CN108441359A - A kind of glass cleaner containing wood vinegar - Google Patents
A kind of glass cleaner containing wood vinegar Download PDFInfo
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- CN108441359A CN108441359A CN201810153119.0A CN201810153119A CN108441359A CN 108441359 A CN108441359 A CN 108441359A CN 201810153119 A CN201810153119 A CN 201810153119A CN 108441359 A CN108441359 A CN 108441359A
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- wood vinegar
- glass cleaner
- containing wood
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/008—Polymeric surface-active agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/044—Hydroxides or bases
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
- C11D3/048—Nitrates or nitrites
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/24—Organic compounds containing halogen
- C11D3/245—Organic compounds containing halogen containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/30—Amines; Substituted amines ; Quaternized amines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3942—Inorganic per-compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of glass cleaners containing wood vinegar, are mainly made of following active constituent：Trichorotrifluoroethane, hydroxyacetic acid receive, wood vinegar, triethanolamine, surfactant, caustic potash, sodium citrate, sulfamic acid, sodium nitrate, hydrogen peroxide and dimethyl succinate.The glass cleaner of the present invention, containing wood vinegar, by the synergistic effect of wood vinegar and other substances, cleaning efficiency is high, significantly shortens scavenging period, and can substantially reduce reagent consumption amount.Cleaning efficiency is high, and cleaning effect is good.
Description
Technical field
The present invention relates to cleaning agent field, more particularly to a kind of glass cleaner containing wood vinegar.
Background technology
Glass outside window, due to for a long time by expose to the weather and air in the pollutions such as harmful gas and oil smoke
With the erosion of chemical reaction, the stain being difficult to clean off together is formed already.So that skin produces dirt and wind
Change, had not only affected the beautiful and appearance of the city of building, but also damaged building.Therefore, the exterior wall of building is cleaned, is not only beautified
Environment, and play the role of protecting building.After glass dirt, it is necessary to use glass cleaner, however current glass
The cleaning performance of glass cleaning agent is bad, and cost is higher.
Being disclosed in the information of the background technology part, it is only intended to increase understanding of the overall background of the invention, without answering
It has been the prior art well known to persons skilled in the art when being considered as recognizing or imply that the information is constituted in any form.
Invention content
The purpose of the present invention is to provide a kind of glass cleaners containing wood vinegar, to overcome cleaning agent of high cost,
The bad disadvantage of cleaning performance.
To achieve the above object, the present invention provides a kind of glass cleaners containing wood vinegar, mainly by following activity
Ingredient is made：Trichorotrifluoroethane, hydroxyacetic acid receive, wood vinegar, triethanolamine, surfactant, caustic potash, sodium citrate,
Sulfamic acid, sodium nitrate, hydrogen peroxide and dimethyl succinate.
Preferably, in above-mentioned technical proposal, the glass cleaner containing wood vinegar is counted, mainly in parts by weight
It is made of following active constituent：7-13 parts of trichorotrifluoroethane, hydroxyacetic acid receive 3-6 parts, 9-16 parts of wood vinegar, triethanolamine 4-
8 parts, 2-5 parts of surfactant, 4-8 parts of caustic potash, 1-4 parts of sodium citrate, 2-6 parts of sulfamic acid, 3-7 parts of sodium nitrate, dioxygen
1-3 parts of 4-8 parts of water and dimethyl succinate.
Preferably, in above-mentioned technical proposal, the glass cleaner containing wood vinegar is counted, mainly in parts by weight
It is made of following active constituent：11 parts of trichorotrifluoroethane, hydroxyacetic acid receive 5 parts, 12 parts of wood vinegar, 6 parts of triethanolamine, surface
4 parts of activating agent, 6 parts of caustic potash, 3 parts of sodium citrate, 5 parts of sulfamic acid, 5 parts of sodium nitrate, 6 parts of hydrogen peroxide and dimethyl succinate
2 parts.
Preferably, in above-mentioned technical proposal, the surfactant is fatty alcohol polyoxyethylene ether or polyoxyethylene nonyl phenyl second
Alkene ether.
Preferably, in above-mentioned technical proposal, the wood vinegar is the wood vinegar being prepared using peanut shell.
Preferably, in above-mentioned technical proposal, the preparation method of the wood vinegar includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 4-5 DEG C/min, it is gradually heating to 150-
200 DEG C, completely cut off air, heat resolve 2-4h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min,
The flue gas of generation imports refrigerator pipe liquefaction, collects liquid, obtains crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, 20-24 hours static, distillate point three
Layer；
(4) it takes distillate middle layer air-distillation 4-5 hours at 100-110 DEG C, collects condensate liquid, as acetum pyrolignosum rectificatum
Liquid.
A kind of preparation method of the glass cleaner containing wood vinegar, includes the following steps：
(1) wood vinegar is prepared；
(2) trichorotrifluoroethane, hydroxyacetic acid are received, wood vinegar, triethanolamine, surfactant, caustic potash, citric acid
Sodium, sulfamic acid, sodium nitrate, hydrogen peroxide and dimethyl succinate add water to be mixed, and stir as in rotating speed 250-350r/min,
40-70min is reacted under conditions of 85-90 DEG C.
Preferably, in above-mentioned technical proposal, described plus water amount is 20-30 times of active constituent gross mass.
Compared with prior art, the present invention has the advantages that：The glass cleaner of the present invention, containing wood vinegar,
By the synergistic effect of wood vinegar and other substances, cleaning efficiency is high, significantly shortens scavenging period, and can substantially reduce medicament and disappear
Consumption.Cleaning efficiency is high, and cleaning effect is good.
Specific implementation mode
With reference to specific embodiment, the specific implementation mode of the present invention is described in detail, it is to be understood that this hair
Bright protection domain is not restricted by specific implementation.
Embodiment 1
A kind of glass cleaner containing wood vinegar, is counted in parts by weight, is mainly made of following active constituent：Trichlorine three
11 parts of fluoroethane, hydroxyacetic acid receive 5 parts, 12 parts of peanut shell wood vinegar, 6 parts of triethanolamine, 4 parts of surfactant, caustic potash 6
Part, 3 parts of sodium citrate, 5 parts of sulfamic acid, 5 parts of sodium nitrate, 6 parts of hydrogen peroxide and 2 parts of dimethyl succinate.
The surfactant is nonylphenol polyoxyethylene ether.
A kind of preparation method of the glass cleaner containing wood vinegar, includes the following steps：
Prepare wood vinegar；
The preparation method of the wood vinegar includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 4 DEG C/min, 180 DEG C are gradually heating to,
Completely cut off air, heat resolve 3h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min,
The flue gas of generation imports refrigerator pipe liquefaction, collects liquid, obtains crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, static 23 hours, three layers of distillate point；
(4) distillate middle layer air-distillation 4 hours at 100-110 DEG C are taken, condensate liquid, as acetum pyrolignosum rectificatum are collected
Liquid.
Prepare glass cleaner
Trichorotrifluoroethane, hydroxyacetic acid are received, wood vinegar, triethanolamine, surfactant, caustic potash, sodium citrate,
Sulfamic acid, sodium nitrate, hydrogen peroxide and dimethyl succinate mixing, are added 25 times of water and are mixed, stir as in rotating speed 250-
60min is reacted under conditions of 350r/min, 85-90 DEG C.
Using cleaning agent made from the present embodiment, by cleaning agent for cleaning glassware.Glassware is handled,
Take the glass of 10cm × 10cm, check weighing W1, the dirt of one layer about 30 grams of coating, roasts 1 hour, check weighing at 120 DEG C on glass
4 grams of glass cleaners containing wood vinegar are uniformly sprayed solarization on glass, are placed at room temperature to natural cooling, then normal by W2
It is rinsed, is then dried glass, check weighing W3 with sponge under warm water flowing.By gravimetric method, soil removal efficiency is obtained.
Above-mentioned dirt percentage, is made of following component：21% lard, 26% vegetable oil, 15% flour,
15% lanolin, 16% industrial vaseline, 7% particulate sugar.
Test result：Soil removal efficiency is 97.6%.
Embodiment 2
A kind of glass cleaner containing wood vinegar, is counted in parts by weight, is mainly made of following active constituent：Trichlorine three
7 parts of fluoroethane, hydroxyacetic acid receive 3 parts, 16 parts of peanut shell wood vinegar, 4 parts of triethanolamine, 5 parts of surfactant, 8 parts of caustic potash,
3 parts of 4 parts of sodium citrate, 2 parts of sulfamic acid, 7 parts of sodium nitrate, 4 parts of hydrogen peroxide and dimethyl succinate.
The surfactant is fatty alcohol polyoxyethylene ether.
A kind of preparation method of the glass cleaner containing wood vinegar, includes the following steps：
Prepare wood vinegar；
The preparation method of the wood vinegar includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 4 DEG C/min, 150 DEG C are gradually heating to,
Completely cut off air, heat resolve 4h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min,
The flue gas of generation imports refrigerator pipe liquefaction, collects liquid, obtains crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, static 24 hours, three layers of distillate point；
(4) distillate middle layer air-distillation 5 hours at 100-110 DEG C are taken, condensate liquid, as acetum pyrolignosum rectificatum are collected
Liquid.
Prepare glass cleaner
Trichorotrifluoroethane, hydroxyacetic acid are received, wood vinegar, triethanolamine, surfactant, caustic potash, sodium citrate,
Sulfamic acid, sodium nitrate, hydrogen peroxide and dimethyl succinate mixing, are added 30 times of water and are mixed, stir as in rotating speed 250-
70min is reacted under conditions of 350r/min, 85-90 DEG C.
Using cleaning agent made from the present embodiment, by cleaning agent for cleaning glassware.Glassware is handled,
Take the glass of 10cm × 10cm, check weighing W1, the dirt of one layer about 30 grams of coating, roasts 1 hour, check weighing at 120 DEG C on glass
4 grams of glass cleaners containing wood vinegar are uniformly sprayed solarization on glass, are placed at room temperature to natural cooling, then normal by W2
It is rinsed, is then dried glass, check weighing W3 with sponge under warm water flowing.By gravimetric method, soil removal efficiency is obtained.
Above-mentioned dirt percentage, is made of following component：21% lard, 26% vegetable oil, 15% flour,
15% lanolin, 16% industrial vaseline, 7% particulate sugar.
Test result：Soil removal efficiency is 96.3%.
Embodiment 3
A kind of glass cleaner containing wood vinegar, is counted in parts by weight, is mainly made of following active constituent：Trichlorine three
13 parts of fluoroethane, hydroxyacetic acid receive 6 parts, 9 parts of peanut shell wood vinegar, 8 parts of triethanolamine, 2 parts of surfactant, 4 parts of caustic potash,
1 part of 1 part of sodium citrate, 6 parts of sulfamic acid, 3 parts of sodium nitrate, 8 parts of hydrogen peroxide and dimethyl succinate.
The surfactant is fatty alcohol polyoxyethylene ether.
A kind of preparation method of the glass cleaner containing wood vinegar, includes the following steps：
Prepare wood vinegar；
The preparation method of the wood vinegar includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 5 DEG C/min, 200 DEG C are gradually heating to,
Completely cut off air, heat resolve 2h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min,
The flue gas of generation imports refrigerator pipe liquefaction, collects liquid, obtains crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, static 20 hours, three layers of distillate point；
(4) distillate middle layer air-distillation 4 hours at 100-110 DEG C are taken, condensate liquid, as acetum pyrolignosum rectificatum are collected
Liquid.
Prepare glass cleaner
Trichorotrifluoroethane, hydroxyacetic acid are received, wood vinegar, triethanolamine, surfactant, caustic potash, sodium citrate,
Sulfamic acid, sodium nitrate, hydrogen peroxide and dimethyl succinate mixing, are added 20 times of water and are mixed, stir as in rotating speed 250-
40min is reacted under conditions of 350r/min, 85-90 DEG C.
Using cleaning agent made from the present embodiment, by cleaning agent for cleaning glassware.Glassware is handled,
Take the glass of 10cm × 10cm, check weighing W1, the dirt of one layer about 30 grams of coating, roasts 1 hour, check weighing at 120 DEG C on glass
4 grams of glass cleaners containing wood vinegar are uniformly sprayed solarization on glass, are placed at room temperature to natural cooling, then normal by W2
It is rinsed, is then dried glass, check weighing W3 with sponge under warm water flowing.By gravimetric method, soil removal efficiency is obtained.
Above-mentioned dirt percentage, is made of following component：21% lard, 26% vegetable oil, 15% flour,
15% lanolin, 16% industrial vaseline, 7% particulate sugar.
Test result：Soil removal efficiency is 95.9%.
Comparative example 1
A kind of glass cleaner containing wood vinegar, is counted in parts by weight, is mainly made of following active constituent：Trichlorine three
11 parts of fluoroethane, hydroxyacetic acid receive 5 parts, 6 parts of triethanolamine, 4 parts of surfactant, 6 parts of caustic potash, 3 parts of sodium citrate, amino
2 parts of 5 parts of sulfonic acid, 5 parts of sodium nitrate, 6 parts of hydrogen peroxide and dimethyl succinate.
The surfactant is nonylphenol polyoxyethylene ether.
A kind of preparation method of the glass cleaner containing wood vinegar, includes the following steps：By trichorotrifluoroethane, hydroxyl
Acetic acid receives, triethanolamine, surfactant, caustic potash, sodium citrate, sulfamic acid, sodium nitrate, hydrogen peroxide and succinic acid diformazan
Ester mixes, and 25 times of water are added and are mixed, stir to react 60min under conditions of rotating speed 250-350r/min, 85-90 DEG C.
Using cleaning agent made from the present embodiment, by cleaning agent for cleaning glassware.Glassware is handled,
Take the glass of 10cm × 10cm, check weighing W1, the dirt of one layer about 30 grams of coating, roasts 1 hour, check weighing at 120 DEG C on glass
4 grams of glass cleaners containing wood vinegar are uniformly sprayed solarization on glass, are placed at room temperature to natural cooling, then normal by W2
It is rinsed, is then dried glass, check weighing W3 with sponge under warm water flowing.By gravimetric method, soil removal efficiency is obtained.
Above-mentioned dirt percentage, is made of following component：21% lard, 26% vegetable oil, 15% flour,
15% lanolin, 16% industrial vaseline, 7% particulate sugar.
Test result：Soil removal efficiency is 82.4%.
The description of the aforementioned specific exemplary embodiment to the present invention is in order to illustrate and illustration purpose.These descriptions
It is not wishing to limit the invention to disclosed precise forms, and it will be apparent that according to the above instruction, can much be changed
And variation.The purpose of selecting and describing the exemplary embodiment is that explaining the specific principle of the present invention and its actually answering
With so that those skilled in the art can realize and utilize the present invention a variety of different exemplary implementation schemes and
Various chooses and changes.The scope of the present invention is intended to be limited by claims and its equivalents.
Claims (8)
1. a kind of glass cleaner containing wood vinegar, which is characterized in that be mainly made of following active constituent：Trichlorine trifluoro second
Alkane, hydroxyacetic acid receive, wood vinegar, triethanolamine, surfactant, caustic potash, sodium citrate, sulfamic acid, sodium nitrate, dioxygen
Water and dimethyl succinate.
2. the glass cleaner according to claim 1 containing wood vinegar, which is characterized in that count in parts by weight, mainly
It is made of following active constituent：7-13 parts of trichorotrifluoroethane, hydroxyacetic acid receive 3-6 parts, 9-16 parts of wood vinegar, triethanolamine 4-
8 parts, 2-5 parts of surfactant, 4-8 parts of caustic potash, 1-4 parts of sodium citrate, 2-6 parts of sulfamic acid, 3-7 parts of sodium nitrate, dioxygen
1-3 parts of 4-8 parts of water and dimethyl succinate.
3. the glass cleaner according to claim 1 containing wood vinegar, which is characterized in that count in parts by weight, mainly
It is made of following active constituent：11 parts of trichorotrifluoroethane, hydroxyacetic acid receive 5 parts, 12 parts of wood vinegar, 6 parts of triethanolamine, surface
4 parts of activating agent, 6 parts of caustic potash, 3 parts of sodium citrate, 5 parts of sulfamic acid, 5 parts of sodium nitrate, 6 parts of hydrogen peroxide and dimethyl succinate
2 parts.
4. the glass cleaner according to claim 1 containing wood vinegar, which is characterized in that the surfactant is fat
Fat alcohol polyoxyethylene ether or nonylphenol polyoxyethylene ether.
5. the glass cleaner according to claim 1 containing wood vinegar, which is characterized in that the wood vinegar is to utilize flower
The wood vinegar that raw shell is prepared.
6. the glass cleaner according to claim 1 containing wood vinegar, which is characterized in that the preparation side of the wood vinegar
Method includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 4-5 DEG C/min, it is gradually heating to 150-200
DEG C, completely cut off air, heat resolve 2-4h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min, is generated
Flue gas import refrigerator pipe liquefaction, collect liquid, obtain crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, 20-24 hours static, three layers of distillate point；
(4) it takes distillate middle layer air-distillation 4-5 hours at 100-110 DEG C, collects condensate liquid, as acetum pyrolignosum rectificatum liquid.
7. a kind of preparation method of the glass cleaner containing wood vinegar as described in claim 1, which is characterized in that including with
Lower step：
(1) wood vinegar is prepared；
(2) trichorotrifluoroethane, hydroxyacetic acid are received, wood vinegar, triethanolamine, surfactant, caustic potash, sodium citrate,
Sulfamic acid, sodium nitrate, hydrogen peroxide and dimethyl succinate add water to be mixed, and stir as in rotating speed 250-350r/min, 85-
40-70min is reacted under conditions of 90 DEG C.
8. the preparation method of the glass cleaner according to claim 7 containing wood vinegar, which is characterized in that described plus water
Amount be 20-30 times of active constituent gross mass.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810153119.0A CN108441359A (en) | 2018-02-13 | 2018-02-13 | A kind of glass cleaner containing wood vinegar |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810153119.0A CN108441359A (en) | 2018-02-13 | 2018-02-13 | A kind of glass cleaner containing wood vinegar |
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| CN108441359A true CN108441359A (en) | 2018-08-24 |
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| CN201810153119.0A Pending CN108441359A (en) | 2018-02-13 | 2018-02-13 | A kind of glass cleaner containing wood vinegar |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111909676A (en) * | 2020-07-29 | 2020-11-10 | 四川圣诺油气工程技术服务有限公司 | Plugging remover for oil pipe of sulfur-containing gas well and preparation method thereof |
| CN114181788A (en) * | 2021-11-25 | 2022-03-15 | 万津实业(赤壁)有限公司 | Glass cleaning agent and preparation method and application thereof |
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| CN104342308A (en) * | 2014-10-26 | 2015-02-11 | 青岛智谷创新技术有限公司 | Traceless glass detergent |
| CN105062704A (en) * | 2015-08-13 | 2015-11-18 | 上海德联化工有限公司 | Glass cleaning agent |
| CN107118870A (en) * | 2017-06-13 | 2017-09-01 | 合肥钢骨玻璃制品有限公司 | A kind of glass cleaner and its preparation technology |
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| CN111909676A (en) * | 2020-07-29 | 2020-11-10 | 四川圣诺油气工程技术服务有限公司 | Plugging remover for oil pipe of sulfur-containing gas well and preparation method thereof |
| CN111909676B (en) * | 2020-07-29 | 2022-08-16 | 四川圣诺油气工程技术服务有限公司 | Plugging remover for oil pipe of sulfur-containing gas well and preparation method thereof |
| CN114181788A (en) * | 2021-11-25 | 2022-03-15 | 万津实业(赤壁)有限公司 | Glass cleaning agent and preparation method and application thereof |
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Application publication date: 20180824 |