximumlly remained, has distinctive sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, the smell of cactus application and taste Taste, free from extraneous odour add the preference of animal.

（5）Eggshell is first subjected to drying and other treatment through high temperature using charing egg-shell meal, further through spice, charing, activation, clear It washes, dry and sieves, form a kind of excellent adsorbent, which not only forms absorption to the saccharomycete in product Power, while making the eggshell after charing that still there is the organic calcium effect activated, meanwhile, after animal feeding, have well to stomach The toxin of enteron aisle has suction-operated, has stop dysentery, antidiarrheal effect for the animal of diarrhea and diarrhea, has good activated carbon Medicinal effects.

（6）To the preparation of sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus freeze-dried powder in the present invention, do not remove the peel, remove seed step Suddenly, it is therefore an objective to by being crushed after freeze-drying, so that its skin and seed is worn into fine powder, make anthocyanidin, oil in its skin and seed Class, organic acid, bud fragrance substance are retained, and the nutritive value of its freeze-dried powder is promoted.

（7）The present invention is lyophilized using sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus Powder, matrix of the charing egg-shell meal as additive contain constants such as a large amount of calcium, phosphorus, potassium, sodium, magnesium, zinc and micro in matrix Element still contains abundant vitamin C, anthocyanidin, beta carotene, malic acid, citric acid, protein, amino acid, nucleic acid, Portugal Grape sugar, lipoidis, carbohydrate, B family vitamin such as B₁、B₂、B₆、B₁₂And the physiological activity such as folic acid, niacin, pantothenic acid, inositol Substance, not only improves the nutritive value of microbe additive, while promoting the metabolism of animal, improves the disease-resistant energy of body Power promotes growth of animal, finally improves the economic benefit of its aquaculture.

（8）Product of the present invention uses interior outer bag composite packaging, interior outer bag interlayer to be filled with silica-gel desiccant, and product does not return Tide, no caking, product is loose, good fluidity, can preferably keep exterior quality and inherent quality.

Operation to its technical process for not having to state in detail in the present invention, be those skilled in the art common sense in Operation.With regard to the purchase and storage of heretofore described sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant fresh fruit and fresh cactus, the present invention The construction of thousand Co., Ltds of Yao Tang traditional Chinese medical science research institute of cooperation unit Jiangsu has 20,000 tons of freezer facility, is to have to storage fresh fruit material It ensures enough.

Specific implementation mode

Embodiment 1

The preparation of sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder：

Sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, the cactus for taking fresh mature respectively, remove carpopodium, and the impurity such as rotten fruit are heavy with containing 40 DEG C of aqueous solutions of 0.1% citric acid are measured, 15min is rinsed under constant stirring and pulls out, be put into pure water and rinse 3 times, pull out It is drained；It will be moved into refrigerator after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot respectively, be cooled to -45 DEG C rapidly Below；Respectively by the sea-buckthorn freezed, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus move into lyophilization machine in, sublimation temperature control- 22--32 DEG C, vacuum degree 120-150Pa makes dry materials to moisture ＜ 6%（w）, the time about needs 18 hours, is put into after taking-up In freezing crusher, control material temperature is no more than 0 DEG C, after being crushed to 100 mesh of fineness ＞, respectively obtains sea-buckthorn freeze-dried powder, thorn Pears freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder, are fitted into polybag and seal, and are stored in 0 DEG C or less It is spare in freezer.

Embodiment 2

Carbonize the preparation of egg-shell meal：

Eggshell is cleaned up first, dries moisture, is placed in electric baking case, the heated-air drying 2 hours under the conditions of 200 DEG C, After taking-up is let cool, 20 mesh coarse powder are pulverized into, by weight 1:0.5 sprays prepared weight ratio for 25% on eggshell coarse powder Salt solution（That is egg-shell meal：25% salt solution=1:0.5 ratio）, mixed in sprinkling, place 6 hours after mixing, then Uniformly mixing is primary again, then places 6 hours；The eggshell powder raw material impregnated is put into rotary carbonizing pot, in 420 DEG C of backspins Turn charing 80 minutes, until observing the complete blackening of raw material（Carbonization process prevents charcoal in being equipped with the scraping blade rotated automatically in charing pot Raw material glues pot and caking during change）；The raw material carbonized is rapidly moved in activation furnace, CO is passed through₂Gas is caught up with therein to the greatest extent Air, anoxybiotic activates 80 minutes at 760 DEG C（Controllable stirring is set in activation furnace and stirs blade, is made every in activation raw material It is stirred within 10 minutes once, ensures activation material fully and uniformly）；After activation, activated material is taken out, is allowed to cool normal Temperature gradually rinses activated material in rinse bath with clear water, until basic inspection does not measure sodium chloride, has cleaned sodium chloride Afterwards, it with the hydrochloric acid of mass ratio 12% submergence activated material 2.5 hours, waits impregnating and finishes, with 95 DEG C of pure water washing activated materials, until After expecting grain there is no white, then with room temperature pure water rinse to pH value 7.0, filtering obtains rinse activator material；By rinsed clean Activated material, which is dried at 115 DEG C to water content, is less than 6%, crosses 60 mesh sieve, and the coarse grain after screening is pulverized again, makes all to pass through 60 mesh sieve is to get charing egg-shell meal product.

Embodiment 3

Carbonize the preparation of egg-shell meal：

Eggshell is cleaned up first, dries moisture, is placed in far-infrared dryer, it is 1 hour dry under the conditions of 300 DEG C, it takes Go out after letting cool, pulverize into 30 mesh coarse powder, by weight 1:0.5 sprays the food that prepared weight ratio is 25% on eggshell coarse powder Salting liquid（That is egg-shell meal：25% salt solution=1:0.5 ratio）, mixed in sprinkling, place 7 hours after mixing, then again Uniformly mixing is primary, then places 7 hours；The eggshell powder raw material impregnated is put into rotary carbonizing pot, is rotated at 450 DEG C Charing 70 minutes, until observing the complete blackening of raw material（Carbonization process prevents from carbonizing in being equipped with the scraping blade rotated automatically in charing pot Raw material glues pot and caking in the process）；The raw material carbonized is rapidly moved in activation furnace, CO is passed through₂Gas catches up with sky therein to the greatest extent Gas, anoxybiotic activates 55 minutes at 800 DEG C（Controllable stirring is set in activation furnace and stirs blade, is made in activation raw material every 10 Minute is stirred once, ensures activation material fully and uniformly）；After activation, activated material is taken out, is allowed to cool normal Temperature gradually rinses activated material in rinse bath with clear water, until basic inspection does not measure sodium chloride, has cleaned sodium chloride Afterwards, it with the hydrochloric acid of mass ratio 12% submergence activated material 3 hours, waits impregnating and finishes, with 95 DEG C of pure water washing activated materials, until material After grain is there is no white, then with room temperature pure water rinse to pH value 7.0, filtering obtains rinse activator material；By the work of rinsed clean Material, which is dried at 120 DEG C to water content, is less than 6%, crosses 60 mesh sieve, and the coarse grain after screening is pulverized, made all by 60 again Mesh sieve is to get charing egg-shell meal product.

Embodiment 4

A kind of microbe additive is by bacillus licheniformis dry powder, streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus licheniformis 60000 hundred million in every 1000g additives, streptococcus lactis 5000 hundred million are husky Spine freeze-dried powder 5g, Rosa roxburghii freeze-dried powder 50g, wintercherry freeze-dried powder 3g, blackcurrant freeze-dried powder 3g, cactus freeze-dried powder 50g, remaining is charcoal Change egg-shell meal；Specifically production method is：Weigh embodiment 1 sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-drying respectively Powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 5

A kind of microbe additive is by bacillus subtilis dry powder, lactobacillus fermenti dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus subtilis 5000 hundred million in every 1000g additives, lactobacillus fermenti 10000 hundred million are husky Spine freeze-dried powder 45g, Rosa roxburghii freeze-dried powder 10g, wintercherry freeze-dried powder 5g, blackcurrant freeze-dried powder 5g, cactus freeze-dried powder 100g, remaining is Carbonize egg-shell meal；Specifically production method is：Weigh embodiment 1 sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-drying respectively Powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 3, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 6

A kind of microbe additive is by bacillus lentus dry powder, plant lactobacillus powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus lentus 10000 hundred million in every 1000g additives, lactobacillus plantarum 10000 hundred million are husky Spine freeze-dried powder 30g, Rosa roxburghii freeze-dried powder 15g, wintercherry freeze-dried powder 10g, blackcurrant freeze-dried powder 10g, cactus freeze-dried powder 115g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 3, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 7

A kind of microbe additive is by bacillus cereus dry powder, lactobacillus acidophilus dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus cereus 60000 hundred million in every 1000g additives, lactobacillus acidophilus 10000 hundred million are husky Spine freeze-dried powder 25g, Rosa roxburghii freeze-dried powder 15g, wintercherry freeze-dried powder 15g, blackcurrant freeze-dried powder 12g, cactus freeze-dried powder 100g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 8

A kind of microbe additive is by bacillus pumilus dry powder, streptococcus thermophilus dried powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus pumilus 60000 hundred million in every 1000g additives, streptococcus thermophilus 60000 hundred million are husky Spine freeze-dried powder 10g, Rosa roxburghii freeze-dried powder 30g, wintercherry freeze-dried powder 20g, blackcurrant freeze-dried powder 20g, cactus freeze-dried powder 110g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 9

A kind of microbe additive is by bafillus natto dry powder, Lactobacillus helveticus dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bafillus natto 9000 hundred million in every 1000g additives, Lactobacillus helveticus 50000 hundred million are husky Spine freeze-dried powder 25g, Rosa roxburghii freeze-dried powder 25g, wintercherry freeze-dried powder 15g, blackcurrant freeze-dried powder 15g, cactus freeze-dried powder 120g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 10

A kind of microbe additive is by Japan's bacillus dry powder, Pediococcus acidilactici dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：Japan bacillus 50000 hundred million in every 1000g additives, Pediococcus acidilactici 40000 hundred million are husky Spine freeze-dried powder 50g, Rosa roxburghii freeze-dried powder 30g, wintercherry freeze-dried powder 30g, blackcurrant freeze-dried powder 30g, cactus freeze-dried powder 95g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 11

A kind of microbe additive is by bacillus laterosporus dry powder, lactobacillus plantarum dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus laterosporus 45000 hundred million in every 1000g additives, lactobacillus plantarum 45000 hundred million are husky Spine freeze-dried powder 40g, Rosa roxburghii freeze-dried powder 40g, wintercherry freeze-dried powder 25g, blackcurrant freeze-dried powder 25g, cactus freeze-dried powder 115g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 12

A kind of microbe additive is by bacillus licheniformis dry powder, lactobacillus bulgaricus dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt Freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add surplus charing egg-shell meal it is mixed It closes uniformly, composite packaging is made：Bacillus licheniformis 55000 hundred million, lactobacillus bulgaricus in every 1000g additives 55000 hundred million, sea-buckthorn freeze-dried powder 50g, Rosa roxburghii freeze-dried powder 50g, wintercherry freeze-dried powder 20g, blackcurrant freeze-dried powder 20g, cactus are frozen Dry powder 100g, remaining is charing egg-shell meal；Specifically production method is：Weigh embodiment 1 sea-buckthorn freeze-dried powder obtained, Rosa roxburghii Tratt respectively Freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then by bacillus licheniformis dry powder and lactic acid chain Coccus dry powder is uniformly admixed, and after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 3, is carried out compound Packaging；Composite packaging is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica dehydrators between interior outer bag Agent, to prevent water suction.

Embodiment 13

A kind of microbe additive, be by bacillus subtilis dry powder, bifidobacteria dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, Wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder be uniformly mixed, then add surplus charing egg-shell meal be uniformly mixed, Composite packaging is made：The bacillus subtilis 45000 hundred million in every 1000g additives, Bifidobacterium 60000 hundred million, sea-buckthorn are frozen Dry powder 50g, Rosa roxburghii freeze-dried powder 50g, wintercherry freeze-dried powder 15g, blackcurrant freeze-dried powder 15g, cactus freeze-dried powder 45g, remaining is charcoal Change egg-shell meal；Specifically production method is：Weigh embodiment 1 sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-drying respectively Powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 3, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 14

A kind of microbe additive is by Japan's bacillus dry powder, lactobacillus acidophilus dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：Japan bacillus 60000 hundred million in every 1000g additives, lactobacillus acidophilus 40000 hundred million are husky Spine freeze-dried powder 25g, Rosa roxburghii freeze-dried powder 30g, wintercherry freeze-dried powder 10g, blackcurrant freeze-dried powder 10g, cactus freeze-dried powder 80g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 3, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 15

A kind of microbe additive is by bafillus natto dry powder, lactobacillus fermenti dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bafillus natto 50000 hundred million in every 1000g additives, lactobacillus fermenti 45000 hundred million are husky Spine freeze-dried powder 35g, Rosa roxburghii freeze-dried powder 40g, wintercherry freeze-dried powder 18g, blackcurrant freeze-dried powder 12g, cactus freeze-dried powder 95g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 3, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 16

A kind of microbe additive is by bacillus subtilis dry powder, streptococcus thermophilus dried powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus subtilis 60000 hundred million in every 1000g additives, streptococcus thermophilus 30000 hundred million are husky Spine freeze-dried powder 45g, Rosa roxburghii freeze-dried powder 45g, wintercherry freeze-dried powder 15g, blackcurrant freeze-dried powder 15g, cactus freeze-dried powder 85g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 3, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 17

A kind of microbe additive is by bacillus cereus dry powder, Pediococcus acidilactici dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus cereus 45000 hundred million in every 1000g additives, Pediococcus acidilactici 45000 hundred million are husky Spine freeze-dried powder 25g, Rosa roxburghii freeze-dried powder 25g, wintercherry freeze-dried powder 25g, blackcurrant freeze-dried powder 25g, cactus freeze-dried powder 70g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 18

A kind of microbe additive, be by bacillus licheniformis dry powder, bifidobacteria dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, Wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder be uniformly mixed, then add surplus charing egg-shell meal be uniformly mixed, Composite packaging is made：The bacillus licheniformis 30000 hundred million in every 1000g additives, Bifidobacterium 60000 hundred million, sea-buckthorn are frozen Dry powder 35g, Rosa roxburghii freeze-dried powder 35g, wintercherry freeze-dried powder 20g, blackcurrant freeze-dried powder 20g, cactus freeze-dried powder 65g, remaining is charcoal Change egg-shell meal；Specifically production method is：Weigh embodiment 1 sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-drying respectively Powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 19

A kind of microbe additive is by bacillus licheniformis dry powder, streptococcus thermophilus dried powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus licheniformis 60000 hundred million in every 1000g additives, streptococcus thermophilus 35000 hundred million are husky Spine freeze-dried powder 45g, Rosa roxburghii freeze-dried powder 45g, wintercherry freeze-dried powder 18g, blackcurrant freeze-dried powder 18g, cactus freeze-dried powder 100g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 2, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Embodiment 20

A kind of microbe additive is by bacillus subtilis dry powder, plant lactobacillus powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt freeze-drying Powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus Even, composite packaging is made：The bacillus subtilis 60000 hundred million in every 1000g additives, lactobacillus plantarum 40000 hundred million are husky Spine freeze-dried powder 35g, Rosa roxburghii freeze-dried powder 35g, wintercherry freeze-dried powder 25g, blackcurrant freeze-dried powder 25g, cactus freeze-dried powder 80g, remaining To carbonize egg-shell meal；Specifically production method is：Weighing embodiment 1, sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry are frozen respectively Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder mixing, then bacillus licheniformis dry powder and streptococcus lactis dry powder are uniformly mixed Enter, after then addition surplus is sufficiently mixed uniformly by the charing egg-shell meal obtained of embodiment 3, carries out composite packaging；Composite packaging It is that inner bag uses polypropylene plastics pocket, outer bag to use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.

Claims (11)

1. a kind of microbe additive, feature it be first by bacillus, lactic acid bacteria, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, Wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder be uniformly mixed, then add surplus charing egg-shell meal be uniformly mixed, Composite packaging is made：Bacillus 5000 hundred million -60000 hundred million in every 1000g additives, lactic acid bacteria 5000 hundred million -60000 A hundred million, sea-buckthorn freeze-dried powder 5-50g, Rosa roxburghii freeze-dried powder 5-50g, wintercherry freeze-dried powder 3-30g, blackcurrant freeze-dried powder 3-30g, cactus Freeze-dried powder 50-150g, remaining is charing egg-shell meal；The sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant Freeze-dried powder, cactus freeze-dried powder, are made by following methods, and technical process is to take fresh sea-buckthorn, Rosa roxburghii Tratt, wintercherry, black respectively Gallon, cactus remove carpopodium, the impurity such as rotten fruit, and rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, remove seed step； Rinsing condition described above is the citric acid that weight 0.1% is added with 40 DEG C of water, rinses 15min, and be stirred continuously, pulls out and put Enter in pure water and rinses 3 times；Above-mentioned freezing is will rapidly to cool down after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot respectively To -45 DEG C or less；The process conditions of above-mentioned lyophilization are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is dry to water Divide until being less than 6%/w；The charing egg-shell meal is made by following methods：（1）Dry, dipping first cleans eggshell Totally, moisture is dried, is dried 1-2 hours in advance, then pulverizes into 20-30 mesh coarse powder, by weight 1:0.5 is thick in eggshell The salt that prepared weight fraction is 25% is sprayed on powder（Sodium chloride）Solution, mixes in sprinkling, and it is small that 6-7 is placed after mixing When, then uniformly mixing is primary again, then places 6-7 hours；It is empty the purpose is to allow salt effectively to penetrate into eggshell organization internal In gap；（2）The eggshell powder raw material impregnated is put into rotary carbonizing pot by charing, rotates charcoal at a temperature of 420-450 DEG C Change 70-80 minutes, until observing the complete blackening of raw material；（3）The raw material carbonized is rapidly moved in activation furnace by activation, closes stove Door, is passed through carbon dioxide gas, catches up with air therein to the greatest extent, and anoxybiotic activates 55-85 minutes at 720-800 DEG C；（4）Cleaning is taken out After activated material, it is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, chlorination is not measured until examining substantially Until sodium；After having cleaned sodium chloride, the hydrochloric acid for being 12% with mass ratio submerges activated material 2.5-3 hours, waits after impregnating, and uses 95 DEG C of pure water washing activated materials, until material grain there is no white after, then use room temperature pure water rinse to neutrality, filter, must float Wash activated material；（5）Dry and screening, which dries the activated material of rinsed clean at 115-120 DEG C to water content, is less than 6%/w, mistake 60 mesh sieve, and the coarse grain after screening pulverized again, make all by 60 mesh sieve to get.

2. a kind of microbe additive, feature it be first by bacillus, lactic acid bacteria, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, Wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder be uniformly mixed, then add surplus charing egg-shell meal be uniformly mixed, Composite packaging is made：Bacillus 7000 hundred million -60000 hundred million in every 1000g additives, lactic acid bacteria 7000 hundred million -60000 A hundred million, sea-buckthorn freeze-dried powder 10-50g, Rosa roxburghii freeze-dried powder 8-50g, wintercherry freeze-dried powder 5-30g, blackcurrant freeze-dried powder 5-30g, celestial being Freeze-dried powder 70-150g is slapped, remaining is charing egg-shell meal；The sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, it is black plus Logical sequence freeze-dried powder, cactus freeze-dried powder, are made by following methods, technical process be take respectively fresh sea-buckthorn, Rosa roxburghii Tratt, wintercherry, Blackcurrant, cactus remove carpopodium, the impurity such as rotten fruit, and rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, remove seed step Suddenly；Rinsing condition described above is the citric acid that weight 0.1% is added with 40 DEG C of water, rinses 15min, and be stirred continuously, and is dragged for Go out to be put into pure water and rinse 3 times；Above-mentioned freezing is respectively will be rapid after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot It is cooled to -45 DEG C or less；The process conditions of above-mentioned lyophilization are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is dry Until moisture is less than 6%/w；The charing egg-shell meal is made by following methods：（1）Drying, dipping are clear by eggshell first Wash clean dries moisture, is dried 1-2 hours in advance, then pulverizes into 20-30 mesh coarse powder, by weight 1:0.5 in eggshell The salt that prepared weight fraction is 25% is sprayed on coarse powder（Sodium chloride）Solution mixes in sprinkling, 6-7 is placed after mixing Hour, then uniformly mixing is primary again, then places 6-7 hours；The purpose is to allow salt effectively to penetrate into eggshell organization internal In gap；（2）The eggshell powder raw material impregnated is put into rotary carbonizing pot by charing, is rotated at a temperature of 420-450 DEG C Charing 70-80 minutes, until observing the complete blackening of raw material；（3）The raw material carbonized is rapidly moved in activation furnace by activation, is closed Fire door is passed through carbon dioxide gas, catches up with air therein to the greatest extent, and anoxybiotic activates 55-85 minutes at 720-800 DEG C；（4）Cleaning takes After going out activated material, it is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, chlorine is not measured until examining substantially Until changing sodium；After having cleaned sodium chloride, the hydrochloric acid for being 12% with mass ratio submerges activated material 2.5-3 hours, waits after impregnating, With 95 DEG C of pure water washing activated materials, after material grain is there is no white, then room temperature pure water rinse to neutrality is used, filter, obtain Rinse activator material；（5）Dry and screening, which dries the activated material of rinsed clean at 115-120 DEG C to water content, is less than 6%/w, Cross 60 mesh sieve, the coarse grain after screening pulverized again, make all by 60 mesh sieve to get.

3. a kind of microbe additive, feature it be first by bacillus, lactic acid bacteria, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, Wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder be uniformly mixed, then add surplus charing egg-shell meal be uniformly mixed, Composite packaging is made：Bacillus 9000 hundred million -60000 hundred million in every 1000g additives, lactic acid bacteria 9000 hundred million -60000 A hundred million, sea-buckthorn freeze-dried powder 15-50g, Rosa roxburghii freeze-dried powder 12-50g, wintercherry freeze-dried powder 8-30g, blackcurrant freeze-dried powder 8-30g, celestial being Freeze-dried powder 85-150g is slapped, remaining is charing egg-shell meal；The sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, it is black plus Logical sequence freeze-dried powder, cactus freeze-dried powder, are made by following methods, technical process be take respectively fresh sea-buckthorn, Rosa roxburghii Tratt, wintercherry, Blackcurrant, cactus remove carpopodium, the impurity such as rotten fruit, and rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, remove seed step Suddenly；Rinsing condition described above is the citric acid that weight 0.1% is added with 40 DEG C of water, rinses 15min, and be stirred continuously, and is dragged for Go out to be put into pure water and rinse 3 times；Above-mentioned freezing is respectively will be rapid after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot It is cooled to -45 DEG C or less；The process conditions of above-mentioned lyophilization are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is dry Until moisture is less than 6%/w；The charing egg-shell meal is made by following methods：（1）Drying, dipping are clear by eggshell first Wash clean dries moisture, is dried 1-2 hours in advance, then pulverizes into 20-30 mesh coarse powder, by weight 1:0.5 in eggshell The salt that prepared weight fraction is 25% is sprayed on coarse powder（Sodium chloride）Solution mixes in sprinkling, 6-7 is placed after mixing Hour, then uniformly mixing is primary again, then places 6-7 hours；The purpose is to allow salt effectively to penetrate into eggshell organization internal In gap；（2）The eggshell powder raw material impregnated is put into rotary carbonizing pot by charing, is rotated at a temperature of 420-450 DEG C Charing 70-80 minutes, until observing the complete blackening of raw material；（3）The raw material carbonized is rapidly moved in activation furnace by activation, is closed Fire door is passed through carbon dioxide gas, catches up with air therein to the greatest extent, and anoxybiotic activates 55-85 minutes at 720-800 DEG C；（4）Cleaning takes After going out activated material, it is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, chlorine is not measured until examining substantially Until changing sodium；After having cleaned sodium chloride, the hydrochloric acid for being 12% with mass ratio submerges activated material 2.5-3 hours, waits after impregnating, With 95 DEG C of pure water washing activated materials, after material grain is there is no white, then room temperature pure water rinse to neutrality is used, filter, obtain Rinse activator material；（5）Dry and screening, which dries the activated material of rinsed clean at 115-120 DEG C to water content, is less than 6%/w, Cross 60 mesh sieve, the coarse grain after screening pulverized again, make all by 60 mesh sieve to get.

4. a kind of microbe additive, feature it be first by bacillus, lactic acid bacteria, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, Wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder be uniformly mixed, then add surplus charing egg-shell meal be uniformly mixed, Composite packaging is made：Bacillus 10000 hundred million -60000 hundred million, lactic acid bacteria 10000 hundred million-in every 1000g additives 60000 hundred million, sea-buckthorn freeze-dried powder 20-50g, Rosa roxburghii freeze-dried powder 15-50g, wintercherry freeze-dried powder 10-30g, blackcurrant freeze-dried powder 10- 30g, cactus freeze-dried powder 100-150g, remaining is charing egg-shell meal；The sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry are frozen Dry powder, blackcurrant freeze-dried powder, cactus freeze-dried powder, are made by following methods, and technical process is to take fresh sea-buckthorn, thorn respectively Pears, wintercherry, blackcurrant, cactus remove carpopodium, the impurity such as rotten fruit, and rinsing, freezing, lyophilization, low-temperature grinding are not gone Skin, remove seed step；Rinsing condition described above is the citric acid that weight 0.1% is added with 40 DEG C of water, rinses 15min, not Disconnected stirring, pulls out to be put into pure water and rinses 3 times；Above-mentioned freezing is respectively to fill sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus - 45 DEG C or less are cooled to after disk rapidly；The process conditions of above-mentioned lyophilization are temperature-22-- 32 DEG C, vacuum degree 120- 150Pa is dry until moisture is less than 6%/w；The charing egg-shell meal is made by following methods：（1）Dry, dipping head First eggshell is cleaned up, dries moisture, is dried 1-2 hours in advance, then pulverizes into 20-30 mesh coarse powder, by weight 1:0.5 sprays the salt that prepared weight fraction is 25% on eggshell coarse powder（Sodium chloride）Solution is mixed in sprinkling, is mixed It is placed after even 6-7 hours, then uniformly mixing is primary again, then places 6-7 hours；The purpose is to allow salt effectively to penetrate into egg In shell organization internal gap；（2）The eggshell powder raw material impregnated is put into rotary carbonizing pot by charing, at 420-450 DEG C At a temperature of rotation charing 70-80 minute, observation the complete blackening of raw material until；（3）The raw material carbonized is rapidly moved to live by activation Change in stove, closes fire door, be passed through carbon dioxide gas, catch up with air therein to the greatest extent, 55-85 points of the anoxybiotic activation at 720-800 DEG C Clock；（4）After activated material is taken out in cleaning, it is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, Zhi Daoji Until this inspection does not measure sodium chloride；After having cleaned sodium chloride, the hydrochloric acid for being 12% with mass ratio submerges activated material 2.5-3 hours, It waits after impregnating, with 95 DEG C of pure water washing activated materials, after material grain is there is no white, then extremely with room temperature pure water rinse Neutrality, filtering, obtains rinse activator material；（5）Dry and screening dries the activated material of rinsed clean at 115-120 DEG C to aqueous Amount is less than 6%/w, crosses 60 mesh sieve, and the coarse grain after screening pulverized again, make all by 60 mesh sieve to get.

5. a kind of microbe additive as described in claim 1-4, which is characterized in that the bacillus and lactic acid bacteria, The respectively every gram thalline dry powder product that 200 hundred million are no less than containing viable bacteria concentration.

6. a kind of microbe additive as described in claim 1-4, which is characterized in that the bacillus is lichens gemma Bacillus, bacillus lentus, bacillus cereus, bacillus subtilis, bacillus coagulans, Japan bacillus, side spore bud Any one in spore bacillus, bacillus pumilus, bafillus natto.

7. a kind of microbe additive as described in claim 1-4, which is characterized in that the lactic acid bacteria is lactic acid breast bar Bacterium, streptococcus lactis, lactobacillus acidophilus, lactobacillus plantarum, lactobacillus fermenti, streptococcus thermophilus, propionibacterium freudenreichii, lactic acid sheet Coccus, Lactobacillus helveticus, Xie Shi Propionibacteriums, Pediococcus pentosaceus, cheese lactic acid bacteria, lactobacillus plantarum, German-style lactobacillus, fiber Any one in disaccharides lactobacillus, Bifidobacterium.

8. a kind of microbe additive as described in claim 1-4, which is characterized in that the low-temperature grinding is temperature of charge It is crushed in 0 DEG C or less.

9. a kind of microbe additive as described in claim 1-4, which is characterized in that the composite packaging uses interior outer bag Composite packaging, inner bag use polypropylene plastics pocket, outer packing to use aluminium foil bag, and it is small to be filled with silica-gel desiccant between interior outer bag Bag.

10. a kind of microbe additive as described in claim 1-4, which is characterized in that the eggshell is egg shell, duck's egg Any one or a few mixing eggshell in shell, goose egg-shell and quail eggshell.

11. a kind of microbe additive as described in claim 1-4, which is characterized in that the drying uses heated-air drying Or far-infrared ray drying；The drying condition is 180 DEG C -300 DEG C.