CN108300544A - A kind of mechanical lubrication fluid composition and its preparation process - Google Patents

A kind of mechanical lubrication fluid composition and its preparation process Download PDF

Info

Publication number
CN108300544A
CN108300544A CN201810072323.XA CN201810072323A CN108300544A CN 108300544 A CN108300544 A CN 108300544A CN 201810072323 A CN201810072323 A CN 201810072323A CN 108300544 A CN108300544 A CN 108300544A
Authority
CN
China
Prior art keywords
parts
added
fluid composition
lubrication fluid
tackifier
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810072323.XA
Other languages
Chinese (zh)
Inventor
刘春燕
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201810072323.XA priority Critical patent/CN108300544A/en
Publication of CN108300544A publication Critical patent/CN108300544A/en
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/041—Carbon; Graphite; Carbon black
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
    • C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/085—Phosphorus oxides, acids or salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/026—Butene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/04—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing aromatic monomers, e.g. styrene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/024—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings having at least two phenol groups but no condensed ring
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/08—Aldehydes; Ketones
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/283—Esters of polyhydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
    • C10M2209/084—Acrylate; Methacrylate
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/12—Polysaccharides, e.g. cellulose, biopolymers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2213/00—Organic macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2213/06—Perfluoro polymers
    • C10M2213/062—Polytetrafluoroethylene [PTFE]
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
    • C10M2219/022—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of hydrocarbons, e.g. olefines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/042—Sulfate esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/02—Pour-point; Viscosity index
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of mechanical lubrication fluid composition and its preparation processes; lubricant oil composite component includes 28 parts of 20 50 parts of glycerine, 10 20 parts of triethanolamine, 8 20 parts of turkey red oil, 4 12 parts of tackifier, 39 parts of anti-wear agent, 4 16 parts of diene terpolymers and polyisobutene in parts by weight; preparation process of the present invention is simple; lubricant oil composite obtained has excellent wear-resisting, greasy property; layer protecting film can be formed on mechanical gear surface, effectively extend its service life.

Description

A kind of mechanical lubrication fluid composition and its preparation process
Technical field
The present invention relates to machine oil preparing technical field, specially a kind of mechanical lubrication fluid composition and its preparation work Skill.
Background technology
Lubricating oil is added made of extreme pressure anti-wear additives and oiliness improver modulation based on mineral base oil or synthetic base oil A kind of important lubricating oil is used for various gear assemblies, to prevent tooth surface abrasion, scratch, sintering etc., extends it and uses the longevity Life improves and transmits power efficiency, reduces power loss.Lubricating oil has good wear-resistant, load resistance energy and suitable viscosity. Even if in addition, should also have good thermal oxidation stability, anti-foaming property, water separable performance energy and rustless property synthetic gear oil very Under high operation temperature and load, still ensure that all parts of transmission system are not frayed.
Lubricating oil for machinery can play certain lubricant effect at present, but its long-term greasy property is poor, and not Have repair function, is further improved.
Invention content
The purpose of the present invention is to provide a kind of mechanical lubrication fluid composition and its preparation processes, to solve above-mentioned background skill The problem of being proposed in art.
To achieve the above object, the present invention provides the following technical solutions：A kind of mechanical lubrication fluid composition, lubricating oil composition Object component includes 20-50 parts of glycerine, 10-20 parts of triethanolamine, 8-20 parts of turkey red oil, tackifier 4-12 in parts by weight Part, 3-9 parts of anti-wear agent, 4-16 parts of diene terpolymers and 2-8 parts of polyisobutene.
Preferably, the preferred composition proportion of lubricant oil composite includes 35 parts of glycerine, 15 parts of triethanolamine, turkey red oil 5 parts of 14 parts, 8 parts of tackifier, 6 parts of anti-wear agent, 10 parts of diene terpolymers and polyisobutene.
Preferably, the tackifier are by 20% sodium pyrophosphate, 20% sulfide isobutene, 30% ethyl alcohol, 20% flavones, 10% rosin Glyceryl alcohol forms.
Preferably, the anti-wear agent is by 20% octadecyl alcolol, 10% white carbon, 5% styrene-acrylic emulsion, 15% magnesia powder, 25% poly- four Vinyl fluoride micro mist, 25% sodium carboxymethylcellulose pyce composition.
Preferably, preparation process includes the following steps：
A, it is added in agitator tank after mixing glycerine, triethanolamine, turkey red oil, diene terpolymers, polyisobutene High stirring at low speed, stands 15min later, obtains mixture A；
B, heating water bath in water-bath is added in tackifier, anti-wear agent after mixing, heating temperature is 55 DEG C -75 DEG C, and the time is 20min-40min, later constant temperature 20min, then be slowly cooled to room temperature, obtain mixture B；
C, mixture B is added in mixture A, is added in heating tank and heats after being sufficiently mixed, heating temperature is 120 DEG C -160 DEG C, time 8min-20min after slowly cooling to room temperature later, stands 2h to get to lubricating oil.
Preferably, it is 100-200 revs/min that stirring at low speed, stir speed (S.S.) are first used in the step A, time 8min；It It is 3000-4000 revs/min to use high-speed stirred, stir speed (S.S.) afterwards, time 12min.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation process of the present invention is simple, lubricating oil composition obtained Object has excellent wear-resisting, greasy property, can form layer protecting film on mechanical gear surface, effectively extend its use Service life；Wherein, the tackifier added in the present invention can improve the stability of lubricating oil, extend the holding time of lubricating oil； The anti-wear agent wear-resisting property of addition is good, also has repair function, can repair metal surface fine defects；In addition, the present invention adopts Preparation process is easy to operate, at low cost, wherein the heating water bath used, can prevent active ingredient to be lost in, further carry The high activity of lubricating oil.
Specific implementation mode
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field The every other embodiment that art personnel are obtained without making creative work belongs to the model that the present invention protects It encloses.
The present invention provides the following technical solutions：A kind of mechanical lubrication fluid composition, lubricant oil composite component is by weight Number include 20-50 parts of glycerine, 10-20 parts of triethanolamine, 8-20 parts of turkey red oil, 4-12 parts of tackifier, 3-9 parts of anti-wear agent, 2-8 parts of 4-16 parts of diene terpolymers and polyisobutene；Wherein, tackifier are by 20% sodium pyrophosphate, 20% vulcanization isobutyl Alkene, 30% ethyl alcohol, 20% flavones, 10% rosin glyceryl alcohol composition；Anti-wear agent by 20% octadecyl alcolol, 10% white carbon, 5% styrene-acrylic emulsion, 15% magnesia powder, 25% ptfe micropowder, 25% sodium carboxymethylcellulose pyce composition.
Embodiment one：
Lubricant oil composite component includes 20 parts of glycerine, 10 parts of triethanolamine, 8 parts of turkey red oil, tackifier 4 in parts by weight Part, 3 parts of anti-wear agent, 4 parts of diene terpolymers and 2 parts of polyisobutene.
The preparation process of the present embodiment includes the following steps：
A, it is added in agitator tank after mixing glycerine, triethanolamine, turkey red oil, diene terpolymers, polyisobutene High stirring at low speed, stands 15min later, obtains mixture A；
B, heating water bath in water-bath is added after mixing tackifier, anti-wear agent, heating temperature is 55 DEG C, time 20min, it Constant temperature 20min afterwards, then be slowly cooled to room temperature, obtain mixture B；
C, mixture B is added in mixture A, is added in heating tank and heats after being sufficiently mixed, heating temperature is 120 DEG C, the time For 8min, after slowly cooling to room temperature later, 2h is stood to get to lubricating oil.
In the present embodiment, it is 100 revs/min that stirring at low speed, stir speed (S.S.) are first used in step A, time 8min；It adopts later With high-speed stirred, stir speed (S.S.) is 3000 revs/min, time 12min.
Embodiment two：
Lubricant oil composite component includes 50 parts of glycerine, 20 parts of triethanolamine, 20 parts of turkey red oil, tackifier in parts by weight 8 parts of 12 parts, 9 parts of anti-wear agent, 16 parts of diene terpolymers and polyisobutene.
The preparation process of the present embodiment includes the following steps：
A, it is added in agitator tank after mixing glycerine, triethanolamine, turkey red oil, diene terpolymers, polyisobutene High stirring at low speed, stands 15min later, obtains mixture A；
B, heating water bath in water-bath is added after mixing tackifier, anti-wear agent, heating temperature is 75 DEG C, time 40min, it Constant temperature 20min afterwards, then be slowly cooled to room temperature, obtain mixture B；
C, mixture B is added in mixture A, is added in heating tank and heats after being sufficiently mixed, heating temperature is 160 DEG C, the time For 20min, after slowly cooling to room temperature later, 2h is stood to get to lubricating oil.
In the present embodiment, it is 200 revs/min that stirring at low speed, stir speed (S.S.) are first used in step A, time 8min；It adopts later With high-speed stirred, stir speed (S.S.) is 4000 revs/min, time 12min.
Embodiment three：
Lubricant oil composite component includes 25 parts of glycerine, 12 parts of triethanolamine, 10 parts of turkey red oil, tackifier in parts by weight 3 parts of 6 parts, 4 parts of anti-wear agent, 6 parts of diene terpolymers and polyisobutene.
The preparation process of the present embodiment includes the following steps：
A, it is added in agitator tank after mixing glycerine, triethanolamine, turkey red oil, diene terpolymers, polyisobutene High stirring at low speed, stands 15min later, obtains mixture A；
B, heating water bath in water-bath is added after mixing tackifier, anti-wear agent, heating temperature is 56 DEG C, time 24min, it Constant temperature 20min afterwards, then be slowly cooled to room temperature, obtain mixture B；
C, mixture B is added in mixture A, is added in heating tank and heats after being sufficiently mixed, heating temperature is 125 DEG C, the time For 10min, after slowly cooling to room temperature later, 2h is stood to get to lubricating oil.
In the present embodiment, it is 120 revs/min that stirring at low speed, stir speed (S.S.) are first used in step A, time 8min；It adopts later With high-speed stirred, stir speed (S.S.) is 3200 revs/min, time 12min.
Example IV：
Lubricant oil composite component includes 45 parts of glycerine, 18 parts of triethanolamine, 18 parts of turkey red oil, tackifier in parts by weight 7 parts of 10 parts, 8 parts of anti-wear agent, 13 parts of diene terpolymers and polyisobutene.
The preparation process of the present embodiment includes the following steps：
A, it is added in agitator tank after mixing glycerine, triethanolamine, turkey red oil, diene terpolymers, polyisobutene High stirring at low speed, stands 15min later, obtains mixture A；
B, heating water bath in water-bath is added after mixing tackifier, anti-wear agent, heating temperature is 70 DEG C, time 38min, it Constant temperature 20min afterwards, then be slowly cooled to room temperature, obtain mixture B；
C, mixture B is added in mixture A, is added in heating tank and heats after being sufficiently mixed, heating temperature is 150 DEG C, the time For 16min, after slowly cooling to room temperature later, 2h is stood to get to lubricating oil.
In the present embodiment, it is 180 revs/min that stirring at low speed, stir speed (S.S.) are first used in step A, time 8min；It adopts later With high-speed stirred, stir speed (S.S.) is 3800 revs/min, time 12min.
Embodiment five：
Lubricant oil composite component includes 32 parts of glycerine, 16 parts of triethanolamine, 15 parts of turkey red oil, tackifier in parts by weight 3 parts of 9 parts, 3 parts of anti-wear agent, 12 parts of diene terpolymers and polyisobutene.
The preparation process of the present embodiment includes the following steps：
A, it is added in agitator tank after mixing glycerine, triethanolamine, turkey red oil, diene terpolymers, polyisobutene High stirring at low speed, stands 15min later, obtains mixture A；
B, heating water bath in water-bath is added after mixing tackifier, anti-wear agent, heating temperature is 72 DEG C, time 34min, it Constant temperature 20min afterwards, then be slowly cooled to room temperature, obtain mixture B；
C, mixture B is added in mixture A, is added in heating tank and heats after being sufficiently mixed, heating temperature is 132 DEG C, the time For 12min, after slowly cooling to room temperature later, 2h is stood to get to lubricating oil.
In the present embodiment, it is 140 revs/min that stirring at low speed, stir speed (S.S.) are first used in step A, time 8min；It adopts later With high-speed stirred, stir speed (S.S.) is 3400 revs/min, time 12min.
Embodiment six：
Lubricant oil composite component includes 35 parts of glycerine, 15 parts of triethanolamine, 14 parts of turkey red oil, tackifier in parts by weight 5 parts of 8 parts, 6 parts of anti-wear agent, 10 parts of diene terpolymers and polyisobutene.
The preparation process of the present embodiment includes the following steps：
A, it is added in agitator tank after mixing glycerine, triethanolamine, turkey red oil, diene terpolymers, polyisobutene High stirring at low speed, stands 15min later, obtains mixture A；
B, heating water bath in water-bath is added after mixing tackifier, anti-wear agent, heating temperature is 65 DEG C, time 30min, it Constant temperature 20min afterwards, then be slowly cooled to room temperature, obtain mixture B；
C, mixture B is added in mixture A, is added in heating tank and heats after being sufficiently mixed, heating temperature is 140 DEG C, the time For 14min, after slowly cooling to room temperature later, 2h is stood to get to lubricating oil.
In the present embodiment, it is 150 revs/min that stirring at low speed, stir speed (S.S.) are first used in step A, time 8min；It adopts later With high-speed stirred, stir speed (S.S.) is 3500 revs/min, time 12min.
Preparation process of the present invention is simple, and lubricant oil composite obtained has excellent wear-resisting, greasy property, can be in machine Tool gear surface forms layer protecting film, effectively extends its service life；Wherein, the tackifier added in the present invention can The stability for improving lubricating oil, extends the holding time of lubricating oil；The anti-wear agent wear-resisting property of addition is good, also has and repairs work( Can, metal surface fine defects can be repaired；In addition, the preparation process that the present invention uses is easy to operate, and it is at low cost, wherein using Heating water bath, active ingredient can be prevented to be lost in, further improve the activity of lubricating oil.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of mechanical lubrication fluid composition, it is characterised in that：Lubricant oil composite component includes glycerine 20-50 in parts by weight Part, 10-20 parts of triethanolamine, 8-20 parts of turkey red oil, 4-12 parts of tackifier, 3-9 parts of anti-wear agent, diene terpolymers 4-16 parts and 2-8 parts of polyisobutene.
2. a kind of mechanical lubrication fluid composition according to claim 1, it is characterised in that：Lubricant oil composite preferably at Distribution ratio includes 35 parts of glycerine, 15 parts of triethanolamine, 14 parts of turkey red oil, 8 parts of tackifier, 6 parts of anti-wear agent, alkadienes ternary 5 parts of 0 part of copolymer 1 and polyisobutene.
3. a kind of mechanical lubrication fluid composition according to claim 1 or 2, it is characterised in that：The tackifier are by 20% coke Sodium phosphate, 20% sulfide isobutene, 30% ethyl alcohol, 20% flavones, 10% rosin glyceryl alcohol composition.
4. a kind of mechanical lubrication fluid composition according to claim 1 or 2, it is characterised in that：The anti-wear agent is by 2,0%0 Eight alcohol, 10% white carbon, 5% styrene-acrylic emulsion, 15% magnesia powder, 25% ptfe micropowder, 25% sodium carboxymethylcellulose pyce composition.
5. realizing a kind of preparation process of mechanical lubrication fluid composition as claimed in claim 1 or 2, it is characterised in that：It is prepared Technique includes the following steps：
A, it is added in agitator tank after mixing glycerine, triethanolamine, turkey red oil, diene terpolymers, polyisobutene High stirring at low speed, stands 15min later, obtains mixture A；
B, heating water bath in water-bath is added in tackifier, anti-wear agent after mixing, heating temperature is 55 DEG C -75 DEG C, and the time is 20min-40min, later constant temperature 20min, then be slowly cooled to room temperature, obtain mixture B；
C, mixture B is added in mixture A, is added in heating tank and heats after being sufficiently mixed, heating temperature is 120 DEG C -160 DEG C, time 8min-20min after slowly cooling to room temperature later, stands 2h to get to lubricating oil.
6. a kind of preparation process of mechanical lubrication fluid composition according to claim 5, it is characterised in that：The step A It is middle first use stirring at low speed, stir speed (S.S.) be 100-200 revs/min, time 8min；High-speed stirred, stir speed (S.S.) are used later It is 3000-4000 revs/min, time 12min.
CN201810072323.XA 2018-01-25 2018-01-25 A kind of mechanical lubrication fluid composition and its preparation process Pending CN108300544A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810072323.XA CN108300544A (en) 2018-01-25 2018-01-25 A kind of mechanical lubrication fluid composition and its preparation process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810072323.XA CN108300544A (en) 2018-01-25 2018-01-25 A kind of mechanical lubrication fluid composition and its preparation process

Publications (1)

Publication Number Publication Date
CN108300544A true CN108300544A (en) 2018-07-20

Family

ID=62866670

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810072323.XA Pending CN108300544A (en) 2018-01-25 2018-01-25 A kind of mechanical lubrication fluid composition and its preparation process

Country Status (1)

Country Link
CN (1) CN108300544A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10793759B2 (en) * 2018-11-15 2020-10-06 Yangtze University Sulfur- and phosphorus-free extreme pressure lubricant and preparation method and application thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87105053A (en) * 1987-08-03 1988-02-03 本溪市润滑材料厂 Long-term effective anti-corrosive lubricating grease and manufacture method
EP1346016B1 (en) * 2000-12-20 2009-05-13 Ecolab Inc. Method of lubricating conveyors with a stable transparent glycerine/water/silicone microemulsion
CN103602450A (en) * 2013-10-23 2014-02-26 青岛海伴塑胶工贸有限公司 Machinery lubricating oil composition
CN106190488A (en) * 2016-07-15 2016-12-07 柳州三木科技有限公司 A kind of lubricating oil for mechanical gear
CN107460026A (en) * 2017-09-22 2017-12-12 海门臻凯工业设计有限公司 A kind of machine oil

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87105053A (en) * 1987-08-03 1988-02-03 本溪市润滑材料厂 Long-term effective anti-corrosive lubricating grease and manufacture method
EP1346016B1 (en) * 2000-12-20 2009-05-13 Ecolab Inc. Method of lubricating conveyors with a stable transparent glycerine/water/silicone microemulsion
CN103602450A (en) * 2013-10-23 2014-02-26 青岛海伴塑胶工贸有限公司 Machinery lubricating oil composition
CN106190488A (en) * 2016-07-15 2016-12-07 柳州三木科技有限公司 A kind of lubricating oil for mechanical gear
CN107460026A (en) * 2017-09-22 2017-12-12 海门臻凯工业设计有限公司 A kind of machine oil

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10793759B2 (en) * 2018-11-15 2020-10-06 Yangtze University Sulfur- and phosphorus-free extreme pressure lubricant and preparation method and application thereof

Similar Documents

Publication Publication Date Title
CN104031732B (en) Special micro lubricating agent of oil-water-gas three-phase lubricating system with trace amount and preparation method thereof
CN105732968B (en) Ficoll fatty acid ester and preparation method thereof and prepare micro lubricating oil with the ester
CN103113970B (en) Water-soluble quasi-dry cutting liquid as well as preparation method and use thereof
CN104450104A (en) Method of preparing biodegradable lubricating oil
CN106244295A (en) A kind of extreme boundary lubrication metalworking fluid
CN106244296A (en) A kind of metalworking fluid with excellent rustless property
CN104327930A (en) Green environment-friendly type metal cutting fluid and preparation method thereof
CN104818103B (en) Cold extrusion forming lubricant for low-carbon steel parts for automobiles and preparation method thereof
CN102604723A (en) Lubricating grease composition and preparation method thereof
CN108300544A (en) A kind of mechanical lubrication fluid composition and its preparation process
CN102703185A (en) Compound calcium sulfonate base lubricating grease and preparation method thereof
CN107142134A (en) A kind of metalworking fluid with excellent extreme pressure property
CN107236582A (en) A kind of lube oil additive applied on fullerene
CN108998155A (en) A kind of strong anti-oxidation type lubricating oil and preparation method thereof
CN107245365B (en) Engine oil composition and preparation method thereof
CN110305716A (en) Wear-resistant repairing type energy conservation and environmental protection lubricating oil and preparation method thereof
CN102766500A (en) High-base-number compound-sulfonic lithium/calcium composite lubricating grease and preparation method thereof
CN105154192B (en) A kind of ROLLING OIL for aluminium hot rolling and preparation method thereof
CN104152219B (en) A kind of lubricating grease that is exclusively used in engineering machinery and preparation method thereof
CN106350170A (en) Energy-saving emission-reducing lubricant composition
CN108192705A (en) A kind of environment-friendly type mechanical lubrication fluid composition and its preparation process
CN107502415A (en) A kind of environment-friendly type steam turbine oil and its preparation technology
CN108998176A (en) A kind of aluminum alloy cutting fluid and preparation method thereof
CN109913300A (en) A kind of biodegradable environment protective lubricant and preparation method thereof
CN107164057A (en) It is a kind of for environment-protective lubricant oil of electromechanical equipment and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20180720

RJ01 Rejection of invention patent application after publication