CN108467784A - A kind of concentrated type chrysanthemum aromatic particulate and preparation method thereof - Google Patents
A kind of concentrated type chrysanthemum aromatic particulate and preparation method thereof Download PDFInfo
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- CN108467784A CN108467784A CN201810280470.6A CN201810280470A CN108467784A CN 108467784 A CN108467784 A CN 108467784A CN 201810280470 A CN201810280470 A CN 201810280470A CN 108467784 A CN108467784 A CN 108467784A
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- chrysanthemum
- powder
- straws
- bar
- concentrated type
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The invention discloses a kind of concentrated type chrysanthemum aromatic particulates and preparation method thereof, concentrated type chrysanthemum aromatic particulate per 1kg includes the chrysanthemum essential oil of the chrysanthemum bar essence dew of 1kg, the tealeaves bar powder of the medicinal powder of 0.125kg, 0.125kg, the chrysanthemum bar powder of 1.5kg, 0.00003kg, chrysanthemum bar essence dew wherein per 1kg needs to display middle extraction for the first time from the chrysanthemum bar of 1.5kg, it displays needs for the first time per 1kg chrysanthemum bars to extract from the chrysanthemum bar of 15kg, the chrysanthemum essential oil needs per 1kg are extracted from the chrysanthemum of 1000kg.The present invention can effectively solve the problem that existing chrysanthemum aromatic particulate only takes full advantage of chrysanthemum, and not utilize chrysanthemum straws, and the problem of result in waste of resources and be unable to get chrysanthemum straws effect.
Description
Technical field
The present invention relates to a kind of concentrated type chrysanthemum aromatic particulates and preparation method thereof.
Background technology
Chrysanthemum is perennial catananche, and capitulum is that medicine food as defined in conventional Chinese medicine and the Ministry of Public Health is simultaneous
With plant, there is the effect of dispelling wind, heat-clearing, improving eyesight, removing toxic substances.Primary treatment headache, hot eyes, ambition dysphoria with smothery sensation, furunculosis, is swollen at dizziness
The diseases such as poison.Modern pharmacological studies have shown that chrysanthemum has treatment coronary heart disease, reduces blood pressure, prevent hyperlipidemia, is antibacterial, antiviral, anti-
A variety of pharmacological activity such as inflammation, anti-aging.Classify both at home and abroad to it, identify, chemistry, clinical, pharmacology etc. have been reported that.Research
It was found that the chemical composition of chrysanthemum is more complicated, wherein flavone compound, triterpene compound and volatile oil are that it is main effective
Ingredient.Studies have shown that chrysanthemum essential oil can enhance capillary resistance, metabolism of lipid and cholesterol content in blood is reduced, is had
Improve myocardial nutrition, anti-inflammatory, scavenging capacity oxygen radical effect;To inhibition tumour, slows down aging and enhance human immunity
There is certain effect.
Contain chlorogenic acid in chrysanthemum straws, chlorogenic acid is that acid is poured a libation in a kind of contracting, and category pours a libation class compound, is plant in aerobic respiration
In the process, a kind of phenylpropanoids formed through shikimic acid pathway.Chlorogenic acid is a kind of important physiological activator, tool
There is antibacterial, antiviral, increasing leukocyte, hepatic cholagogic, antitumor, lowering blood pressure and blood fat, remove the effects that free radical.It is wide
It is general to be present in many plants, in sunflower seeds (benevolence, cypress), water fruits and vegetables, soybean, wheat, cocoa bean, coffee bean, especially certain herbaceous plants with big flowers
Flower seed, cocoa bean, coffee bean, fructus hippophae and Chinese traditional herbs, as its content is higher in honeysuckle, Cortex Eucommiae.It is many medicinal materials
One of with the principle active component of Chinese patent drug, how much chlorogenic acid content is again the quality index of certain patent medicine and much fruit juice
One of drink health-care ingredient.The annual chrysanthemum harvest season has a large amount of straws to discard field, as can be used, can become give up into
Treasured reduces pollution of the straw burning to environment.
Chrysanthemum aromatic particulate is usually used in medicine-filled pillow filling, and existing common chrysanthemum aromatic particulate on the market is with Chrysanthemum Petal essence
Aromatic particulate made of oil, the non-core of hydrosol, and the example for not thering are chrysanthemum straws to be used to prepare medicine-filled pillow filling aromatic particulate.
Invention content
The object of the present invention is to provide a kind of concentrated type chrysanthemum aromatic particulates and preparation method thereof, solve existing chrysanthemum virtue
Fragrant particle only takes full advantage of chrysanthemum, and does not utilize chrysanthemum straws, and results in waste of resources and be unable to get chrysanthemum straws effect
The problem of.
The technical solution adopted by the present invention to solve the technical problems is:A kind of concentrated type chrysanthemum aromatic particulate, per 1kg
Concentrated type chrysanthemum aromatic particulate include the chrysanthemum bar essence dew of 1kg, the medicinal powder of 0.125kg, 0.125kg tealeaves bar powder,
The chrysanthemum bar powder of 1.5kg, the chrysanthemum essential oil of 0.00003kg, wherein the chrysanthemum bar essence dew per 1kg needs the chrysanthemum from 1.5kg
Bar displays middle extraction for the first time, displays needs for the first time per 1kg chrysanthemum bars and is extracted from the chrysanthemum bar of 15kg, the chrysanthemum essential oil per 1kg needs certainly
It is extracted in the chrysanthemum of 1000kg.
Further, the medicinal powder is tuber of multiflower knotweed powder, raspberry powder, wormwood powder, does the mixed of lavender powder
Close object.
Further, the medicinal powder is the mixing of Rhizoma Chuanxiong, Rhizoma Gastrodiae, peppermint, windproof, purple perilla, the root of Dahurain angelica, Fineleaf Schizonepeta Herb
Object.
A kind of preparation method of concentrated type chrysanthemum aromatic particulate, includes the following steps:
Step (1) harvesting screening:After chrysanthemum picking, chrysanthemum straws are gathered in, its root 18- upward from native 3-4cm is intercepted
The parts 20cm are extraction section, and interception extraction section is partly milling section upwards;
Step (2) is milled:Dried after the milling section of interception is cleaned up, until after its moisture content is down to 8% or less, send to
The chrysanthemum straws powder of 300 mesh is sterilized and is ground into through pulverizer in ozone chamber;
Step (3) extracts:Step (1) described extraction section is sent to essential oil, hydrosol, stalk slag may be implemented and is automatically separated
In essential oil distillation still, essential oil distillation still is heated using steam, and the ratio of extraction section and water is 1:1, cooling water temperature is controlled 35
DEG C, entire distillation process is divided into two stages being carried out continuously, and first stage distillation is to extract based on chrysanthemum straws essential oil, and the
Two-stage distillation is to extract based on chrysanthemum straws hydrosol;
Step (4) pill:Chrysanthemum straws powder, chrysanthemum straws essential oil, chrysanthemum straws hydrosol, chrysanthemum essential oil, chrysanthemum is pure
Dew, dry chrysanthemum petal, dry lavender, the tuber of multiflower knotweed, raspberry, tealeaves, wormwood are prepared after being mixed according to specific ratio with pellet processing machine
At chrysanthemum aromatic particulate;
Step (5) polishing packaging:Chrysanthemum aromatic particulate is polished smooth and packed in gnotobasis.
The preparation method of concentrated type chrysanthemum aromatic particulate according to claim 2, it is characterised in that:In step (1)
The harvesting selection cloudy morning or fine day 9 of the chrysanthemum for chrysanthemum straws in Huangshan Gongju either Mount Huang mother chrysanthemum step (1)
Before point, the same day completes extraction section after harvesting interception and the extraction described in step (3).
Further, in step (3) described extraction process, after chrysanthemum straws essential oil and chrysanthemum straws hydrosol extract,
It is acquired in the holding vessel for being stored in and being provided with automatic washing and sterilizing device;Extraction and acquisition are in 100,000 grades of aseptic rooms
It completes.
Further, in step (3) extraction, stalk slag of the chrysanthemum straws after distillation is subjected to slag by dehydration device
Liquid detaches, and the stalk liquid isolated filters feeding enrichment facility with filter device and is condensed into chrysanthemum straws liquid magma, and is packaged into
Freezer stores, and the moisture evaporated in concentration process stores for future use after being collected by condensing unit;The fibre composition separated with
Stalk slag is sent into drying equipment and is dried, and send to air flow crushing device and crushes after dry, and freezer storage is packaged into after crushing
It deposits.
Further, enrichment facility selects continuous vacuum Low-temperature concentration device;Drying equipment selects tunnel type micro wave dry
Dry equipment.
In order to improve quality and the safety of product, the system of concentrated type chrysanthemum aromatic particulate according to claim 2
Preparation Method, it is characterised in that:Step (3) extraction, step (4) pill, step (5) rounding packaging carry out in desinfection chamber.
Beneficial effects of the present invention:This concentrated type chrysanthemum aromatic particulate takes full advantage of chrysanthemum straws, is turned waste into wealth,
Pollution of the straw burning to environment is reduced, while this chrysanthemum aromatic particulate is also equipped with the healthcare function effect for having chrysanthemum straws,
It thoroughly solves existing chrysanthemum aromatic particulate and only takes full advantage of chrysanthemum, and do not utilize chrysanthemum straws, and result in waste of resources
And the problem of being unable to get chrysanthemum straws effect.Meanwhile the preparation method of this concentrated type chrysanthemum aromatic particulate makes full use of chrysanthemum
Stalk is applied not only to extraction essential oil, hydrosol, is also fully utilized by chrysanthemum straws powder, at the same to extraction essential oil, hydrosol during
The chrysanthemum straws slag separated has also been made adequately processing and utilizes, and improves the utilization rate of resource.
Below with reference to embodiment, the present invention is described in detail.
Specific implementation mode
Embodiment, a kind of concentrated type chrysanthemum aromatic particulate, the concentrated type chrysanthemum aromatic particulate per 1kg include the chrysanthemum of 1kg
The chrysanthemum of bar essence dew, the tealeaves bar powder of the medicinal powder of 0.125kg, 0.125kg, the chrysanthemum bar powder of 1.5kg, 0.00003kg
Flower essential oil, wherein the chrysanthemum bar essence dew per 1kg needs to display middle extraction for the first time from the chrysanthemum bar of 1.5kg, being displayed for the first time per 1kg chrysanthemum bars needs
It to be extracted from the chrysanthemum bar of 15kg, the chrysanthemum essential oil needs per 1kg are extracted from the chrysanthemum of 1000kg.
Further, the medicinal powder is tuber of multiflower knotweed powder, raspberry powder, wormwood powder, does the mixed of lavender powder
Close object.
Further, the medicinal powder is the mixing of Rhizoma Chuanxiong, Rhizoma Gastrodiae, peppermint, windproof, purple perilla, the root of Dahurain angelica, Fineleaf Schizonepeta Herb
Object.
A kind of preparation method of concentrated type chrysanthemum aromatic particulate, includes the following steps:
Step (1) harvesting screening:After chrysanthemum picking, chrysanthemum straws are gathered in, its root 18- upward from native 3-4cm is intercepted
The parts 20cm are extraction section, and interception extraction section is partly milling section upwards;
Step (2) is milled:Dried after the milling section of interception is cleaned up, until after its moisture content is down to 8% or less, send to
The chrysanthemum straws powder of 300 mesh is sterilized and is ground into through pulverizer in ozone chamber;
Step (3) extracts:Step (1) described extraction section is sent to essential oil, hydrosol, stalk slag may be implemented and is automatically separated
In essential oil distillation still, essential oil distillation still is heated using steam, and the ratio of extraction section and water is 1:1, cooling water temperature is controlled 35
DEG C, entire distillation process is divided into two stages being carried out continuously, and first stage distillation is to extract based on chrysanthemum straws essential oil, and the
Two-stage distillation is to extract based on chrysanthemum straws hydrosol;
Step (4) pill:Chrysanthemum straws powder, chrysanthemum straws essential oil, chrysanthemum straws hydrosol, chrysanthemum essential oil, chrysanthemum is pure
Dew, dry chrysanthemum petal, dry lavender, the tuber of multiflower knotweed, raspberry, tealeaves, wormwood are prepared after being mixed according to specific ratio with pellet processing machine
At chrysanthemum aromatic particulate;
Step (5) polishing packaging:Chrysanthemum aromatic particulate is polished smooth and packed in gnotobasis.
Chrysanthemum described in step (1) is Huangshan Gongju or Mount Huang mother chrysanthemum, the harvesting selection of chrysanthemum straws in step (1)
Before 9 points of the cloudy morning or fine day, the same day completes extraction section after harvesting interception and the extraction described in step (3).
In step (3) described extraction process, after chrysanthemum straws essential oil and chrysanthemum straws hydrosol extract, is acquired and deposited
Storage is in the holding vessel for being provided with automatic washing and sterilizing device;Extraction and acquisition are completed in 100,000 grades of aseptic rooms.
In step (3) extraction, stalk slag of the chrysanthemum straws after distillation is subjected to slag-liquid separation by dehydration device, point
The stalk liquid separated out filters feeding enrichment facility with filter device and is condensed into chrysanthemum straws liquid magma, and is packaged into freezer storage,
The moisture evaporated in concentration process stores for future use after being collected by condensing unit;The fibre composition separated is sent into stalk slag
Drying equipment is dried, and send to air flow crushing device and crushes after dry, and freezer storage is packaged into after crushing.
Enrichment facility selects continuous vacuum Low-temperature concentration device;Drying equipment selects tunnel type micro wave drying equipment.
The preparation method of concentrated type chrysanthemum aromatic particulate according to claim 2, it is characterised in that:Step (3) extracts
It takes, step (4) pill, step (5) rounding packaging carry out in desinfection chamber.
It is that the present invention is exemplarily described above.Obviously, present invention specific implementation is not limited by aforesaid way
System.As long as using the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress;Or it is not improved,
The above-mentioned design of the present invention and technical solution are directly applied into other occasions, within protection scope of the present invention.
Claims (9)
1. a kind of concentrated type chrysanthemum aromatic particulate, it is characterised in that:Concentrated type chrysanthemum aromatic particulate per 1kg includes the chrysanthemum of 1kg
Line rod essence dew, the tealeaves bar powder of the medicinal powder of 0.125kg, 0.125kg, the chrysanthemum bar powder of 1.5kg, 0.00003kg
Chrysanthemum essential oil, wherein the chrysanthemum bar essence dew per 1kg needs to display middle extraction for the first time from the chrysanthemum bar of 1.5kg, being displayed for the first time per 1kg chrysanthemum bars needs
It to be extracted from the chrysanthemum bar of 15kg, the chrysanthemum essential oil needs per 1kg are extracted from the chrysanthemum of 1000kg.
2. concentrated type chrysanthemum aromatic particulate according to claim 1, it is characterised in that:The medicinal powder is radix polygoni multiflori powder
End, raspberry powder, wormwood powder, the mixture for doing lavender powder.
3. concentrated type chrysanthemum aromatic particulate according to claim 1, it is characterised in that:The medicinal powder is Rhizoma Chuanxiong, day
Fiber crops, peppermint, windproof, purple perilla, the root of Dahurain angelica, Fineleaf Schizonepeta Herb mixture.
4. a kind of preparation method of concentrated type chrysanthemum aromatic particulate, it is characterised in that:Include the following steps:
Step (1) harvesting screening:After chrysanthemum picking, chrysanthemum straws are gathered in, its root portions 18-20cm upward from native 3-4cm are intercepted
It is divided into extraction section, interception extraction section is partly milling section upwards;
Step (2) is milled:It dries after the milling section of interception is cleaned up, until after its moisture content is down to 8% or less, send to ozone
Indoor disinfection and the chrysanthemum straws powder that 300 mesh are ground into through pulverizer;
Step (3) extracts:Step (1) described extraction section is sent to the essential oil for essential oil, hydrosol, stalk slag may be implemented being automatically separated
In distillation still, essential oil distillation still is heated using steam, and the ratio of extraction section and water is 1:1, cooling water temperature is controlled at 35 DEG C, whole
A distillation process is divided into two stages being carried out continuously, and first stage distillation is to extract based on chrysanthemum straws essential oil, second-order
Section distillation is to extract based on chrysanthemum straws hydrosol;
Step (4) pill:By chrysanthemum bar essence dew, tuber of multiflower knotweed powder, raspberry powder, wormwood powder, dry lavender powder, tealeaves bar
Powder, chrysanthemum bar powder, chrysanthemum essential oil are prepared into chrysanthemum aromatic particulate according to after the mixing of specific ratio with pellet processing machine;
Step (5) polishing packaging:Chrysanthemum aromatic particulate is polished smooth and packed in gnotobasis.
5. the preparation method of concentrated type chrysanthemum aromatic particulate according to claim 4, it is characterised in that:Institute in step (1)
The harvesting selection cloudy morning or fine day 9 point of the chrysanthemum stated for chrysanthemum straws in Huangshan Gongju either Mount Huang mother chrysanthemum step (1)
Before, the interception and the extraction described in step (3) that the same day completes extraction section after harvesting.
6. the preparation method of concentrated type chrysanthemum aromatic particulate according to claim 4, it is characterised in that:Step (3) is described
In extraction process, after chrysanthemum straws essential oil and chrysanthemum straws hydrosol extract, is acquired to be stored in and be provided with automatic cleaning
In the holding vessel of bactericidal unit;Extraction and acquisition are completed in 100,000 grades of aseptic rooms.
7. the preparation method of the concentrated type chrysanthemum aromatic particulate according to claim 4 or 6, it is characterised in that:Step (3) extracts
In taking, stalk slag of the chrysanthemum straws after distillation is subjected to slag-liquid separation by dehydration device, the stalk liquid isolated is used
Filter device filtering is sent into enrichment facility and is condensed into chrysanthemum straws liquid magma, and is packaged into freezer storage, is evaporated in concentration process
Moisture stores for future use after being collected by condensing unit;The fibre composition separated is sent into drying equipment with stalk slag and is done
It is dry, it send to air flow crushing device and crushes after dry, freezer storage is packaged into after crushing.
8. the preparation method of concentrated type chrysanthemum aromatic particulate according to claim 7, it is characterised in that:Enrichment facility is selected
Continuous vacuum Low-temperature concentration device;Drying equipment selects tunnel type micro wave drying equipment.
9. the preparation method of concentrated type chrysanthemum aromatic particulate according to claim 4, it is characterised in that:Step (3) extraction,
Step (4) pill, step (5) rounding packaging carry out in desinfection chamber.
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CN201810280470.6A CN108467784A (en) | 2018-04-02 | 2018-04-02 | A kind of concentrated type chrysanthemum aromatic particulate and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109379664A (en) * | 2018-09-29 | 2019-02-22 | 钟贵富 | Fragrance ball preparation method and the magnetic suspension sound box device for using the fragrance ball |
-
2018
- 2018-04-02 CN CN201810280470.6A patent/CN108467784A/en not_active Withdrawn
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109379664A (en) * | 2018-09-29 | 2019-02-22 | 钟贵富 | Fragrance ball preparation method and the magnetic suspension sound box device for using the fragrance ball |
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Application publication date: 20180831 |