CN101328424B - Formula of biomass emulsified diesel oil - Google Patents
Formula of biomass emulsified diesel oil Download PDFInfo
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- CN101328424B CN101328424B CN2007100696484A CN200710069648A CN101328424B CN 101328424 B CN101328424 B CN 101328424B CN 2007100696484 A CN2007100696484 A CN 2007100696484A CN 200710069648 A CN200710069648 A CN 200710069648A CN 101328424 B CN101328424 B CN 101328424B
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Abstract
The invention relates to a formula of biomass emulsified diesel oil. The invention is characterized in that: the formula consists of heavy oil, diesel oil, water and an addition agent, wherein the weight percentages of the compositions of the formula include: 56 to 90 percent of the diesel oil, 5 to 25 percent of the water and 5 to 18 percent of the addition agent; moreover, the addition agent comprises the following compositions in percentage by weight: 9.9 to 69.9 percent of fatty acid, 25 to 85 percent of oleic acid, 4 to 14 percent of ethanolamine, 0.5 to 4 percent of isoamyl alcohol, 0.1to 3 percent of sulfanilate and 0.5 to 10 percent of sorbitol monoester. The formula has the advantages that: the formula has reasonable proportioning, and the product does not have side effect on a machine body, has effective energy conservation and high stability, and can replace diesel oil.
Description
Technical field
The present invention relates to a kind of biomass emulsified diesel oil compsn, the invention belongs to chemical industry, energy field, specifically belong to a kind of biofuel oil emulsifying additive field.
Background technology
Present domestic diesel oil short supply, on the high side, stability is low; The content of oxynitride, oxysulfide and flue dust is high in the flue gas of burning back; And petroleum resources belong to Nonrenewable resources, too rely on oil fuel and can cause irreversible destruction and waste to environment and resource.
Summary of the invention
Technical problem to be solved by this invention provides a kind of reasonable ratio, and product has no side effect to body, can be effectively energy-conservation, and the biomass emulsified diesel oil compsn of stable height, alternative diesel oil.
It is this biomass emulsified diesel oil compsn that the present invention solves the problems of the technologies described above the technical scheme that is adopted; Its prescription characteristics are: be made up of heavy oil, diesel oil, water and additive; Wherein, the weight percent of each component is: diesel oil 56%-90%, water 5%-25%, additive 5%-18%; Additive is made up of lipid acid, oleic acid, thanomin, primary isoamyl alcohol, amino phenyl sulfonyl hydrochlorate and sorbyl alcohol monoesters, and the shared weight percent of each component is in the additive: lipid acid 9.9%-69.9%, oleic acid 25%-85%, thanomin 4%-14, primary isoamyl alcohol 0.5%-4%, amino phenyl sulfonyl hydrochlorate 0.1-3% and sorbyl alcohol monoesters 0.5-10%.
Contain the 0-1% auxiliary agent in the prescription of the present invention, auxiliary agent is carbon 1-carbon 6 alcohol.
Additive ph value of the present invention is neutral, and 0-40 degree centigrade of following viscosity is 400-120 pascal.
Water particle particle diameter of the present invention is less than optical wavelength.
The present invention compares with prior art and has the following advantages and effect: the present invention's reasonable science of filling a prescription, preparation technology is reasonable in design.The product of producing has that sulphur content is low, oxygen level is high; Do not increase characteristics such as aromatic hydrocarbon content; Greatly reduce the discharging of obnoxious flavour (like oxysulfide, oxynitride, hydrocarbons etc.), reduced the exhaust gas emission temperature, improved the effect of rate of energy and environmental protection and energy saving.Because the water particle particle diameter is less than optical wavelength, so product is as clear as crystal, the ph value is neutral, can not corrode body, and body is had no side effect.Finished product diesel oil emulsification addictive of the present invention has combustion-supporting, catalytic effect, can fully burn, and emulsion process of the present invention is consciousness emulsification, only needs fully to stir to get final product.Product of the present invention-5 is higher than 360 days ℃-40 ℃ of stationary phases, can be-10 ℃ to 45 ℃ normal uses.Efficiency of combustion is high, and tail gas pollution is little.Refined biometric matter diesel oil emulsification each item physical and chemical index is all similar with natural diesel oil, and alternative diesel oil uses on industrial machinery, power unit, shipping vehicle etc.And can reduce smoke intensity more than 40%, the exhaust emissions obnoxious flavour descends 30%.Additive of the present invention has combustion-supporting, catalytic effect, can fully burn.The present invention can substitute traditional solar oil, is used for various Motor vehicles and various industrial fuel oil equipment.It is the human undue oil-fired new forms of energy that rely on of a kind of alleviation, also is the transitional product that progressively comprehensively substitutes Nonrenewable energy resources.
Embodiment
Below in conjunction with embodiment the present invention is done further detailed description, following examples are to explanation of the present invention and the present invention is not limited to following examples.
Embodiment 1
The preparation process of additive of the present invention has been described with the lower section:
5 kilograms of 50 kilograms in lipid acid, 31 kilograms of oleic acid, 10 kilograms of thanomins, 2 kilograms of primary isoamyl alcohol, 2 kilograms of amino phenyl sulfonyl hydrochlorates and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
62 kilograms of diesel oil, 22 kg of water, 15.5 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.5 kilogram of auxiliary agent according to state after observing oil product, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 2
The preparation process of additive of the present invention has been described with the lower section:
2 kilograms of 40 kilograms in lipid acid, 50 kilograms of oleic acid, 6 kilograms of thanomins, 1 kilogram of primary isoamyl alcohol, 1 kilogram of amino phenyl sulfonyl hydrochlorate and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
69 kilograms of diesel oil, 20.7 kg of water, 10 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.3 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 3 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 3
The preparation process of additive of the present invention has been described with the lower section:
1 kilogram of 25 kilograms in lipid acid, 65 kilograms of oleic acid, 4 kilograms of thanomins, 3 kilograms of primary isoamyl alcohol, 2 kilograms of amino phenyl sulfonyl hydrochlorates and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
80 kilograms of diesel oil, 13.2 kg of water, 6 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.8 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 6 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 4
The preparation process of additive of the present invention has been described with the lower section:
10 kilograms of 20 kilograms in lipid acid, 55 kilograms of oleic acid, 10 kilograms of thanomins, 2 kilograms of primary isoamyl alcohol, 3 kilograms of amino phenyl sulfonyl hydrochlorates and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
65 kilograms of diesel oil, 16 kg of water, 18 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 1 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 1 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 5
The preparation process of additive of the present invention has been described with the lower section:
1.8 kilograms of 11 kilograms in lipid acid, 78 kilograms of oleic acid, 8 kilograms of thanomins, 0.5 kilogram of primary isoamyl alcohol, 0.7 kilogram of amino phenyl sulfonyl hydrochlorate and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
68 kilograms of diesel oil, 18 kg of water, 13.6 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.4 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 4 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 6
The preparation process of additive of the present invention has been described with the lower section:
0.9 kilogram of 9.9 kilograms in lipid acid, 76.1 kilograms of oleic acid, 11.5 kilograms of thanomins, 1.5 kilograms of primary isoamyl alcohol, 0.1 kilogram of amino phenyl sulfonyl hydrochlorate and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
56 kilograms of diesel oil, 23 kg of water, 20.3 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.7 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 5 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 7
The preparation process of additive of the present invention has been described with the lower section:
0.5 kilogram of 55 kilograms in lipid acid, 25 kilograms of oleic acid, 13.5 kilograms of thanomins, 3.5 kilograms of primary isoamyl alcohol, 2.5 kilograms of amino phenyl sulfonyl hydrochlorates and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
74 kilograms of diesel oil, 13 kg of water, 12.8 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.2 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 2 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 8
The preparation process of additive of the present invention has been described with the lower section:
7 kilograms of 37 kilograms in lipid acid, 36.5 kilograms of oleic acid, 13 kilograms of thanomins, 4 kilograms of primary isoamyl alcohol, 2.5 kilograms of amino phenyl sulfonyl hydrochlorates and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
90 kilograms of diesel oil, 5 kg of water, 5 kilograms of biomass emulsified additives are added stirring tank successively, stirred 30 minutes, stirring velocity is 600 rev/mins, obtains 100 kilograms of as clear as crystal biomass emulsified diesel oils.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 9
The preparation process of additive of the present invention has been described with the lower section:
8.5 kilograms of 31.5 kilograms in lipid acid, 42 kilograms of oleic acid, 14 kilograms of thanomins, 2.5 kilograms of primary isoamyl alcohol, 1.5 kilograms of amino phenyl sulfonyl hydrochlorates and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
83 kilograms of diesel oil, 8 kg of water, 8.1 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.9 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 6 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 10
The preparation process of additive of the present invention has been described with the lower section:
2 kilograms of 45 kilograms in lipid acid, 46 kilograms of oleic acid, 5 kilograms of thanomins, 0.7 kilogram of primary isoamyl alcohol, 1.3 kilograms of amino phenyl sulfonyl hydrochlorates and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
77 kilograms of diesel oil, 6 kg of water, 16.3 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.7 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 3 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 11
The preparation process of additive of the present invention has been described with the lower section:
0.5 kilogram of 69.9 kilograms in lipid acid, 25 kilograms of oleic acid, 4 kilograms of thanomins, 0.5 kilogram of primary isoamyl alcohol, 0.1 kilogram of amino phenyl sulfonyl hydrochlorate and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
82 kilograms of diesel oil, 10 kg of water, 7 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 1 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 4 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 12
The preparation process of additive of the present invention has been described with the lower section:
0.5 kilogram of 9.9 kilograms in lipid acid, 85 kilograms of oleic acid, 4 kilograms of thanomins, 0.5 kilogram of primary isoamyl alcohol, 0.1 kilogram of amino phenyl sulfonyl hydrochlorate and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
88 kilograms of diesel oil, 6 kg of water, 5 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 1 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 1 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Embodiment 13
The preparation process of additive of the present invention has been described with the lower section:
6 kilograms of 30 kilograms in lipid acid, 51 kilograms of oleic acid, 9 kilograms of thanomins, 3.7 kilograms of primary isoamyl alcohol, 0.3 kilogram of amino phenyl sulfonyl hydrochlorate and sorbyl alcohol monoesters mix and stir, and the biomass emulsified additive of processing 100 kilograms is subsequent use.
The preparation process of biomass emulsified diesel oil of the present invention has been described with the lower section:
63 kilograms of diesel oil, 25 kg of water, 11.9 kilograms of biomass emulsified additives are added stirring tank successively; Stirred 30 minutes; Stirring velocity is 600 rev/mins; Add an amount of 0.1 kilogram of auxiliary agent according to state after observing oil product, auxiliary agent is carbon 6 alcohol, 100 kilograms of the biomass emulsified diesel oils that the continuation stirring got final product as clear as crystally in 10 minutes.Be higher than 360 days-5 ℃-40 ℃ stationary phases, satisfies the suitability for industrialized production needs.
Above embodiment it should be noted that when using that biomass emulsified diesel oil of the present invention can not mix use mutually with ordinary diesel oil.
Biomass emulsified diesel oil is the human undue oil-fired new forms of energy that rely on of a kind of alleviation, also is the transitional product that progressively comprehensively substitutes Nonrenewable energy resources.Biofuel has that sulphur content is low, oxygen level is high; Do not increase characteristics such as aromatic hydrocarbon content; Greatly reduce the discharging of obnoxious flavour (like oxysulfide, oxynitride, hydrocarbons etc.), reduced the exhaust gas emission temperature, improved the effect of rate of energy and environmental protection and energy saving.Refined biometric matter diesel oil emulsification each item physical and chemical index is all similar with natural diesel oil, and alternative diesel oil uses on industrial machinery, power unit, shipping vehicle etc.And can reduce smoke intensity more than 40%, the exhaust emissions obnoxious flavour descends 30%.The finished product diesel oil emulsification can be-10 ℃ to 45 ℃ normal uses.Refined biometric matter diesel oil emulsification, as clear as crystal, the ph value is neutral, can not corrode body, is consciousness emulsification to the body emulsion process that has no side effect, and only needs fully to stir to get final product, and the preparation process is simple.
Thorough, transparent clearly, disperse homogeneous extremely, the microemulsion of particle below 100nm of biomass emulsified diesel oil of the present invention.Because particle is less than visible wavelength, so transparent, quite stable on thermodynamics helps storage and transportation and not stratified.
The physical-chemical parameters of the embodiment of the invention 1 is following:
Instance:
What Hangzhou associating meat group company boiler used is GB 0# diesel oil, outlet dust concentration 98.2mg/m
3, sulfur dioxide emissioning concentration 384mg/m
3, discharged nitrous oxides concentration is 665.4mg/m
3After using biomass emulsified diesel oil of the present invention, outlet dust concentration 93.3mg/m
3, sulfur dioxide emissioning concentration 244.5mg/m
3, discharged nitrous oxides concentration is 365.4mg/m
3Above data are by Zhejiang Province Environmental Monitoring Center's station test.
Claims (2)
1. biomass emulsified diesel oil compsn, the prescription characteristic is: be made up of diesel oil, water and additive, wherein, the weight percent of each component is: diesel oil 56%-90%, water 5%-25%, additive 5%-18%, each component percentage composition sum is 100%; Additive is made up of lipid acid, oleic acid, thanomin, primary isoamyl alcohol, amino phenyl sulfonyl hydrochlorate and sorbyl alcohol monoesters, and the shared weight percent of each component is in the additive: lipid acid 9.9%-69.9%, oleic acid 25%-85%, thanomin 4%-14%, primary isoamyl alcohol 0.5%-4%, amino phenyl sulfonyl hydrochlorate 0.1%-3% and sorbyl alcohol monoesters 0.5%-10%.
2. biomass emulsified diesel oil compsn according to claim 1 is characterized in that: described additive ph value is for neutral, and 0-40 degree centigrade of following viscosity is 400-120 pascal. second.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007100696484A CN101328424B (en) | 2007-06-22 | 2007-06-22 | Formula of biomass emulsified diesel oil |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2007100696484A CN101328424B (en) | 2007-06-22 | 2007-06-22 | Formula of biomass emulsified diesel oil |
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| CN101328424A CN101328424A (en) | 2008-12-24 |
| CN101328424B true CN101328424B (en) | 2012-10-31 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2007100696484A Expired - Fee Related CN101328424B (en) | 2007-06-22 | 2007-06-22 | Formula of biomass emulsified diesel oil |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101775318A (en) * | 2010-02-10 | 2010-07-14 | 山西华顿实业有限公司 | Micro-emulsion clean fuel and preparation method thereof |
| CN101824343A (en) * | 2010-05-27 | 2010-09-08 | 熊道陵 | Clean and energy-saving micro-emulsified diesel oil with high flash point and preparation method thereof |
| CN102329668A (en) * | 2011-09-02 | 2012-01-25 | 彭千 | Preparation method of biomass additive for preparing emulsified diesel oil |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1079499A (en) * | 1992-05-27 | 1993-12-15 | 孙德贵 | Method for preparing water in oil emulsified diesel oil |
| CN1410514A (en) * | 2002-09-29 | 2003-04-16 | 季忠 | Production technology and formulation of microemulsion fuel oil |
| CN1542099A (en) * | 2003-11-07 | 2004-11-03 | 陆翼德 | Additive for emulsified oil and method for preparing the same |
-
2007
- 2007-06-22 CN CN2007100696484A patent/CN101328424B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1079499A (en) * | 1992-05-27 | 1993-12-15 | 孙德贵 | Method for preparing water in oil emulsified diesel oil |
| CN1410514A (en) * | 2002-09-29 | 2003-04-16 | 季忠 | Production technology and formulation of microemulsion fuel oil |
| CN1542099A (en) * | 2003-11-07 | 2004-11-03 | 陆翼德 | Additive for emulsified oil and method for preparing the same |
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