CN103756486B - A kind of aqueous colorful building coating and preparation method - Google Patents

A kind of aqueous colorful building coating and preparation method Download PDF

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CN103756486B
CN103756486B CN201410029110.0A CN201410029110A CN103756486B CN 103756486 B CN103756486 B CN 103756486B CN 201410029110 A CN201410029110 A CN 201410029110A CN 103756486 B CN103756486 B CN 103756486B
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parts
deionized water
prepared
varnish
sol solution
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CN201410029110.0A
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CN103756486A (en
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陈明凤
胡启良
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重庆美斯丽涂料有限公司
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Abstract

The invention discloses a kind of aqueous colorful building coating and preparation method, its composition and mass fraction ratio are: varnish 3-8 part, color grain 100 parts;Its making step is followed successively by: the preparation of (1) 10% protection sol solution;(2) preparation of white basis paint;(3) toning;(4) preparation of disperse medium;(5) preparation of varnish;(6) preparation of color grain;Finally prepare this aqueous colorful building coating。Coating prepared by the present invention will not bond agglomerating, float or sink, between color grain not colour contamination, sharpness of border;Coating system viscosity stabilization, thickening behavior without issue;Color grain intensity is high, pliable and tough, and size shape is adjustable, and multiple different colours coloured silk grain can arbitrary proportion collocation mixing;Once spraying gets final product imitation granite true to nature and marmorean effect and texture, meets the imitative stone finishing requirements of the colorful floral designs of external wall。

Description

A kind of aqueous colorful building coating and preparation method
Technical field
The present invention relates to building coating technical field, particularly relate to a kind of aqueous colorful building coating and preparation method。
Background technology
In recent years, External Thermal Insulation Technology for External has become the mainstream technology of China's building energy conservation, and owing to external thermal insulation bearing capacity is more weak, the exterior coating therefore with advantages such as light weight, environmental protection, safety, easy renovations has become the main way of current exterior wall finish。But generic latex paint color is single, it is impossible to realize the finishing requirements of the imitative stone material of external wall。The color true mineral varnish preparation process of sandstone sheet is complicated, and true mineral varnish consumption is big, and every square meter cost is high, and during spraying application, sliver and color sand splash down in a large number and causes waste。Oil-in-water type multicolor finish is containing toxic solvent, and environmental pollution is big, unfavorable environmental protection。At present on the market water type multicolor paint for water drum storage time easy to stick clump together, color grain floats or sinks, and affect the uniformity of coating, color grain intensity is low, it is impossible to bear vibration, collision, impact and spray gun pressure, causes easy colour contamination, obscurity boundary between coloured silk grain。After coating system, thickening is serious, it is impossible to spraying。
Summary of the invention
For prior art above shortcomings, the purpose of the present invention is that a kind of aqueous colorful building coating of offer and preparation method, to overcome the shortcoming and defect of existing product, meets decorating outer wall of building requirement;Will not bond agglomerating, float or sink, between color grain not colour contamination, sharpness of border;Coating system viscosity stabilization, thickening behavior without issue;Color grain intensity is high, pliable and tough, and size shape is adjustable, and multiple different colours coloured silk grain can arbitrary proportion collocation mixing。
To achieve these goals, the technical solution used in the present invention is such that a kind of aqueous colorful building coating, it is characterised in that: its composition and mass fraction ratio be: 3-8 part varnish, 100 parts of color grains;Wherein:
The composition of described varnish and mass fraction ratio be: 50-60 part deionized water, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 25-35 part styrene-acrylic emulsion, 1-3 part defoamer, 10-18 part alkali-soluble is swollen Polyacrylic Acid Thickener, 10-15 part polyurethane thickener;
Composition and the mass fraction ratio of described color grain be: 100 parts of disperse medium, 100 parts of colored base paints;
The composition of described disperse medium and mass fraction ratio be: 45-49 part deionized water, 0.5-1 part sodium pyrophosphate, 0.5-1 part sodium tripolyphosphate, 0.5-1 part sodium hexameta phosphate, 8-10 part lithium magnesium silicate, 45-55 part 10% concentration protection sol solution;
Described colored base paint, composition and mass fraction ratio be: 100 parts of white basis paints, 0.1-1 part mill base;
Composition and the mass fraction ratio of described white basis paint be: 60-65 part deionized water, 0.5-1 part make the ammonium polyacrylate salt of dispersant, 0.5-1 part makes the alkylphenol polyoxyethylene of wetting agent, 1-2 part makes the mineral oil of defoamer, 10-13 part hydroxyethyl cellulose, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 5-10 part propylene glycol, 10-20 part titanium dioxide, 10-30 part Kaolin, 20-30 part elastomeric propylene yogurt liquid, 1-3 part make the silicone oil of defoamer, 5-8 part 10% concentration protection sol solution;
The described 10% concentration protection composition of sol solution and mass fraction ratio be: 89.5-89 part deionized water, 0.5-1 part sodium pyrophosphate, 10 parts of lithium magnesium silicates。
The preparation method of a kind of above-mentioned aqueous colorful building coating, comprises the steps:
The preparation of (1) 10% protection sol solution: first add in a mixing bowl by 89.5-89 part deionized water, adds 0.5-1 part sodium pyrophosphate to being dissolved completely in water under 500r/min stirring at low speed;Add 10 parts of lithium magnesium silicate 1500r/min high-speed stirred more than 45min, then keep 500r/min stirring at low speed, standby;
(2) preparation of white basis paint: raw material and weight be: 60-65 part deionized water, 0.5-1 part makes the ammonium polyacrylate salt of dispersant, 0.5-1 part makes the alkylphenol polyoxyethylene of wetting agent, 1-2 part makes the mineral oil of defoamer, 10-13 part hydroxyethyl cellulose, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 5-10 part propylene glycol, 10-20 part titanium dioxide, 10-30 part Kaolin, 20-30 part elastomeric propylene yogurt liquid, 1-3 part makes the silicone oil of defoamer, the 10% concentration protection sol solution that 5-8 part is prepared by step (1), is placed in a mixing bowl by the raw material of above-mentioned weight, first adds deionized water, is then sequentially added into dispersant under 500 revs/min of rotating speeds, wetting agent, mineral oil antifoam agent, hydroxyethyl cellulose, pH adjusting agent, antibacterial, coalescents, propylene glycol, then carries rotating speed to 1200-1500 rev/min of addition titanium dioxide, Kaolin stirs 30 minutes, then rotating speed is down to the 500-600 rev/min of elastic pure-acrylic emulsion of addition and silicon oil foam killer stirs, and is eventually adding the 10% concentration protection sol solution prepared by step (1), continues to stir more than 30 minutes, standby;
(3) toning: by designing requirement, the white basis paint prepared with 100 parts of steps (2) mixes with 0.1-1 part mill base, stirs, furnishing colour base paint;
(4) preparation of disperse medium: raw material and weight are 45-49 part deionized waters, 0.5-1 part sodium pyrophosphate, 0.5-1 part sodium tripolyphosphate, 0.5-1 part sodium hexameta phosphate, 8-10 part lithium magnesium silicate, the 10% concentration protection sol solution that 45-55 part is prepared by step (1), in a mixing bowl, deionized water is first added by above-mentioned weight portion, by sodium pyrophosphate under stirring at 500 revs/min, sodium tripolyphosphate, sodium hexameta phosphate is added to the water, stirring is to being completely dissolved, it is eventually adding lithium magnesium silicate and the 10% concentration protection sol solution prepared by step (1) stirs more than 45 minutes at 1500 revs/min, standby;
(5) preparation of varnish: raw material and weight are 50-60 part deionized water, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 25-35 part styrene-acrylic emulsion, 1-3 part defoamer, 10-18 part alkali-soluble is swollen Polyacrylic Acid Thickener, 10-15 part polyurethane thickener, in a mixing bowl, deionized water is first added by above-mentioned weight portion, be sequentially added into pH adjusting agent, antibacterial, coalescents, styrene-acrylic emulsion, defoamer under stirring at 500 revs/min, alkali-soluble is swollen Polyacrylic Acid Thickener, polyurethane thickener stir, standby;
(6) preparation of color grain: raw material and weight are 100 parts of disperse medium prepared by step (4), 100 parts of monochromes prepared by step (3), secondary colour or polychrome base paints, open blender and monochrome, secondary colour or polychrome base paint are added in disperse medium, rotating speed 40 revs/min is not so that monochrome, secondary colour or polychrome base paint sink to being as the criterion, monochrome, secondary colour or polychrome base paint add rear rotating speed and carry to 90~130 revs/min, observe color grain particle diameter while stirring, until reaching designing requirement;
(7) last: raw material and weight are the varnish that 3-8 part is prepared by step (5), 100 parts of color grains prepared by step (6), open blender coloured silk grain addition varnish to stir and obtain this coating, rotating speed controls to be as the criterion just making color grain and varnish can stir evenly and not destroy color grain, if lacquering viscosity does not reach construction requirement can add the swollen Polyacrylic Acid Thickener adjustment of alkali-soluble in right amount, viscosity adjusts complete stopping immediately and stirs。
Compared with prior art, it is an advantage of the current invention that:
1, preparation technology is simple, and the general production equipment of general emulsion paint can be suitable for。
2, will not bond agglomerating, float or sink, between color grain not colour contamination, sharpness of border;Coating system viscosity stabilization, thickening behavior without issue;Color grain intensity is high, pliable and tough, and size shape is adjustable, and multiple different colours coloured silk grain can arbitrary proportion collocation mixing。
3, once spraying gets final product imitation granite true to nature and marmorean effect and texture, meets the imitative stone finishing requirements of the colorful floral designs of external wall。
Detailed description of the invention
Embodiment: a kind of aqueous colorful building coating, its composition and mass fraction ratio be: 3-8 part varnish, 100 parts of color grains。Wherein:
The composition of described varnish and mass fraction ratio be: 50-60 part deionized water, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 25-35 part styrene-acrylic emulsion, 1-3 part defoamer, 10-18 part alkali-soluble is swollen Polyacrylic Acid Thickener, 10-15 part polyurethane thickener。
Composition and the mass fraction ratio of described color grain be: 100 parts of disperse medium, 100 parts of colored base paints。
The composition of described disperse medium and mass fraction ratio be: 45-49 part deionized water, 0.5-1 part sodium pyrophosphate, 0.5-1 part sodium tripolyphosphate, 0.5-1 part sodium hexameta phosphate, 8-10 part lithium magnesium silicate, 45-55 part 10% concentration protection sol solution。
Described colored base paint, composition and mass fraction ratio be: 100 parts of white basis paints, 0.1-1 part mill base。
Composition and the mass fraction ratio of described white basis paint be: 60-65 part deionized water, 0.5-1 part make the ammonium polyacrylate salt of dispersant, 0.5-1 part makes the alkylphenol polyoxyethylene of wetting agent, 1-2 part makes the mineral oil of defoamer, 10-13 part hydroxyethyl cellulose, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 5-10 part propylene glycol, 10-20 part titanium dioxide, 10-30 part Kaolin, 20-30 part elastomeric propylene yogurt liquid, 1-3 part make the silicone oil of defoamer, 5-8 part 10% concentration protection sol solution。
The described 10% concentration protection composition of sol solution and mass fraction ratio be: 89.5-89 part deionized water, 0.5-1 part sodium pyrophosphate, 10 parts of lithium magnesium silicates。
A kind of above-mentioned aqueous colorful building coating and preparation method, comprise the steps:
The preparation of (1) 10% concentration protection sol solution: first 89.5-89 part deionized water is added in a mixing bowl, add 0.5-1 part sodium pyrophosphate under 500r/min stirring at low speed to being dissolved completely in water;It is slow added into 10 parts of lithium magnesium silicate 1500r/min high-speed stirred more than 45min, then keeps 500r/min stirring at low speed standby。
(2) preparation of white basis paint: raw material and weight are 60-65 part deionized waters, 0.5-1 part makes the ammonium polyacrylate salt of dispersant, 0.5-1 part makes the alkylphenol polyoxyethylene of wetting agent, 1-2 part makes the mineral oil of defoamer, 10-13 part hydroxyethyl cellulose, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 5-10 part propylene glycol, 10-20 part titanium dioxide, 10-30 part Kaolin, 20-30 part elastomeric propylene yogurt liquid, 1-3 part makes the silicone oil of defoamer, the 10% concentration protection sol solution that 5-8 part is prepared by step (1), first adds deionized water by above-mentioned weight portion, be sequentially added into dispersant under 500 revs/min of rotating speeds in a mixing bowl, wetting agent, mineral oil antifoam agent, hydroxyethyl cellulose, pH adjusting agent, antibacterial, coalescents, propylene glycol, carries rotating speed to 1200-1500 rev/min of addition titanium dioxide, Kaolin stirs 30 minutes, rotating speed is down to the 500-600 rev/min of elastic pure-acrylic emulsion of addition and silicon oil foam killer stirs, after being eventually adding the 10% concentration protection sol solution prepared by step (1), rotating speed brings up to and is as the criterion stirring, stirring and formation thixotroping body moist to perusal coating, the general used time is more than 30 minutes, standby。
(3) toning: by designing requirement, the white basis paint prepared with 100 parts of steps (2) mixes with 0.1-1 part mill base (red, yellow, blue or its combination), stir, furnishing colour base paint, distinguish furnishing colors base paint according to the above ratio with different monochromatic, secondary colours or polychrome。
(4) preparation of disperse medium: raw material and weight are 45-49 part deionized waters, 0.5-1 part sodium pyrophosphate, 0.5-1 part sodium tripolyphosphate, 0.5-1 part sodium hexameta phosphate, 8-10 part lithium magnesium silicate, the 10% concentration protection sol solution that 45-55 part is prepared by step (1), in a mixing bowl, deionized water is first added by above-mentioned weight portion, by sodium pyrophosphate under stirring at 500 revs/min, sodium tripolyphosphate, sodium hexameta phosphate is added to the water, stirring is to being completely dissolved, it is eventually adding lithium magnesium silicate and the 10% concentration protection sol solution prepared by step (1) is standby more than 45 minutes 1500 revs/min of stirrings。
(5) preparation of varnish: raw material and weight are 50-60 part deionized water, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 25-35 part styrene-acrylic emulsion, 1-3 part defoamer, 10-18 part alkali-soluble is swollen Polyacrylic Acid Thickener, 10-15 part polyurethane thickener, in a mixing bowl, first add deionized water by above-mentioned weight portion, be sequentially added into pH adjusting agent, antibacterial, coalescents, styrene-acrylic emulsion, defoamer under stirring at 500 revs/min, alkali-soluble is swollen Polyacrylic Acid Thickener, polyurethane thickener stir standby。
(6) preparation of color grain: raw material and weight are 100 parts of disperse medium prepared by step (4), 100 parts of monochromes prepared by step (3), secondary colour or polychrome base paints, open blender and monochrome, secondary colour or polychrome base paint are added in disperse medium, rotating speed 40 revs/min is not so that monochrome, secondary colour or polychrome base paint sink to being as the criterion, monochrome, secondary colour or polychrome base paint add rear rotating speed and carry to 90~130 revs/min, observe color grain particle diameter while stirring, until reaching designing requirement。
(7) preparation of water-soluble colorful coating: raw material and weight are the varnish that 3-8 part is prepared by step (5), 100 parts of color grains prepared by step (6), open blender coloured silk grain addition varnish to stir and obtain this coating, rotating speed controls to be as the criterion just making color grain and varnish can stir evenly and not destroy color grain, if lacquering viscosity does not reach construction requirement can add the swollen Polyacrylic Acid Thickener adjustment of alkali-soluble in right amount, viscosity adjusts complete stopping immediately and stirs。
Detailed description of the invention is as follows:
Table 1 is that 10% concentration protection sol solution prepares embodiment, raw material and weight proportion number list 1:
(table 1)
Table 2 is that white basis paint prepares embodiment, raw material and weight proportion number list 2:
(table 2)
Raw material 1 2 3 4
Deionized water 60 62 63 65
Ammonium polyacrylate salt 0.5 0.6 0.8 1.0
Alkylphenol polyoxyethylene 1 0.8 0.6 0.5
Mineral oil 1 1 2 2
Hydroxyethyl cellulose 12 11 13 10
PH adjusting agent 2 1 1 2
Titanium dioxide 20 15 10 10
Kaolin 10 15 20 30
Antibacterial 1 2 3 1
Coalescents 5 10 8 6
Propylene glycol 10 5 8 6
Elastomeric propylene yogurt liquid 20 30 25 25
Silicone oil 2 1 3 2
10% concentration protection sol solution 5 6 7 8
Table 3 is that colored base paint prepares embodiment, raw material and weight proportion number list 3:
(table 3)
Table 4 is that disperse medium prepares embodiment, raw material and weight proportion number list 4:
(table 4)
Table 5 is that varnish prepares embodiment, raw material and weight proportion number list 5:
(table 5)
Table 6 is that water-soluble colorful coating prepares embodiment, raw material and weight proportion number list 6:
(table 6)
Finally it should be noted that, above example is only in order to illustrate technical scheme but not restriction technologies scheme, it will be understood by those within the art that, technical scheme is modified or equivalent replacement by those, without deviating from objective and the scope of the technical program, all should be encompassed in the middle of scope of the presently claimed invention。

Claims (1)

1. a preparation method for aqueous colorful building coating, composition and the mass fraction ratio of described aqueous colorful building coating be: 3-8 part varnish, 100 parts of color grains;Wherein:
The composition of described varnish and mass fraction ratio be: 50-60 part deionized water, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 25-35 part styrene-acrylic emulsion, 1-3 part defoamer, 10-18 part alkali-soluble is swollen Polyacrylic Acid Thickener, 10-15 part polyurethane thickener;
Composition and the mass fraction ratio of described color grain be: 100 parts of disperse medium, 100 parts of colored base paints;
The composition of described disperse medium and mass fraction ratio be: 45-49 part deionized water, 0.5-1 part sodium pyrophosphate, 0.5-1 part sodium tripolyphosphate, 0.5-1 part sodium hexameta phosphate, 8-10 part lithium magnesium silicate, 45-55 part 10% concentration protection sol solution;
Described colored base paint, composition and mass fraction ratio be: 100 parts of white basis paints, 0.1-1 part mill base;
Composition and the mass fraction ratio of described white basis paint be: 60-65 part deionized water, 0.5-1 part make the ammonium polyacrylate salt of dispersant, 0.5-1 part makes the alkylphenol polyoxyethylene of wetting agent, 1-2 part makes the mineral oil of defoamer, 10-13 part hydroxyethyl cellulose, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 5-10 part propylene glycol, 10-20 part titanium dioxide, 10-30 part Kaolin, 20-30 part elastomeric propylene yogurt liquid, 1-3 part make the silicone oil of defoamer, 5-8 part 10% concentration protection sol solution;
The described 10% concentration protection composition of sol solution and mass fraction ratio be: 89.5-89 part deionized water, 0.5-1 part sodium pyrophosphate, 10 parts of lithium magnesium silicates;
It is characterized in that: comprise the steps:
The preparation of (1) 10% protection sol solution: first add in a mixing bowl by 89.5-89 part deionized water, adds 0.5-1 part sodium pyrophosphate to being dissolved completely in water under 500r/min stirring at low speed;Add 10 parts of lithium magnesium silicate 1500r/min high-speed stirred more than 45min, then keep 500r/min stirring at low speed, standby;
(2) preparation of white basis paint: raw material and weight be: 60-65 part deionized water, 0.5-1 part makes the ammonium polyacrylate salt of dispersant, 0.5-1 part makes the alkylphenol polyoxyethylene of wetting agent, 1-2 part makes the mineral oil of defoamer, 10-13 part hydroxyethyl cellulose, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 5-10 part propylene glycol, 10-20 part titanium dioxide, 10-30 part Kaolin, 20-30 part elastomeric propylene yogurt liquid, 1-3 part makes the silicone oil of defoamer, the 10% concentration protection sol solution that 5-8 part is prepared by step (1), is placed in a mixing bowl by the raw material of above-mentioned weight, first adds deionized water, is then sequentially added into dispersant under 500 revs/min of rotating speeds, wetting agent, mineral oil antifoam agent, hydroxyethyl cellulose, pH adjusting agent, antibacterial, coalescents, propylene glycol, then carries rotating speed to 1200-1500 rev/min of addition titanium dioxide, Kaolin stirs 30 minutes, then rotating speed is down to 500-600 rev/min of addition elastomeric propylene yogurt liquid and silicon oil foam killer stirs, and is eventually adding the 10% concentration protection sol solution prepared by step (1), continues stirring more than 30 minutes, standby;
(3) toning: by designing requirement, the white basis paint prepared with 100 parts of steps (2) mixes with 0.1-1 part mill base, stirs, furnishing colour base paint;
(4) preparation of disperse medium: raw material and weight are 45-49 part deionized waters, 0.5-1 part sodium pyrophosphate, 0.5-1 part sodium tripolyphosphate, 0.5-1 part sodium hexameta phosphate, 8-10 part lithium magnesium silicate, the 10% concentration protection sol solution that 45-55 part is prepared by step (1), in a mixing bowl, deionized water is first added by above-mentioned weight portion, by sodium pyrophosphate under stirring at 500 revs/min, sodium tripolyphosphate, sodium hexameta phosphate is added to the water, stirring is to being completely dissolved, it is eventually adding lithium magnesium silicate and the 10% concentration protection sol solution prepared by step (1) stirs more than 45 minutes at 1500 revs/min, standby;
(5) preparation of varnish: raw material and weight are 50-60 part deionized water, 1-2 part pH adjusting agent, 1-2 part antibacterial, 5-10 part coalescents, 25-35 part styrene-acrylic emulsion, 1-3 part defoamer, 10-18 part alkali-soluble is swollen Polyacrylic Acid Thickener, 10-15 part polyurethane thickener, in a mixing bowl, deionized water is first added by above-mentioned weight portion, be sequentially added into pH adjusting agent, antibacterial, coalescents, styrene-acrylic emulsion, defoamer under stirring at 500 revs/min, alkali-soluble is swollen Polyacrylic Acid Thickener, polyurethane thickener stir, standby;
(6) preparation of color grain: raw material and weight are 100 parts of disperse medium prepared by step (4), 100 parts of colored base paints prepared by step (3), open blender and colour base paint is added in disperse medium, rotating speed 40 revs/min is not so that colored base paint sinks to being as the criterion, colored base paint adds rear rotating speed and carries to 90~130 revs/min, observe color grain particle diameter while stirring, until reaching designing requirement;
(7) last: raw material and weight are the varnish that 3-8 part is prepared by step (5), 100 parts of color grains prepared by step (6), open blender coloured silk grain addition varnish to stir and obtain this coating, rotating speed controls to be as the criterion just making color grain and varnish can stir evenly and not destroy color grain, if lacquering viscosity does not reach construction requirement can add the swollen Polyacrylic Acid Thickener adjustment of alkali-soluble in right amount, viscosity adjusts complete stopping immediately and stirs。
CN201410029110.0A 2014-01-22 2014-01-22 A kind of aqueous colorful building coating and preparation method CN103756486B (en)

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CN102719162A (en) * 2012-06-20 2012-10-10 浙江博星化工涂料有限公司 Water-based artificial granite paint
CN103333566A (en) * 2013-06-05 2013-10-02 新疆屯河涂料有限公司 Environmentally-friendly waterborne multicolor paint, preparation method and application method thereof

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