CN108467801A - A kind of detergent containing wood vinegar - Google Patents
A kind of detergent containing wood vinegar Download PDFInfo
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- CN108467801A CN108467801A CN201810148601.5A CN201810148601A CN108467801A CN 108467801 A CN108467801 A CN 108467801A CN 201810148601 A CN201810148601 A CN 201810148601A CN 108467801 A CN108467801 A CN 108467801A
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- wood vinegar
- containing wood
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- benzotriazole
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/06—Phosphates, including polyphosphates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2082—Polycarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/28—Heterocyclic compounds containing nitrogen in the ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/30—Amines; Substituted amines ; Quaternized amines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3707—Polyethers, e.g. polyalkyleneoxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3942—Inorganic per-compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Abstract
The invention discloses a kind of detergents containing wood vinegar, are mainly made of following active constituent：Acetic acid polyoxyethylene ester, sodium molybdate, wood vinegar, triethanolamine, surfactant, benzotriazole, butyl ester, sodium tripolyphosphate, oxalic acid, hydrogen peroxide and and Tea Saponin.The glass cleaner of the present invention, containing wood vinegar, by the synergistic effect of wood vinegar and other substances, cleaning efficiency is high, significantly shortens scavenging period, and can substantially reduce reagent consumption amount.Cleaning efficiency is high, and cleaning effect is good.
Description
Technical field
The present invention relates to cleaning agent field, more particularly to a kind of detergent containing wood vinegar.
Background technology
Glass outside window, due to for a long time by expose to the weather and air in the pollutions such as harmful gas and oil smoke
With the erosion of chemical reaction, the stain being difficult to clean off together is formed already.So that skin produces dirt and wind
Change, had not only affected the beautiful and appearance of the city of building, but also damaged building.Therefore, the exterior wall of building is cleaned, is not only beautified
Environment, and play the role of protecting building.After glass dirt, it is necessary to use glass cleaner, however current glass
The cleaning performance of glass cleaning agent is bad, and cost is higher.
Being disclosed in the information of the background technology part, it is only intended to increase understanding of the overall background of the invention, without answering
It has been the prior art well known to persons skilled in the art when being considered as recognizing or imply that the information is constituted in any form.
Invention content
The purpose of the present invention is to provide a kind of detergents containing wood vinegar, to overcome cleaning agent of high cost, cleaning
The bad disadvantage of effect.
To achieve the above object, the present invention provides a kind of detergents containing wood vinegar, mainly by following active constituent
It is made：Acetic acid polyoxyethylene ester, sodium molybdate, wood vinegar, triethanolamine, surfactant, benzotriazole, butyl ester, trimerization phosphorus
Sour sodium, oxalic acid, hydrogen peroxide and and Tea Saponin.
Preferably, in above-mentioned technical proposal, the detergent containing wood vinegar is counted in parts by weight, mainly by with
Lower active constituent is made：4-9 parts of acetic acid polyoxyethylene ester, 3-6 parts of sodium molybdate, 9-16 parts of wood vinegar, 7-12 parts of triethanolamine, table
Activating agent 3-7 parts of face, 5-10 parts of benzotriazole, 1-4 parts of butyl ester, 2-6 parts of sodium tripolyphosphate, 1-3 parts of oxalic acid, hydrogen peroxide 4-8
Part and with 1-3 parts of Tea Saponin.
Preferably, in above-mentioned technical proposal, the detergent containing wood vinegar is counted in parts by weight, mainly by with
Lower active constituent is made：6 parts of acetic acid polyoxyethylene ester, 5 parts of sodium molybdate, 12 parts of wood vinegar, 10 parts of triethanolamine, surfactant
6 parts, 7 parts of benzotriazole, 3 parts of butyl ester, 5 parts of sodium tripolyphosphate, 2 parts of oxalic acid, 6 parts of hydrogen peroxide and with 2 parts of Tea Saponin.
Preferably, in above-mentioned technical proposal, the surfactant is fatty alcohol polyoxyethylene ether or polyoxyethylene nonyl phenyl second
Alkene ether.
Preferably, in above-mentioned technical proposal, the wood vinegar is the wood vinegar being prepared using peanut shell.
Preferably, in above-mentioned technical proposal, the preparation method of the wood vinegar includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 4-5 DEG C/min, it is gradually heating to 150-
200 DEG C, completely cut off air, heat resolve 2-4h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min,
The flue gas of generation imports refrigerator pipe liquefaction, collects liquid, obtains crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, 20-24 hours static, distillate point three
Layer；
(4) it takes distillate middle layer air-distillation 4-5 hours at 100-110 DEG C, collects condensate liquid, as acetum pyrolignosum rectificatum
Liquid.
A kind of preparation method of the detergent containing wood vinegar, includes the following steps：
(1) wood vinegar is prepared；
(2) by acetic acid polyoxyethylene ester, sodium molybdate, wood vinegar, triethanolamine, surfactant, benzotriazole, fourth
Ester, sodium tripolyphosphate, oxalic acid, hydrogen peroxide and add water to be mixed with Tea Saponin, stirs as in rotating speed 250-350r/min, 85-
40-70min is reacted under conditions of 90 DEG C.
Preferably, in above-mentioned technical proposal, described plus water amount is 20-30 times of active constituent gross mass.
Compared with prior art, the present invention has the advantages that：The glass cleaner of the present invention, containing wood vinegar,
By the synergistic effect of wood vinegar and other substances, cleaning efficiency is high, significantly shortens scavenging period, and can substantially reduce medicament and disappear
Consumption.Cleaning efficiency is high, and cleaning effect is good.
Specific implementation mode
With reference to specific embodiment, the specific implementation mode of the present invention is described in detail, it is to be understood that this hair
Bright protection domain is not restricted by specific implementation.
Embodiment 1
A kind of detergent containing wood vinegar, is counted in parts by weight, is mainly made of following active constituent：Acetic acid polyoxy second
6 parts of enester, 5 parts of sodium molybdate, 12 parts of wood vinegar, 10 parts of triethanolamine, 6 parts of surfactant, 7 parts of benzotriazole, butyl ester 3
Part, 5 parts of sodium tripolyphosphate, 2 parts of oxalic acid, 6 parts of hydrogen peroxide and with 2 parts of Tea Saponin.
The surfactant is nonylphenol polyoxyethylene ether.
A kind of preparation method of the detergent containing wood vinegar, includes the following steps：
Prepare wood vinegar；
The preparation method of the wood vinegar includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 4 DEG C/min, 180 DEG C are gradually heating to,
Completely cut off air, heat resolve 3h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min,
The flue gas of generation imports refrigerator pipe liquefaction, collects liquid, obtains crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, static 23 hours, three layers of distillate point；
(4) distillate middle layer air-distillation 4 hours at 100-110 DEG C are taken, condensate liquid, as acetum pyrolignosum rectificatum are collected
Liquid.
Prepare glass cleaner
By acetic acid polyoxyethylene ester, sodium molybdate, wood vinegar, triethanolamine, surfactant, benzotriazole, butyl ester, three
It polyphosphate sodium, oxalic acid, hydrogen peroxide and is mixed with Tea Saponin, 25 times of water is added and are mixed, stir as in rotating speed 250-350r/
60min is reacted under conditions of min, 85-90 DEG C.
Using cleaning agent made from the present embodiment, by cleaning agent for cleaning glassware.Glassware is handled,
Take the glass of 10cm × 10cm, check weighing W1, the dirt of one layer about 30 grams of coating, roasts 1 hour, check weighing at 120 DEG C on glass
4 grams of detergents containing wood vinegar are uniformly sprayed solarization on glass, are placed at room temperature to natural cooling, then in normal-temperature water by W2
It is rinsed with sponge under flowing, then dries glass, check weighing W3.By gravimetric method, soil removal efficiency is obtained.
Above-mentioned dirt percentage, is made of following component：21% lard, 26% vegetable oil, 15% flour,
15% lanolin, 16% industrial vaseline, 7% particulate sugar.
Test result：Soil removal efficiency is 96.9%.
Embodiment 2
A kind of detergent containing wood vinegar, is counted in parts by weight, is mainly made of following active constituent：Acetic acid polyoxy second
4 parts of enester, 6 parts of sodium molybdate, 16 parts of wood vinegar, 7 parts of triethanolamine, 7 parts of surfactant, 5 parts of benzotriazole, 4 parts of butyl ester,
6 parts of sodium tripolyphosphate, 3 parts of oxalic acid, 4 parts of hydrogen peroxide and with 3 parts of Tea Saponin.
The surfactant is fatty alcohol polyoxyethylene ether.
A kind of preparation method of the detergent containing wood vinegar, includes the following steps：
Prepare wood vinegar；
The preparation method of the wood vinegar includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 4 DEG C/min, 150 DEG C are gradually heating to,
Completely cut off air, heat resolve 4h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min,
The flue gas of generation imports refrigerator pipe liquefaction, collects liquid, obtains crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, static 24 hours, three layers of distillate point；
(4) distillate middle layer air-distillation 5 hours at 100-110 DEG C are taken, condensate liquid, as acetum pyrolignosum rectificatum are collected
Liquid.
Prepare glass cleaner
By acetic acid polyoxyethylene ester, sodium molybdate, wood vinegar, triethanolamine, surfactant, benzotriazole, butyl ester, three
It polyphosphate sodium, oxalic acid, hydrogen peroxide and is mixed with Tea Saponin, 30 times of water is added and are mixed, stir as in rotating speed 250-350r/
70min is reacted under conditions of min, 85-90 DEG C.
Using cleaning agent made from the present embodiment, by cleaning agent for cleaning glassware.Glassware is handled,
Take the glass of 10cm × 10cm, check weighing W1, the dirt of one layer about 30 grams of coating, roasts 1 hour, check weighing at 120 DEG C on glass
4 grams of detergents containing wood vinegar are uniformly sprayed solarization on glass, are placed at room temperature to natural cooling, then in normal-temperature water by W2
It is rinsed with sponge under flowing, then dries glass, check weighing W3.By gravimetric method, soil removal efficiency is obtained.
Above-mentioned dirt percentage, is made of following component：21% lard, 26% vegetable oil, 15% flour,
15% lanolin, 16% industrial vaseline, 7% particulate sugar.
Test result：Soil removal efficiency is 95.8%.
Embodiment 3
A kind of detergent containing wood vinegar, is counted in parts by weight, is mainly made of following active constituent：Acetic acid polyoxy second
9 parts of enester, 3 parts of sodium molybdate, 9 parts of wood vinegar, 12 parts of triethanolamine, 3 parts of surfactant, 10 parts of benzotriazole, butyl ester 1
Part, 2 parts of sodium tripolyphosphate, 1 part of oxalic acid, 8 parts of hydrogen peroxide and with 1 part of Tea Saponin.
The surfactant is fatty alcohol polyoxyethylene ether.
A kind of preparation method of the detergent containing wood vinegar, includes the following steps：
Prepare wood vinegar；
The preparation method of the wood vinegar includes the following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 5 DEG C/min, 200 DEG C are gradually heating to,
Completely cut off air, heat resolve 2h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min,
The flue gas of generation imports refrigerator pipe liquefaction, collects liquid, obtains crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, static 20 hours, three layers of distillate point；
(4) distillate middle layer air-distillation 4 hours at 100-110 DEG C are taken, condensate liquid, as acetum pyrolignosum rectificatum are collected
Liquid.
Prepare glass cleaner
By acetic acid polyoxyethylene ester, sodium molybdate, wood vinegar, triethanolamine, surfactant, benzotriazole, butyl ester, three
It polyphosphate sodium, oxalic acid, hydrogen peroxide and is mixed with Tea Saponin, 20 times of water is added and are mixed, stir as in rotating speed 250-350r/
40min is reacted under conditions of min, 85-90 DEG C.
Using cleaning agent made from the present embodiment, by cleaning agent for cleaning glassware.Glassware is handled,
Take the glass of 10cm × 10cm, check weighing W1, the dirt of one layer about 30 grams of coating, roasts 1 hour, check weighing at 120 DEG C on glass
4 grams of detergents containing wood vinegar are uniformly sprayed solarization on glass, are placed at room temperature to natural cooling, then in normal-temperature water by W2
It is rinsed with sponge under flowing, then dries glass, check weighing W3.By gravimetric method, soil removal efficiency is obtained.
Above-mentioned dirt percentage, is made of following component：21% lard, 26% vegetable oil, 15% flour,
15% lanolin, 16% industrial vaseline, 7% particulate sugar.
Test result：Soil removal efficiency is 96.4%.
Comparative example 1
A kind of detergent containing wood vinegar, is counted in parts by weight, is mainly made of following active constituent：Acetic acid polyoxy second
6 parts of enester, 5 parts of sodium molybdate, 10 parts of triethanolamine, 6 parts of surfactant, 7 parts of benzotriazole, 3 parts of butyl ester, sodium tripolyphosphate
6 parts of 5 parts, 2 parts of oxalic acid and hydrogen peroxide.
The surfactant is nonylphenol polyoxyethylene ether.
A kind of preparation method of the detergent containing wood vinegar, includes the following steps：By acetic acid polyoxyethylene ester, molybdic acid
Sodium, triethanolamine, surfactant, benzotriazole, butyl ester, sodium tripolyphosphate, oxalic acid and hydrogen peroxide mixing, are added 25 times of water
It is mixed, stirs to react 60min under conditions of rotating speed 250-350r/min, 85-90 DEG C.
Using cleaning agent made from the present embodiment, by cleaning agent for cleaning glassware.Glassware is handled,
Take the glass of 10cm × 10cm, check weighing W1, the dirt of one layer about 30 grams of coating, roasts 1 hour, check weighing at 120 DEG C on glass
4 grams of detergents containing wood vinegar are uniformly sprayed solarization on glass, are placed at room temperature to natural cooling, then in normal-temperature water by W2
It is rinsed with sponge under flowing, then dries glass, check weighing W3.By gravimetric method, soil removal efficiency is obtained.
Above-mentioned dirt percentage, is made of following component：21% lard, 26% vegetable oil, 15% flour,
15% lanolin, 16% industrial vaseline, 7% particulate sugar.
Test result：Soil removal efficiency is 81.8%.
The description of the aforementioned specific exemplary embodiment to the present invention is in order to illustrate and illustration purpose.These descriptions
It is not wishing to limit the invention to disclosed precise forms, and it will be apparent that according to the above instruction, can much be changed
And variation.The purpose of selecting and describing the exemplary embodiment is that explaining the specific principle of the present invention and its actually answering
With so that those skilled in the art can realize and utilize the present invention a variety of different exemplary implementation schemes and
Various chooses and changes.The scope of the present invention is intended to be limited by claims and its equivalents.
Claims (8)
1. a kind of detergent containing wood vinegar, which is characterized in that be mainly made of following active constituent：Acetic acid polyoxyethylene
Ester, sodium molybdate, wood vinegar, triethanolamine, surfactant, benzotriazole, butyl ester, sodium tripolyphosphate, oxalic acid, hydrogen peroxide and
And Tea Saponin.
2. the detergent according to claim 1 containing wood vinegar, which is characterized in that count in parts by weight, mainly by with
Lower active constituent is made：4-9 parts of acetic acid polyoxyethylene ester, 3-6 parts of sodium molybdate, 9-16 parts of wood vinegar, 7-12 parts of triethanolamine, table
Activating agent 3-7 parts of face, 5-10 parts of benzotriazole, 1-4 parts of butyl ester, 2-6 parts of sodium tripolyphosphate, 1-3 parts of oxalic acid, hydrogen peroxide 4-8
Part and with 1-3 parts of Tea Saponin.
3. the detergent according to claim 1 containing wood vinegar, which is characterized in that count in parts by weight, mainly by with
Lower active constituent is made：6 parts of acetic acid polyoxyethylene ester, 5 parts of sodium molybdate, 12 parts of wood vinegar, 10 parts of triethanolamine, surfactant
6 parts, 7 parts of benzotriazole, 3 parts of butyl ester, 5 parts of sodium tripolyphosphate, 2 parts of oxalic acid, 6 parts of hydrogen peroxide and with 2 parts of Tea Saponin.
4. the detergent according to claim 1 containing wood vinegar, which is characterized in that the surfactant is fatty alcohol
Polyoxyethylene ether or nonylphenol polyoxyethylene ether.
5. the detergent according to claim 1 containing wood vinegar, which is characterized in that the wood vinegar is to utilize peanut shell
The wood vinegar being prepared.
6. the detergent according to claim 1 containing wood vinegar, which is characterized in that the preparation method packet of the wood vinegar
Include following steps：
(1) peanut shell is placed in heat resolve in retort；With the heating rate of 4-5 DEG C/min, it is gradually heating to 150-200
DEG C, completely cut off air, heat resolve 2-4h；
(2) during temperature-rise period and heat resolve, the gas in reaction is flowed out with the flow of 0.1-0.3L/min, is generated
Flue gas import refrigerator pipe liquefaction, collect liquid, obtain crude peanut shell wood vinegar；
(3) crude peanut shell wood vinegar is taken to be evaporated under reduced pressure at 100-110 DEG C, 20-24 hours static, three layers of distillate point；
(4) it takes distillate middle layer air-distillation 4-5 hours at 100-110 DEG C, collects condensate liquid, as acetum pyrolignosum rectificatum liquid.
7. a kind of preparation method of the detergent containing wood vinegar as described in claim 1, which is characterized in that including following step
Suddenly：
(1) wood vinegar is prepared；
(2) by acetic acid polyoxyethylene ester, sodium molybdate, wood vinegar, triethanolamine, surfactant, benzotriazole, butyl ester, three
Polyphosphate sodium, oxalic acid, hydrogen peroxide and add water to be mixed with Tea Saponin, stirs as in rotating speed 250-350r/min, 85-90 DEG C
Under the conditions of react 40-70min.
8. the preparation method of the detergent according to claim 7 containing wood vinegar, which is characterized in that described plus water amount
It is 20-30 times of active constituent gross mass.
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| CN201810148601.5A CN108467801A (en) | 2018-02-13 | 2018-02-13 | A kind of detergent containing wood vinegar |
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| CN201810148601.5A CN108467801A (en) | 2018-02-13 | 2018-02-13 | A kind of detergent containing wood vinegar |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112795439A (en) * | 2020-12-15 | 2021-05-14 | 黑龙江边外香农业有限责任公司 | Efficient deoiling agent and preparation method thereof |
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