CN108850526A - Diacetyl streptococcus lactis feed addictive - Google Patents
Diacetyl streptococcus lactis feed addictive Download PDFInfo
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- CN108850526A CN108850526A CN201810512101.5A CN201810512101A CN108850526A CN 108850526 A CN108850526 A CN 108850526A CN 201810512101 A CN201810512101 A CN 201810512101A CN 108850526 A CN108850526 A CN 108850526A
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- A23K10/16—Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions
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Abstract
Diacetyl streptococcus lactis feed addictive disclosed by the invention, it is characterized in that being uniformly mixed first by diacetyl streptococcus lactis, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder, the charing egg-shell meal for adding surplus again is uniformly mixed, and composite packaging is made:Diacetyl streptococcus lactis 30000 hundred million -150000 hundred million in every 1000g feed addictive, sea-buckthorn freeze-dried powder 5-50g, Rosa roxburghii freeze-dried powder 5-50g, wintercherry freeze-dried powder 3-30g, blackcurrant freeze-dried powder 3-30g, cactus freeze-dried powder 50-150g, remaining is charing egg-shell meal.Viable bacteria contained by the present invention is clear, application and Quantitatively Selecting conducive to user, using sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus freeze-dried powder and charing egg-shell meal as the matrix of additive, stability, trophism and the adsorptivity of additive institute mycetome can not only be improved, the nutritive value for promoting product simultaneously promotes the metabolism of animal, improves body resistance against diseases, promote growth of animal, the final economic benefit for improving aquaculture.
Description
Technical field
The invention belongs to feed additive fields, are related to a kind of for cultivated animals probiotic feed additive.Specifically
It is related to a kind of diacetyl streptococcus lactis feed addictive.
Background technique
Lactic acid bacteria(Lactic acid bacteria, LAB)The lactic acid bacteria being currently known has more than 100 kind.Lactic acid bacteria
Applicating history is very long, such as the production and production of dairy products, pickles, ensilage.In the enteron aisle of humans and animals there is
A large amount of lactic acid bacteria.Lactobacillus preparation is a kind of preparation containing live lactobacillus, entitled alctasin.Lactic acid bacteria grows in enteron aisle
Development decomposes carbohydrate and generates lactic acid and form acidic environment, to inhibit the proliferation of harmful bacteria in intestinal canal, and prevent from producing poison and
It causes a disease.The strain for preparing lactobacillus preparation has lactobacillus acidophilus, lactobacillus bulgaricus, streptococcus lactis and streptococcus fecalis etc..
Lactobacillus is animal(Especially poultry) enteron aisle normal settler.Poultry went out after shell in a few hours can be
Streptococcus fecalis, the enterobacteria that discovery is dispersed in enteron aisle() and clostridium Enterobateria(Clostridia), with
Bacillus acidi lactici just starts to settle down in alimentary canal in a couple of days afterwards.Lactobacillus is the main Pseudomonas of fowl piperazine capsule flora, with large intestine
Bacillus, streptococcus(Streptococi it) compares and occupies advantage.Bacillus acidi lactici is adhered to fowl prolixity capsular epithelium, and this adhesion has kind
Specificity.Fowl piperazine capsule Bacillus acidi lactici is the Bacillus acidi lactici source that poultry maintains intestinal bacteria balance.Bacillus acidi lactici is maintaining to digest
The aspect of stablizing of the normal microflora system in road plays conclusive effect.Most probiotic products be Lactobacillus or other
Lactic acid-producing bacteria.
Lactic acid bacteria anaerobism or amphimicrobian growth, still are able to survive under pH3.0-4.5 acid condition.It is in animal intestinal tract
Middle by monosaccharide, especially Lactose conversion is lactic acid, to reduce intestinal pH, prevents foreign bacteria in the field planting of enteron aisle, inhibits large intestine
The growth of the pathogens such as bacillus, detection of Salmonella, and the growth of final lactic acid bacteria inhibiting itself.Lactic acid bacteria also can be by adjusting enteron aisle
PH promotes gastrointestinal peristalsis to activate pepsin, helps the digestion of food, absorbs, mitigate flatulence and promote liver function etc..
Lactic acid bacteria is acted on by competitive exclusion(Competitive binding site) inhibit pathogen growth.Lactic acid bacteria can also stimulate siberian crabapple
System improves immunity of organisms, improves intestinal tissue to the resistivity of bacteria attack.Some Bacillus acidi lacticis can neutralize certain toxin,
As lactobacillus bulgaricus can neutralize escherichia coli enterotoxin, but precise mechanism is unclear.Bacillus acidi lactici also can produce itself
Some digestive ferments, such as invertase, lactase and peptase, help to improve animal digestion function.Sawada report, certain lactic acid
Contain a kind of safe and effective natural anti-hypertension compound SG-1 in bacilli-cell wall.Lang Zhongwu is equal to 1994 in egg young bird
Brood of layers chichen is added in daily grain of chicken, as a result feed efficiency improves 8.73%-11.23%;Xiao Zhenfeng etc.(1995) it tries
Verify bright, Brood of layers chichen is compared compared with antibiotic control group, improves feed efficiency 4.6%.Furthermore Bacillus acidi lactici can
The digestive function of small intestine is improved by increasing surface area.Animal is in stress(As birth, wean, daily ration variation, intestinal pH are abnormal
It increases)Period, total variation tendency are that pathogen is increased, and Bacillus acidi lactici quantity is reduced.Lactobacillus is successfully established in enteron aisle
PH can be made to become stable.
The characteristics of lactic acid bacteria is:1. being the main fungal component of many animals alimentary canal, normal flora can be formed:2. in micro- need
Lactic acid is generated under oxygen or anaerobic condition;3. there is stronger acid resistance;4. generating a kind of bacteriocin
(Bacteriocin), hay bacillus, staphylococcic growth can effectively be inhibited.The shortcomings that lactic acid bacteria is that temperature capacity is poor,
Dead under the conditions of 65-75 DEG C, instantaneous high-temperature can be killed and be failed during feed granules.The type of preparation of such bacterium
It is various, using earliest, most extensively.
Diacetyl streptococcus lactis(Streptococcus diacetylactis)It is Food and Drug Administration and feeding
Expects pipe reason association is considered safe microorganism fodder, there is relatively broad application in aquaculture industry of China in recent years.Just at present
The dosage form that diacetyl streptococcus lactis is used as additive, there is aqua and pulvis two major classes, and aqueous solution dosage form is held because of thallus
Easily continuing to be metabolized using the nutritional substance in aqua, growth fermentation, therefore, the thallus of this dosage form plays pendulum,
Storage life is shorter.Powder formulation is then that thallus is taken off at a slow speed the thallus lived to using drying means such as low temperature hot wind, freezings
Water makes thallus be in stable drying dormant state, recycles substance that can be feeding to be uniformly mixed as filler and is made
Relatively stable powder-type biological feed additive.But with regard to current manufacturing enterprise in view of raw material be easy to get and processing cost,
Often select rice bran, wheat bran, corn flour, maize cob meal, peanut shell powder, conch meal, vermiculite power, mountain flour, calcium carbonate, medical stone, boiling
One or more of mountain flour mixture, some also use plant straw powder or grass meal as filler material.These are in line with being produced into
This considerations of, then has ignored the stability of microbial bacteria and the trophism value of feed addictive.
In order in use, have certain adhesion, microbial bacteria feed addictive be made to exist in microbial bacteria additive
It admixes when being mixed in animal feed, can be adsorbed on animal feed, convenient for the uniformity in animal feeding and be fed into bacterium amount
Maximization, some products take pains a certain amount of binder of addition.
In order to make to raise the relative constant of animal stomach inner pH value, acid is continued up to after so that the foodstuff being fed into is entered small intestine
The effect of change, in the product often simultaneously using acidulants such as citric acid, lactic acid, hydrochloric acid, fumaric acid, but these acidulants are not only straight
It connects and locally causes acidity too strong microbial bacteria contained by additive, influence the survival of thallus, meanwhile, these acidifying substances are to cultivation
Animal also without the nutritive value directly utilized, meanwhile, there is very big irritation to the gastrointestinal tract of the cubs of livestock and poultry, chick,
Compatibility is using not ideal enough.
Above-mentioned deficiency can be overcome by developing one kind, can either keep stability, the trophism of institute's mycetome, be had again to thallus
There is adhesion, while having again to the filler used and providing the additive for microbe feedstuff of nutritive value to cultivated animals, is
Promote the basis of feed additive industry long-term stability development.
Summary of the invention
The purpose of the present invention is to provide a kind of new single type diacetyl streptococcus lactis feed addictive, the diacetyl
Not only there is streptococcus lactis feed addictive thallus to stablize, and the thallus time-to-live is long, and used auxiliary agents have
Certain adhesiveness and adsorptivity can make thallus preferably be bonding on one with auxiliary agents, meanwhile, complementary additive tool
There is certain acidity, after animal feeding, nutriment abundant can not only be provided, while its acidic materials is able to maintain pH in stomach
Be worth it is relative constant, into small intestine after the effect of continuing up to acidification.The purpose is to provide a kind of more stability and trophism
Diacetyl streptococcus lactis feed addictive.
Diacetyl streptococcus lactis feed addictive of the present invention, it is characterized in that by diacetyl streptococcus lactis with it is a certain amount of
Seabuckthorn fruit powder, Ribes burejense powder, wintercherry powder, blackcurrant powder, cactus powder and charing egg-shell meal uniformly mix, and obtain a kind of new diacetyl
The thallus of streptococcus lactis feed addictive, this additive is stablized, and the thallus time-to-live is long, and seabuckthorn fruit powder, Ribes burejense powder, wintercherry
Powder, blackcurrant powder sugar content are high, and especially cactus powder all has preferable Adhesion property, and charing egg-shell meal also has preferably
Adsorptivity.Wherein sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant are the ascorbic fruits of high-content, and acidity is extremely strong, not only to cultivation
Animal provides the nutriments such as vitamin abundant, and the acidic materials after feeding play the effect for promoting digestion well,
To highlight the purpose of the present invention.
In order to realize the present invention, the following technical solutions are specifically adopted:
Diacetyl streptococcus lactis feed addictive, feature it be first by diacetyl streptococcus lactis, sea-buckthorn freeze-dried powder, thorn
Pears freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal of surplus
It is uniformly mixed, composite packaging is made:Diacetyl streptococcus lactis 30000 hundred million -150000 in every 1000g feed addictive
Hundred million, sea-buckthorn freeze-dried powder 5-50g, Rosa roxburghii freeze-dried powder 5-50g, wintercherry freeze-dried powder 3-30g, blackcurrant freeze-dried powder 3-30g, cactus are frozen
Dry powder 50-150g, remaining is charing egg-shell meal.
Diacetyl streptococcus lactis described above is diacetyl streptococcus lactis dry powder product.
The diacetyl streptococcus lactis dry powder product can be used and commercially available be used as every gram of feed addictive and contain
Viable bacteria concentration is no less than 250 hundred million preparations, the diacetyl streptococcus lactis dry powder product and the filler material in formula
Weight proportion is determined by the thallus content of thalli dry powder and final products.
The diacetyl streptococcus lactis dry powder product also can use existing method and select the culture medium accordingly optimized
By liquid fermentation equipment culture, then the thallus in fermentation liquid is separated with high speed centrifugation mode, is placed in hothouse
Bacterium mud drying is made with cold wind or with vacuum freeze drying mode, every gram of viable bacteria concentration of acquisition is no less than 250 hundred million
Thalli dry powder product.
Sea-buckthorn freeze-dried powder described above, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder,
It being made by following methods, technical process is that fresh sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus is taken to remove carpopodium respectively,
The impurity such as rotten fruit, rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, deseeding step;Rinsing condition described above is
With the citric acid of 40 DEG C of water addition weight 0.1%, 15min is rinsed, and be stirred continuously, pulls out to be put into pure water and rinse 3 times;On
Stating freezing is that will be cooled to rapidly -45 DEG C or less after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot respectively;Above-mentioned distillation
Dry process conditions are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is dry until moisture is less than 6%/w;It is above-mentioned
Low-temperature grinding is the crushing that temperature of charge is in 0 DEG C or less progress, 100 mesh of grinding particle size >.
Composite packaging described above uses interior outer bag composite packaging, and inner bag uses polypropylene plastics pocket, and outer packing uses aluminium
Foil bag is filled with silica-gel desiccant between interior outer bag.
Charing egg-shell meal described above is made by following methods:
(1)Dry, dipping first cleans up eggshell, dries moisture, is dried 1-2 hours, then pulverizes into advance
20-30 mesh coarse powder, by weight 1:0.5 sprays the salt that prepared weight fraction is 25% on eggshell coarse powder(Sodium chloride)
Solution is mixed in sprinkling, is placed after mixing 6-7 hours, then uniformly mixing is primary again, then places 6-7 hours;The purpose is to
Salt is allowed effectively to penetrate into eggshell organization internal gap;
(2)Charing impregnated eggshell powder raw material is put into rotary carbonizing pot, 420-450 DEG C at a temperature of rotate charcoal
Change 70-80 minutes, until observing the complete blackening of raw material(Carbonization process should have corresponding scraping blade, to prevent raw material in carbonization process
Viscous pot and agglomeration);
(3)The raw material carbonized is rapidly moved in activation furnace by activation, is closed fire door, is passed through carbon dioxide gas, is caught up with to the greatest extent wherein
Air, at 720-800 DEG C anoxybiotic activate 55-85 minutes(Corresponding turning mechanism is set in activation furnace, keeps activation raw material every
It can be stirred within 10 minutes once, to guarantee activation fully and uniformly);
(4)After activated material is taken out in cleaning, it is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, until
Until basic inspection does not measure sodium chloride;After having cleaned sodium chloride, it is small that activated material 2.5-3 is submerged with the hydrochloric acid that mass ratio is 12%
When, after impregnating, with 95 DEG C of pure water washing activated materials, until material grain is there is no after white, then with the drift of room temperature pure water
It is washed till neutrality(PH value is about in 6.9-7.1), filter, obtain rinse activator material;
(5)Dry and screening, which dries the activated material of rinsed clean at 115-120 DEG C to water content, is lower than 6%(w), cross 60
Mesh, the coarse grain after screening are pulverized again, are made all by 60 meshes to get charing egg-shell meal product.
Drying described above uses heated-air drying or far-infrared ray drying;Dry condition is 180 DEG C -300 DEG C.It is dried
Purpose be that can make the crisp matter of eggshell, increase eggshell hole be conducive to sprinkling saline solution effectively penetrate eggshell internal voids
In.
Eggshell described above is the mixed of any one or a few in egg shell, Ovum Anas domestica putamina, goose egg-shell and quail eggshell
Close eggshell.
The prioritization scheme of diacetyl streptococcus lactis feed addictive of the present invention is, first by diacetyl streptococcus lactis,
Sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add surplus
Charing egg-shell meal be uniformly mixed, composite packaging is made:The diacetyl streptococcus lactis 50000 in every 1000g feed addictive
A hundred million -150000 hundred million, sea-buckthorn freeze-dried powder 10-50g, Rosa roxburghii freeze-dried powder 10-50g, wintercherry freeze-dried powder 5-30g, blackcurrant freeze-drying
Powder 5-30g, cactus freeze-dried powder 70-150g, remaining is charing egg-shell meal.
The further prioritization scheme of the present invention is diacetyl streptococcus lactis feed addictive, it is characterized in that first by two
Acetolactic acid streptococcus, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, the mixing of cactus freeze-dried powder
Uniformly, then add surplus charing egg-shell meal be uniformly mixed, composite packaging is made:The diacetyl in every 1000g feed addictive
Streptococcus lactis 70000 hundred million -150000 hundred million, sea-buckthorn freeze-dried powder 15-50g, Rosa roxburghii freeze-dried powder 15-50g, wintercherry freeze-dried powder 8-
30g, blackcurrant freeze-dried powder 8-30g, cactus freeze-dried powder 85-150g, remaining is charing egg-shell meal.
Further optimization plan of the present invention is diacetyl streptococcus lactis feed addictive, it is characterized in that first by
Diacetyl streptococcus lactis, sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are mixed
Close uniformly, then add surplus charing egg-shell meal be uniformly mixed, composite packaging is made:The diethyl in every 1000g feed addictive
Acyl streptococcus lactis 90000 hundred million -150000 hundred million, sea-buckthorn freeze-dried powder 20-50g, Rosa roxburghii freeze-dried powder 20-50g, wintercherry freeze-dried powder
10-30g, blackcurrant freeze-dried powder 10-30g, cactus freeze-dried powder 100-150g, remaining is charing egg-shell meal.
Sea-buckthorn(Hippophae rhamnoides Linn.), fruit nutriment rich in and biological active matter
Matter can be widely applied to many fields of the national economy such as food, medicine, light industry, space flight, agriculture and animal husbandry fishery.Fructus hippophae and oil
With very high medical value, there is a cough-relieving apophlegmatic, relieving dyspepsia, promoting blood circulation to remove blood stasis effect, can treat gastric duodenal ulcer with
And indigestion etc..
Sea buckthorn fruit is full of nutrition, according to surveying and determination in its fruit containing multivitamin, fatty acid, microelement, sub- oil element,
The various amino acid of Hippophate flavone, superoxides isoreactivity substance and needed by human body.Wherein Vitamin C content is high, and every 100 grams
In fruit juice, Vitamin C content can reach 825-1100 milligrams, is 2-3 times of Kiwi berry, is known as the laudatory title of the king of vitamin C.Contain
Sugared 7.5%-10%, the 3%-5% containing acid.
Rosa roxburghii Tratt(Rosa roxbunghii)For the fruit of the perennial machaka rosa roxburghii of rosaceae also known as mountain king fruit, thorn
Certain kind of berries fruit, thatch pears etc..With clearing heat and promoting fluid, stomach strengthening and digestion promoting, relieving summer-heat and other effects.Rosa roxburghii Tratt vitamin B rich in, C, carrotene,
The ingredients such as malic acid, citric acid are usually used in deficiency of stomach-Yin, appetite stimulator, indigestion or eating accumulation, glutted full bored, diarrhea
Loose stool;Pyreticosis or hot summer weather hurt saliva, thirsty, scanty drak urine.
Mature Rosa roxburghii Tratt is fleshy hypertrophy, sweet and sour, fruit are rich in sugar, vitamin, carrotene, organic acid and more than 20 kinds of ammonia
More than base acid, 10 microelement and superoxide dismutase, especially Vitamin C content beneficial to human body are high, are to work as
It is highest in preceding fruit, it is 50 times of citrus 841.58 milligrams -3541.13 milligrams of content in every 100 grams of fresh fruits, Kiwi berry
10 times, the laudatory title with " king of vitamin C ".Fruit of Grossularia burejensis Berger has very high nutritive value and medical value, sour, puckery, flat,
Digestion-promoting spleen-invigorating restrains stopping leak, for treating having indigestion abdominal distension, dysentery, enteritis, vitamin C deficiency etc..
Wintercherry(Physali alkekengiL.)Also known as groundcherry, franchet groundcherry persistent calyx or fruit, cape gooseberry etc..Containing more in Fruit of Physalis
Kind of nutritional ingredient, wherein the content of calcium be 73.1 times of tomato, 13.8 times of carrot, ascorbic content is tomato
6.4 times, 5.4 times of carrot.With unique flavor and nutrition abundant.Fruit of Physalis aromatic flavour, delicious.Berry is rich
Containing vitamin C, beta carotene, more than 20 kinds of mineral elements and 18 kinds of amino acid, there is heat-clearing, removing toxic substances, diuresis effect is usually used in
Control heat-syndrome cough, pharyngalgia, jaundice, dysentery, in water, the treatment of furunculosis, erysipelas etc..
Blackcurrant scientific name elements of black currant(Ribes nigrum L.)Also known as currant, purple plum etc., ripening fruits are black
Small berries, it is interior to be rich in vitamin C, anthocyanidin.Blackcurrant is not only a kind of delicious flavour, fruit full of nutrition, and has
Good medicinal efficacy.Blackcurrant fruit is rich in mineral matter element, and the Zn content in mineral matter element is high, can be used as and comes for zinc
Source;Ascorbic content is high, hence it is evident that is higher than citrus, hawthorn, also contains phosphorus, magnesium, potassium, calcium, anthocyanidin, phenolic substances.Seed
Linoleic acid content is high.Ascorbic content is very rich in blackcurrant, it is often more important that is also melted into containing a large amount of antioxygen
Point, this assures ascorbic function and effect.Blackcurrant is rich in such as anthocyanidin, vitamin C, flavones, Quercetin, red bayberry
The substances such as alcohol, phenolic acid, catechin and blackcurrant polysaccharide, these are all the bioactive substances with good anti-oxidation function.
Cactus(Scientific name:Opuntia stricta(Haw.)Haw.var.dillenii(Ker-Gawl.) Benson),
It is a kind of plant of Opuntia.Alias celestial being palm, kwan-yin palm etc..Cactus is the meat shrub that grows thickly, the wide ovum of top branch
Shape, obovate elliptic or subcircular;Flower spoke shape, holder obovate.It is used as medicine with complete stool.The four seasons can adopt.
Cactus is cool in nature, sour, nontoxic.Have the promoting flow of qi and blood circulation, heat-clearing toxin-expelling functions.Mainly have clearing heat and detoxicating, eliminating stasis to subdue swelling,
The functions such as the promoting flow of qi and blood circulation, benefiting stomach and stopping pain.Cactus contains amino acid and various trace elements in needed by human 8, and embraces green
The preciousness ingredient such as lotus, Kok Beattie cents, cholla stem, starches through cactus crude drug and analyzes, contain pectin, polysaccharide and glue exudate.From herb point
From extracting to obtain freidelin ketone(friedelin), -3 α -ol of freidelin(friedelan-3-α-ol), taraxerone
(taraxerone)And taraxerol(taraxerol).
Eggshell, quantity is biggish in China's poultry farming chicken, duck, goose and quail etc., using egg, duck's egg,
As in food processing process, the useless eggshell enormous amount generated is provided according to existing disclosed report for goose egg and quail egg
Material display, the eggshell total amount that a medium-sized city is monthly discarded reach 60-100 tons, and account for egg size by Eggshell weight 11% calculates,
The eggshell that about 1,500,000 tons of the daily output in China, not only pollutes environment, but also waste of resource in this way.Discarded eggshell is integrated
It utilizes, resource utilization can not only be improved and avoids environmental pollution, and be greatly improved the economic benefit and social benefit of enterprise.
Wherein egg shell is in China's yield maximum, and egg shell accounts for the 10-12% in entire egg, by under film, shell on shell
Film and eggshell three parts composition, eggshell is a kind of calcareous hard shell, is located on shell between film and shell lower film.In the change of egg shell
In studying point, minerals account for 95%, and protein 3.3%, moisture 1%, fat 0.03%, remaining is carbohydrate and other have
Machine substance(It certainly, does not include a large amount of remaining egg white in eggshell in the above ingredient).Eggshell mineral ingredient is mainly
Calcium carbonate accounts for 94% or so, remaining is magnesium carbonate and calcium phosphate, and calcium, phosphorus content account for 34.9% and of eggshell dry matter respectively
0.2%.In eggshell, seven kinds of vitamins and various trace elements and some important enzymes, peptide matters can be measured, he
Although content seldom, be all the substance needed in human body or animal body.
In the prior art, it is replenished the calcium with egg-shell meal, has the product of the grinds after sterilizing by eggshell in people's product, also have
The application of organic calcium is prepared into using primary or secondary clacining method.It is at present most widely in drug, food and nutriment
In preparation, micron order, submicron order and nano level superfine powder are mostly used, is added to various food, nutrition kind, has reached very
Good effect.Application of the eggshell in China's animal-breeding is taken mostly by eggshell cleaning, drying, and milling is added into feed
The method of feeding, since grinding particle size is larger, being absorbed and utilized for animal is poor, can't reach good application effect.
The present invention is to clean eggshell, after high temperature drying, then be made one through spice, charing, activation, cleaning, drying, screening
The adsorbent of kind function admirable, the program not only remains the nutrition that eggshell utilizes, while making the abundant carbonaceous of eggshell, not only right
It is contained it is calcareous form organic calcium, and form the filling substrate with adsorption capacity.
The beneficial effects of the invention are as follows:
(1)Product of the present invention can highlight the viable bacteria content of diacetyl streptococcus lactis, significantly improve thallus in closed compound packet
Survival rate in dress, through batches of products reserved sample observing 12 months at room temperature, diacetyl streptococcus lactis average viability
94.3%, and reference substance(The filler of reference substance is wheat bran)In diacetyl streptococcus lactis survival rate be 78.2%;This
Invention product is single type diacetyl streptococcus lactis feed addictive, and the specific aim with application can be provided to producer
With the selection of quantization, targetedly it is easy to use conducive to livestock and poultry.
(2)Pass through sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder and two
Acetolactic acid streptococcus mixes, due to the stickum in the colloidal substance that these dry powder formulations are rich in, especially cactus, energy
The adhesive effect between additive and feed is preferably increased, and improves the utilization rate of additive;
(3)By sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus freeze-dried powder high-content amino acid, vitamin, mineral element, more
Sugar.The nutritional ingredients such as the vitamin C of organic acid, especially high-content and various bioactivators, to raising animal immune energy
Power is simultaneously obviously improved meat, Egg Quality, the acidic materials in especially above-mentioned dry powder, utilization, promotion animal to contained microorganism
Digestion all has significant effect;
(4)Due to using Freeze Drying Technique means, enable sea-buckthorn obtained, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus freeze-dried powder
Its active constituent is maximumlly remained, has distinctive sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, the smell of cactus application and taste
Taste, free from extraneous odour add the preference of animal.
(5)Eggshell is first subjected to drying and other treatment through high temperature using charing egg-shell meal, further through spice, charing, activation, clear
It washes, dry and sieves, form a kind of excellent adsorbent, which not only forms absorption to the saccharomycete in product
Power, while making the eggshell after charing that still there is the organic calcium effect of activation, meanwhile, after animal feeding, have well to stomach
The toxin of enteron aisle has suction-operated, has stop dysentery, antidiarrheal effect for the animal of diarrhea and diarrhea, has good active carbon
Medicinal effects.
(6)To the preparation of sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus freeze-dried powder in the present invention, do not remove the peel, deseeding step
Suddenly, it is therefore an objective to by being crushed after freeze-drying, so that its skin and seed is worn into fine powder, make anthocyanidin, oil in its skin and seed
Class, organic acid, bud fragrance substance are retained, and the nutritive value of its freeze-dried powder is promoted.
(7)The present invention is lyophilized using sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus
Powder, matrix of the charing egg-shell meal as additive contain constants such as a large amount of calcium, phosphorus, potassium, sodium, magnesium, zinc and micro in matrix
Element, vitamin C still rich in, anthocyanidin, beta carotene, malic acid, citric acid, protein, amino acid, nucleic acid, Portugal
Grape sugar, lipoidis, carbohydrate, B family vitamin such as B1、B2、B6、B12And the physiological activity such as folic acid, niacin, pantothenic acid, inositol
Substance, not only improves the nutritive value of diacetyl nisin bacteria additive, while promoting the metabolism of animal, improves body
Disease resistance, promote growth of animal, finally improve the economic benefit of its aquaculture.
(8)Product of the present invention uses interior outer bag composite packaging, and interior outer bag interlayer is filled with silica-gel desiccant, and product does not return
Tide, no agglomeration, product is loose, good fluidity, can preferably keep exterior quality and inherent quality.
Operation to not having its technical process stated in detail in the present invention is in the common sense of those skilled in the art
Operation.With regard to the purchase and storage of heretofore described sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant fresh fruit and fresh cactus, the present invention
The construction of people's unit has 20,000 tons of freezer facility, has enough guarantees to storage fresh fruit material.
Specific embodiment
Embodiment 1
The preparation of sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder:
Sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, the cactus for taking fresh mature respectively remove carpopodium, the impurity such as rotten fruit, with containing heavy
40 DEG C of aqueous solutions of 0.1% citric acid are measured, 15min is rinsed under constant stirring and pulls out, be put into pure water and rinse 3 times, pull out
It is drained;It will be moved into refrigerator after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot respectively, be cooled to -45 DEG C rapidly
Below;Respectively by the sea-buckthorn freezed, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus move into lyophilization machine in, sublimation temperature control-
22--32 DEG C, vacuum degree 120-150Pa makes dry materials to moisture < 6%(w), the time about needs 18 hours, is put into after taking-up
In freezing crusher, control temperature of charge is no more than 0 DEG C, after being crushed to 100 mesh of fineness >, respectively obtains sea-buckthorn freeze-dried powder, thorn
Pears freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder, are fitted into polybag and seal, and are stored in 0 DEG C or less
It is spare in freezer.
Embodiment 2
Carbonize the preparation of egg-shell meal:
Eggshell is cleaned up first, dries moisture, is placed in electric baking case, the heated-air drying 2 hours under the conditions of 200 DEG C,
After taking-up is let cool, 20 mesh coarse powder are pulverized into, by weight 1:0.5 sprays prepared weight ratio on eggshell coarse powder for 25%
Salt solution(That is egg-shell meal:25% salt solution=1:0.5 ratio), mixed in sprinkling, place 6 hours after mixing, then
Uniformly mixing is primary again, then places 6 hours;Impregnated eggshell powder raw material is put into rotary carbonizing pot, in 420 DEG C of backspins
Turn charing 80 minutes, until observing the complete blackening of raw material(Carbonization process prevents charcoal in being equipped with the scraping blade rotated automatically in charing pot
Raw material glues pot and agglomeration during change);The raw material carbonized is rapidly moved in activation furnace, CO is passed through2Gas is caught up with therein to the greatest extent
Air, anoxybiotic activates 80 minutes at 760 DEG C(Controllable stirring is set in activation furnace and stirs blade, is made every in activation raw material
It is stirred within 10 minutes once, guarantees activation material fully and uniformly);After activation, activated material is taken out, is allowed to cool normal
Temperature gradually rinses activated material in rinse bath with clear water, until basic inspection does not measure sodium chloride, has cleaned sodium chloride
Afterwards, it is submerged activated material 2.5 hours with the hydrochloric acid of mass ratio 12%, is finished wait impregnate, with 95 DEG C of pure water washing activated materials, until
Expect that grain filters 7.0 there is no after white, then with room temperature pure water rinse to pH value, obtains rinse activator material;By rinsed clean
Activated material, which is dried at 115 DEG C to water content, is lower than 6%, crosses 60 meshes, and the coarse grain after screening is pulverized again, makes all to pass through
60 meshes are to get charing egg-shell meal product.
Embodiment 3
Carbonize the preparation of egg-shell meal:
Eggshell is cleaned up first, dries moisture, is placed in far-infrared dryer, it is 1 hour dry under the conditions of 300 DEG C, it takes
After letting cool out, 30 mesh coarse powder are pulverized into, by weight 1:0.5 sprays the food that prepared weight ratio is 25% on eggshell coarse powder
Salting liquid(That is egg-shell meal:25% salt solution=1:0.5 ratio), mixed in sprinkling, place 7 hours after mixing, then again
Uniformly mixing is primary, then places 7 hours;Impregnated eggshell powder raw material is put into rotary carbonizing pot, is rotated at 450 DEG C
Charing 70 minutes, until observing the complete blackening of raw material(Carbonization process prevents from carbonizing in being equipped with the scraping blade rotated automatically in charing pot
Raw material glues pot and agglomeration in the process);The raw material carbonized is rapidly moved in activation furnace, CO is passed through2Gas catches up with sky therein to the greatest extent
Gas, anoxybiotic activates 55 minutes at 800 DEG C(Controllable stirring is set in activation furnace and stirs blade, is made in activation raw material every 10
Minute is stirred once, guarantees activation material fully and uniformly);After activation, activated material is taken out, is allowed to cool normal
Temperature gradually rinses activated material in rinse bath with clear water, until basic inspection does not measure sodium chloride, has cleaned sodium chloride
Afterwards, it is submerged activated material 3 hours with the hydrochloric acid of mass ratio 12%, is finished wait impregnate, with 95 DEG C of pure water washing activated materials, until material
Grain filters 7.0 there is no after white, then with room temperature pure water rinse to pH value, obtains rinse activator material;By the work of rinsed clean
Material, which is dried at 120 DEG C to water content, is lower than 6%, crosses 60 meshes, the coarse grain after screening is pulverized again, made all by 60
Mesh is to get charing egg-shell meal product.
Embodiment 4
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 30000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
5g, Rosa roxburghii freeze-dried powder 5g, wintercherry freeze-dried powder 3g, blackcurrant freeze-dried powder 3g, cactus freeze-dried powder 150g, remaining is charing eggshell
Powder;Specific production method be weigh embodiment 1 respectively sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, it is black plus
Logical sequence freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by implementing
After the charing egg-shell meal obtained of example 2 is sufficiently mixed uniformly, composite packaging is carried out;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Embodiment 5
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 50000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
50g, Rosa roxburghii freeze-dried powder 10g, wintercherry freeze-dried powder 5g, blackcurrant freeze-dried powder 5g, cactus freeze-dried powder 85g, remaining is charing eggshell
Powder;Specific production method be weigh embodiment 1 respectively sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, it is black plus
Logical sequence freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by implementing
After the charing egg-shell meal obtained of example 2 is sufficiently mixed uniformly, composite packaging is carried out;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Embodiment 6
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 70000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
15g, Rosa roxburghii freeze-dried powder 50g, wintercherry freeze-dried powder 8g, blackcurrant freeze-dried powder 8g, cactus freeze-dried powder 90g, remaining is charing eggshell
Powder;Specific production method be weigh embodiment 1 respectively sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, it is black plus
Logical sequence freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by implementing
After the charing egg-shell meal obtained of example 2 is sufficiently mixed uniformly, composite packaging is carried out;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Embodiment 7
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 90000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
25g, Rosa roxburghii freeze-dried powder 25g, wintercherry freeze-dried powder 15g, blackcurrant freeze-dried powder 15g, cactus freeze-dried powder 70g, remaining is charing egg
Shell powder;Specific production method is to weigh the sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, black respectively of embodiment 1
Gallon freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by reality
It applies after the charing egg-shell meal obtained of example 2 is sufficiently mixed uniformly, carries out composite packaging;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Embodiment 8
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 150000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
10g, Rosa roxburghii freeze-dried powder 30g, wintercherry freeze-dried powder 15g, blackcurrant freeze-dried powder 15g, cactus freeze-dried powder 75g, remaining is charing egg
Shell powder;Specific production method is to weigh the sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, black respectively of embodiment 1
Gallon freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by reality
It applies after the charing egg-shell meal obtained of example 2 is sufficiently mixed uniformly, carries out composite packaging;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Embodiment 9
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 130000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
40g, Rosa roxburghii freeze-dried powder 25g, wintercherry freeze-dried powder 20g, blackcurrant freeze-dried powder 20g, cactus freeze-dried powder 80g, remaining is charing egg
Shell powder;Specific production method is to weigh the sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, black respectively of embodiment 1
Gallon freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by reality
It applies after the charing egg-shell meal obtained of example 3 is sufficiently mixed uniformly, carries out composite packaging;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Embodiment 10
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 100000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
25g, Rosa roxburghii freeze-dried powder 40g, wintercherry freeze-dried powder 30g, blackcurrant freeze-dried powder 30g, cactus freeze-dried powder 90g, remaining is charing egg
Shell powder;Specific production method is to weigh the sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, black respectively of embodiment 1
Gallon freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by reality
It applies after the charing egg-shell meal obtained of example 3 is sufficiently mixed uniformly, carries out composite packaging;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Embodiment 11
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 110000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
50g, Rosa roxburghii freeze-dried powder 40g, wintercherry freeze-dried powder 15g, blackcurrant freeze-dried powder 15g, cactus freeze-dried powder 80g, remaining is charing egg
Shell powder;Specific production method is to weigh the sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, black respectively of embodiment 1
Gallon freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by reality
It applies after the charing egg-shell meal obtained of example 3 is sufficiently mixed uniformly, carries out composite packaging;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Embodiment 12
A kind of diacetyl streptococcus lactis feed addictive is frozen by diacetyl streptococcus lactis dry powder, sea-buckthorn freeze-dried powder, Rosa roxburghii Tratt
Dry powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing egg-shell meal mixing of surplus
Uniformly, composite packaging is made:Diacetyl streptococcus lactis 120000 hundred million, sea-buckthorn freeze-dried powder in every 1000g feed addictive
50g, Rosa roxburghii freeze-dried powder 50g, wintercherry freeze-dried powder 10g, blackcurrant freeze-dried powder 10g, cactus freeze-dried powder 100g, remaining is charing egg
Shell powder;Specific production method is to weigh the sea-buckthorn freeze-dried powder obtained, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, black respectively of embodiment 1
Gallon freeze-dried powder, cactus freeze-dried powder mix, then diacetyl streptococcus lactis dry powder are uniformly admixed, and then add surplus by reality
It applies after the charing egg-shell meal obtained of example 3 is sufficiently mixed uniformly, carries out composite packaging;Composite packaging is inner bag using polypropylene plastics
Bag, outer bag use aluminium foil bag, add a few packet silica-gel desiccants between interior outer bag, to prevent water suction.
Claims (9)
1. diacetyl streptococcus lactis feed addictive, feature it be to be frozen first by diacetyl streptococcus lactis, sea-buckthorn
Dry powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing of surplus
Egg-shell meal is uniformly mixed, and composite packaging is made:The diacetyl streptococcus lactis 30000 hundred million-in every 1000g feed addictive
150000 hundred million, sea-buckthorn freeze-dried powder 5-50g, Rosa roxburghii freeze-dried powder 5-50g, wintercherry freeze-dried powder 3-30g, blackcurrant freeze-dried powder 3-30g,
Cactus freeze-dried powder 50-150g, remaining is charing egg-shell meal;The sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder,
Blackcurrant freeze-dried powder, cactus freeze-dried powder, are made by following methods, and technical process is to take fresh sea-buckthorn, Rosa roxburghii Tratt, acid respectively
Slurry, blackcurrant, cactus remove carpopodium, the impurity such as rotten fruit, and rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, deseeding
Step;Rinsing condition described above is the citric acid that weight 0.1% is added with 40 DEG C of water, rinses 15min, and be stirred continuously,
It pulls out to be put into pure water and rinse 3 times;Above-mentioned freezing is respectively will be fast after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot
Speed is cooled to -45 DEG C or less;The process conditions of above-mentioned lyophilization are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is done
It is dry to moisture be less than 6%/w until;The charing egg-shell meal is made by following methods:(1)Dry, dipping is first by egg
Shell cleans up, and dries moisture, is dried 1-2 hours in advance, then pulverizes into 20-30 mesh coarse powder, by weight 1:0.5
The salt that prepared weight fraction is 25% is sprayed on eggshell coarse powder(Sodium chloride)Solution is mixed in sprinkling, is put after mixing
It sets 6-7 hours, then uniformly mixing is primary again, then places 6-7 hours;The purpose is to allow salt effectively to penetrate into eggshell tissue
In internal voids;(2)Charing impregnated eggshell powder raw material is put into rotary carbonizing pot, 420-450 DEG C at a temperature of
Rotation charing 70-80 minutes, until observing the complete blackening of raw material;(3)The raw material carbonized is rapidly moved to activation furnace by activation
In, fire door is closed, carbon dioxide gas is passed through, catches up with air therein to the greatest extent, anoxybiotic activates 55-85 minutes at 720-800 DEG C;
(4)After activated material is taken out in cleaning, it is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, until basic
Until inspection does not measure sodium chloride;After having cleaned sodium chloride, submerged activated material 2.5-3 hours with the hydrochloric acid that mass ratio is 12%, to
After immersion, with 95 DEG C of pure water washing activated materials, until material grain is there is no after white, then with room temperature pure water rinse into
Property, filtering obtains rinse activator material;(5)Dry and screening dries the activated material of rinsed clean at 115-120 DEG C to aqueous
Amount is lower than 6%/w, crosses 60 meshes, and the coarse grain after screening pulverized again, make all by 60 meshes to get.
2. diacetyl streptococcus lactis feed addictive, feature it be first by diacetyl streptococcus lactis, sea-buckthorn freeze-dried powder,
Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing eggshell of surplus
Powder is uniformly mixed, and composite packaging is made:Diacetyl streptococcus lactis 50000 hundred million -150000 in every 1000g feed addictive
A hundred million, sea-buckthorn freeze-dried powder 10-50g, Rosa roxburghii freeze-dried powder 10-50g, wintercherry freeze-dried powder 5-30g, blackcurrant freeze-dried powder 5-30g, celestial being
Freeze-dried powder 70-150g is slapped, remaining is charing egg-shell meal;The sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, it is black plus
Logical sequence freeze-dried powder, cactus freeze-dried powder, are made by following methods, technical process be take respectively fresh sea-buckthorn, Rosa roxburghii Tratt, wintercherry,
Blackcurrant, cactus remove carpopodium, the impurity such as rotten fruit, and rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, deseeding step
Suddenly;Rinsing condition described above is the citric acid that weight 0.1% is added with 40 DEG C of water, rinses 15min, and be stirred continuously, and is fished out
It is put into pure water and rinses 3 times out;Above-mentioned freezing is respectively will be rapid after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot
It is cooled to -45 DEG C or less;The process conditions of above-mentioned lyophilization are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is dry
Until moisture is less than 6%/w;The charing egg-shell meal is made by following methods:(1)Dry, dipping is first by eggshell
It cleans up, dries moisture, be dried 1-2 hours in advance, then pulverize into 20-30 mesh coarse powder, by weight 1:0.5 in egg
The salt that prepared weight fraction is 25% is sprayed on shell coarse powder(Sodium chloride)Solution is mixed in sprinkling, is placed after mixing
6-7 hours, then uniformly mixing was primary again, then places 6-7 hours;The purpose is to allow salt effectively to penetrate into eggshell tissue
In portion gap;(2)Impregnated eggshell powder raw material is put into rotary carbonizing pot by charing, in 420-450 DEG C of temperature backspin
Turn charing 70-80 minutes, until observing the complete blackening of raw material;(3)The raw material carbonized is rapidly moved in activation furnace by activation,
Fire door is closed, carbon dioxide gas is passed through, catches up with air therein to the greatest extent, anoxybiotic activates 55-85 minutes at 720-800 DEG C;(4)Clearly
It washes after taking out activated material, is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, until detecting substantially
Until not going out sodium chloride;After having cleaned sodium chloride, submerged activated material 2.5-3 hours with the hydrochloric acid that mass ratio is 12%, wait impregnate
After, with 95 DEG C of pure water washing activated materials, until material grain is there is no after white, then with room temperature pure water rinse to neutrality,
Filtering, obtains rinse activator material;(5)By the activated material of rinsed clean, the drying at 115-120 DEG C is low to water content for dry and screening
In 6%/w, cross 60 meshes, the coarse grain after screening is pulverized again, make all by 60 meshes to get.
3. diacetyl streptococcus lactis feed addictive, feature it be first by diacetyl streptococcus lactis, sea-buckthorn freeze-dried powder,
Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing eggshell of surplus
Powder is uniformly mixed, and composite packaging is made:Diacetyl streptococcus lactis 70000 hundred million -150000 in every 1000g feed addictive
A hundred million, sea-buckthorn freeze-dried powder 15-50g, Rosa roxburghii freeze-dried powder 15-50g, wintercherry freeze-dried powder 8-30g, blackcurrant freeze-dried powder 8-30g, celestial being
Freeze-dried powder 85-150g is slapped, remaining is charing egg-shell meal;The sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, it is black plus
Logical sequence freeze-dried powder, cactus freeze-dried powder, are made by following methods, technical process be take respectively fresh sea-buckthorn, Rosa roxburghii Tratt, wintercherry,
Blackcurrant, cactus remove carpopodium, the impurity such as rotten fruit, and rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, deseeding step
Suddenly;Rinsing condition described above is the citric acid that weight 0.1% is added with 40 DEG C of water, rinses 15min, and be stirred continuously, and is fished out
It is put into pure water and rinses 3 times out;Above-mentioned freezing is respectively will be rapid after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot
It is cooled to -45 DEG C or less;The process conditions of above-mentioned lyophilization are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is dry
Until moisture is less than 6%/w;The charing egg-shell meal is made by following methods:(1)Dry, dipping is first by eggshell
It cleans up, dries moisture, be dried 1-2 hours in advance, then pulverize into 20-30 mesh coarse powder, by weight 1:0.5 in egg
The salt that prepared weight fraction is 25% is sprayed on shell coarse powder(Sodium chloride)Solution is mixed in sprinkling, is placed after mixing
6-7 hours, then uniformly mixing was primary again, then places 6-7 hours;The purpose is to allow salt effectively to penetrate into eggshell tissue
In portion gap;(2)Impregnated eggshell powder raw material is put into rotary carbonizing pot by charing, in 420-450 DEG C of temperature backspin
Turn charing 70-80 minutes, until observing the complete blackening of raw material;(3)The raw material carbonized is rapidly moved in activation furnace by activation,
Fire door is closed, carbon dioxide gas is passed through, catches up with air therein to the greatest extent, anoxybiotic activates 55-85 minutes at 720-800 DEG C;(4)Clearly
It washes after taking out activated material, is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, until detecting substantially
Until not going out sodium chloride;After having cleaned sodium chloride, submerged activated material 2.5-3 hours with the hydrochloric acid that mass ratio is 12%, wait impregnate
After, with 95 DEG C of pure water washing activated materials, until material grain is there is no after white, then with room temperature pure water rinse to neutrality,
Filtering, obtains rinse activator material;(5)By the activated material of rinsed clean, the drying at 115-120 DEG C is low to water content for dry and screening
In 6%/w, cross 60 meshes, the coarse grain after screening is pulverized again, make all by 60 meshes to get.
4. diacetyl streptococcus lactis feed addictive, feature it be first by diacetyl streptococcus lactis, sea-buckthorn freeze-dried powder,
Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, blackcurrant freeze-dried powder, cactus freeze-dried powder are uniformly mixed, then add the charing eggshell of surplus
Powder is uniformly mixed, and composite packaging is made:Diacetyl streptococcus lactis 90000 hundred million -150000 in every 1000g feed addictive
A hundred million, sea-buckthorn freeze-dried powder 20-50g, Rosa roxburghii freeze-dried powder 20-50g, wintercherry freeze-dried powder 10-30g, blackcurrant freeze-dried powder 10-30g, celestial being
People slaps freeze-dried powder 100-150g, remaining is charing egg-shell meal;It is the sea-buckthorn freeze-dried powder, Rosa roxburghii freeze-dried powder, wintercherry freeze-dried powder, black
Gallon freeze-dried powder, cactus freeze-dried powder, are made by following methods, and technical process is to take fresh sea-buckthorn, Rosa roxburghii Tratt, acid respectively
Slurry, blackcurrant, cactus remove carpopodium, the impurity such as rotten fruit, and rinsing, freezing, lyophilization, low-temperature grinding are not removed the peel, deseeding
Step;Rinsing condition described above is the citric acid that weight 0.1% is added with 40 DEG C of water, rinses 15min, and be stirred continuously,
It pulls out to be put into pure water and rinse 3 times;Above-mentioned freezing is respectively will be fast after sea-buckthorn, Rosa roxburghii Tratt, wintercherry, blackcurrant, cactus sabot
Speed is cooled to -45 DEG C or less;The process conditions of above-mentioned lyophilization are temperature-22-- 32 DEG C, and vacuum degree 120-150Pa is done
It is dry to moisture be less than 6%/w until;The charing egg-shell meal is made by following methods:(1)Dry, dipping is first by egg
Shell cleans up, and dries moisture, is dried 1-2 hours in advance, then pulverizes into 20-30 mesh coarse powder, by weight 1:0.5
The salt that prepared weight fraction is 25% is sprayed on eggshell coarse powder(Sodium chloride)Solution is mixed in sprinkling, is put after mixing
It sets 6-7 hours, then uniformly mixing is primary again, then places 6-7 hours;The purpose is to allow salt effectively to penetrate into eggshell tissue
In internal voids;(2)Charing impregnated eggshell powder raw material is put into rotary carbonizing pot, 420-450 DEG C at a temperature of
Rotation charing 70-80 minutes, until observing the complete blackening of raw material;(3)The raw material carbonized is rapidly moved to activation furnace by activation
In, fire door is closed, carbon dioxide gas is passed through, catches up with air therein to the greatest extent, anoxybiotic activates 55-85 minutes at 720-800 DEG C;
(4)After activated material is taken out in cleaning, it is allowed to cool room temperature, activated material is gradually rinsed in rinse bath with clear water, until basic
Until inspection does not measure sodium chloride;After having cleaned sodium chloride, submerged activated material 2.5-3 hours with the hydrochloric acid that mass ratio is 12%, to
After immersion, with 95 DEG C of pure water washing activated materials, until material grain is there is no after white, then with room temperature pure water rinse into
Property, filtering obtains rinse activator material;(5)Dry and screening dries the activated material of rinsed clean at 115-120 DEG C to aqueous
Amount is lower than 6%/w, crosses 60 meshes, and the coarse grain after screening pulverized again, make all by 60 meshes to get.
5. the diacetyl streptococcus lactis feed addictive as described in claim 1-4, which is characterized in that the diacetyl cream
The thalli dry powder product that acid streptococci is every gram of viable bacteria concentration no less than 250 hundred million.
6. the diacetyl streptococcus lactis feed addictive as described in claim 1-4, which is characterized in that the low-temperature grinding
It is that temperature of charge is crushed in 0 DEG C or less.
7. the diacetyl streptococcus lactis feed addictive as described in claim 1-4, which is characterized in that the composite packaging
Using interior outer bag composite packaging, inner bag uses polypropylene plastics pocket, and outer packing uses aluminium foil bag, is filled with silica gel between interior outer bag
Desiccant pouch.
8. the diacetyl streptococcus lactis feed addictive as described in claim 1-4, which is characterized in that the eggshell is chicken
Any one or a few mixing eggshell in eggshell, Ovum Anas domestica putamina, goose egg-shell and quail eggshell.
9. the diacetyl streptococcus lactis feed addictive as described in claim 1-4, which is characterized in that the dry use
Heated-air drying or far-infrared ray drying;The drying condition is 180 DEG C -300 DEG C.
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CN201810512101.5A CN108850526A (en) | 2018-05-25 | 2018-05-25 | Diacetyl streptococcus lactis feed addictive |
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Application Number | Priority Date | Filing Date | Title |
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CN201810512101.5A CN108850526A (en) | 2018-05-25 | 2018-05-25 | Diacetyl streptococcus lactis feed addictive |
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CN108850526A true CN108850526A (en) | 2018-11-23 |
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2018
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Application publication date: 20181123 |