CN108464442A - A kind of preparation method of the natural selenium-rich food of cytotrophy - Google Patents
A kind of preparation method of the natural selenium-rich food of cytotrophy Download PDFInfo
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- CN108464442A CN108464442A CN201810205429.2A CN201810205429A CN108464442A CN 108464442 A CN108464442 A CN 108464442A CN 201810205429 A CN201810205429 A CN 201810205429A CN 108464442 A CN108464442 A CN 108464442A
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- selenium
- parts
- cytotrophy
- corn
- natural
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- 239000011669 selenium Substances 0.000 title claims abstract description 268
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 title claims abstract description 227
- 229910052711 selenium Inorganic materials 0.000 title claims abstract description 215
- 235000013305 food Nutrition 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 36
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- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 claims description 47
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- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 claims description 23
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/161—Puffed cereals, e.g. popcorn or puffed rice
- A23L7/165—Preparation of puffed cereals involving preparation of meal or dough as an intermediate step
- A23L7/17—Preparation of puffed cereals involving preparation of meal or dough as an intermediate step by extrusion
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01B—SOIL WORKING IN AGRICULTURE OR FORESTRY; PARTS, DETAILS, OR ACCESSORIES OF AGRICULTURAL MACHINES OR IMPLEMENTS, IN GENERAL
- A01B79/00—Methods for working soil
- A01B79/02—Methods for working soil combined with other agricultural processing, e.g. fertilising, planting
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G22/00—Cultivation of specific crops or plants not otherwise provided for
- A01G22/20—Cereals
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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Abstract
The present invention provides a kind of preparation methods of the natural selenium-rich food of cytotrophy, including:Prepare nanometer selenium plant nutrient;Using nanometer selenium plant nutrient conditioned soil soil;Non-transgenic corn is planted, is applied fertilizer according to default dose in default fertilization time section, and is watered 12 times;It is harvested to get to High-Se corn after maturation;It takes High-Se corn to carry out Physical Processing, obtains the natural selenium-rich food of cytotrophy.Utilize the selenium-enriched food prepared by the preparation method in the present invention, for pure natural healthy selenium-rich organic food, the selenium-enriched food of cytotrophy is easier directly to be absorbed by gastrointestinal tract rapidly after human body intake, improve bioavilability, and due to being natural organic food, other artificial synthesized drugs need not be taken in during selenium-supply or the virose inorganic food of tool, hidden danger without any side effects exist, and use is more safe and reliable.
Description
Technical field
The invention belongs to a kind of preparation sides of the natural selenium-rich food of selenium-enriched food technical field more particularly to cytotrophy
Method.
Background technology
Selenium is the essential trace elements of the human body.Selenium participates in a variety of selenoenzymes and Selenonic protein in synthesized human.Wherein paddy Guang
Sweet peptide peroxidase is catalyzed hydroperoxides in vivo or lipid peroxide is changed into water or various alcohols, eliminates
Attack of the free radical to biomembrane, protects biomembrane from oxidative damage;Selenium participates in constituting the de- iodine enzyme of iodate thyroid gland amino acid.
Cytotrophy selenium-enriched food is made of being compounded by raw materials such as a variety of inorganic sodium selenites.Currently, existing on the market
Some selenium-enriched foods are used for the intake of cytotrophy selenium.
Although the food for being turned on selenium-rich banner on domestic market has very much, on the one hand, cytotrophy selenium-enriched food is more
For inorganic nutraceutical, the bad direct absorption of human body, the inorganic nutraceutical in other part is more toxic, has centainly to body
Side effect.
Invention content
To solve the above problems, the present invention provides a kind of preparation method of the natural selenium-rich food of cytotrophy, including:
Prepare nanometer selenium plant nutrient;
Using nanometer selenium plant nutrient conditioned soil soil;
Non-transgenic corn is planted, is applied fertilizer according to default dose in default fertilization time section, and the 1-2 that waters
It is secondary;It is harvested to get to High-Se corn after maturation;
It takes High-Se corn to carry out Physical Processing, obtains the natural selenium-rich food of cytotrophy.
Preferably, described " using nanometer selenium plant nutrient conditioned soil soil " includes:
10-30 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The nanometer selenium plant nutrient
Se content be 1000-5000 mgs/kg.
Preferably, the nanometer selenium plant nutrient includes the component of following parts by weight:
10-50 parts of selenate;
5000-20000 parts of humic acid;
5000-20000 parts of organic fertilizer;
50-100 parts of zinc fertilizer.
Preferably, the nanometer selenium plant nutrient further includes the component of following parts by weight:
20-50 parts of fulvic acid selenium;
10-75 parts of selenomethionine.
Preferably, the nanometer selenium plant nutrient further includes the component of following parts by weight:
8-55 parts of selenizing polysaccharide.
Preferably, described " preparing nanometer selenium plant nutrient " includes:
Fulvic acid selenium, selenomethionine and selenizing polysaccharide are prepared respectively;
20-50 parts of fulvic acid selenium, 10-75 parts of selenomethionine and 8-55 parts of selenizing polysaccharide is taken, is added 1-5 parts
Sodium carboxymethylcellulose and 5-20 parts of lactose are added 5-20 parts of water and are mixed to get selenium-rich mixture;
Take selenium-rich mixture be added 10-50 parts of selenate, 5000-20000 parts of humic acid, 5000-20000 parts have
Machine fertilizer and 50-100 part of zinc fertilizer add after 1-15 parts of water mixed, and progress wet granulation, whole grain are to get to receiving
Rice selenium plant nutrient.
Preferably, described " preparing fulvic acid selenium, selenomethionine and selenizing polysaccharide respectively " includes:
It is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;
2- amino -4- benzyl selenomethionines are taken, sodium chloride, ammonium hydroxide and iodomethane is added and is reacted, seleno egg is obtained
Propylhomoserin;
The selenizing polysaccharide is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3It adjusts
Solution ph obtains chitosan selenium.
Preferably, described " taking High-Se corn to carry out Physical Processing, to obtain the natural selenium-rich food of cytotrophy " includes:
High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
It cleans the purifying High-Se corn 2-3 times, dries, obtain dry product;The moisture of the dry product is controlled first
Within the scope of moisture condition;
Remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 100-150 mesh, obtains pulverized particles;
It takes the pulverized particles to carry out extrusion under the conditions of 110-120 DEG C, obtains extrusion object;
Physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 80-100 mesh, obtains puff crushing
Grain;
The moisture for controlling the puff pulverized particles controls within the second moisture condition, carries out aseptic packaging, obtains
The natural selenium-rich food of the cytotrophy.
Preferably,
First moisture condition is 5%-7%;
Second moisture condition is 7% or less.
Preferably, the default fertilization time section is the seedlings of cereal crops of non-transgenic corn when bearing 3-6 piece leaves.
The default dose is 5-30 kgs/acre.
The present invention provides a kind of preparation method of the natural selenium-rich food of cytotrophy, and the preparation method includes:It prepares
Nanometer selenium plant nutrient;Using nanometer selenium plant nutrient conditioned soil soil;Non-transgenic corn is planted, in default fertilising
It applies fertilizer, and waters 1-2 times according to default dose in period;It is harvested to get to High-Se corn after maturation;Take high selenium
Corn carries out Physical Processing, obtains the natural selenium-rich food of cytotrophy.The western plant nutrient of nanometer provided through the invention
After agent improves the soil in soil, transgenic corns are planted, are harvested after corn maturation, this is obtained using Physical Processing
The natural selenium-rich food of provided cytotrophy is provided.Using the selenium-enriched food prepared by the preparation method in the present invention, it is
The selenium-enriched food of pure natural healthy selenium-rich organic food, cytotrophy is more easily direct by gastrointestinal tract rapidly after human body intake
It absorbs, improves bioavilability, and due to being natural organic food, it is artificial synthesized that other need not be taken in during selenium-supply
Drug or the virose inorganic food of tool, hidden danger without any side effects exist, and use is more safe and reliable.
Specific implementation mode
Technical scheme of the present invention is described in further detail with reference to the mode of specific embodiment, but not structure
At any limitation of the invention, the modification of anyone limited number of time made within the scope of the invention as claimed, still in this hair
Within bright right.
To solve the above problems, the present invention provides a kind of preparation method of the natural selenium-rich food of cytotrophy, including:
Prepare nanometer selenium plant nutrient;
Using nanometer selenium plant nutrient conditioned soil soil;
Non-transgenic corn is planted, is applied fertilizer according to default dose in default fertilization time section, and the 1-2 that waters
It is secondary;It is harvested to get to High-Se corn after maturation;
It takes High-Se corn to carry out Physical Processing, obtains the natural selenium-rich food of cytotrophy.
It is above-mentioned, it is to be understood that selenium is the essential trace elements of the human body, is the constituent of a variety of enzymes in human body,
The effects that resisting disease, anti-aging, enhancing immune function is played in life.Selenium has protect liver, anticancer, protection angiocarpy, adjusts
It saves hormone secretion, antagonism heavy metal, chemoradiation therapy, treatment cataract, remove many biological effects such as superfluous free radical.Selenium system
Product occupy an important position in health food and pharmaceuticals.The Selenium supplement agent that people use earliest, which is inorganic selenium, (mainly has sodium selenate
And sodium selenite).Relatively, safety and bioactivity are all relatively low, now for the Dosages and toxicity dose of inorganic selenium
Through substantially being replaced by the very high and nontoxic nanometer selenium of bioactivity.In the present invention, used nanometer Xi Zhiwuying
It is the preparation for having effects that organic nano selenium soil improvement to support agent.
It is above-mentioned, it is to be understood that soil improvement is the bad quality and structure for soil, take corresponding physics,
Biological or chemical measure improves soil property, increases soil fertility, and increases crop yield, and improve human survival soil ring
The process in border.Can also include by using soil specifically, may include the arrangement of soil itself, physical operations of ploughing etc.
Earth improves medicament and carries out chemical modifying, to improve the fertility of soil.In the present invention, using nanometer selenium plant nutrient as
Soil conditioner carries out soil improvement.
Additionally, it should be appreciated that soil conditioner has multiclass:(1) mineral substance, mainly have peat, lignite, weathered coal,
Lime, gypsum, vermiculite, bentonite, zeolite, perlite and sepiolite etc.;(2) natural and semi-synthetic water soluble polymer class, it is main
There are stalk, polysaccharide material, cellulose substances, lignin material and resin glue substance;(3) artificial synthesized macromolecule chemical combination
Object mainly has polyacrylic, vinyl acetate Malaysia acids and polyvinyl alcohol;(4) effective microorganism preparation class etc..
Above-mentioned, transgenic corns are exactly to utilize Modern Molecular Biotechnology, race relation is very remote and useful plant
Channel genes need in the maize genetic substance improved, and having of making that its offspring embodies that people are pursued stablizes heredity
The corn of shape.Transgenic technology is to produce the core technology of transgenic corns, is to utilize DNA recombinant techniques, foreign gene is turned
It moves on in receptor biological, is allowed to generate change orienting, stablizing heredity, that is, new receptor biological is made to obtain new property
Shape.
It is above-mentioned, physics deep processing is carried out to High-Se corn, can be cleaned, be sterilized, packaging and other steps, is become to prepare
The selenium-rich wholefood that conveniently can further eat.
The present invention provides a kind of preparation method of the natural selenium-rich food of cytotrophy, and the preparation method utilizes the present invention
In preparation method prepared by selenium-enriched food, be pure natural healthy selenium-rich organic food, the selenium-enriched food of cytotrophy is more
It is easy directly to be absorbed by gastrointestinal tract rapidly after human body is taken in, improves bioavilability, and due to being natural organic food, mending
Other artificial synthesized drugs need not be taken in during selenium or the virose inorganic food of tool, hidden danger without any side effects are deposited
Use is more safe and reliable.
In addition, using the natural selenium-rich food of the cytotrophy prepared by preparation method provided by the present invention, more easily
In the absorption and utilization of human body, supplement natural selenium-rich food is for the liver diseases of patient, cancer, ophthalmology disease, prostate disease
The diseases such as disease, thyroid disease, diabetes have certain treatment and restitution, and in terms of beauty, have certain resist
Aging acts on.
Preferably, described " using nanometer selenium plant nutrient conditioned soil soil " includes:
10-30 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The nanometer selenium plant nutrient
Se content be 1000-5000 mgs/kg.
Preferably, the nanometer selenium plant nutrient includes the component of following parts by weight:
10-50 parts of selenate;
5000-20000 parts of humic acid;
5000-20000 parts of organic fertilizer;
50-100 parts of zinc fertilizer.
Preferably, the nanometer selenium plant nutrient further includes the component of following parts by weight:
20-50 parts of fulvic acid selenium;
10-75 parts of selenomethionine.
It is above-mentioned, it is to be understood that fulvic acid also known as fulvic acid are a kind of substance extracted from humus, molecular weight
Relatively low, appearance is in brownish black or sepia, dissolves in acid, is dissolved in alkali, is dissolved in ethyl alcohol, is dissolved in water, is molecule structure and row
For the compound of all similar substance of characteristic.Selenium is amphotere, have 3d104S24P4 electronic structures, with oxygen-containing group have compared with
Selenium-fulvic acid the chelate for generating low molecular weight is complexed with fulvic acid under low acid and weak basic condition for strong bonding tendency,
Stable structure, activity is very strong, soluble easily in water, and in soil, fulvic acid reference state selenium is easy movable selenium.
It is above-mentioned, it is to be understood that methionine is a kind of amino acid needed by human, and key structural feature is containing sulphur
Element, the element sulphur in methionine can be replaced under certain conditions by selenium element, generate selenium content up to 403000 μ g/
The selenomethionine of g.
Preferably, the nanometer selenium plant nutrient further includes the component of following parts by weight:
8-55 parts of selenizing polysaccharide.
It is above-mentioned, it is to be understood that polysaccharide is the sugar chain combined by glycosidic bond, to be at least more than that 10 monosaccharide forms
Polymerization sugar polymeric carbohydrate can use general formula (C6H10O5)nIt indicates.It is known as with more by the polysaccharide that identical monosaccharide forms
Sugar, such as starch, cellulose and glycogen;Be known as heteroglycan with the polysaccharide that different monosaccharide forms, as Arabic gum be by pentose and
The compositions such as galactolipin.Not a kind of pure chemical substance of polysaccharide, the mixture of the different substance of extent of polymerization.Polysaccharide
General not soluble in water, no sweet taste, cannot form crystallization, no reproducibility and mutarotation.Polysaccharide is also glucosides, it is possible to water
Solution, in hydrolytic process, often generates a series of intermediate product, final complete hydrolysis obtains monosaccharide.Selenizing polysaccharide is artificial
The selenium polysaccharide of synthesis, synthetic method generally comprise:First, using monomer selenium, selenous acid or sodium selenite etc. pair in a mild condition
Polysaccharide carries out selenizing modification;Second is that the active, SeOCl with acyl chlorides structure using chemical property, as selenizing reagent;Third, by
Functional group containing selenium is grafted on polysaccharide molecule.
Preferably, described " preparing nanometer selenium plant nutrient " includes:
Fulvic acid selenium, selenomethionine and selenizing polysaccharide are prepared respectively;
20-50 parts of fulvic acid selenium, 10-75 parts of selenomethionine and 8-55 parts of selenizing polysaccharide is taken, is added 1-5 parts
Sodium carboxymethylcellulose and 5-20 parts of lactose are added 5-20 parts of water and are mixed to get selenium-rich mixture;
Take selenium-rich mixture be added 10-50 parts of selenate, 5000-20000 parts of humic acid, 5000-20000 parts have
Machine fertilizer and 50-100 part of zinc fertilizer add after 1-15 parts of water mixed, and progress wet granulation, whole grain are to get to receiving
Rice selenium plant nutrient.
It is above-mentioned, it is to be understood that wet granulation is that binder is added in drug powder, leans on the crane span structure or glutinous of binder
Knot acts on the method for making powder coalesce together and preparing particle.It includes squeezing granulation, rotation granulation, fluidized granulation and stirring
Granulation etc..Particle made of wet method passes through moistened surface, has granular mass good, and good appearance, wearability be relatively strong, compression forming
The advantages that property is good, is most widely used in medical industry.
In the present invention, wet granulation is carried out to the raw material of nanometer selenium plant nutrient, in addition, it is possible to use dry granulation
It is prepared.
It is above-mentioned, when carrying out wet granulation, raw material need to be mixed by blender, for example, two-dimensional mixing machine, three-dimensional
Mixing machine, slot mix machine, homogenizer etc. equipment.Suitable water and adhesive is added in carrying out mixed process, in this hair
It is lactose and sodium carboxymethylcellulose in bright, is mixed after machine mixed by slot, obtain softwood;Further to softwood system
Grain obtains wet granular, then dry wet granular progress baking oven to obtain coarse granule for example, carrying out automatic pelleting by sieve.To institute
The coarse granule of obtained moisture qualification carries out whole grain, is arranged using sieve, obtains the particle of uniform particle sizes to get to nanometer
Selenium plant nutrient.
Preferably, described " preparing fulvic acid selenium, selenomethionine and selenizing polysaccharide respectively " includes:
It is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;
It is above-mentioned, in the present invention, carry out preparing fulvic acid selenium using the technique of secondary synthesis.Step includes prepared by fulvic acid
With the preparation of fulvic acid selenium.As by being implanted into saccharomycete and streptococcus fecalis in the humic acid in fermentation tank, fermentation training is carried out
It supports 15 days, and then further extracts fulvic acid therein;Will in fulvic acid be added selenium salt be heated to 40 DEG C keep 20 hours, finally
By Purification by filtration, fulvic acid selenium is obtained.
2- amino -4- benzyl selenomethionines are taken, sodium chloride, ammonium hydroxide and iodomethane is added and is reacted, seleno egg is obtained
Propylhomoserin;
Based on 2- amino -4- benzyl selenomethionines, iodomethane is added under conditions of sodium and ammoniacal liquor, the reaction was continued half
Hour, final ammoniacal liquor further can be heated to remove by nitrogen and low-grade fever state.
The selenizing polysaccharide is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3It adjusts
Solution ph obtains chitosan selenium.
It is above-mentioned, it is to be understood that chitosan (chitosan) is also known as chitosan, is widely present by nature
Chitin (chitin) obtained by deacetylation, chemical name is Chitosan (1-4) -2- amino-B-D grapes
Sugar.Acetum is added in chitosan, stirring to solution is clarified, and appropriate NaSeO is slowly added to3, use 10%HNO3Adjust pH value of solution
Value after centrifugation, takes supernatant, and 3 times of 95% ethyl alcohol of amount are added, centrifuge, washing centrifuges again, washs, low temperature drying, most
After obtain faint yellow chitosan selenium to get.
Preferably, described " taking High-Se corn to carry out Physical Processing, to obtain the natural selenium-rich food of cytotrophy " includes:
High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
It is above-mentioned, the soil in corn, sand, stone, metal impurities are cleaned out using impurity removing equipment.
It cleans the purifying High-Se corn 2-3 times, dries, obtain dry product;The moisture of the dry product is controlled first
Within the scope of moisture condition;
It is above-mentioned, corn is cleaned 2-3 times with clear water;It is dried for standby, the corn after drying controls moisture.
Remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 100-150 mesh, obtains pulverized particles;
It is above-mentioned, it is peeled to spare corn using peeler, yield 60-70%;Corn after decortication crushes,
100-150 mesh.
It takes the pulverized particles to carry out extrusion under the conditions of 110-120 DEG C, obtains extrusion object;
Physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 80-100 mesh, obtains puff crushing
Grain;
The moisture for controlling the puff pulverized particles controls within the second moisture condition, carries out aseptic packaging, obtains
The natural selenium-rich food of the cytotrophy.
It is above-mentioned, aseptic packaging is carried out, moisture is controlled, controls 50 microgram containing selenium in every bag of 10 grams of natural selenium-rich food.
Preferably,
First moisture condition is 5%-7%;
Second moisture condition is 7% or less.
Preferably, the default fertilization time section is the seedlings of cereal crops of non-transgenic corn when bearing 3-6 piece leaves.
The default dose is 5-30 kgs/acre.
To facilitate the understanding of the present invention, the technical solution further illustrated the present invention with reference to embodiment.Applicant
Statement, the present invention illustrate detailed process equipment and the technological process of the present invention, but the present invention not office by above-described embodiment
It is limited to above-mentioned detailed process equipment and technological process, that is, does not mean that the present invention has to rely on above-mentioned detailed process equipment and technique
Flow could be implemented.Person of ordinary skill in the field is each to product of the present invention it will be clearly understood that any improvement in the present invention
The equivalence replacement of raw material and the addition of auxiliary element, the selection of concrete mode etc. all fall within protection scope of the present invention and openly
Within the scope of.
The predominant quantity number of the nanometer selenium plant nutrient added in 1 embodiment 1-6 of table
Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | |
Selenate | 10 | 20 | 30 | 40 | 45 | 50 |
Humic acid | 5000 | 7000 | 5500 | 15000 | 10000 | 20000 |
Organic fertilizer | 5000 | 8000 | 10000 | 11000 | 16000 | 20000 |
Zinc fertilizer | 50 | 60 | 70 | 80 | 90 | 100 |
Fulvic acid selenium | 20 | 25 | 35 | 45 | 50 | 40 |
Selenomethionine | 10 | 20 | 35 | 50 | 60 | 75 |
Selenizing polysaccharide | 8 | 20 | 30 | 40 | 50 | 55 |
Embodiment 1:
The present embodiment provides a kind of natural selenium-rich food of cytotrophy, preparation method is as follows:
1, it is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;Take 2- ammonia
Base -4- benzyl selenomethionines are added sodium chloride, ammonium hydroxide and iodomethane and are reacted, obtain selenomethionine;The selenizing is more
Sugar is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3Solution ph is adjusted, chitosan is obtained
Selenium;
2, fulvic acid selenium, selenomethionine and selenizing polysaccharide are taken according to the parts by weight of table 1, it is fine that 1 part of carboxymethyl is added
The plain sodium of dimension and 6 parts of lactose are added 6 parts of water and are mixed to get selenium-rich mixture;
3, according to the parts by weight of table 1, take selenium-rich mixture that selenate, humic acid, organic fertilizer and zinc fertilizer is added, then add
Enter after 2 parts of water mixed, carries out wet granulation, whole grain to get to nanometer selenium plant nutrient;
4,10 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The nanometer selenium plant nutrient
Se content is 1100 mgs/kg;
5, plant non-transgenic corn, non-transgenic corn the seedlings of cereal crops when bearing 3-6 piece leaves according to 5-30 kilograms/
Mu applies fertilizer, and waters 1-2 times;It is harvested to get to High-Se corn after maturation;
6, High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
7, the purifying High-Se corn is cleaned 2-3 times, drying obtains dry product;The moisture control of the dry product exists
5%;
8, remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 100 mesh, obtains pulverized particles;
9, it takes the pulverized particles to carry out extrusion under the conditions of 110 DEG C, obtains extrusion object;
10, physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 80 mesh, obtains puff crushing
Grain;
11, the moisture for controlling the puff pulverized particles is controlled 7% hereinafter, progress aseptic packaging, obtains described thin
The natural selenium-rich food of born of the same parents' nutrition.
Embodiment 2:
The present embodiment provides a kind of natural selenium-rich food of cytotrophy, preparation method is as follows:
1, it is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;Take 2- ammonia
Base -4- benzyl selenomethionines are added sodium chloride, ammonium hydroxide and iodomethane and are reacted, obtain selenomethionine;The selenizing is more
Sugar is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3Solution ph is adjusted, chitosan is obtained
Selenium;
2, fulvic acid selenium, selenomethionine and selenizing polysaccharide are taken according to the parts by weight of table 1, it is fine that 1 part of carboxymethyl is added
The plain sodium of dimension and 5 parts of lactose are added 5 parts of water and are mixed to get selenium-rich mixture;
3, according to the parts by weight of table 1, take selenium-rich mixture that selenate, humic acid, organic fertilizer and zinc fertilizer is added, then add
Enter after 1 part of water mixed, carries out wet granulation, whole grain to get to nanometer selenium plant nutrient;
4,15 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The nanometer selenium plant nutrient
Se content is 1200 mgs/kg;
5, plant non-transgenic corn, non-transgenic corn the seedlings of cereal crops when bearing 3-6 piece leaves according to 5-30 kilograms/
Mu applies fertilizer, and waters 1-2 times;It is harvested to get to High-Se corn after maturation;
6, High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
7, the purifying High-Se corn is cleaned 2-3 times, drying obtains dry product;The moisture control of the dry product exists
5%;
8, remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 100 mesh, obtains pulverized particles;
9, it takes the pulverized particles to carry out extrusion under the conditions of 110 DEG C, obtains extrusion object;
10, physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 80 mesh, obtains puff crushing
Grain;
11, the moisture for controlling the puff pulverized particles is controlled 7% hereinafter, progress aseptic packaging, obtains described thin
The natural selenium-rich food of born of the same parents' nutrition.
Embodiment 3:
The present embodiment provides a kind of natural selenium-rich food of cytotrophy, preparation method is as follows:
1, it is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;Take 2- ammonia
Base -4- benzyl selenomethionines are added sodium chloride, ammonium hydroxide and iodomethane and are reacted, obtain selenomethionine;The selenizing is more
Sugar is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3Solution ph is adjusted, chitosan is obtained
Selenium;
2, fulvic acid selenium, selenomethionine and selenizing polysaccharide are taken according to the parts by weight of table 1, it is fine that 2 parts of carboxymethyl is added
The plain sodium of dimension and 8 parts of lactose are added 7 parts of water and are mixed to get selenium-rich mixture;
3, according to the parts by weight of table 1, take selenium-rich mixture that selenate, humic acid, organic fertilizer and zinc fertilizer is added, then add
Enter after 3 parts of water mixed, carries out wet granulation, whole grain to get to nanometer selenium plant nutrient;
4,20 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The nanometer selenium plant nutrient
Se content is 2000 mgs/kg;
5, plant non-transgenic corn, non-transgenic corn the seedlings of cereal crops when bearing 3-6 piece leaves according to 10 kgs/acre
It applies fertilizer, and waters 1-2 times;It is harvested to get to High-Se corn after maturation;
6, High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
7, the purifying High-Se corn is cleaned 2-3 times, drying obtains dry product;The moisture control of the dry product exists
6%;
8, remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 150 mesh, obtains pulverized particles;
9, it takes the pulverized particles to carry out extrusion under the conditions of 120 DEG C, obtains extrusion object;
10, physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 100 mesh, obtains puff crushing
Grain;
11, the moisture for controlling the puff pulverized particles is controlled 7% hereinafter, progress aseptic packaging, obtains described thin
The natural selenium-rich food of born of the same parents' nutrition.
Embodiment 4:
The present embodiment provides a kind of natural selenium-rich food of cytotrophy, preparation method is as follows:
1, it is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;Take 2- ammonia
Base -4- benzyl selenomethionines are added sodium chloride, ammonium hydroxide and iodomethane and are reacted, obtain selenomethionine;The selenizing is more
Sugar is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3Solution ph is adjusted, chitosan is obtained
Selenium;
2, fulvic acid selenium, selenomethionine and selenizing polysaccharide are taken according to the parts by weight of table 1, it is fine that 4 parts of carboxymethyl is added
The plain sodium of dimension and 15 parts of lactose are added 15 parts of water and are mixed to get selenium-rich mixture;
3, according to the parts by weight of table 1, take selenium-rich mixture that selenate, humic acid, organic fertilizer and zinc fertilizer is added, then add
Enter after 10 parts of water mixed, carries out wet granulation, whole grain to get to nanometer selenium plant nutrient;
4,25 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The nanometer selenium plant nutrient
Se content is 4000 mgs/kg;
5, plant non-transgenic corn, non-transgenic corn the seedlings of cereal crops when bearing 3-6 piece leaves according to 5-30 kilograms/
Mu applies fertilizer, and waters 1-2 times;It is harvested to get to High-Se corn after maturation;
6, High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
7, the purifying High-Se corn is cleaned 2-3 times, drying obtains dry product;The moisture control of the dry product exists
7%;
8, remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 150 mesh, obtains pulverized particles;
9, it takes the pulverized particles to carry out extrusion under the conditions of 120 DEG C, obtains extrusion object;
10, physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 100 mesh, obtains puff crushing
Grain;
11, the moisture for controlling the puff pulverized particles is controlled 7% hereinafter, progress aseptic packaging, obtains described thin
The natural selenium-rich food of born of the same parents' nutrition.
Embodiment 5:
The present embodiment provides a kind of natural selenium-rich food of cytotrophy, preparation method is as follows:
1, it is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;Take 2- ammonia
Base -4- benzyl selenomethionines are added sodium chloride, ammonium hydroxide and iodomethane and are reacted, obtain selenomethionine;The selenizing is more
Sugar is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3Solution ph is adjusted, chitosan is obtained
Selenium;
2, fulvic acid selenium, selenomethionine and selenizing polysaccharide are taken according to the parts by weight of table 1,4.5 parts of carboxymethyl is added
Sodium cellulosate and 18 parts of lactose are added 5-20 parts of water and are mixed to get selenium-rich mixture;
3, according to the parts by weight of table 1, take selenium-rich mixture that selenate, humic acid, organic fertilizer and zinc fertilizer is added, then add
Enter after 13 parts of water mixed, carries out wet granulation, whole grain to get to nanometer selenium plant nutrient;
4,22 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The nanometer selenium plant nutrient
Se content is 3500 mgs/kg;
5, plant non-transgenic corn, non-transgenic corn the seedlings of cereal crops when bearing 3-6 piece leaves according to 25 kgs/acre
It applies fertilizer, and waters 1-2 times;It is harvested to get to High-Se corn after maturation;
6, High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
7, the purifying High-Se corn is cleaned 2-3 times, drying obtains dry product;The moisture control of the dry product exists
5%;
8, remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 100 mesh, obtains pulverized particles;
9, it takes the pulverized particles to carry out extrusion under the conditions of 110 DEG C, obtains extrusion object;
10, physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 80-100 mesh, obtains puff powder
Broken particle;
11, the moisture for controlling the puff pulverized particles is controlled 7% hereinafter, progress aseptic packaging, obtains described thin
The natural selenium-rich food of born of the same parents' nutrition.
Embodiment 6:
The present embodiment provides a kind of natural selenium-rich food of cytotrophy, preparation method is as follows:
1, it is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;Take 2- ammonia
Base -4- benzyl selenomethionines are added sodium chloride, ammonium hydroxide and iodomethane and are reacted, obtain selenomethionine;The selenizing is more
Sugar is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3Solution ph is adjusted, chitosan is obtained
Selenium;
2, fulvic acid selenium, selenomethionine and selenizing polysaccharide are taken according to the parts by weight of table 1, it is fine that 5 parts of carboxymethyl is added
The plain sodium of dimension and 20 parts of lactose are added 20 parts of water and are mixed to get selenium-rich mixture;
3, according to the parts by weight of table 1, take selenium-rich mixture that selenate, humic acid, organic fertilizer and zinc fertilizer is added, then add
Enter after 15 parts of water mixed, carries out wet granulation, whole grain to get to nanometer selenium plant nutrient;
4,10-30 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The nanometer selenium plant nutrient
The Se content of agent is 5000 mgs/kg;
5, plant non-transgenic corn, non-transgenic corn the seedlings of cereal crops when bearing 3-6 piece leaves according to 30 kgs/acre
It applies fertilizer, and waters 1-2 times;It is harvested to get to High-Se corn after maturation;
6, High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
7, the purifying High-Se corn is cleaned 2-3 times, drying obtains dry product;The moisture control of the dry product exists
6.5%;
8, remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 100-150 mesh, obtains crushing
Grain;
9, it takes the pulverized particles to carry out extrusion under the conditions of 120 DEG C, obtains extrusion object;
10, physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 100 mesh, obtains puff crushing
Grain;
11, the moisture for controlling the puff pulverized particles is controlled 7% hereinafter, progress aseptic packaging, obtains described thin
The natural selenium-rich food of born of the same parents' nutrition.
The present invention is prepared for the natural selenium-rich food of the cytotrophy of 1-6 in embodiment by above-mentioned preparation method, and counts
DPPH free radical scavenging activities are calculated, concrete outcome is shown in Table 1.
Specifically, being tested by the following method:
1, the drying sample of the natural selenium-rich food of the cytotrophy in Example 1-6 after crushing, passes through 60% ethyl alcohol
It is extracted 1 hour at 50 DEG C, obtains ethanol extract;
2, ethanol extract is subjected to gradient elution (eluent is the aqueous solution of ethyl alcohol) by D101 macroporous absorbent resins,
Retain 40% ethanol sample, concentrates, and be dried to powder;
3, the powder is subjected to high speed extraction by high speed adverse current chromatogram, eluent is dichloromethane:Ethyl alcohol:Water=
20:5:5, eluent and drying are collected, purified is obtained;
4, the purified is dissolved as extracting solution sample solution with distilled water;Take 2mL extracting solutions sample solution to capacity
Bottle, is added the DPPH 3mL of methanol 2mL, 0.1mol/L, and light reaction 30 minutes obtains reaction solution;
5, it extracts reaction solution 1mL to be put into cuvette, the absorbance of reaction solution is detected under 520nm wavelength, calculate clear
Except rate, 2 are the results are shown in Table.
DPPH clearance rates=[1- (Ai-Aj)/Ac] × 100%;
In formula:AiFor the absorbance of DPPH and test liquid;AjFor the absorbance of test liquid and absolute ethyl alcohol;AcFor
The absorbance of DPPH and absolute ethyl alcohol.
The DPPH free radical scavenging activities of the natural selenium-rich food for the cytotrophy being prepared in 2 embodiment 1-6 of table
To sum up, the natural selenium-rich food of the cytotrophy prepared by embodiment 1-6 as can be seen from Table 2, in different journeys
Degree has certain antioxidant activity, has anti-aging, the effect of beautifying face and moistering lotion to a certain extent.Utilize the system in the present invention
The natural selenium-rich food of cytotrophy prepared by Preparation Method is pure natural healthy selenium-rich organic food, the richness of cytotrophy
Selenium food is easier directly to be absorbed by gastrointestinal tract rapidly after human body intake, improves bioavilability, and due to being natural organic
Food need not take in other artificial synthesized drugs or the virose inorganic food of tool, no any secondary work during selenium-supply
Hidden danger exists, and use is more safe and reliable.
Claims (10)
1. a kind of preparation method of the natural selenium-rich food of cytotrophy, which is characterized in that including:
Prepare nanometer selenium plant nutrient;
Using nanometer selenium plant nutrient conditioned soil soil;
Non-transgenic corn is planted, is applied fertilizer according to default dose in default fertilization time section, and water 1-2 times;
It is harvested to get to High-Se corn after maturation;
It takes High-Se corn to carry out Physical Processing, obtains the natural selenium-rich food of cytotrophy.
2. the preparation method of the natural selenium-rich food of cytotrophy as described in claim 1, which is characterized in that described " using receiving
Rice selenium plant nutrient improves soil soil " include:
10-30 kilograms of nanometer selenium plant nutrient is used in soil soil per acre;The selenium of the nanometer selenium plant nutrient
Content is 1000-5000 mgs/kg.
3. the preparation method of the natural selenium-rich food of cytotrophy as claimed in claim 1 or 2, which is characterized in that the nanometer
Selenium plant nutrient includes the component of following parts by weight:
10-50 parts of selenate;
5000-20000 parts of humic acid;
5000-20000 parts of organic fertilizer;
50-100 parts of zinc fertilizer.
4. the preparation method of the natural selenium-rich food of cytotrophy as claimed in claim 3, which is characterized in that the nanometer selenium is planted
Object nutritional agents further includes the component of following parts by weight:
20-50 parts of fulvic acid selenium;
10-75 parts of selenomethionine.
5. the preparation method of the natural selenium-rich food of cytotrophy as claimed in claim 4, which is characterized in that the nanometer selenium is planted
Object nutritional agents further includes the component of following parts by weight:
8-55 parts of selenizing polysaccharide.
6. the preparation method of the natural selenium-rich food of cytotrophy as claimed in claim 4, which is characterized in that described " preparation is received
Rice selenium plant nutrient " include:
Fulvic acid selenium, selenomethionine and selenizing polysaccharide are prepared respectively;
20-50 parts of fulvic acid selenium, 10-75 parts of selenomethionine and 8-55 parts of selenizing polysaccharide is taken, 1-5 parts of carboxylic first is added
Base sodium cellulosate and 5-20 parts of lactose are added 5-20 parts of water and are mixed to get selenium-rich mixture;
Take selenium-rich mixture that 10-50 parts of selenate, 5000-20000 parts of humic acid, 5000-20000 parts of organic fertilizer is added
And 50-100 parts of zinc fertilizer, it adds after 1-15 parts of water mixed, carries out wet granulation, whole grain to get to nanometer selenium
Plant nutrient agent.
7. the preparation method of the natural selenium-rich food of cytotrophy as claimed in claim 6, which is characterized in that described " to make respectively
For fulvic acid selenium, selenomethionine and selenizing polysaccharide " include:
It is implanted into strain in humic acid, extracts fulvic acid after fermentation, selenium salt is added to get to fulvic acid selenium;
2- amino -4- benzyl selenomethionines are taken, sodium chloride, ammonium hydroxide and iodomethane is added and is reacted, selenomethionine is obtained;
The selenizing polysaccharide is chitosan selenium;It takes chitosan that acetic acid is added, adds NaSeO3, pass through 10%HNO3Adjust solution
PH value obtains chitosan selenium.
8. the preparation method of the natural selenium-rich food of cytotrophy as described in claim 1, which is characterized in that described " to take high selenium
Corn carries out Physical Processing, obtains the natural selenium-rich food of cytotrophy " include:
High-Se corn is taken, edulcoration purification is carried out, obtains purifying High-Se corn;
It cleans the purifying High-Se corn 2-3 times, dries, obtain dry product;The moisture of the dry product is controlled in the first moisture
Within the scope of condition;
Remove the peel simultaneously precomminution to the dry product, and be sieved, sieve mesh number is 100-150 mesh, obtains pulverized particles;
It takes the pulverized particles to carry out extrusion under the conditions of 110-120 DEG C, obtains extrusion object;
Physical crushing, sieving are carried out to the extrusion object, sieve mesh number is 80-100 mesh, obtains puff pulverized particles;
The moisture for controlling the puff pulverized particles controls within the second moisture condition, carries out aseptic packaging, obtains described
The natural selenium-rich food of cytotrophy.
9. the preparation method of the natural selenium-rich food of cytotrophy as claimed in claim 8, which is characterized in that first moisture
Condition is 5%-7%;
Second moisture condition is 7% or less.
10. the preparation method of the natural selenium-rich food of cytotrophy as described in claim 8 or 9, which is characterized in that described default
Fertilization time section is the seedlings of cereal crops of non-transgenic corn when bearing 3-6 piece leaves.
The default dose is 5-30 kgs/acre.
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CN113968649A (en) * | 2021-10-20 | 2022-01-25 | 林欣 | Selenium-enriched drinking water and preparation method thereof |
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