CN108298814A - A kind of novel building glass and preparation method thereof - Google Patents
A kind of novel building glass and preparation method thereof Download PDFInfo
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- CN108298814A CN108298814A CN201810125704.XA CN201810125704A CN108298814A CN 108298814 A CN108298814 A CN 108298814A CN 201810125704 A CN201810125704 A CN 201810125704A CN 108298814 A CN108298814 A CN 108298814A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/002—Use of waste materials, e.g. slags
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
Abstract
The invention discloses a kind of novel building glass and preparation method thereof, are related to glass technology field, specifically include the raw material of following parts by weight meter：40 70 parts of discarded glass, 15 25 parts of quartz sand, 8 16 parts of kaolin, 6 15 parts of dolomite, 10 18 parts of soda ash, 59 parts of barium carbonate, 12 22 parts of calcium sulfate, 26 parts of tourmaline powder, 26 parts of lanthanum sesquioxide, 08 parts of nm-class boron nitride, 28 parts of nano-silicon nitride, 1.5 3.6 parts of fining agent, 0.8 3.2 parts of colorant, floats turbid dose 1.3 2.7 parts, 2.5 4 parts of fluxing agent at 38 parts of lime stone；Building glass of the present invention is prepared as a raw material with discarded glass, with compression strength height, impact resistance is strong, the high advantage of thermal stability, the needs of problems of building glass is not only solved, while solving the process problem of discarded glass, is recycled, it economizes on resources, meets novel ecological economic trend.
Description
Technical field
The present invention relates to glass technology fields, and in particular to a kind of novel building glass and preparation method thereof.
Background technology
In building decoration engineering, glass is a kind of ornament materials being most widely used, with the development of construction industry, glass
Use in building is more and more extensive.Decoration functions of the glass from initial single daylighting function till now are gradually sent out
Transform into the mainstream for modern architecture.In the past 10 years with modernization the building of glass, various hotels, restaurant, apartment, mansion, quotient
The buildings such as industry facility, sports and amusement center and resident's high residential building develop rapidly, and building is to personalized, art up building
Direction is developed, and is increasingly paid close attention to by people.The demand of building glass also gradually increases.
Since the industries such as the unique performance of glass go is widely built, chemical industry use, with the hair of building trade
Exhibition, door glass, the various glass such as wall glass are largely widely used in national economy so that and scrap glass increases significantly,
These scrap glasses are recycled as a major issue in city management.
Invention content
For problems of the prior art, the present invention provides a kind of novel building glass and preparation method thereof, originally
Invention building glass is prepared as a raw material with discarded glass, has compression strength high, and impact resistance is strong, high excellent of thermal stability
Point, not only solves the needs of problems of building glass, while solving the process problem of discarded glass, recycles, and saves money
Source meets novel ecological economic trend.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
A kind of novel building glass includes the raw material of following parts by weight meter：
40-70 parts of discarded glass, 3-8 parts of lime stone, 15-25 parts of quartz sand, 8-16 parts of kaolin, 6-15 parts of dolomite,
10-18 parts of soda ash, 5-9 parts of barium carbonate, 12-22 parts of calcium sulfate, 2-6 parts of tourmaline powder, 2-6 parts of lanthanum sesquioxide, nano silicon nitride
0-8 parts of boron, 1.5-3.6 parts of fining agent, 0.8-3.2 parts of colorant, floats turbid dose 1.3-2.7 parts, is fluxing at 2-8 parts of nano-silicon nitride
2.5-4 parts of agent.
Preferably, include the raw material of following parts by weight meter：40-70 parts of discarded glass, 3-8 parts of lime stone, quartz sand 15-25
Part, 8-16 parts of kaolin, 6-15 parts of dolomite, 10-18 parts of soda ash, 5-9 parts of barium carbonate, 12-22 parts of calcium sulfate, tourmaline powder 2-
6 parts, 2-6 parts of lanthanum sesquioxide, 0-8 parts of nm-class boron nitride, 2-8 parts of nano-silicon nitride, 1.5-3.6 parts of fining agent, colorant
0.8-3.2 parts, floating turbid dose 1.3-2.7 parts, 2.5-4 parts of fluxing agent.
Preferably, the fining agent combines for one or both of antimony oxide and ceria.
Preferably, the colorant be manganese dioxide, potassium bichromate, copper oxide, calcirm-fluoride and cobalt oxide in one kind or
Several combinations.
Preferably, described floating turbid dose is the mixing of one or more of prodan, calcium phosphate and apatite.
Preferably, the fluxing agent is any one of fluorine compounds, boron compound and barium compound.
A kind of preparation method of above-mentioned novel building glass is also disclosed in the present invention specifically to include the following steps：
(1) each raw material is weighed according to the components by weight percent of novel building glass；
(2) discarded glass surface smut is removed, is crushed to bulk of the length less than 5 centimetres and sends out small, it is molten with 40% nitric acid
It after liquid impregnates 3-5 hours, is rinsed well, is dried with clear water, it is spare；
(3) by treated in step (2) discarded glass and lime stone, quartz sand, kaolin, dolomite part, soda ash, carbon
Sour barium, calcium sulfate, tourmaline powder, lanthanum sesquioxide, nm-class boron nitride, nano-silicon nitride after mixing, put into ball mill machine
In be ground to grain diameter be 50-100 mesh, obtain mixture 1；
(4) by mixture 1 obtained in step (3) and fining agent, colorant, floating turbid dose and fluxing agent input mixed at high speed
In machine, mixed at high speed 15-30 minutes obtains mixture 2；
(5) mixture 2 obtained in step (4) is put into smelting furnace, under 1500-1600 degrees Celsius, carries out melting, clear
Clearly, homogenizing is to get melting charge；
(6) melting charge obtained in step (6) is sent into machine die, carries out compression molding；
(7) it is made annealing treatment under glass after molding in step (6) being sent into annealing kiln, natural cooling, cutting, packet
Dress is to get the novel building glass.
Preferably, the moisture of mixture 2 controls below 3% in the step (4).
Preferably, the temperature of the annealing in the step (6) is controlled at 680-800 degrees Celsius.
The present invention has following advantageous effect：
(1) building glass of the present invention is prepared as a raw material with discarded glass, has compression strength high, and impact resistance is strong,
The high advantage of thermal stability, not only solves the needs of problems of building glass, while solving the process problem of discarded glass, follows
Ring utilizes, and economizes on resources, meets novel ecological economic trend；
(2) nano-silicon nitride is added in the present invention, silicon nitride hardness is high, and corrosion resistance is high, inoxidizability is high and good
Heat shock resistance and mechanical shock performance, the glass good combination property prepared；
(3) in raw material of the present invention be added with tourmaline powder, tourmaline powder can absorb the products such as paint, colloid sent out it is different
Taste.For the peculiar smell that in building glass, paint, colloid, coating are sent out in adsorbable architectural environment；
(4) nm-class boron nitride is added in raw material of the present invention, nm-class boron nitride has coefficient of thermal expansion low and thermal conductivity height
The advantages of, it is added in glass material, the thermal shock resistance of glass can be improved.
Specific implementation mode
The specific implementation mode of the present invention is further described with reference to embodiment, following embodiment is only used for more
Technical scheme of the present invention is clearly demonstrated, and not intended to limit the protection scope of the present invention.
Embodiment 1
A kind of novel building glass includes the raw material of following parts by weight meter：
40 parts of discarded glass, 3 parts of lime stone, 15 parts of quartz sand, 8 parts of kaolin, 6 parts of dolomite, 10 parts of soda ash, barium carbonate
5 parts, 12 parts of calcium sulfate, 2 parts of tourmaline powder, 2 parts of lanthanum sesquioxide, 2 parts of nano-silicon nitride, 1.5 parts of fining agent, colorant 0.8
Part floats turbid dose 1.3 parts, 2.5 parts of fluxing agent.
Fining agent is antimony oxide.
Colorant is manganese dioxide and copper oxide according to 2:1 mixing composition.
Floating turbid dose is prodan.
Fluxing agent is fluorine compounds.
A kind of preparation method of above-mentioned novel building glass is also disclosed in the present embodiment specifically to include the following steps：
(1) each raw material is weighed according to the components by weight percent of novel building glass；
(2) discarded glass surface smut is removed, is crushed to bulk of the length less than 5 centimetres and sends out small, it is molten with 40% nitric acid
It after liquid impregnates 3 hours, is rinsed well, is dried with clear water, it is spare；
(3) by treated in step (2) discarded glass and lime stone, quartz sand, kaolin, dolomite part, soda ash, carbon
Sour barium, calcium sulfate, tourmaline powder, lanthanum sesquioxide, nm-class boron nitride, nano-silicon nitride after mixing, put into ball mill machine
In be ground to grain diameter be 50 mesh, obtain mixture 1；
(4) by mixture 1 obtained in step (3) and fining agent, colorant, floating turbid dose and fluxing agent input mixed at high speed
In machine, mixed at high speed 15 minutes obtains mixture 2；
(5) mixture 2 obtained in step (4) is put into smelting furnace, under 1500 degrees Celsius, carries out melting, clarification, equal
Change to get melting charge；
(6) melting charge obtained in step (6) is sent into machine die, carries out compression molding；
(7) it is made annealing treatment under glass after molding in step (6) being sent into annealing kiln, natural cooling, cutting, packet
Dress is to get the novel building glass.
The moisture of mixture 2 is controlled 2.8% in step (4).
The temperature of annealing in step (6) is controlled at 680 degrees Celsius.
Embodiment 2
A kind of novel building glass includes the raw material of following parts by weight meter：
70 parts of discarded glass, 8 parts of lime stone, 25 parts of quartz sand, 16 parts of kaolin, 15 parts of dolomite, 18 parts of soda ash, carbonic acid
9 parts of barium, 22 parts of calcium sulfate, 6 parts of tourmaline powder, 6 parts of lanthanum sesquioxide, 8 parts of nm-class boron nitride, 8 parts of nano-silicon nitride, fining agent
3.6 parts, 3.2 parts of colorant, float turbid dose 2.7 parts, 4 parts of fluxing agent.
Fining agent is ceria.
Colorant is in potassium bichromate and cobalt oxide according to mass ratio 1:3 mixing compositions.
Floating turbid dose is calcium phosphate and apatite according to mass ratio 1:1 mixing composition.
Preferably, the fluxing agent is any one of fluorine compounds, boron compound and barium compound.
A kind of preparation method of above-mentioned novel building glass is also disclosed in the present embodiment specifically to include the following steps：
(1) each raw material is weighed according to the components by weight percent of novel building glass；
(2) discarded glass surface smut is removed, is crushed to bulk of the length less than 5 centimetres and sends out small, it is molten with 40% nitric acid
It after liquid impregnates 5 hours, is rinsed well, is dried with clear water, it is spare；
(3) by treated in step (2) discarded glass and lime stone, quartz sand, kaolin, dolomite part, soda ash, carbon
Sour barium, calcium sulfate, tourmaline powder, lanthanum sesquioxide, nm-class boron nitride, nano-silicon nitride after mixing, put into ball mill machine
In be ground to grain diameter be 100 mesh, obtain mixture 1；
(4) by mixture 1 obtained in step (3) and fining agent, colorant, floating turbid dose and fluxing agent input mixed at high speed
In machine, mixed at high speed 30 minutes obtains mixture 2；
(5) mixture 2 obtained in step (4) is put into smelting furnace, under 1600 degrees Celsius, carries out melting, clarification, equal
Change to get melting charge；
(6) melting charge obtained in step (6) is sent into machine die, carries out compression molding；
(7) it is made annealing treatment under glass after molding in step (6) being sent into annealing kiln, natural cooling, cutting, packet
Dress is to get the novel building glass.
The moisture of mixture 2 is controlled 2% in step (4).
The temperature of annealing in step (6) is controlled at 800 degrees Celsius.
Embodiment 3
A kind of novel building glass includes the raw material of following parts by weight meter：
65 parts of discarded glass, 6 parts of lime stone, 20 parts of quartz sand, 12 parts of kaolin, 10 parts of dolomite, 13 parts of soda ash, carbonic acid
7 parts of barium, 15 parts of calcium sulfate, 4 parts of tourmaline powder, 3 parts of lanthanum sesquioxide, 4 parts of nm-class boron nitride, 5 parts of nano-silicon nitride, fining agent
2.2 parts, 1.8 parts of colorant, float turbid dose 1.5 parts, 3.1 parts of fluxing agent.
Fining agent is antimony oxide and ceria according to mass ratio 1:1 mixing composition.
Colorant is calcirm-fluoride and cobalt oxide according to mass ratio 1:1 mixing composition.
Floating turbid dose is prodan.
Fluxing agent is barium compound.
A kind of preparation method of above-mentioned novel building glass is also disclosed in the present embodiment specifically to include the following steps：
(1) each raw material is weighed according to the components by weight percent of novel building glass；
(2) discarded glass surface smut is removed, is crushed to bulk of the length less than 5 centimetres and sends out small, it is molten with 40% nitric acid
It after liquid impregnates 4 hours, is rinsed well, is dried with clear water, it is spare；
(3) by treated in step (2) discarded glass and lime stone, quartz sand, kaolin, dolomite part, soda ash, carbon
Sour barium, calcium sulfate, tourmaline powder, lanthanum sesquioxide, nm-class boron nitride, nano-silicon nitride after mixing, put into ball mill machine
In be ground to grain diameter be 85 mesh, obtain mixture 1；
(4) by mixture 1 obtained in step (3) and fining agent, colorant, floating turbid dose and fluxing agent input mixed at high speed
In machine, mixed at high speed 25 minutes obtains mixture 2；
(5) mixture 2 obtained in step (4) is put into smelting furnace, under 1560 degrees Celsius, carries out melting, clarification, equal
Change to get melting charge；
(6) melting charge obtained in step (6) is sent into machine die, carries out compression molding；
(7) it is made annealing treatment under glass after molding in step (6) being sent into annealing kiln, natural cooling, cutting, packet
Dress is to get the novel building glass.
The moisture of mixture 2 controls below 3% in step (4).
The temperature of annealing in step (6) is controlled at 750 degrees Celsius.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features.All essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (9)
1. a kind of novel building glass, which is characterized in that including following raw material by weight：40-70 parts of discarded glass, stone
3-8 parts of lime stone, 15-25 parts of quartz sand, 8-16 parts of kaolin, 6-15 parts of dolomite, 10-18 parts of soda ash, 5-9 parts of barium carbonate, sulphur
Sour calcium 12-22 parts, it is 2-6 parts of tourmaline powder, 2-6 parts of lanthanum sesquioxide, 0-8 parts of nm-class boron nitride, 2-8 parts of nano-silicon nitride, clear
Clear 1.5-3.6 parts of agent, floats turbid dose 1.3-2.7 parts, 2.5-4 parts of fluxing agent at 0.8-3.2 parts of colorant.
2. novel building glass according to claim 1, which is characterized in that include the raw material of following parts by weight meter：It is waste and old
65 parts of glass, 6 parts of lime stone, 20 parts of quartz sand, 12 parts of kaolin, 10 parts of dolomite, 13 parts of soda ash, 7 parts of barium carbonate, calcium sulfate
15 parts, 4 parts of tourmaline powder, 3 parts of lanthanum sesquioxide, 4 parts of nm-class boron nitride, 5 parts of nano-silicon nitride, 2.2 parts of fining agent, colorant
1.8 parts, floating turbid dose 1.5 parts, 3.1 parts of fluxing agent.
3. novel building glass according to claim 1, which is characterized in that the fining agent is antimony oxide and ceria
One or both of combine.
4. novel building glass according to claim 1, which is characterized in that the colorant is manganese dioxide, dichromic acid
One or more of potassium, copper oxide, calcirm-fluoride and cobalt oxide combine.
5. novel building glass according to claim 1, which is characterized in that described floating turbid dose is prodan, calcium phosphate
With the mixing of one or more of apatite.
6. novel building glass according to claim 1, which is characterized in that the fluxing agent is fluorine compounds, boronation conjunction
Any one of object and barium compound.
7. a kind of preparation method of novel building glass as claimed in any one of claims 1 to 6, which is characterized in that including following
Step：
(1) each raw material is weighed according to the components by weight percent of novel building glass；
(2) discarded glass surface smut is removed, is crushed to bulk of the length less than 5 centimetres and sends out small, is soaked with 40% salpeter solution
Bubble is rinsed well after 3-5 hours with clear water, is dried, spare；
(3) by treated in step (2) discarded glass and lime stone, quartz sand, kaolin, dolomite part, soda ash, carbonic acid
Barium, calcium sulfate, tourmaline powder, lanthanum sesquioxide, nm-class boron nitride, nano-silicon nitride after mixing, are put into ball mill machine
It is 50-100 mesh to be ground to grain diameter, obtains mixture 1；
(4) by mixture 1 obtained in step (3) and fining agent, colorant, floating turbid dose and fluxing agent input high-speed mixer
In, mixed at high speed 15-30 minutes obtains mixture 2；
(5) mixture 2 obtained in step (4) is put into smelting furnace, under 1500-1600 degrees Celsius, carry out melting, clarification,
Homogenizing is to get melting charge；
(6) melting charge obtained in step (6) is sent into machine die, carries out compression molding；
(7) it is made annealing treatment under glass after molding in step (6) being sent into annealing kiln, natural cooling, cutting, packaging,
Up to the novel building glass.
8. the preparation method of novel building glass according to claim 7, which is characterized in that mixing in the step (4)
The moisture of object 2 controls below 3%.
9. the preparation method of novel building glass according to claim 7, which is characterized in that moving back in the step (6)
The temperature of fire processing is controlled at 680-800 degrees Celsius.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810125704.XA CN108298814A (en) | 2018-02-08 | 2018-02-08 | A kind of novel building glass and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810125704.XA CN108298814A (en) | 2018-02-08 | 2018-02-08 | A kind of novel building glass and preparation method thereof |
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| CN108298814A true CN108298814A (en) | 2018-07-20 |
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| CN201810125704.XA Withdrawn CN108298814A (en) | 2018-02-08 | 2018-02-08 | A kind of novel building glass and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107759189A (en) * | 2016-08-22 | 2018-03-06 | 银川隆基硅材料有限公司 | Thermostable heat-isolating coating and the method for improving single crystal growing furnace crucible side service life |
| CN110615609A (en) * | 2019-07-16 | 2019-12-27 | 北京水木九天科技有限公司 | Novel glass material |
| CN111925119A (en) * | 2020-08-05 | 2020-11-13 | 郑州市华源玻璃制品有限公司 | Glass beer bottle and preparation method thereof |
| CN111943510A (en) * | 2020-08-19 | 2020-11-17 | 石家庄泰图生态科技有限公司 | Method for manufacturing handicraft added with glass color stone |
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| CN101643316A (en) * | 2009-09-04 | 2010-02-10 | 云南家华新型墙体玻璃有限公司 | Method for producing U-shaped glass by taking waste glass as raw material |
| CN105461223A (en) * | 2014-08-29 | 2016-04-06 | 天津市瀚凯玻璃科技有限公司 | Manufacturing process for colored glass |
| CN105819689A (en) * | 2016-05-19 | 2016-08-03 | 台玻安徽玻璃有限公司 | Heat-shock-resistant float glass |
| CN106892559A (en) * | 2017-03-23 | 2017-06-27 | 合肥协耀玻璃制品有限公司 | A kind of production technology of building glass |
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2018
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101643316A (en) * | 2009-09-04 | 2010-02-10 | 云南家华新型墙体玻璃有限公司 | Method for producing U-shaped glass by taking waste glass as raw material |
| CN105461223A (en) * | 2014-08-29 | 2016-04-06 | 天津市瀚凯玻璃科技有限公司 | Manufacturing process for colored glass |
| CN105819689A (en) * | 2016-05-19 | 2016-08-03 | 台玻安徽玻璃有限公司 | Heat-shock-resistant float glass |
| CN106892559A (en) * | 2017-03-23 | 2017-06-27 | 合肥协耀玻璃制品有限公司 | A kind of production technology of building glass |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107759189A (en) * | 2016-08-22 | 2018-03-06 | 银川隆基硅材料有限公司 | Thermostable heat-isolating coating and the method for improving single crystal growing furnace crucible side service life |
| CN107759189B (en) * | 2016-08-22 | 2020-07-24 | 银川隆基硅材料有限公司 | High-temperature-resistant heat-insulating coating and method for prolonging service life of crucible side of single crystal furnace |
| CN110615609A (en) * | 2019-07-16 | 2019-12-27 | 北京水木九天科技有限公司 | Novel glass material |
| CN110615609B (en) * | 2019-07-16 | 2021-08-10 | 北京水木九天科技有限公司 | Novel glass material |
| CN111925119A (en) * | 2020-08-05 | 2020-11-13 | 郑州市华源玻璃制品有限公司 | Glass beer bottle and preparation method thereof |
| CN111943510A (en) * | 2020-08-19 | 2020-11-17 | 石家庄泰图生态科技有限公司 | Method for manufacturing handicraft added with glass color stone |
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Application publication date: 20180720 |