CN108342274A - A kind of Wooden fish stone health-care white spirit and preparation method thereof rich in various trace elements - Google Patents
A kind of Wooden fish stone health-care white spirit and preparation method thereof rich in various trace elements Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/02—Preparation of other alcoholic beverages by fermentation
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/24—Heavy metals; Compounds thereof
- A61K33/26—Iron; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/481—Astragalus (milkvetch)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/537—Salvia (sage)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
- A61K36/736—Prunus, e.g. plum, cherry, peach, apricot or almond
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/79—Schisandraceae (Schisandra family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/80—Scrophulariaceae (Figwort family)
- A61K36/804—Rehmannia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8968—Ophiopogon (Lilyturf)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/14—Prodigestives, e.g. acids, enzymes, appetite stimulants, antidyspeptics, tonics, antiflatulents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P25/00—Drugs for disorders of the nervous system
- A61P25/20—Hypnotics; Sedatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P39/00—General protective or antinoxious agents
Abstract
The invention discloses a kind of Wooden fish stone health-care white spirit and preparation method thereof rich in various trace elements, using green plum, limonite etc. is raw material, it is processed into the Wooden fish stone health-care white spirit rich in various trace elements, simultaneously also a new way is provided for the use of limonite, pass through pretreatment of raw material, extraction, glutinous rice pre-processes, curing, diastatic fermentation, fill altar fermentation, the brewing process of purification and flavouring after-ripening, the active material of raw material can be sufficiently reserved, improve the nutritive value of health liquor, keep the mouthfeel of health liquor soft pure, aroma is assailed the nostrils, also there is spleen benefiting and stimulating the appetite, slow down fatigue and improves the health-care efficacies such as immunocompetence.
Description
Technical field
The invention belongs to wine product technique fields, and in particular to a kind of Wooden fish stone health-care white spirit rich in various trace elements and
Preparation method.
Background technology
Although with people's consumption consciousness and improvement of living standard, health liquor market scale is increasing, Jin Liquor,
YEDAO LUGUI JIU causes the leading enterprises such as neutralization cortex acanthopanacis to quickly grow.But health liquor type in the market is not very much, and deposit
It is being formulated the phenomenon single, effect is single, therefore is also having prodigious development prospect in this respect.
Invention content
The object of the present invention is to provide a kind of Wooden fish stone health-care white spirit and preparation method thereof rich in various trace elements, use
Green plum, limonite etc. are raw material, are processed into the Wooden fish stone health-care white spirit rich in various trace elements, while being also the use of limonite
One new way is provided.
The present invention is realized by following technical scheme：
A kind of Wooden fish stone health-care white spirit rich in various trace elements, is made of the raw material of following parts by weight：Green plum 8~
12.5 parts, 0.13~0.22 part of limonite, 20~30 parts of glutinous rice, 13~20 parts of bitter buckwheat, 3~5 parts of Semen Setariae italicae, milled glutinous broomcorn millet 1.6~2.5
Part, 0.4~0.5 part of koji, 0.15~0.18 part of red yeast rice, 0.05~0.06 part of amylase, 1~1.5 part of wheat koji, dry ferment
0.3~0.75 part, 0.1~0.15 part of carbohydrase, 3~6 parts of Chinese medicine extract.
Preferably, a kind of Wooden fish stone health-care white spirit rich in various trace elements, is made of the raw material of following parts by weight：It is green
8.9~11.6 parts of plum, 0.153~0.198 part of limonite, 22.5~27.5 parts of glutinous rice, 14.75~18.25 parts of bitter buckwheat, Semen Setariae italicae
3.5~4.5 parts, 1.825~2.275 parts of milled glutinous broomcorn millet, 0.425~0.475 part of koji, 0.158~0.173 part of red yeast rice, amylase
0.053~0.058 part, 1.125~1.375 parts of wheat koji, 0.413~0.638 part of dry ferment, 0.113~0.138 part of carbohydrase,
3.75~5.25 parts of Chinese medicine extract.
It is highly preferred that a kind of Wooden fish stone health-care white spirit rich in various trace elements, is made of the raw material of following parts by weight：
10.25 parts of green plum, 0.175 part of limonite, 25 parts of glutinous rice, 16.5 parts of bitter buckwheat, 4 parts of Semen Setariae italicae, 2.05 parts of milled glutinous broomcorn millet, koji 0.45
Part, 0.165 part of red yeast rice, 0.055 part of amylase, 1.25 parts of wheat koji, 0.525 part of dry ferment, 0.125 part of carbohydrase, traditional Chinese medicine extraction
4.5 parts of liquid.
Further, the Chinese medicine extract is made of the raw material of following parts by weight：2~7 parts of Radix Salviae Miltiorrhizae, Radix Astragali 3~9
Part, 4~10 parts of radix rehmanniae preparata, 3~8 parts of Schisandra chinensis, 2~7 parts of sun-dried ginseng, 1~5 part of Radix Ophiopogonis.
Preferably, the Chinese medicine extract is made of the raw material of following parts by weight：3.25~5.75 parts of Radix Salviae Miltiorrhizae, Radix Astragali
4.5~7.5 parts, 5.5~8.5 parts of radix rehmanniae preparata, 4.25~6.75 parts of Schisandra chinensis, 3.25~5.75 parts of sun-dried ginseng, 2~4 parts of Radix Ophiopogonis.
It is highly preferred that the Chinese medicine extract is made of the raw material of following parts by weight：It is 4.5 parts of Radix Salviae Miltiorrhizae, 6 parts of Radix Astragali, ripe
7 parts of ground, 5.5 parts of Schisandra chinensis, 4.5 parts of sun-dried ginseng, 3 parts of Radix Ophiopogonis.
Further, the preparation method of the Chinese medicine extract is：By Radix Salviae Miltiorrhizae, Radix Astragali, radix rehmanniae preparata, Schisandra chinensis, sun-dried ginseng, wheat
Winter, drying to constant weight at 60~70 DEG C, crushes, and is 1 by solid-liquid ratio:20~30 are added 10% ethyl alcohol, in 70~75 DEG C of water-bath temperature
Degree 5~7h of lower reflux extracting time, 1/4~1/2 that original volume is concentrated into after extracting 2~3 times just obtain.
A kind of Wooden fish stone health-care white spirit rich in various trace elements of the present invention, the dry ferment are the dry ferment of activation.
A kind of preparation method of the Wooden fish stone health-care white spirit rich in various trace elements of the present invention, includes the following steps：
(1) pretreatment of raw material：It will be sliced, be uniformly mixed by weight again after low temperature drying after green plum, limonite cleaning
It crushes and raw material mixed powder is made；
(2) it extracts：It is 1 by solid-liquid ratio:5~7 are added 70~90% ethyl alcohol into raw material mixed powder is heated to 60~70 DEG C,
Refluxing extraction 2 times is every time 26~30min, after centrifugation, raw material extracting solution and material residue is made, then raw material extracting solution is existed
Rotary evaporation at 48~54 DEG C removes solvent, obtains green plum concentrate；
(3) matrix pre-processes：After glutinous rice, bitter buckwheat, Semen Setariae italicae and milled glutinous broomcorn millet are cleaned impurity elimination by weight, glutinous rice weight is added
A concentration of 35% rice vinegar of 7~8 times of amount impregnates 11~15h at 28~40 DEG C, then takes out, drain, and matrix is made；
(4) it cures：Material residue obtained by step (2) is added into the matrix after immersion, is uniformly mixed, enters pot and cook, then rouse
Clinker is made to room temperature in air cooling；
(5) diastatic fermentation：It is drenched into clinker into concentrate, adds koji, red yeast rice and amylase, after stirring evenly,
Ferment 25~29h in 30~40 DEG C, and material unstrained spirits is made；
(6) altar fermentation is filled：Wheat koji, dry ferment, carbohydrase and Chinese medicine extract is added in unstrained spirits cooling to be expected, stirs evenly, fills
Altar sets 31~34 DEG C of 46~50d of ferment at constant temperature, and when the residual sugar in karusen is down to 0.55~0.95%, fermentation ends are made
Karusen；
(7) it purifies：Fermentation liquid and fermentation wort sludge is made after duplex filters in karusen, is 1 by solid-liquid ratio:1.4~
1.8 are added distilled water to fermentation wort sludge, and 7~9min of refluxing extraction, is cooled to room temperature at 50~54 DEG C, and extraction is made in filtering
Liquid finally merges fermentation liquid and leaching liquor, and wine liquid is made；
(8) flavouring after-ripening：Wine liquid is placed under air-proof condition and stands 2~2.5d in 55 DEG C, finally carries out sterile filling, it is close
After package dress, as finished product.
The effect propety of each raw material of the present invention is as follows：
Green plum, pulp contain a variety of mines such as multivitamin, amino acid, citric acid, malic acid, tartaric acid and potassium, calcium, iron
Prime element, the more parotin of energy saliva stimulating glandular secretion, parotin can boost metabolism, and slow down fatigue, slow down aging.
Red yeast rice applies to make wine, and can be not only the hyperchromic flavouring of wine liquid, but also the active constituent of red yeast rice metabolism can also increase
The nutritive value and healthcare function of bitter buckwheat wine, ergosterol can promote absorption of the human body to calcium, phosphorus.
Radix Salviae Miltiorrhizae also known as red ginseng, radix salviae miltiorrhizae, red root etc., have promoting blood circulation, inducing meastruation to relieve menalgia, relieving restlessness that clears away heart-fire, cool blood to disappear carbuncle it
Effect.
Bitter buckwheat, buckwheat plant, biological Flavonoid substances rutin, have reduce human body blood fat, cholesterol and
The effect for improving capillary permeability and nagiopasthyrosis has fine curative effect to prevention and treatment hypertension, cardiovascular disease.
Radix Astragali, polysaccharide mainly act on panimmunity competent cell, promotes secretion and the normal body of cell factor
Antibody tormation；Radix rehmanniae preparata has certain effect to hemopoietic system, endocrine, nervous system, cardiovascular and cerebrovascular and immune system etc.；It is sun-dried
Ginseng is partial to help gas the moon, enhances Abwehrkraft des Koepers, plays immunoregulation effect.
Limonite, mineral composition are limonite, Fe2O3Content be 20~78%, other impurity often be phosphate, also
There are a small amount of metasilicate, Yi Jisi, molybdenum, lithium, zinc, selenium and other trace elements, the rare Chinese medicine of limonite system, the sweet flat nothing of property
Poison, there is the effect of determining six internal organs, town the five internal organs, long-term use keeps fit and healthy, cold-resistant tolerance to heat, delaying senility, the effect of promoting longevity,
Containing there are many essential trace elements of the human body and minerals, such as strontium, selenium, zinc, metasilicic acid, copper, cobalt, germanium in limonite, have very
Strong health care and beautification function can adjust the metabolism of human body, soften blood vessel, prevent artery sclerosis.
The present invention has following advantageous effect：
(1) bitter buckwheat amylose content is more, accounts for 33~44%, and starch is easy to aging after boiling, and when fermentation is difficult to be saccharified, glutinous rice
Amylopectin content is more, accounts for 98%, so bitter buckwheat glutinous rice mixed fermentation is conducive to accelerate diastatic fermentation, improves distillation yield, makes original
Have complementary advantages between material.
(2) Wooden fish stone health-care white spirit that this method makes, using the high green plum of health value and rich in various trace elements
Limonite is raw material, and glutinous rice etc. is matrix, adds the nutritional ingredient of health liquor, is located in advance by pretreatment of raw material, extraction, glutinous rice
Reason, curing, diastatic fermentation, the brewing process for filling altar fermentation, purification and flavouring after-ripening, can be sufficiently reserved the active matter of raw material
Matter improves the nutritive value of health liquor, keeps the mouthfeel of health liquor soft pure, and aroma is assailed the nostrils, and also has spleen benefiting and stimulating the appetite, blood-nourishing
Calm the nerves, slows down the health-care efficacies such as fatigue.
Specific implementation mode
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1
A kind of Wooden fish stone health-care white spirit rich in various trace elements, is made of the raw material of following parts by weight：Green plum 10.25
Part, 0.175 part of limonite, 25 parts of glutinous rice, 16.5 parts of bitter buckwheat, 4 parts of Semen Setariae italicae, 2.05 parts of milled glutinous broomcorn millet, 0.45 part of koji, red yeast rice
0.165 part, 0.055 part of amylase, 1.25 parts of wheat koji, 0.525 part of dry ferment, 0.125 part of carbohydrase, 4.5 parts of Chinese medicine extract.
Further, the Chinese medicine extract is made of the raw material of following parts by weight：It is 4.5 parts of Radix Salviae Miltiorrhizae, 6 parts of Radix Astragali, ripe
7 parts of ground, 5.5 parts of Schisandra chinensis, 4.5 parts of sun-dried ginseng, 3 parts of Radix Ophiopogonis.
Further, the preparation method of the Chinese medicine extract is：By Radix Salviae Miltiorrhizae, Radix Astragali, radix rehmanniae preparata, Schisandra chinensis, sun-dried ginseng, wheat
Winter, drying to constant weight at 65 DEG C, crushes, and is 1 by solid-liquid ratio:25 are added 10% ethyl alcohol, flow back and carry under 72.5 DEG C of bath temperatures
Time 6h is taken, 1/3 that original volume is concentrated into after extracting 2 times just obtains.
A kind of Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, the dry ferment are the dry ferment of activation.
A kind of preparation method of the Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, includes the following steps：
(1) pretreatment of raw material：It will be sliced, be uniformly mixed by weight again after low temperature drying after green plum, limonite cleaning
It crushes and raw material mixed powder is made；
(2) it extracts：It is 1 by solid-liquid ratio:6 80% ethyl alcohol is added into raw material mixed powder is heated to 65 DEG C, refluxing extraction 2
It is secondary, it is every time 28min, after centrifugation, raw material extracting solution and material residue is made, then raw material extracting solution is rotated to steaming at 51 DEG C
Hair removes solvent, obtains green plum concentrate；
(3) matrix pre-processes：After glutinous rice, bitter buckwheat, Semen Setariae italicae and milled glutinous broomcorn millet are cleaned impurity elimination by weight, glutinous rice weight is added
A concentration of 35% rice vinegar of 7.5 times of amount, impregnates 13h at 34 DEG C, then takes out, drain, and matrix is made；
(4) it cures：Material residue obtained by step (2) is added into the matrix after immersion, is uniformly mixed, enters pot and cook, then rouse
Clinker is made to room temperature in air cooling；
(5) diastatic fermentation：It is drenched into clinker into concentrate, adds koji, red yeast rice and amylase, after stirring evenly,
Ferment 27h in 35 DEG C, and material unstrained spirits is made；
(6) altar fermentation is filled：Wheat koji, dry ferment, carbohydrase and Chinese medicine extract is added in unstrained spirits cooling to be expected, stirs evenly, fills
Altar sets 32.5 DEG C of ferment at constant temperature 48d, and when the residual sugar in karusen is down to 0.75, karusen is made in fermentation ends；
(7) it purifies：Fermentation liquid and fermentation wort sludge is made after duplex filters in karusen, is 1 by solid-liquid ratio:1.6 to hair
Distilled water is added in ferment wort sludge, and refluxing extraction 8min, is cooled to room temperature at 52 DEG C, and leaching liquor is made in filtering, finally merges fermentation
Wine liquid is made in mash and leaching liquor；
(8) flavouring after-ripening：Wine liquid is placed under air-proof condition and stands 2.25d in 55 DEG C, finally carries out sterile filling, is sealed
After packaging, as finished product.
Embodiment 2
A kind of Wooden fish stone health-care white spirit rich in various trace elements, is made of the raw material of following parts by weight：8 parts of green plum,
0.13 part of limonite, 13 parts of bitter buckwheat, 3 parts of Semen Setariae italicae, 1.6 parts of milled glutinous broomcorn millet, 0.4 part of koji, 0.15 part of red yeast rice, forms sediment at 20 parts of glutinous rice
0.05 part of powder enzyme, 1 part of wheat koji, 0.3 part of dry ferment, 0.1 part of carbohydrase, 3 parts of Chinese medicine extract.
Further, the Chinese medicine extract is made of the raw material of following parts by weight：2 parts of Radix Salviae Miltiorrhizae, 3 parts of Radix Astragali, radix rehmanniae preparata 4
Part, 3 parts of Schisandra chinensis, 2 parts of sun-dried ginseng, 1 part of Radix Ophiopogonis.
Further, the preparation method of the Chinese medicine extract is：By Radix Salviae Miltiorrhizae, Radix Astragali, radix rehmanniae preparata, Schisandra chinensis, sun-dried ginseng, wheat
Winter, drying to constant weight at 60 DEG C, crushes, and is 1 by solid-liquid ratio:20 are added 10% ethyl alcohol, the refluxing extraction under 70 DEG C of bath temperatures
Time 5h, 1/4 that original volume is concentrated into after extracting 2 times just obtain.
A kind of Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, the dry ferment are the dry ferment of activation.
A kind of preparation method of the Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, includes the following steps：
(1) pretreatment of raw material：It will be sliced, be uniformly mixed by weight again after low temperature drying after green plum, limonite cleaning
It crushes and raw material mixed powder is made；
(2) it extracts：It is 1 by solid-liquid ratio:5 70% ethyl alcohol is added into raw material mixed powder is heated to 60 DEG C, refluxing extraction 2
It is secondary, it is every time 26min, after centrifugation, raw material extracting solution and material residue is made, then raw material extracting solution is rotated to steaming at 48 DEG C
Hair removes solvent, obtains green plum concentrate；
(3) matrix pre-processes：After glutinous rice, bitter buckwheat, Semen Setariae italicae and milled glutinous broomcorn millet are cleaned impurity elimination by weight, glutinous rice weight is added
A concentration of 35% rice vinegar of 7 times of amount, impregnates 11h at 28 DEG C, then takes out, drain, and matrix is made；
(4) it cures：Material residue obtained by step (2) is added into the matrix after immersion, is uniformly mixed, enters pot and cook, then rouse
Clinker is made to room temperature in air cooling；
(5) diastatic fermentation：It is drenched into clinker into concentrate, adds koji, red yeast rice and amylase, after stirring evenly,
Ferment 25h in 30 DEG C, and material unstrained spirits is made；
(6) altar fermentation is filled：Wheat koji, dry ferment, carbohydrase and Chinese medicine extract is added in unstrained spirits cooling to be expected, stirs evenly, fills
Altar sets 31 DEG C of ferment at constant temperature 46d, and when the residual sugar in karusen is down to 0.55%, karusen is made in fermentation ends；
(7) it purifies：Fermentation liquid and fermentation wort sludge is made after duplex filters in karusen, is 1 by solid-liquid ratio:1.4 to hair
Distilled water is added in ferment wort sludge, and refluxing extraction 7min, is cooled to room temperature at 50 DEG C, and leaching liquor is made in filtering, finally merges fermentation
Wine liquid is made in mash and leaching liquor；
(8) flavouring after-ripening：Wine liquid is placed under air-proof condition and stands 2d in 55 DEG C, finally carries out sterile filling, sealing packet
After dress, as finished product.
Embodiment 3
A kind of Wooden fish stone health-care white spirit rich in various trace elements, is made of the raw material of following parts by weight：Green plum 12.5
Part, 0.22 part of limonite, 30 parts of glutinous rice, 20 parts of bitter buckwheat, 5 parts of Semen Setariae italicae, 2.5 parts of milled glutinous broomcorn millet, 0.5 part of koji, 0.18 part of red yeast rice,
0.06 part of amylase, 1.5 parts of wheat koji, 0.75 part of dry ferment, 0.15 part of carbohydrase, 6 parts of Chinese medicine extract.
Further, the Chinese medicine extract is made of the raw material of following parts by weight：7 parts of Radix Salviae Miltiorrhizae, 9 parts of Radix Astragali, radix rehmanniae preparata
10 parts, 8 parts of Schisandra chinensis, 7 parts of sun-dried ginseng, 5 parts of Radix Ophiopogonis.
Further, the preparation method of the Chinese medicine extract is：By Radix Salviae Miltiorrhizae, Radix Astragali, radix rehmanniae preparata, Schisandra chinensis, sun-dried ginseng, wheat
Winter, drying to constant weight at 70 DEG C, crushes, and is 1 by solid-liquid ratio:30 are added 10% ethyl alcohol, the refluxing extraction under 75 DEG C of bath temperatures
Time 7h, 1/2 that original volume is concentrated into after extracting 3 times just obtain.
A kind of Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, the dry ferment are the dry ferment of activation.
A kind of preparation method of the Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, includes the following steps：
(1) pretreatment of raw material：It will be sliced, be uniformly mixed by weight again after low temperature drying after green plum, limonite cleaning
It crushes and raw material mixed powder is made；
(2) it extracts：It is 1 by solid-liquid ratio:7 90% ethyl alcohol is added into raw material mixed powder is heated to 70 DEG C, refluxing extraction 2
It is secondary, it is every time 30min, after centrifugation, raw material extracting solution and material residue is made, then raw material extracting solution is rotated to steaming at 54 DEG C
Hair removes solvent, obtains green plum concentrate；
(3) matrix pre-processes：After glutinous rice, bitter buckwheat, Semen Setariae italicae and milled glutinous broomcorn millet are cleaned impurity elimination by weight, glutinous rice weight is added
A concentration of 35% rice vinegar of 8 times of amount, impregnates 15h at 40 DEG C, then takes out, drain, and matrix is made；
(4) it cures：Material residue obtained by step (2) is added into the matrix after immersion, is uniformly mixed, enters pot and cook, then rouse
Clinker is made to room temperature in air cooling；
(5) diastatic fermentation：It is drenched into clinker into concentrate, adds koji, red yeast rice and amylase, after stirring evenly,
Ferment 29h in 40 DEG C, and material unstrained spirits is made；
(6) altar fermentation is filled：Wheat koji, dry ferment, carbohydrase and Chinese medicine extract is added in unstrained spirits cooling to be expected, stirs evenly, fills
Altar sets 34 DEG C of ferment at constant temperature 50d, and when the residual sugar in karusen is down to 0.95%, karusen is made in fermentation ends；
(7) it purifies：Fermentation liquid and fermentation wort sludge is made after duplex filters in karusen, is 1 by solid-liquid ratio:1.8 to hair
Distilled water is added in ferment wort sludge, and refluxing extraction 9min, is cooled to room temperature at 54 DEG C, and leaching liquor is made in filtering, finally merges fermentation
Wine liquid is made in mash and leaching liquor；
(8) flavouring after-ripening：Wine liquid is placed under air-proof condition and stands 2.5d in 55 DEG C, finally carries out sterile filling, is sealed
After packaging, as finished product.
Embodiment 4
A kind of Wooden fish stone health-care white spirit rich in various trace elements, is made of the raw material of following parts by weight：Green plum 8.9
Part, 0.153 part of limonite, 22.5 parts of glutinous rice, 14.75 parts of bitter buckwheat, 3.5 parts of Semen Setariae italicae, 1.825 parts of milled glutinous broomcorn millet, koji 0.425
Part, 0.158 part of red yeast rice, 0.053 part of amylase, 1.125 parts of wheat koji, 0.413 part of dry ferment, 0.113 part of carbohydrase, traditional Chinese medicine extraction
3.75 parts of liquid.
Further, the Chinese medicine extract is made of the raw material of following parts by weight：3.25 parts of Radix Salviae Miltiorrhizae, 4.5 parts of Radix Astragali,
5.5 parts of radix rehmanniae preparata, 4.25 parts of Schisandra chinensis, 3.25 parts of sun-dried ginseng, 2 parts of Radix Ophiopogonis.
Further, the preparation method of the Chinese medicine extract is：By Radix Salviae Miltiorrhizae, Radix Astragali, radix rehmanniae preparata, Schisandra chinensis, sun-dried ginseng, wheat
Winter, drying to constant weight at 70 DEG C, crushes, and is 1 by solid-liquid ratio:30 are added 10% ethyl alcohol, the refluxing extraction under 75 DEG C of bath temperatures
Time 7h, 1/2 that original volume is concentrated into after extracting 3 times just obtain.
A kind of Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, the dry ferment are the dry ferment of activation.
A kind of preparation method of the Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, includes the following steps：
(1) pretreatment of raw material：It will be sliced, be uniformly mixed by weight again after low temperature drying after green plum, limonite cleaning
It crushes and raw material mixed powder is made；
(2) it extracts：It is 1 by solid-liquid ratio:7 90% ethyl alcohol is added into raw material mixed powder is heated to 70 DEG C, refluxing extraction 2
It is secondary, it is every time 30min, after centrifugation, raw material extracting solution and material residue is made, then raw material extracting solution is rotated to steaming at 54 DEG C
Hair removes solvent, obtains green plum concentrate；
(3) matrix pre-processes：After glutinous rice, bitter buckwheat, Semen Setariae italicae and milled glutinous broomcorn millet are cleaned impurity elimination by weight, glutinous rice weight is added
A concentration of 35% rice vinegar of 8 times of amount, impregnates 15h at 40 DEG C, then takes out, drain, and matrix is made；
(4) it cures：Material residue obtained by step (2) is added into the matrix after immersion, is uniformly mixed, enters pot and cook, then rouse
Clinker is made to room temperature in air cooling；
(5) diastatic fermentation：It is drenched into clinker into concentrate, adds koji, red yeast rice and amylase, after stirring evenly,
Ferment 29h in 40 DEG C, and material unstrained spirits is made；
(6) altar fermentation is filled：Wheat koji, dry ferment, carbohydrase and Chinese medicine extract is added in unstrained spirits cooling to be expected, stirs evenly, fills
Altar sets 34 DEG C of ferment at constant temperature 50d, and when the residual sugar in karusen is down to 0.95%, karusen is made in fermentation ends；
(7) it purifies：Fermentation liquid and fermentation wort sludge is made after duplex filters in karusen, is 1 by solid-liquid ratio:1.8 to hair
Distilled water is added in ferment wort sludge, and refluxing extraction 9min, is cooled to room temperature at 54 DEG C, and leaching liquor is made in filtering, finally merges fermentation
Wine liquid is made in mash and leaching liquor；
(8) flavouring after-ripening：Wine liquid is placed under air-proof condition and stands 2.5d in 55 DEG C, finally carries out sterile filling, is sealed
After packaging, as finished product.
Embodiment 5
A kind of Wooden fish stone health-care white spirit rich in various trace elements, is made of the raw material of following parts by weight：Green plum 11.6
Part, 0.198 part of limonite, 27.5 parts of glutinous rice, 18.25 parts of bitter buckwheat, 4.5 parts of Semen Setariae italicae, 2.275 parts of milled glutinous broomcorn millet, koji 0.475
Part, 0.173 part of red yeast rice, 0.058 part of amylase, 1.375 parts of wheat koji, 0.638 part of dry ferment, 0.138 part of carbohydrase, traditional Chinese medicine extraction
5.25 parts of liquid.
Further, the Chinese medicine extract is made of the raw material of following parts by weight：5.75 parts of Radix Salviae Miltiorrhizae, 7.5 parts of Radix Astragali,
8.5 parts of radix rehmanniae preparata, 6.75 parts of Schisandra chinensis, 5.75 parts of sun-dried ginseng, 4 parts of Radix Ophiopogonis.
Further, the preparation method of the Chinese medicine extract is：By Radix Salviae Miltiorrhizae, Radix Astragali, radix rehmanniae preparata, Schisandra chinensis, sun-dried ginseng, wheat
Winter, drying to constant weight at 60 DEG C, crushes, and is 1 by solid-liquid ratio:20 are added 10% ethyl alcohol, the refluxing extraction under 70 DEG C of bath temperatures
Time 5h, 1/4 that original volume is concentrated into after extracting 2 times just obtain.
A kind of Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, the dry ferment are the dry ferment of activation.
A kind of preparation method of the Wooden fish stone health-care white spirit rich in various trace elements of the present embodiment, includes the following steps：
(1) pretreatment of raw material：It will be sliced, be uniformly mixed by weight again after low temperature drying after green plum, limonite cleaning
It crushes and raw material mixed powder is made；
(2) it extracts：It is 1 by solid-liquid ratio:5 70% ethyl alcohol is added into raw material mixed powder is heated to 60 DEG C, refluxing extraction 2
It is secondary, it is every time 26min, after centrifugation, raw material extracting solution and material residue is made, then raw material extracting solution is rotated to steaming at 48 DEG C
Hair removes solvent, obtains green plum concentrate；
(3) matrix pre-processes：After glutinous rice, bitter buckwheat, Semen Setariae italicae and milled glutinous broomcorn millet are cleaned impurity elimination by weight, glutinous rice weight is added
A concentration of 35% rice vinegar of 7 times of amount, impregnates 11h at 28 DEG C, then takes out, drain, and matrix is made；
(4) it cures：Material residue obtained by step (2) is added into the matrix after immersion, is uniformly mixed, enters pot and cook, then rouse
Clinker is made to room temperature in air cooling；
(5) diastatic fermentation：It is drenched into clinker into concentrate, adds koji, red yeast rice and amylase, after stirring evenly,
Ferment 25h in 30 DEG C, and material unstrained spirits is made；
(6) altar fermentation is filled：Wheat koji, dry ferment, carbohydrase and Chinese medicine extract is added in unstrained spirits cooling to be expected, stirs evenly, fills
Altar sets 31 DEG C of ferment at constant temperature 46d, and when the residual sugar in karusen is down to 0.55%, karusen is made in fermentation ends；
(7) it purifies：Fermentation liquid and fermentation wort sludge is made after duplex filters in karusen, is 1 by solid-liquid ratio:1.4 to hair
Distilled water is added in ferment wort sludge, and refluxing extraction 7min, is cooled to room temperature at 50 DEG C, and leaching liquor is made in filtering, finally merges fermentation
Wine liquid is made in mash and leaching liquor；
(8) flavouring after-ripening：Wine liquid is placed under air-proof condition and stands 2d in 55 DEG C, finally carries out sterile filling, sealing packet
After dress, as finished product.
Comparative example 1
Difference lies in do not add green plum with embodiment 1 in health liquor.
Comparative example 2
Difference lies in do not add Chinese medicine extract with embodiment 1 in health liquor.
Comparative example 3
Difference lies in do not add limonite with embodiment 1 in health liquor.
Compliance test result
80 20~30 years old working clans are chosen, 8 groups is divided into, drinks 25mL Examples 1 to 5 and comparative example respectively daily
The health liquor of 1~3 brewing, the feedback after being drunk to them in two months do primary summary, and score is averaged, such as the following table 1 institute
Show.
Table 1
| Sensory evaluation scores | Sensory assessment | Total score | |
| Embodiment 1 | 47.8 | 46.5 | 94.3 |
| Embodiment 2 | 45.4 | 44.8 | 90.2 |
| Embodiment 3 | 45.6 | 45 | 90.6 |
| Embodiment 4 | 46.3 | 45.6 | 91.9 |
| Embodiment 5 | 46.9 | 46.1 | 93 |
| Comparative example 1 | 34.3 | 28.1 | 62.4 |
| Comparative example 2 | 35.8 | 22.7 | 58.5 |
| Comparative example 3 | 36 | 27.6 | 63.6 |
Note：(1) standards of grading：
Table 2
As shown on, the data of Examples 1 to 5 are not much different, and are better than comparative example, and embodiment 1 and comparative example 1~3 are made
Compare, the score average of feedback is respectively 94.3,62.4,58.5,63.6, illustrates that wherein ingredient is interaction, lacks one
The deficiency on sense organ and quality, the health liquor comfortable acid that the present invention makes, wine liquid can be caused uniformly to clarify, and the wine is mellow and,
There are stomach strengthening and digestion promoting, antifatigue and raising immunocompetence.
Several embodiments of the invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
Cannot the limitation to the scope of the claims of the present invention therefore be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the guarantor of the present invention
Protect range.
Claims (9)
1. a kind of Wooden fish stone health-care white spirit rich in various trace elements, which is characterized in that be made of the raw material of following parts by weight：
8~12.5 parts of green plum, 0.13~0.22 part of limonite, 20~30 parts of glutinous rice, 13~20 parts of bitter buckwheat, 3~5 parts of Semen Setariae italicae, milled glutinous broomcorn millet
1.6~2.5 parts, 0.4~0.5 part of koji, 0.15~0.18 part of red yeast rice, 0.05~0.06 part of amylase, 1~1.5 part of wheat koji,
0.3~0.75 part of dry ferment, 0.1~0.15 part of carbohydrase, 3~6 parts of Chinese medicine extract.
2. a kind of Wooden fish stone health-care white spirit rich in various trace elements according to claim 1, which is characterized in that by following
The raw material of parts by weight form：8.9~11.6 parts of green plum, 0.153~0.198 part of limonite, 22.5~27.5 parts of glutinous rice, bitter buckwheat
14.75~18.25 parts, 3.5~4.5 parts of Semen Setariae italicae, 1.825~2.275 parts of milled glutinous broomcorn millet, 0.425~0.475 part of koji, red yeast rice
0.158~0.173 part, 0.053~0.058 part of amylase, 1.125~1.375 parts of wheat koji, 0.413~0.638 part of dry ferment,
0.113~0.138 part of carbohydrase, 3.75~5.25 parts of Chinese medicine extract.
3. a kind of Wooden fish stone health-care white spirit rich in various trace elements according to claim 2, which is characterized in that by following
The raw material of parts by weight form：10.25 parts of green plum, 0.175 part of limonite, 25 parts of glutinous rice, 16.5 parts of bitter buckwheat, 4 parts of Semen Setariae italicae, broomcorn millet
2.05 parts of rice, 0.45 part of koji, 0.165 part of red yeast rice, 0.055 part of amylase, 1.25 parts of wheat koji, 0.525 part of dry ferment, saccharification
0.125 part of enzyme, 4.5 parts of Chinese medicine extract.
4. according to a kind of Wooden fish stone health-care white spirit rich in various trace elements of claims 1 to 3 any one of them, feature exists
In the Chinese medicine extract is made of the raw material of following parts by weight：2~7 parts of Radix Salviae Miltiorrhizae, 3~9 parts of Radix Astragali, 4~10 parts of radix rehmanniae preparata,
3~8 parts of Schisandra chinensis, 2~7 parts of sun-dried ginseng, 1~5 part of Radix Ophiopogonis.
5. a kind of Wooden fish stone health-care white spirit rich in various trace elements according to claim 4, which is characterized in that in described
Medicament extracting solution is made of the raw material of following parts by weight：3.25~5.75 parts of Radix Salviae Miltiorrhizae, 4.5~7.5 parts of Radix Astragali, radix rehmanniae preparata 5.5~8.5
Part, 4.25~6.75 parts of Schisandra chinensis, 3.25~5.75 parts of sun-dried ginseng, 2~4 parts of Radix Ophiopogonis.
6. a kind of Wooden fish stone health-care white spirit rich in various trace elements according to claim 5, which is characterized in that in described
Medicament extracting solution is made of the raw material of following parts by weight：4.5 parts of Radix Salviae Miltiorrhizae, 6 parts of Radix Astragali, 7 parts of radix rehmanniae preparata, 5.5 parts of Schisandra chinensis, sun-dried ginseng
4.5 parts, 3 parts of Radix Ophiopogonis.
7. a kind of Wooden fish stone health-care white spirit rich in various trace elements according to any one of claim 4 to 6, feature exist
In the preparation method of the Chinese medicine extract is：By Radix Salviae Miltiorrhizae, Radix Astragali, radix rehmanniae preparata, Schisandra chinensis, sun-dried ginseng, Radix Ophiopogonis at 60~70 DEG C
Drying to constant weight, crushes, and is 1 by solid-liquid ratio:20~30 are added 10% ethyl alcohol, under 70~75 DEG C of bath temperatures when refluxing extraction
Between 5~7h, the 1/4~1/2 of original volume is concentrated into after extraction 2~3 times just.
8. according to a kind of Wooden fish stone health-care white spirit rich in various trace elements of claims 1 to 3 any one of them, feature exists
In the dry ferment is the dry ferment of activation.
9. a kind of prepare such as a kind of Wooden fish stone health-care white spirit rich in various trace elements of claim 1~8 any one of them
Method, which is characterized in that include the following steps：
(1) pretreatment of raw material：It will be sliced after green plum, limonite cleaning, be uniformly mixed crushed after low temperature drying again by weight
Raw material mixed powder is made；
(2) it extracts：It is 1 by solid-liquid ratio:5~7 70~90% ethyl alcohol are added into raw material mixed powder is heated to 60~70 DEG C, reflux
Extraction 2 times, is every time 26~30min, after centrifugation, is made raw material extracting solution and material residue, then by raw material extracting solution 48~
Rotary evaporation at 54 DEG C removes solvent, obtains green plum concentrate；
(3) matrix pre-processes：After glutinous rice, bitter buckwheat, Semen Setariae italicae and milled glutinous broomcorn millet are cleaned impurity elimination by weight, glutinous rice weight 7 is added
~8 times of a concentration of 35% rice vinegar impregnates 11~15h at 28~40 DEG C, then takes out, drain, and matrix is made；
(4) it cures：Material residue obtained by step (2) is added into the matrix after immersion, is uniformly mixed, enters pot and cook, then air blast is cold
But to room temperature, clinker is made；
(5) diastatic fermentation：It is drenched into clinker into concentrate, adds koji, red yeast rice and amylase, after stirring evenly, in 30
~40 DEG C of 25~29h of fermentation, are made material unstrained spirits；
(6) altar fermentation is filled：Wheat koji, dry ferment, carbohydrase and Chinese medicine extract is added in unstrained spirits cooling to be expected, stirs evenly, fills altar, set
31~34 DEG C of 46~50d of ferment at constant temperature, when the residual sugar in karusen is down to 0.55~0.95%, fermentation is made in fermentation ends
Wine with dregs；
(7) it purifies：Fermentation liquid and fermentation wort sludge is made after duplex filters in karusen, is 1 by solid-liquid ratio:1.4~1.8 to
Distilled water is added in the wort sludge that ferments, and 7~9min of refluxing extraction, is cooled to room temperature at 50~54 DEG C, and leaching liquor is made, most in filtering
Merge fermentation liquid and leaching liquor afterwards, wine liquid is made；
(8) flavouring after-ripening：Wine liquid is placed under air-proof condition and stands 2~2.5d in 55 DEG C, finally carries out sterile filling, sealing packet
After dress, as finished product.
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