CN108410274A - A kind of aqua type solid vehicle glazing protection wax and preparation method thereof - Google Patents
A kind of aqua type solid vehicle glazing protection wax and preparation method thereof Download PDFInfo
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- CN108410274A CN108410274A CN201710200797.3A CN201710200797A CN108410274A CN 108410274 A CN108410274 A CN 108410274A CN 201710200797 A CN201710200797 A CN 201710200797A CN 108410274 A CN108410274 A CN 108410274A
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- Prior art keywords
- wax
- vehicle glazing
- aqua type
- type solid
- solid vehicle
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D123/00—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers
- C09D123/02—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
- C09D123/04—Homopolymers or copolymers of ethene
- C09D123/06—Polyethene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
- C09D191/06—Waxes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/08—Other polishing compositions based on wax
- C09G1/10—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin
- C09G1/12—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin mixtures of wax and silicon-containing polycondensates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Cosmetics (AREA)
Abstract
A kind of aqua type solid vehicle glazing protection wax and preparation method thereof, the present invention relates to Motor Maintenance technical fields；It is by following mass percent at being grouped as：Polyethylene synthetic wax 5.0 10.0%, paraffin 3.0 8.0%, microwax 3.0 8.0%, Brazil wax 5.0 10.0%, methyl phenyl silicone oil 2.0 8.0%, fluorine silicon resin 2.0 3.0%, anion surfactant 1.0 2.0%, nonionic surfactant 1.0 2.0%, deionized water 40 60%, dispersant 1.0 2.0%, yellow uitramarine 0.1%, acrylic copolymer 1.0 5.0%.The characteristic that the stability of wax is good, hydrophobicity is good, glazing guard time is lasting not only is protected with general pure solvent solid vehicle glazing, but also substantially reduces cost, improves environmental-protecting performance；Increase the security performance of storage and transport.
Description
Technical field
The present invention relates to Motor Maintenance technical fields, and in particular to a kind of aqua type solid vehicle glazing protection wax and its system
Preparation Method.
Background technology
With the rapid development of auto industry, people increasingly pay attention to automobile maintenance, Car polish and polishing agent
The market demand of product is vigorous.The widely used vehicle glazing of domestic market protects wax, mainly pure solvent solid vapour
Vehicle glazing protects wax, oil-in-water (0/W) emulsifying liquid or lotion vehicle glazing to protect wax.The solid wax of pure solvent vehicle glazing protection
Although hydrophobicity is good, guard time is lasting, product is stablized, due to using a large amount of solvents, product cost higher and not environmentally, no
Only unpleasant taste has certain stimulation to skin, eyes and whirling road, while can also discharge a large amount of VOC (Volatile
Organic Compounds), pollution is also resulted in environment, and storing and in transportational process, having prodigious dangerous hidden danger,
Therefore on the basis of existing vehicle glazing protects wax, the technical issues that need to address are to keep dredging for solid automobile polish
Its environmental-protecting performance how is improved on the basis of aqueous, persistence and stability, reduces product cost.
Invention content
In view of the defects and deficiencies of the prior art, the present invention intends to provide a kind of reasonable designs, easy to make
Aqua type solid vehicle glazing protects wax and preparation method thereof, not only with general pure solvent solid vehicle glazing protection wax
The characteristic that stability is good, hydrophobicity is good, glazing guard time is lasting, and cost is substantially reduced, improve environmental-protecting performance；Increase storage
The security performance deposited and transported.
To achieve the above object, heretofore described aqua type solid vehicle glazing protects wax, it is by following quality hundred
Point ratio at being grouped as：Polyethylene synthetic wax 5.0-10.0%, paraffin 3.0-8.0%, microwax 3.0-8.0%, babassu
Wax 5.0-10.0%, methyl phenyl silicone oil 2.0-8.0%, fluorine silicon resin 2.0-3.0%, anion surfactant 1.0-
2.0%, nonionic surfactant 1.0-2.0%, deionized water 40-60%, dispersant 1.0-2.0%, yellow uitramarine (HC
Yellow 13) 0.1%, acrylic copolymer 1.0-5.0%.
Further, the nonionic surfactant is polyoxethylene octylphenyl phenol ether -10 (OP-10), fatty alcohol
Polyoxyethylene ether (AEO-9), polyoxyethylene sorbitan monooleate (Tween-80), abbreviation Tween-80 or coconut palm
One or more mixtures in seed oil fatty diglycollic amide (6501)；Wherein, -10 (OP- of polyoxethylene octylphenyl phenol ether
10) pH value (1% aqueous) is 6-7, and hydrophilic lipophilic balance (HLB) is 14.5；Fatty alcohol polyoxyethylene ether (AEO-9)
PH value is that 5.0-7.0 hydrophilic lipophilic balances (HLB) are 12-13.
Further, the anion surfactant is lauryl sodium sulfate (K12), neopelex
(LAS), one or more mixtures in alpha-olefin sodium sulfonate (AOS) or enuatrol, wherein lauryl sodium sulfate (K12)
PH be 6.5-7.5；The hydrophilic lipophilic balance (HLB) of neopelex (LAS) is 10.6.
The preparation method of heretofore described aqua type solid vehicle glazing protection wax, preparation process are as follows：
One, on the basis of the total weight that aqua type solid vehicle glazing obtained protects wax, polyethylene synthetic wax is weighed
5.0-10.0%, paraffin 3.0-8.0%, microwax 3.0-8.0%, Brazil wax 5.0-10.0% and partial deionized water
(20-40% for accounting for ion water inventory), is stirred and is heated to 90-100 DEG C, until material dissolution is uniform；
Two, on the basis of the total weight that last aqua type solid vehicle glazing obtained protects wax, aminomethyl phenyl silicon is weighed
Oily 2.0-8.0%, fluorine silicon resin 2.0-3.0%, anion surfactant 1.0-2.0%, nonionic surfactant 1.0-
2.0%, dispersant 1.0-2.0%, yellow uitramarine (HC Yellow 13) 0.1%, acrylic copolymer 1.0-5.0% and residue
Deionized water, be heated with stirring to 90-100 DEG C, be uniformly mixed, dispersion and emulsion react about 20 minutes, keep its emulsion reaction abundant
Uniformly；
Three, the uniform mixed liquor of above-mentioned emulsification is dispersed with stirring after being cooled to 65-70 DEG C, discharging is canned, is down to room naturally
Temperature is packed after being condensed into solid-like, and the aqua type vehicle glazing is made and protects wax.
The present invention has the beneficial effect that：
1, it using the emulsifier of a variety of different structures, and is protected by specific emulsifying process aqueous solid vehicle glazing
Wax, not only there is general pure solvent solid vehicle glazing to protect, and the stability of wax is good, hydrophobicity is good, glazing guard time is lasting
Characteristic, and replace petroleum hydrocarbon solvent as a result of water, substantially reduce cost, there is no smell, eliminate petroleum hydrocarbon
The toxicity that aromatic hydrocarbons contained by solvent is brought there is no VOC emission, improve environmental-protecting performance；
2, it is changed into the automobile polish using water as solvent using automobile polish made from organic solvent by traditional, avoids
Fire hazard and petroleum hydrocarbon solvent in production process are in heating volatilization process to the pollution of air and to direct labor's
Health hazard；
3, automobile polish is changed into non-dangerous article by the dangerous material for storing and transporting；
4, can have good water proofing property on the car body, there is lasting light, can car surface formed one layer it is hard
Protective film has good protective effect to automobile.
Figure of description：
Fig. 1 is the performance comparison table of each embodiment.
Specific implementation mode
Aqua type solid vehicle glazing described in specific implementation mode (embodiment one) protects wax, it is by following quality hundred
Point ratio at being grouped as：Polyethylene synthetic wax 6.0%, paraffin 3.0%, microwax 5.0%, Brazil wax 5.0%, methylbenzene
Base silicone oil 3.0%, fluorine silicon resin 2.0%, acrylic copolymer 2.0%, dispersant 1.0%, polyoxethylene octylphenyl phenol ether -10
(OP-10) 1.0%, fatty alcohol polyoxyethylene ether (AEO-9) 0.4%, lauryl sodium sulfate (K12) 0.5%, deionized water
72%.
The preparation method of aqua type solid vehicle glazing protection wax described in the present embodiment, preparation process are as follows：
One, on the basis of the total weight that aqua type solid vehicle glazing obtained protects wax, polyethylene synthetic wax is weighed
6.0%, paraffin 3.0%, microwax 5.0%, the deionized water of Brazil wax 5.0% and 30% are stirred and are heated to 90-
100 DEG C, until material dissolution is uniform；
Two, on the basis of the total weight that last aqua type solid vehicle glazing obtained protects wax, aminomethyl phenyl silicon is weighed
Oil 3.0%, fluorine silicon resin 2.0%, acrylic copolymer 2.0%, dispersant 1.0%, -10 (OP- of polyoxethylene octylphenyl phenol ether
10) 1.0%, fatty alcohol polyoxyethylene ether (AEO-9) 0.4%, lauryl sodium sulfate (K12) 0.5% and remainder are gone
Ionized water is heated with stirring to 90-100 DEG C, is uniformly mixed, and dispersion and emulsion reacts about 20 minutes, keeps its emulsion reaction full and uniform；
Three, the uniform mixed liquor of above-mentioned emulsification is dispersed with stirring after being cooled to 65-70 DEG C, discharging is canned, is down to room naturally
Temperature is packed after being condensed into solid-like, and the aqua type vehicle glazing is made and protects wax.
The present embodiment has the beneficial effect that：It not only protects the stability of wax with general pure solvent solid vehicle glazing
The characteristic good, hydrophobicity is good, glazing guard time is lasting, and cost is substantially reduced, improve environmental-protecting performance；Increase storage and fortune
Defeated security performance.
Embodiment two：
Aqua type solid vehicle glazing described in the present embodiment protects wax, it is by following mass percent at grouping
At：Polyethylene synthetic wax 8.0%, paraffin 3.0%, microwax 4.0%, Brazil wax 6.0%, methyl phenyl silicone oil 2.0%,
Fluorine silicon resin 2.0%, acrylic copolymer 2.0%, dispersant 1.0%, yellow uitramarine (HC Yellow 13) 0.1%, polyoxy
- 10 (OP-10) 0.5% of ethylene octyl phenol ether, cocoanut fatty acid diethanolamide (6501) 0.5%, detergent alkylate sulphur
Sour sodium (LAS) 0.5%, deionized water 70.4%.
The preparation method of aqua type solid vehicle glazing protection wax described in the present embodiment, preparation process are as follows：
One, on the basis of the total weight that aqua type solid vehicle glazing obtained protects wax, polyethylene synthetic wax is weighed
8.0%, the deionized water of paraffin 3.0%, microwax 4.0%, Brazil wax 6.0% and 30%, is stirred and is heated to 90-
100 DEG C, until material dissolution is uniform；
Two, on the basis of the total weight that last aqua type solid vehicle glazing obtained protects wax, aminomethyl phenyl silicon is weighed
Oil 2.0%, fluorine silicon resin 2.0%, acrylic copolymer 2.0%, dispersant 1.0%, yellow uitramarine (HC Yellow 13)
0.1%, polyoxethylene octylphenyl phenol ether -10 (OP-10) 0.5%, cocoanut fatty acid diethanolamide (6501) 0.5%, ten
The deionized water of dialkyl benzene sulfonic acids sodium (LAS) 0.5% and remainder, is heated with stirring to 90-100 DEG C, is uniformly mixed, dispersion
Emulsion reaction about 20 minutes, keeps its emulsion reaction full and uniform；
Three, the uniform mixed liquor of above-mentioned emulsification is dispersed with stirring after being cooled to 65-70 DEG C, discharging is canned, is down to room naturally
Temperature is packed after being condensed into solid-like, and the aqua type vehicle glazing is made and protects wax.
Embodiment three：
Aqua type solid vehicle glazing described in this implementation protects wax, it is by following mass percent at being grouped as：
Polyethylene synthetic wax 7.0%, paraffin 3.0%, microwax 5.0%, Brazil wax 7.0%, methyl phenyl silicone oil 2.0%, fluorine
Silicones 2.0%, acrylic copolymer 2.0%, dispersant 1.0%, yellow uitramarine (HC Yellow 13) 0.1%, fatty alcohol
Polyoxyethylene ether (AEO-9) 0.5%, polyoxyethylene sorbitan monooleate) (Tween-80) 0.5%, enuatrol 0.5%,
Deionized water 69.4%.
The preparation method of aqua type solid vehicle glazing protection wax described in the present embodiment, preparation process are as follows：
One, on the basis of the total weight that aqua type solid vehicle glazing obtained protects wax, polyethylene synthetic wax is weighed
7.0%, the deionized water of paraffin 3.0%, microwax 5.0%, Brazil wax 7.0% and 30%, is stirred and is heated to 90-
100 DEG C, until material dissolution is uniform；
Two, on the basis of the total weight that last aqua type solid vehicle glazing obtained protects wax, aminomethyl phenyl silicon is weighed
Oil 2.0%, fluorine silicon resin 2.0%, acrylic copolymer 2.0%, dispersant 1.0%, yellow uitramarine (HC Yellow 13)
0.1%, fatty alcohol polyoxyethylene ether (AEO-9) 0.5%, polyoxyethylene sorbitan monooleate) (Tween-80) 0.5%,
The deionized water of enuatrol 0.5% and remainder, is heated with stirring to 90-100 DEG C, is uniformly mixed, dispersion and emulsion reaction about 20
Minute, keep its emulsion reaction full and uniform；
Three, the uniform mixed liquor of above-mentioned emulsification is dispersed with stirring after being cooled to 65-70 DEG C, discharging is canned, is down to room naturally
Temperature is packed after being condensed into solid-like, and the aqua type vehicle glazing is made and protects wax.
Example IV：
Aqua type solid vehicle glazing described in the present embodiment protects wax, it is by following mass percent at grouping
At：Polyethylene synthetic wax 5.0%, paraffin 4.0%, microwax 6.0%, Brazil wax 6.0%, methyl phenyl silicone oil 2.0%,
Fluorine silicon resin 2.0%, acrylic copolymer 2.0%, dispersant 1.0%, yellow uitramarine (HC Yellow 13) 0.1%, coconut
Fatty acid oil diglycollic amide (6501) 0.5%, polyoxyethylene sorbitan monooleate) (Tween-80) 0.5%, α-alkene
Hydrocarbon sulfonate sodium (AOS) 0.5%, deionized water 70.4%.
The preparation method of aqua type solid vehicle glazing protection wax described in the present embodiment, preparation process are as follows：
One, on the basis of the total weight that aqua type solid vehicle glazing obtained protects wax, polyethylene synthetic wax is weighed
5.0%, the deionized water of paraffin 4.0%, microwax 6.0%, Brazil wax 6.0% and 30%, is stirred and is heated to 90-
100 DEG C, until material dissolution is uniform；
Two, on the basis of the total weight that last aqua type solid vehicle glazing obtained protects wax, aminomethyl phenyl silicon is weighed
Oil 2.0%, fluorine silicon resin 2.0%, acrylic copolymer 2.0%, dispersant 1.0%, yellow uitramarine (HC Yellow 13)
0.1%, cocoanut fatty acid diethanolamide (6501) 0.5%, polyoxyethylene sorbitan monooleate) (Tween-80)
0.5%, the deionized water of alpha-olefin sodium sulfonate (AOS) 0.5% and remainder, is heated with stirring to 90-100 DEG C, is uniformly mixed,
Dispersion and emulsion reacts about 20 minutes, keeps its emulsion reaction full and uniform；
Three, the uniform mixed liquor of above-mentioned emulsification is dispersed with stirring after being cooled to 65-70 DEG C, discharging is canned, is down to room naturally
Temperature is packed after being condensed into solid-like, and the aqua type vehicle glazing is made and protects wax.
Aqua type solid vehicle glazing protection wax obtained in above-described embodiment is subjected to outer tube, smell, color and luster, glossiness
Value added, coating expansion easness and the comparison for wiping easness, obtain Fig. 1.
The above is merely illustrative of the technical solution of the present invention and unrestricted, and those of ordinary skill in the art are to this hair
The other modifications or equivalent replacement that bright technical solution is made, as long as it does not depart from the spirit and scope of the technical scheme of the present invention,
It is intended to be within the scope of the claims of the invention.
Claims (4)
1. a kind of aqua type solid vehicle glazing protects wax, it is characterised in that：It is by following mass percent at being grouped as：It is poly-
Ethylene synthase wax 5.0-10.0%, paraffin 3.0-8.0%, microwax 3.0-8.0%, Brazil wax 5.0-10.0%, methyl
Phenyl silicone oil 2.0-8.0%, fluorine silicon resin 2.0-3.0%, anion surfactant 1.0-2.0%, non-ionic surface active
Agent 1.0-2.0%, deionized water 40-60%, dispersant 1.0-2.0%, yellow uitramarine 0.1%, acrylic copolymer 1.0-
5.0%.
2. a kind of aqua type solid vehicle glazing according to claim 1 protects wax, it is characterised in that：The nonionic
Surfactant is polyoxethylene octylphenyl phenol ether -10, fatty alcohol polyoxyethylene ether, polyoxyethylene sorbitan monooleate
Or one or more mixtures in cocoanut fatty acid diethanolamide；Wherein, the pH of polyoxethylene octylphenyl phenol ether -10
Value is 6-7, hydrophilic lipophilic balance 14.5；The pH value of fatty alcohol polyoxyethylene ether is that 5.0-7.0 hydrophilic lipophilic balances are
12-13。
3. a kind of aqua type solid vehicle glazing according to claim 1 protects wax, it is characterised in that：The anion
Surfactant is lauryl sodium sulfate, neopelex, alpha-olefin sodium sulfonate or one kind or more in enuatrol
Kind mixture, wherein the pH of lauryl sodium sulfate is 6.5-7.5；The hydrophilic lipophilic balance of neopelex is
10.6。
4. a kind of preparation method of aqua type solid vehicle glazing protection wax, it is characterised in that：Preparation process is as follows：
(1), on the basis of the total weight that aqua type solid vehicle glazing obtained protects wax, polyethylene synthetic wax 5.0- is weighed
10.0%, paraffin 3.0-8.0%, microwax 3.0-8.0%, Brazil wax 5.0-10.0% and partial deionized water, account for
The 20-40% of deionized water total amount, is stirred and is heated to 90-100 DEG C, until material dissolution is uniform；
(2), on the basis of the total weight that last aqua type solid vehicle glazing obtained protects wax, methyl phenyl silicone oil is weighed
2.0-8.0%, fluorine silicon resin 2.0-3.0%, anion surfactant 1.0-2.0%, nonionic surfactant 1.0-
2.0%, dispersant 1.0-2.0%, yellow uitramarine 0.1%, acrylic copolymer 1.0-5.0% and remaining deionized water, are stirred
It mixes and is heated to 90-100 DEG C, be uniformly mixed, dispersion and emulsion reacts about 20 minutes, keeps its emulsion reaction full and uniform；
(3), the uniform mixed liquor of above-mentioned emulsification is dispersed with stirring after being cooled to 65-70 DEG C, discharging is canned, is down to room temperature naturally
It is packed after being condensed into solid-like, the aqua type vehicle glazing is made and protects wax.
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| CN201710200797.3A CN108410274A (en) | 2017-03-30 | 2017-03-30 | A kind of aqua type solid vehicle glazing protection wax and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710200797.3A CN108410274A (en) | 2017-03-30 | 2017-03-30 | A kind of aqua type solid vehicle glazing protection wax and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111303767A (en) * | 2020-03-26 | 2020-06-19 | 北京京蝠环保科技有限公司 | Tire glazing glaze |
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| CN1766023A (en) * | 2004-10-29 | 2006-05-03 | 中国石油化工股份有限公司 | Water-based rust-proofing protecting wax agent and its preparation method |
| US20090269290A1 (en) * | 2008-04-25 | 2009-10-29 | Diahne Patnode | Melt formula |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111303767A (en) * | 2020-03-26 | 2020-06-19 | 北京京蝠环保科技有限公司 | Tire glazing glaze |
| CN111303767B (en) * | 2020-03-26 | 2021-11-16 | 北京京蝠环保科技有限公司 | Tire glazing glaze |
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Application publication date: 20180817 |
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