CN108442139A - The preparation method of flax dacron fine-denier socks - Google Patents
The preparation method of flax dacron fine-denier socks Download PDFInfo
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- CN108442139A CN108442139A CN201810342059.7A CN201810342059A CN108442139A CN 108442139 A CN108442139 A CN 108442139A CN 201810342059 A CN201810342059 A CN 201810342059A CN 108442139 A CN108442139 A CN 108442139A
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- denier
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- flax
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/0032—Determining dye recipes and dyeing parameters; Colour matching or monitoring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
- D06P1/67358—Halides or oxyhalides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
- D06P3/8238—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using different kinds of dye
- D06P3/8252—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using different kinds of dye using dispersed and reactive dyes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
Abstract
Grow flax the preparation methods of dacron fine-denier socks the invention discloses one, passes through flax dacron fine-denier fibrillation, pretreatment successively, it is dyed again, the present invention, in dyeing course, reactive dye and disperse dyes are added simultaneously, using soda acid transition method, while in different acid-base values, dip time is different, temperature is also different so that two kinds of different fibers reach good color fastness, obtained socks have good gas permeability and penetrability.
Description
Technical field
The present invention relates to a kind of manufacturing method of socks more particularly to the preparation methods of flax dacron fine-denier socks.
Background technology
About the definition of fine-denier, micro Denier, superfine Denier fibre, unified standard there is no in the world；China generally 0.9~
The fiber of 1.4dtex becomes fine count fiber；0.55~1.1dtex is fine-denier fiber；And 0.55dtex fibers below are super
Fine count fiber.Using fabric made of fine count fiber, feel is more preferably fine and smooth, more there is texture, quality higher, added value also higher.
Dacron fine-denier fiber is one kind of the fibre in differentiation quickly grown in recent years, because it is thinner than traditional polyester fiber, therefore
Than traditional polyester fiber with more soft sense of touch；The fabric made with polyester microdenier fiber is comfortable, beautiful, ventilative.
Flax is one of the natural fiber that the mankind use earliest, is a kind of rare natural fiber, have temperature adjustment, antiallergy,
The function of antistatic, antibacterial, and good hygroscopicity, therefore it is widely used in various textile fields.
Dacron fine-denier fiber and linen blend product have good antibacterial property energy, also more ventilative, but since terylene is thin
Denier fiber linear density is low, large specific surface area, and due to two kinds of fibre structure differences of dacron fine-denier and flax, in level-dyeing property and colour developing
There is difference in property, color fastness is also poor.
Invention content
Based on the above issues, the present invention discloses a preparation method for growing flax dacron fine-denier socks production so that flax and washs
Two kinds of different fibers of synthetic fibre fine-denier have good color fastness, while made socks have ventilative and penetrability well.
The technical solution adopted in the present invention is as follows：
The preparation method of flax dacron fine-denier socks,
Step 1：Flax dacron fine-denier fibrillation adds NaOH solution, a concentration of 20g/L, temperature 100-110 in a reservoir
DEG C, 40-50 minutes fibrillation time；
Step 2：Flax dacron fine-denier fiber pre-processes, and obtained by step 1, is placed in 2%NaCO3 solution, temperature 45-
It 55 DEG C, handles 25-30 minutes, is then eluted with water, then extract, in drying in oven；
Step 3：Dyeing obtained by step 2, is placed in dye vat in room temperature, and reactive dye series is added in dye vat and divides
Series dye, 0.5g/L penetration enhancers, 1.0g/L dispersants, 2.5g/L diffusion promoting agents are dissipated, then adds HAc so that solution is in
Acidity is warming up to 70 DEG C with the speed of 3 DEG C/min, and constant temperature is kept for 10 minutes, adds the CaCl2 of 10-50g/L, with 0.5 DEG C/
The speed of min is warming up to 90 DEG C, and constant temperature is kept for 10 minutes, then is warming up to 120 DEG C with the speed of 0.5 DEG C/min, and constant temperature keeps 40
Minute, 100 DEG C are cooled to the speed of 1 DEG C/min, the CaCl2 constant temperature that 20-100g/L is added is kept for 30 minutes, is cleaned,
Crosslinking agent is added, temperature is raised to 90 DEG C, and constant temperature 20 minutes adjusts PH with NaOH at this time, adds 1.0g/L NaCO3, constant temperature
20 minutes, PH finally is adjusted with HAc, reaches 7.
In dye vat, when acid, pH value 3-4.
In dye vat, when alkaline, pH value 10-11.
Preparation method of the present invention is simple, while using acid system and alkaline process, and uses reactive dye and disperse dyes, in difference
Acid-base value under, using different temperature, and using different dippings so that two kinds of different fibers have good color fastness；
It is not only improved in wearability, while socks obtained have good gas permeability and penetrability.
Specific implementation mode
Technical scheme of the present invention described in detail below.The embodiment of the present invention is only for illustrating concrete structure, the rule of the structure
Mould should not be limited by the examples.
The preparation method of flax dacron fine-denier socks, first, flax dacron fine-denier fibrillation add NaOH solution in a reservoir,
A concentration of 20g/L, temperature are 100-110 DEG C, 40-50 minutes fibrillation time；Then it is pre-processed again, by setting obtained by front
In 2%NaCO3 solution, temperature is 45-55 DEG C, handles 25-30 minutes, is then eluted with water, then extract, is dried in baking oven
It is dry；It is dyed, in room temperature, gained is placed in dye vat again, reactive dye series and disperse dyes system are added in dye vat
Row, 0.5g/L penetration enhancers, 1.0g/L dispersants, 2.5g/L diffusion promoting agents, then add HAc so that solution is in acidity, pH value
For 3-4；With the speed of 3 DEG C/min, 70 DEG C are warming up to, constant temperature is kept for 10 minutes, the CaCl2 of 10-50g/L is added, with 0.5
DEG C/speed of min is warming up to 90 DEG C, constant temperature is kept for 10 minutes, then is warming up to 120 DEG C with the speed of 0.5 DEG C/min, and constant temperature is kept
40 minutes, 100 DEG C are cooled to the speed of 1 DEG C/min, the CaCl2 constant temperature that 20-100g/L is added is kept for 30 minutes, is carried out clear
It washes, crosslinking agent is added, temperature is raised to 90 DEG C, and constant temperature 20 minutes adjusts PH, pH value 10-11 with NaOH at this time；It adds
1.0g/LNaCO3, constant temperature 20 minutes, finally adjusts PH with HAc, reaches 7.
Can different reactive dye series and disperse dyes series be added according to actual needs；Reactive dye series is such as high
Warm type Eriofast Series Reactive Dyes three primary colors；Disperse dyes series using diffusion promoting agent Ciba Univadine PB with
TerasilW series matchings use.
Claims (3)
1. the preparation method of flax dacron fine-denier socks, it is characterised in that：
Step 1：Flax dacron fine-denier fibrillation, in a reservoir plus NaOH solution, a concentration of 20g/L, temperature are 100-110 DEG C, are opened
Fine time 40-50 minutes；
Step 2：Flax dacron fine-denier fiber pre-processes, and obtained by step 1, is placed in 2%NaCO3 solution, temperature 45-55
DEG C, it handles 25-30 minutes, is then eluted with water, then extract, in drying in oven；
Step 3：Dyeing obtained by step 2, is placed in dye vat in room temperature, and reactive dye series is added in dye vat and dispersion contaminates
To expect series, 0.5g/L penetration enhancers, 1.0g/L dispersants, 2.5g/L diffusion promoting agents, then adds HAc so that solution is in acidity,
With the speed of 3 DEG C/min, 70 DEG C are warming up to, constant temperature is kept for 10 minutes, the CaCl2 of 10-50g/L is added, with 0.5 DEG C/min's
Speed is warming up to 90 DEG C, and constant temperature is kept for 10 minutes, then is warming up to 120 DEG C with the speed of 0.5 DEG C/min, and constant temperature is kept for 40 minutes,
100 DEG C are cooled to the speed of 1 DEG C/min, the CaCl2 constant temperature that 20-100g/L is added is kept for 30 minutes, is cleaned, and is added and is handed over
Joining agent, temperature is raised to 90 DEG C, and constant temperature 20 minutes adjusts PH with NaOH at this time, adds 1.0g/LNaCO3, constant temperature 20 minutes,
PH finally is adjusted with HAc, reaches 7.
2. the preparation method of flax dacron fine-denier socks according to claim 1, it is characterised in that in step 3, in dye vat,
When acid, pH value 3-4.
3. the preparation method of flax dacron fine-denier socks according to claim 1, it is characterised in that in step 3, in dye vat,
When alkaline, pH value 10-11.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810342059.7A CN108442139A (en) | 2018-04-17 | 2018-04-17 | The preparation method of flax dacron fine-denier socks |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810342059.7A CN108442139A (en) | 2018-04-17 | 2018-04-17 | The preparation method of flax dacron fine-denier socks |
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| Publication Number | Publication Date |
|---|---|
| CN108442139A true CN108442139A (en) | 2018-08-24 |
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|---|---|---|---|
| CN201810342059.7A Pending CN108442139A (en) | 2018-04-17 | 2018-04-17 | The preparation method of flax dacron fine-denier socks |
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| JP2006144146A (en) * | 2004-11-17 | 2006-06-08 | Mizuno Corp | Mixed fiber product containing highly crosslinked polyacrylic fiber and method for producing the same |
| CN101985813A (en) * | 2010-10-18 | 2011-03-16 | 南通曙光染织有限公司 | Process for dyeing polyester/cotton knitting cheeses by one-bath one-step method |
| CN103541247A (en) * | 2013-09-27 | 2014-01-29 | 浙江亿得化工有限公司 | Disperse/active dye one-bath two-step dip dyeing method for polyester-cotton fabric |
| CN105421105A (en) * | 2015-11-26 | 2016-03-23 | 绍兴海神印染制衣有限公司 | One bath process dyeing process of polyester cotton dispersing dye and reactive dye |
| CN105908532A (en) * | 2016-04-27 | 2016-08-31 | 浙江俏尔婷婷服饰有限公司 | Dyeing technique for polyester cotton or polyester viscose/chinlon/spandex multi-component fabric by one-bath two-step process |
| CN106968046A (en) * | 2017-03-09 | 2017-07-21 | 江苏金辰针纺织有限公司 | A kind of cool feeling uvioresistant cotton knitted fabric |
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2018
- 2018-04-17 CN CN201810342059.7A patent/CN108442139A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006144146A (en) * | 2004-11-17 | 2006-06-08 | Mizuno Corp | Mixed fiber product containing highly crosslinked polyacrylic fiber and method for producing the same |
| CN101985813A (en) * | 2010-10-18 | 2011-03-16 | 南通曙光染织有限公司 | Process for dyeing polyester/cotton knitting cheeses by one-bath one-step method |
| CN103541247A (en) * | 2013-09-27 | 2014-01-29 | 浙江亿得化工有限公司 | Disperse/active dye one-bath two-step dip dyeing method for polyester-cotton fabric |
| CN105421105A (en) * | 2015-11-26 | 2016-03-23 | 绍兴海神印染制衣有限公司 | One bath process dyeing process of polyester cotton dispersing dye and reactive dye |
| CN105908532A (en) * | 2016-04-27 | 2016-08-31 | 浙江俏尔婷婷服饰有限公司 | Dyeing technique for polyester cotton or polyester viscose/chinlon/spandex multi-component fabric by one-bath two-step process |
| CN106968046A (en) * | 2017-03-09 | 2017-07-21 | 江苏金辰针纺织有限公司 | A kind of cool feeling uvioresistant cotton knitted fabric |
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Application publication date: 20180824 |
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