CN108329959A - A kind of environmental protection fuel oil compound emulsifying agent - Google Patents

A kind of environmental protection fuel oil compound emulsifying agent Download PDF

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Publication number
CN108329959A
CN108329959A CN201810204568.3A CN201810204568A CN108329959A CN 108329959 A CN108329959 A CN 108329959A CN 201810204568 A CN201810204568 A CN 201810204568A CN 108329959 A CN108329959 A CN 108329959A
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Prior art keywords
parts
organic solvent
added
emulsifying agent
oil
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CN201810204568.3A
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Chinese (zh)
Inventor
骆佳豪
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Jinhua Zhichan Wuyuan Information Technology Co Ltd
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Jinhua Zhichan Wuyuan Information Technology Co Ltd
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Priority to CN201810204568.3A priority Critical patent/CN108329959A/en
Publication of CN108329959A publication Critical patent/CN108329959A/en
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    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2230/00—Function and purpose of a components of a fuel or the composition as a whole
    • C10L2230/22—Function and purpose of a components of a fuel or the composition as a whole for improving fuel economy or fuel efficiency
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2250/00—Structural features of fuel components or fuel compositions, either in solid, liquid or gaseous state
    • C10L2250/08—Emulsion details

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
  • Liquid Carbonaceous Fuels (AREA)

Abstract

The present invention discloses one kind and being used for environmental protection fuel oil compound emulsifying agent, including the mass ratio of basic components and modified component is 46：1, wherein wherein basic components include 40 60 parts of acrylic monomers, 2 10 parts of perfluorooctane sulfonate, 24 parts of butyl benzyl phthalate, 0.5 2 parts of nonylphenol polyoxyethylene ether, 6 10 parts of methyl benzotriazazole；Modified component includes 6 10 parts of sulfomethylated humic acid sodium, 10 20 parts of sorbester p17,10 30 parts of cobalt naphthenate, 5 10 parts of triisopropanolamine, 18 25 parts of phthalic anhydride, 10 15 parts of glyceryl oleate, 48 parts of octadecanoid acid.The compound emulsifying agent of this technology production can be used for oil products system, be widely used, and make simply, cost is relatively low, and stability is good.

Description

A kind of environmental protection fuel oil compound emulsifying agent
Technical field
The present invention relates to emulsifier more particularly to a kind of environmental protection fuel oil compound emulsifying agents.
Background technology
The energy is the lifeline of national security, is asked wherein non-renewable petroleum resources are most important the energy safety of supply One of topic.In order to effectively construct energy security, each state all attaches great importance to oil consumption and deposit, and various methods is taken actively to grind Study carefully reduction or substitutes the consumption of petroleum resources.With the rapid development of social economy, China is the oil demand dominated with fuel Always in rapid growth.
But due to the restriction of crude oil in China refining technique level, oil quality need to be improved, therefore directly burning combustion Material oil, inevitably causes combustion reaction incomplete, forms black smoke, coking and carbon deposit, causes fuel and largely waste, simultaneously The problem of also bringing environmental pollution.Generally for ensureing that burning is abundant, excess air need to be injected, and the discharge of these excess airs But heat has been taken away, thermal loss is caused.
It will generally be burnt after Emulsification of Fuel Oil to solve the above problems at present, but do not have also and a kind of can effectively make emulsification Fuel oil active combustion afterwards, at the same can also environmental emission reduction emulsifier.
Invention content
For overcome the deficiencies in the prior art, the present invention provides a kind of environmental protection fuel oil compound emulsifying agent, by basic components It is prepared in organic solvents with modified component；
Wherein basic components include the substance of following mass fraction：
About 40-60 parts of acrylate monomer,
2-10 parts of perfluorooctane sulfonate,
2-4 parts of butyl benzyl phthalate,
0.5-2 parts of nonylphenol polyoxyethylene ether,
6-10 parts of methyl benzotriazazole；
Modified component includes the substance of following mass fraction：
2-10 parts of sulfomethylated humic acid sodium,
10-20 parts of sorbester p17,
10-30 parts of cobalt naphthenate,
5-10 parts of triisopropanolamine,
18-25 parts of phthalic anhydride,
10-15 parts of glyceryl oleate,
4-8 parts of octadecanoid acid.
Wherein, it according to mass ratio is 1 that the acrylate monomer, which is styrene, methyl methacrylate or the two,：（2- 20）Composition.
Preferably, the mass ratio of compound emulsifying agent of the present invention, basic components and modified component is 4-6：1.Wherein, Basic components include the component of following mass fraction：
40-50 parts of acrylate monomer,
5-10 parts of perfluorooctane sulfonate,
2-3 parts of butyl benzyl phthalate,
0.5-1 parts of nonylphenol polyoxyethylene ether,
6-8 parts of methyl benzotriazazole；
Modified component includes the component of following mass fraction：
3-8 parts of sulfomethylated humic acid sodium,
12-15 parts of sorbester p17,
15-20 parts of cobalt naphthenate,
5-8 parts of triisopropanolamine,
20-25 parts of phthalic anhydride,
12-15 parts of glyceryl oleate,
4-6 parts of octadecanoid acid.
It is oligomeric because generating fluorine-containing using acrylate monomer in component basis and perfluorooctane sulfonate polymerization in the present invention Object so that polymer shows certain physico-chemical properties of fluorochemical to a certain extent.Therefore, having excellent hydrophobicity Meanwhile be also equipped with certain oil repellency, can steadily emulsify containing alcohol-oil interface or heavy oil, diesel oil system, increase alcohols with The intersolubility of diesel oil, application system is extensive, and effect stability；Because using the naphthenic compound being modified in group agent and suitably Charge ratio has the function of catalytic combustion-supporting, and to make the emulsifier of the present invention by after heavy oil emulsive, the discharge of heavy oil combustion is big It is big to reduce, SO2Discharge can reduce 90% or more, methyl benzotriazazole, which also has, prevents gasoline engine or diesel-engine equipment from corroding Effect；The emulsifiers such as modified component octadecanoid acid, phthalic anhydride make the emulsifier of the present invention have very strong emulsifying capacity, heavy oil In emulsification, the ratio of heavy oil and water can reach 1:1, the heavy oil after emulsification is the molecular structure of water-in-oil type, and after emulsification Heavy oil store 1 year or more be not in water-oil separating for a long time, performance is highly stable.
The emulsifier of the present invention can be applied not only to emulsification heavy oil, diesel oil emulsification or contain alcohol radical-diesel oil system, also universal It is applicable in most of fuel oil, application is good, and the compound emulsifying agent of formation has stability good, is easy recycling, recycles The advantages of.
The present invention emulsifier effectively heavy oil, diesel oil or fuel oil can be emulsified, make the heavy oil after emulsification, diesel oil or Fuel oil can more effectively burn, can fuel-economizing 35%-45%, reduction SO after heavy oil emulsifier using the present invention2Discharge 90% More than, storage 1 year or more is not in water-oil separating, and performance is highly stable.The present invention by a part of conventional heavy oils emulsifier at Divide and form composite emulsifying system with new type resin emulsifier, heavy wool system can be emulsified, different oil products is made Dosage is small, and preparation method is simple, at low cost, recyclable, and the stability of oil emulsion is good, not stratified, former taking into account many body system oil product While material, good emulsifying effectiveness may be implemented.
Specific implementation mode
The present invention will be further described in detail with reference to the specific embodiments.
Embodiment 1
Environmental protection fuel oil compound emulsifying agent, by basic components and modified component according to mass ratio 4：1 prepare in organic solvent and At wherein basic components include totally 40 parts of styrene and methyl methacrylate, 2 parts of perfluorooctane sulfonate, phthalic acid fourth 2 parts of base benzyl ester, 0.5 part of nonylphenol polyoxyethylene ether, 6 parts of methyl benzotriazazole；Modified component includes sulfomethylated humic acid 2 parts of sodium, 10 parts of sorbester p17,10 parts of cobalt naphthenate, 5 parts of triisopropanolamine, 18 parts of phthalic anhydride, 10 parts of glyceryl oleate, octadecanoid acid 4 parts.
It prepares in accordance with the following methods：A, organic solvent is added in reaction kettle, is warming up to 50-70 DEG C, then by acrylic acid Ester monomer, perfluorooctane sulfonate are uniformly mixed, then are slowly dropped into organic solvent, control feed time, and charging is finished after continuation of insurance Temperature reaction 2-4h, stops reacting and is cooled to room temperature to obtain fluorine-containing oligomer resin solution；B, by polyoxyethylene nonyl phenyl second In alkene ether, butyl benzyl phthalate input fluorine-containing oligomer resin solution, after being sufficiently stirred 1~2h, it is added Methyl benzotriazazole, stirring, reaction 1h obtain mixed solution；C, by sulfomethylated humic acid sodium, sapn, cobalt naphthenate, three is different Propanolamine is stirred evenly according to proportioning at 40-70 DEG C, and phthalic anhydride, glyceryl oleate and octadecanoid acid is then added, and continues to stir 1h, Form homogeneous solution；D, the homogeneous solution of step c is added in the mixed solution that step b is obtained, keeps 40 DEG C of reaction 1-3h, As needed, excessive organic solvent is removed, mixed emulsifier is obtained.
Embodiment 2
Environmental protection fuel oil compound emulsifying agent, by basic components and modified component according to mass ratio 5：1 prepare in organic solvent and At wherein basic components include totally 40 parts of styrene and methyl methacrylate, 5 parts of perfluorooctane sulfonate, phthalic acid fourth 2 parts of base benzyl ester, 0.5 part of nonylphenol polyoxyethylene ether, 6 parts of methyl benzotriazazole；Modified component includes sulfomethylated humic acid 3 parts of sodium, 12 parts of sorbester p17,15 parts of cobalt naphthenate, 5 parts of triisopropanolamine, 20 parts of phthalic anhydride, 12 parts of glyceryl oleate, octadecanoid acid 4 parts.
It prepares in accordance with the following methods：A, organic solvent is added in reaction kettle, is warming up to 50-70 DEG C, then by acrylic acid Ester monomer, perfluorooctane sulfonate are uniformly mixed, then are slowly dropped into organic solvent, control feed time, and charging is finished after continuation of insurance Temperature reaction 2-4h, stops reacting and is cooled to room temperature to obtain fluorine-containing oligomer resin solution；B, by polyoxyethylene nonyl phenyl second In alkene ether, butyl benzyl phthalate input fluorine-containing oligomer resin solution, after being sufficiently stirred 1~2h, it is added Methyl benzotriazazole, stirring, reaction 1h obtain mixed solution；C, by sulfomethylated humic acid sodium, sapn, cobalt naphthenate, three is different Propanolamine is stirred evenly according to proportioning at 40-70 DEG C, and phthalic anhydride, glyceryl oleate and octadecanoid acid is then added, and continues to stir 1h, Form homogeneous solution；D, the homogeneous solution of step c is added in the mixed solution that step b is obtained, keeps 50 DEG C of reaction 1-3h, As needed, excessive organic solvent is removed, mixed emulsifier is obtained.
Embodiment 3
Environmental protection fuel oil compound emulsifying agent, by basic components and modified component according to mass ratio 5：1 prepare in organic solvent and At wherein basic components include totally 50 parts of styrene and methyl methacrylate, 10 parts of perfluorooctane sulfonate, phthalic acid fourth 3 parts of base benzyl ester, 1 part of nonylphenol polyoxyethylene ether, 8 parts of methyl benzotriazazole；Modified component includes sulfomethylated humic acid sodium 8 Part, 15 parts of sorbester p17,20 parts of cobalt naphthenate, 8 parts of triisopropanolamine, 25 parts of phthalic anhydride, 15 parts of glyceryl oleate, octadecanoid acid 6 Part.
It prepares in accordance with the following methods：A, organic solvent is added in reaction kettle, is warming up to 50-70 DEG C, then by acrylic acid Ester monomer, perfluorooctane sulfonate are uniformly mixed, then are slowly dropped into organic solvent, control feed time, and charging is finished after continuation of insurance Temperature reaction 2-4h, stops reacting and is cooled to room temperature to obtain fluorine-containing oligomer resin solution；B, by polyoxyethylene nonyl phenyl second In alkene ether, butyl benzyl phthalate input fluorine-containing oligomer resin solution, after being sufficiently stirred 1~2h, it is added Methyl benzotriazazole, stirring, reaction 1h obtain mixed solution；C, by sulfomethylated humic acid sodium, sapn, cobalt naphthenate, three is different Propanolamine is stirred evenly according to proportioning at 40-70 DEG C, and phthalic anhydride, glyceryl oleate and octadecanoid acid is then added, and continues to stir 1h, Form homogeneous solution；D, the homogeneous solution of step c is added in the mixed solution that step b is obtained, keeps 60 DEG C of reaction 1-3h, As needed, excessive organic solvent is removed, mixed emulsifier is obtained.
Embodiment 4
Environmental protection fuel oil compound emulsifying agent, by basic components and modified component according to mass ratio 6：1 prepare in organic solvent and At wherein basic components include totally 60 parts of styrene and methyl methacrylate, 10 parts of perfluorooctane sulfonate, phthalic acid fourth 4 parts of base benzyl ester, 2 parts of nonylphenol polyoxyethylene ether, 10 parts of methyl benzotriazazole；Modified component includes sulfomethylated humic acid sodium 10 parts, 20 parts of sorbester p17,30 parts of cobalt naphthenate, 10 parts of triisopropanolamine, 25 parts of phthalic anhydride, 15 parts of glyceryl oleate, octadecanoid acid 8 parts.
It prepares in accordance with the following methods：A, organic solvent is added in reaction kettle, is warming up to 50-70 DEG C, then by acrylic acid Ester monomer, perfluorooctane sulfonate are uniformly mixed, then are slowly dropped into organic solvent, control feed time, and charging is finished after continuation of insurance Temperature reaction 2-4h, stops reacting and is cooled to room temperature to obtain fluorine-containing oligomer resin solution；B, by polyoxyethylene nonyl phenyl second In alkene ether, butyl benzyl phthalate input fluorine-containing oligomer resin solution, after being sufficiently stirred 1~2h, it is added Methyl benzotriazazole, stirring, reaction 1h obtain mixed solution；C, by sulfomethylated humic acid sodium, sapn, cobalt naphthenate, three is different Propanolamine is stirred evenly according to proportioning at 40-70 DEG C, and phthalic anhydride, glyceryl oleate and octadecanoid acid is then added, and continues to stir 1h, Form homogeneous solution；D, the homogeneous solution of step c is added in the mixed solution that step b is obtained, keeps 60 DEG C of reaction 1-3h, As needed, excessive organic solvent is removed, mixed emulsifier is obtained.
By oil product：Compound emulsifying agent：Solvent：Graphene or fullerene are according to 100-120：10-20：5-10：0.1-1 weight Than obtaining oil emulsion after mixing, our experiments show that, it can stablize after oil emulsion is static not stratified；For heavy oil emulsive, by one Year or more still there is not water-oil separating, and sulphur-containing substance discharge can be reduced with fuel-economizing 30%, for diesel oil in alcohol group, due to tool There are the effect of part resin, diesel oil in alcohol group that can dissolve each other very well, less carbon emission, and also component basis can be played with component modification Synergistic effect, can substantially reduce the consumption of diesel oil or heavy oil, and can reduce petrochemical industry cost, while be applicable in multiple systems, Pair simultaneously have the system of diesel oil and/or diesel oil in alcohol group have good emulsifying effectiveness.
Application examples 1
100kg heavy oil is taken, 60 DEG C is heated to and stirs evenly, adds 10 kg emulsifiers, 5g solvents, 0.1g fullerenes, through high speed 5-15min is stirred, appropriate 60 DEG C of water is added as needed, is used after standing 24 hours.
Application examples 2
120kg fuel oil is taken, 60 DEG C is heated to and stirs evenly, adds 10 kg emulsifiers, 10g solvents, 0.5g fullerenes, warp High-speed stirred 5-15min, the water of 70 DEG C of addition, which is mixed evenly, as needed becomes high-efficiency environment friendly oil emulsion, stands 24 It is used after hour.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any Those skilled in the art within the technical scope disclosed by the invention, can without the variation that creative work is expected or It replaces, should be covered by the protection scope of the present invention.Therefore, protection scope of the present invention should be limited with claims Subject to fixed protection domain.

Claims (1)

1. a kind of environmental protection fuel oil compound emulsifying agent, which is characterized in that by basic components and modified component according to mass ratio 5：1 It is prepared in organic solvent, wherein basic components include totally 40 parts of styrene and methyl methacrylate, perfluorooctane sulfonate 5 Part, 2 parts of butyl benzyl phthalate, 0.5 part of nonylphenol polyoxyethylene ether, 6 parts of methyl benzotriazazole；Modified component packet Include 3 parts of sulfomethylated humic acid sodium, 12 parts of sorbester p17,15 parts of cobalt naphthenate, 5 parts of triisopropanolamine, 20 parts of phthalic anhydride, glycerine oleic acid 12 parts of ester, 4 parts of octadecanoid acid；
It prepares in accordance with the following methods：A, organic solvent is added in reaction kettle, is warming up to about 50-70 DEG C, then by acrylate Monomer, perfluorooctane sulfonate are uniformly mixed, then are slowly dropped into organic solvent, control feed time, and charging, which finishes, to be continued to keep the temperature 2-4h is reacted, stop reacting and is cooled to room temperature to obtain fluorine-containing oligomer resin solution；B, by Nonyl pheno In ether, butyl benzyl phthalate input fluorine-containing oligomer resin solution, after being sufficiently stirred 1~2h, first is added Base benzotriazole, stirring, reaction 1h obtain mixed solution；C, by sulfomethylated humic acid sodium, sapn, cobalt naphthenate, three isopropyls Hydramine is stirred evenly according to proportioning at 40-70 DEG C, and phthalic anhydride, glyceryl oleate and octadecanoid acid is then added, and continues to stir 1h, shape At homogeneous solution；D, the homogeneous solution of step c is added in the mixed solution that step b is obtained, keeps 50 DEG C of reaction 1-3h, root According to needs, excessive organic solvent is removed, mixed emulsifier is obtained.
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Application publication date: 20180727