CN108272690A - Have both anti-blue light and the cosmetic material of UV resistance and the preparation method and application thereof - Google Patents
Have both anti-blue light and the cosmetic material of UV resistance and the preparation method and application thereof Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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Abstract
The present invention relates to a kind of cosmetic materials and the preparation method and application thereof having both anti-blue light and UV resistance.The raw material components of cosmetics include jasmine flower extract, Flos Buddlejae extract, bisabolol, glycerine, water, propylene glycol, titanium dioxide, ring five dimethyl silicone polymer, isohexadecane, dimethyl silicone polymer, vaseline, 1,2 hexylene glycols, butylmethoxydibenzoylmethane and xanthans etc..Full photoprotection cosmetics provided by the invention select the plant extract containing active skull cap components to form; contain a variety of nourishing ingredients; slim and graceful ventilative, fine and smooth texture, soft and moist nourishing; clear separation layer can be formed in skin surface; play excellent anti-blue light, UV resistance and anti-oxidant and other effects; it protects skin from interference such as dust, haze, color make-ups, constantly takees good care of delicate skin, all-weather protective is provided for skin.In addition, the full photoprotection cosmetic industry of the present invention is notable, stability is good, easy to use, universality is strong, it is with a wide range of applications.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of cosmetic material having both anti-blue light and UV resistance and
Preparation method and application.
Background technology
It is well known that important component of the blue light as visible light, has the characteristics that wavelength is short, energy is high；Blue light can
To penetrate entire dermal layer of the skin, but the shortcomings that be unable to filter blue light based on human body itself, lutein can not be synthesized, lead to indigo plant
Light is to our skin and the harm getting worse of eyes.Current research shows：Blue light is AMD (age-related macular degeneration)
Cause：High energy shortwave blue light can lead to visual fatigue, visual impairment, cataract, AMD, the even different degrees of eye illness such as blindness；
Night can inhibit melatonin secretion by high energy shortwave blue light, lead to circadian rhythm disturbances, so as to cause a variety of diseases of body.
In addition, the light irradiation of 280nm~400nm can make the epidermis of people tanned；Wherein, the light of 280nm~320nm,
Referred to as UV-B light can cause skin burn and erythema, to destroy the tanned formation of nature, therefore should irradiate UV-B and shield
It removes.Meanwhile the UV-A light itself for making 320nm~400nm wavelength of skin tanning is also easy to bring detrimental effect, especially
For being the skin for for sensitive skin or persistently receiving to shine upon；UV-A light can especially make skin lose elasticity and occur
Wrinkle leads to premature aging；Its accelerate the triggering of erythematous response or it is certain individual with make it is this reinforcement is obtained by the reaction,
And phototoxicity or light allergic reaction may be led to；Therefore, also it is necessary to UV-A is irradiated shielding to remove.
Based on this, occurring minority on the market has anti-blue light or anti-ultraviolet cosmetics, but such cosmetics is universal
There are effect unobvious, easily causes allergic phenomena and do not have the shortcomings of universality.Therefore it provides one kind can effect it is aobvious
Work, full photoprotection cosmetics without side-effects and with universality are particularly important.
Invention content
For the defects in the prior art, the present invention is intended to provide a kind of cosmetic material having both anti-blue light and UV resistance
And the preparation method and application thereof.Full photoprotection cosmetics provided by the invention select the plant extract containing active skull cap components and
At, containing a variety of nourishing ingredients, slim and graceful ventilative, fine and smooth texture, soft and moist nourishing can form clear separation layer in skin surface,
Excellent anti-blue light, UV resistance and anti-oxidant and other effects are played, protects skin from interference such as dust, haze, color make-ups, constantly
Delicate skin is takeed good care of, all-weather protective is provided for skin.In addition, full photoprotection cosmetic industry provided by the invention is significantly, surely
It is qualitative it is good, easy to use, universality is strong, be with a wide range of applications.
For this purpose, the present invention provides the following technical solutions：
In a first aspect, the present invention provides a kind of full photoprotection cosmetics, raw material components include：Jasmine flower extract, close illiteracy
It is one or more in flower extract, chamomile extract and glycerine.
Preferably, raw material components by weight, including：5~15 parts by weight of jasmine flower extract, Flos Buddlejae extract 2
10~20 parts by weight of~6 parts by weight, 5~10 parts by weight of chamomile extract and glycerine.
Preferably, raw material components further include：2~5 parts by weight of ethylhexyl palmitate, 1~3 parts by weight of lanolin, yellow mustard
Sub 2~5 parts by weight and 0.5~0.8 parts by weight of asafoetide.
Preferably, the preparation method of jasmine flower extract includes：By Jasmine use mass percentage concentration for 0.01%~
1% sodium hydrate aqueous solution dipping, refluxing extraction is carried out at 90~105 DEG C, filters and collects filtrate, obtain jasmine later
Flower extract；The preparation method of Flos Buddlejae extract includes：Butterflybush flower is extracted using supercritical carbon dioxide, collects filter
Liquid and adjust pH value be 7.5~8.5, obtain Flos Buddlejae extract；Chamomile extract specifically selects bisabolol.
Second aspect, the present invention provide a kind of preparation method of full photoprotection active component, include the following steps：This is sent out
Each raw material component in bright full photoprotection active component is weighed in proportion, is uniformly mixed later, and full photoprotection active component is obtained.
The third aspect, full photoprotection active component provided by the invention are protected in UV resistance, anti-blue light, slim and graceful ventilative, moisturizing
Application in wet cosmetics and/or cosmetic additive agent.
Fourth aspect, the present invention provide a kind of full photoprotection cosmetics, the raw material components of cosmetics include active component with
And helper component, and the mass ratio of active component and helper component is (1~50)：100.
Preferably, the raw material components of helper component by weight, including：500~2000 parts by weight of water, atoleine 1
~2 parts by weight, 1~3 parts by weight of propylene glycol, 0.1~0.5 parts by weight of titanium dioxide, 1~2 weight of ring five dimethyl silicone polymer
Part, 1~5 parts by weight of isohexadecane, 2~5 parts by weight of dimethyl silicone polymer, 1~2 parts by weight of vaseline, 1~5 weight of cera alba
Part, 1~3 parts by weight of magnesium stearate, 0.2~2 parts by weight of ethylhexyl methoxy cinnamate, two (lauramide glutamine) rely
1~3 parts by weight of propylhomoserin sodium, 2~5 parts by weight of Octocrilene, 1~2 weight of methylene bis-benzotriazolyl tetramethyl butyl phenol
Part, 1~5 parts by weight of butylmethoxydibenzoylmethane, 1~5 parts by weight of C12-15 alcohol benzoic ethers, 3~8 weight of tocopherol
Measure part, 1~5 parts by weight of 1,2- hexylene glycols, 1~2 parts by weight of parahydroxyacet-ophenone, 1~3 parts by weight of Phenoxyethanol, magnesium sulfate 0.1
1~3 parts by weight of~0.8 parts by weight and xanthans.
5th aspect, the present invention provide a kind of preparation method of full photoprotection cosmetics, include the following steps：S101：It presses
Ratio weighs each raw material component in helper component, carries out ultrasonic agitation processing, is centrifuged under 2500~4000r/min after cooling
5~20min removes sediment, obtains helper component；S102：Helper component is heated to 50 DEG C~60 DEG C, active component is added
And be uniformly mixed, obtain full photoprotection cosmetics.
The above technical solution of the present invention has the following advantages over the prior art：
(1) applicant has found by numerous studies：Full photoprotection cosmetics selection provided by the invention contains natural activity
The plant extract of ingredient forms, and contains a variety of nourishing ingredients, slim and graceful ventilative, fine and smooth texture, soft and moist nourishing, can be in skin surface
Form clear separation layer, play excellent anti-blue light, UV resistance and anti-oxidant and other effects, protect skin from dust, haze,
The interference such as color make-up, constantly take good care of delicate skin, and all-weather protective is provided for skin.
(2) the full photoprotection cosmetics being prepared using method provided by the invention, through Efficacy experiments, toxicological test and
Stability experiment, has no toxic side effect, obvious effect, stability are good, easy to use, universality is strong, is with a wide range of applications.
(3) using the preparation method of full photoprotection cosmetics provided by the invention, each original can retained to greatest extent
While expecting medicine active constituent, the active ingredient in each raw medicinal material can be fully released, to make finally to be prepared into
The full photoprotection cosmetics arrived have the effect of excellent；And preparation method process stabilizing, low energy consumption, raw material are extensive, process is simple
Single-unit saves；Production can be completed using existing equipment, equipment requirement is reduced, to zero environmental.
The additional aspect and advantage of the present invention will be set forth in part in the description, and will partly become from the following description
Obviously, or practice through the invention is recognized.
Specific implementation mode
The embodiment of technical solution of the present invention will be described in detail below.Following embodiment is only used for clearer
Illustrate technical scheme of the present invention, therefore be only used as example, and not intended to limit the protection scope of the present invention.
Experimental method in following embodiments is unless otherwise specified conventional method.
Test material as used in the following examples is unless otherwise specified to be commercially available from conventional reagent shop.
Quantitative test in following embodiment, is respectively provided with three repeated experiments, and data are the average value of three repeated experiments
Or mean+SD.
Jasmine, butterflybush flower, yellow chamomile, SEMEN SINAPIS ALBAE and asafoetide as used in the following examples meet Chinese Pharmacopoeia
Pertinent regulations under (version in 2017) each medicinal material item of text.Before feeding intake, by identification, ingredients material object and title phase
Symbol, quality comply with standard.
It illustrates With reference to embodiment：
Embodiment one
The present embodiment provides a kind of full photoprotection cosmetics, it is 5 that the raw material components of cosmetics, which include mass ratio,：100 work
Property component and helper component.Active component includes：5 parts by weight of jasmine flower extract, red do not have 6 parts by weight of Flos Buddlejae extract
20 parts by weight of 5 parts by weight of medicine alcohol and glycerine；And the preparation method of active component is：It is mixed after raw material components are weighed in proportion equal
It is even, obtain active component；The preparation method of jasmine flower extract includes：By Jasmine use mass percentage concentration for 1% hydrogen
Aqueous solution of sodium oxide impregnates, and carries out refluxing extraction at 90 DEG C later, filters and collect filtrate, obtain jasmine flower extract；It is close
Cover flower extract preparation method include：Butterflybush flower is extracted using supercritical carbon dioxide, collect filtrate and adjusts pH
Value is 8.5, obtains Flos Buddlejae extract.Helper component includes：2000 parts by weight of water, 1 parts by weight of atoleine, 3 weight of propylene glycol
Measure part, 0.1 parts by weight of titanium dioxide, 2 parts by weight of ring five dimethyl silicone polymer, 1 parts by weight of isohexadecane, polydimethylsiloxanes
5 parts by weight of alkane, 1 parts by weight of vaseline, 5 parts by weight of cera alba, 1 parts by weight of magnesium stearate, 2 weight of ethylhexyl methoxy cinnamate
Part, two (lauramide glutamine) Sodium lysinates, 1 parts by weight, 5 parts by weight of Octocrilene, di-2-ethylhexylphosphine oxide-benzotriazole base four
1 parts by weight of methyl butyl phenol, 5 parts by weight of butylmethoxydibenzoylmethane, 1 parts by weight of C12-15 alcohol benzoic ethers, life
Educate 8 parts by weight of phenol, 1 parts by weight of 1,2- hexylene glycols, 2 parts by weight of parahydroxyacet-ophenone, 1 parts by weight of Phenoxyethanol, 0.8 weight of magnesium sulfate
Measure part and 1 parts by weight of xanthans.
In addition, according to preparation method provided by the invention, full photoprotection cosmetics are prepared, are included the following steps：
S101：The each raw material component in helper component is weighed in proportion, ultrasonic agitation processing is carried out, in 2500r/ after cooling
20min is centrifuged under min, is removed sediment, is obtained helper component；
S102：Helper component is heated to 50 DEG C, active component is added and is uniformly mixed, full photoprotection cosmetics are obtained.
Embodiment two
The present embodiment provides a kind of full photoprotection cosmetics, it is 30 that the raw material components of cosmetics, which include mass ratio,：100 work
Property component and helper component.Active component includes：15 parts by weight of jasmine flower extract, red do not have 2 parts by weight of Flos Buddlejae extract
10 parts by weight of 10 parts by weight of medicine alcohol and glycerine；The preparation method of active component is：It is mixed after raw material components are weighed in proportion equal
It is even, obtain active component；The preparation method of jasmine flower extract includes：Use mass percentage concentration for 0.01% Jasmine
Sodium hydrate aqueous solution impregnates, and carries out refluxing extraction at 105 DEG C later, filters and collect filtrate, obtain jasmine flower extract；
The preparation method of Flos Buddlejae extract includes：Butterflybush flower is extracted using supercritical carbon dioxide, collect filtrate and is adjusted
PH value is 7.5, obtains Flos Buddlejae extract.Helper component includes：500 parts by weight of water, 2 parts by weight of atoleine, 1 weight of propylene glycol
Measure part, 0.5 parts by weight of titanium dioxide, 1 parts by weight of ring five dimethyl silicone polymer, 5 parts by weight of isohexadecane, polydimethylsiloxanes
2 parts by weight of alkane, 2 parts by weight of vaseline, 1 parts by weight of cera alba, 3 parts by weight of magnesium stearate, 0.2 weight of ethylhexyl methoxy cinnamate
Measure part, two (lauramide glutamine) Sodium lysinates, 3 parts by weight, 2 parts by weight of Octocrilene, di-2-ethylhexylphosphine oxide-benzotriazole base
2 parts by weight of tetramethyl butyl phenol, 1 parts by weight of butylmethoxydibenzoylmethane, 5 parts by weight of C12-15 alcohol benzoic ethers,
3 parts by weight of tocopherol, 5 parts by weight of 1,2- hexylene glycols, 1 parts by weight of parahydroxyacet-ophenone, 3 parts by weight of Phenoxyethanol, magnesium sulfate 0.1
3 parts by weight of parts by weight and xanthans.
In addition, according to preparation method provided by the invention, full photoprotection cosmetics are prepared, are included the following steps：
S101：The each raw material component in helper component is weighed in proportion, ultrasonic agitation processing is carried out, in 4000r/ after cooling
5min is centrifuged under min, is removed sediment, is obtained helper component；
S102：Helper component is heated to 60 DEG C, active component is added and is uniformly mixed, full photoprotection cosmetics are obtained.
Embodiment three
The present embodiment changes relative parameters setting on the basis of embodiment one and forms.
The present embodiment provides a kind of full photoprotection cosmetics, it is 5 that the raw material components of cosmetics, which include mass ratio,：100 work
Property component and helper component.Active component includes：5 parts by weight of jasmine flower extract, red do not have 6 parts by weight of Flos Buddlejae extract
5 parts by weight of medicine alcohol, 5 parts by weight of ethylhexyl palmitate, 1 parts by weight of lanolin, 5 parts by weight of SEMEN SINAPIS ALBAE, 0.5 parts by weight of asafoetide and
20 parts by weight of glycerine；And the preparation method of active component is：It is uniformly mixed after raw material components are weighed in proportion, obtains activearm
Point；The preparation method of jasmine flower extract includes：Mass percentage concentration is used to be soaked for 1% sodium hydrate aqueous solution Jasmine
Stain carries out refluxing extraction at 90 DEG C later, filters and collects filtrate, obtain jasmine flower extract；The system of Flos Buddlejae extract
Preparation Method includes：Butterflybush flower is extracted using supercritical carbon dioxide, it is 8.5 to collect filtrate and adjust pH value, is obtained close
Cover flower extract.Helper component includes：2000 parts by weight of water, 1 parts by weight of atoleine, 3 parts by weight of propylene glycol, titanium dioxide
0.1 parts by weight, 2 parts by weight of ring five dimethyl silicone polymer, 1 parts by weight of isohexadecane, 5 parts by weight of dimethyl silicone polymer, mine
1 parts by weight of fat, 5 parts by weight of cera alba, 1 parts by weight of magnesium stearate, 2 parts by weight of ethylhexyl methoxy cinnamate, two (lauroyl
Amine glutamine) 1 parts by weight of Sodium lysinate, 5 parts by weight of Octocrilene, 1 weight of methylene bis-benzotriazolyl tetramethyl butyl phenol
Part, 5 parts by weight of butylmethoxydibenzoylmethane, 1 parts by weight of C12-15 alcohol benzoic ethers, 8 parts by weight of tocopherol, 1 are measured,
1 parts by weight of 2- hexylene glycols, 2 parts by weight of parahydroxyacet-ophenone, 1 parts by weight of Phenoxyethanol, 0.8 parts by weight of magnesium sulfate and xanthans
1 parts by weight.
In addition, according to preparation method provided by the invention, full photoprotection cosmetics are prepared, are included the following steps：
S101：The each raw material component in helper component is weighed in proportion, ultrasonic agitation processing is carried out, in 2500r/ after cooling
20min is centrifuged under min, is removed sediment, is obtained helper component；
S102：Helper component is heated to 50 DEG C, active component is added and is uniformly mixed, full photoprotection cosmetics are obtained.
Example IV
The present embodiment changes relative parameters setting on the basis of embodiment two and forms.
The present embodiment provides a kind of full photoprotection cosmetics, it is 30 that the raw material components of cosmetics, which include mass ratio,：100 work
Property component and helper component.Active component includes：15 parts by weight of jasmine flower extract, red do not have 2 parts by weight of Flos Buddlejae extract
10 parts by weight of medicine alcohol, 2 parts by weight of ethylhexyl palmitate, 3 parts by weight of lanolin, 2 parts by weight of SEMEN SINAPIS ALBAE, 00.8 parts by weight of asafoetide
With 10 parts by weight of glycerine；The preparation method of active component is：It is uniformly mixed after raw material components are weighed in proportion, obtains activearm
Point；The preparation method of jasmine flower extract includes：Use mass percentage concentration water-soluble for 0.01% sodium hydroxide Jasmine
Liquid impregnates, and carries out refluxing extraction at 105 DEG C later, filters and collect filtrate, obtain jasmine flower extract；Flos Buddlejae extract
Preparation method include：Butterflybush flower is extracted using supercritical carbon dioxide, it is 7.5 to collect filtrate and adjust pH value, is obtained
To Flos Buddlejae extract.Helper component includes：500 parts by weight of water, 2 parts by weight of atoleine, 1 parts by weight of propylene glycol, titanium dioxide
0.5 parts by weight of titanium, 1 parts by weight of ring five dimethyl silicone polymer, 5 parts by weight of isohexadecane, 2 parts by weight of dimethyl silicone polymer,
2 parts by weight of vaseline, 1 parts by weight of cera alba, 3 parts by weight of magnesium stearate, 0.2 parts by weight of ethylhexyl methoxy cinnamate, the two (moons
Osmanthus amide Gln) 3 parts by weight of Sodium lysinate, 2 parts by weight of Octocrilene, di-2-ethylhexylphosphine oxide-benzotriazole base tetramethyl butyl
2 parts by weight of phenol, 1 parts by weight of butylmethoxydibenzoylmethane, 5 parts by weight of C12-15 alcohol benzoic ethers, 3 weight of tocopherol
Part, 5 parts by weight of 1,2- hexylene glycols, 1 parts by weight of parahydroxyacet-ophenone, 3 parts by weight of Phenoxyethanol, 0.1 parts by weight of magnesium sulfate and
3 parts by weight of xanthans.
In addition, according to preparation method provided by the invention, full photoprotection cosmetics are prepared, are included the following steps：
S101：The each raw material component in helper component is weighed in proportion, ultrasonic agitation processing is carried out, in 4000r/ after cooling
5min is centrifuged under min, is removed sediment, is obtained helper component；
S102：Helper component is heated to 60 DEG C, active component is added and is uniformly mixed, full photoprotection cosmetics are obtained.
In addition, in order to further highlight the advantage of technical solution of the present invention, following comparative example is set.It should be noted that
Following comparative examples are arranged on the basis of example IV.
Comparative example one
This comparative example provides a kind of full photoprotection cosmetics, and it is 30 that the raw material components of cosmetics, which include mass ratio,：100 work
Property component and helper component.Active component includes：15 parts by weight of jasmine flower extract, red do not have 2 parts by weight of Flos Buddlejae extract
10 parts by weight of medicine alcohol, 10 parts by weight of 2 parts by weight of ethylhexyl palmitate, 3 parts by weight of lanolin and glycerine；The preparation of active component
Method is：It is uniformly mixed after raw material components are weighed in proportion, obtains active component；The preparation method packet of jasmine flower extract
It includes：It uses mass percentage concentration to be impregnated for 0.01% sodium hydrate aqueous solution Jasmine, flows back at 105 DEG C later
Extraction, filters and collects filtrate, obtain jasmine flower extract；The preparation method of Flos Buddlejae extract includes：Butterflybush flower is used
Supercritical carbon dioxide extracts, and it is 7.5 to collect filtrate and adjust pH value, obtains Flos Buddlejae extract.Helper component includes：
500 parts by weight of water, 2 parts by weight of atoleine, 1 parts by weight of propylene glycol, 0.5 parts by weight of titanium dioxide, five polydimethylsiloxanes of ring
It is 1 parts by weight of alkane, 5 parts by weight of isohexadecane, 2 parts by weight of dimethyl silicone polymer, 2 parts by weight of vaseline, 1 parts by weight of cera alba, hard
3 parts by weight of fatty acid magnesium, 0.2 parts by weight of ethylhexyl methoxy cinnamate, two (lauramide glutamine) Sodium lysinates, 3 weight
Part, 2 parts by weight of Octocrilene, 2 parts by weight of methylene bis-benzotriazolyl tetramethyl butyl phenol, butyl methoxy dibenzoyl
1 parts by weight of methylmethane, 5 parts by weight of C12-15 alcohol benzoic ethers, 3 parts by weight of tocopherol, 5 parts by weight of 1,2- hexylene glycols, to hydroxyl
1 parts by weight of acetophenone, 3 parts by weight of 3 parts by weight of Phenoxyethanol, 0.1 parts by weight of magnesium sulfate and xanthans.
In addition, according to preparation method provided by the invention, full photoprotection cosmetics are prepared, are included the following steps：
S101：The each raw material component in helper component is weighed in proportion, ultrasonic agitation processing is carried out, in 4000r/ after cooling
5min is centrifuged under min, is removed sediment, is obtained helper component；
S102：Helper component is heated to 60 DEG C, active component is added and is uniformly mixed, full photoprotection cosmetics are obtained.
Comparative example two
This comparative example provides a kind of full photoprotection cosmetics, and it is 30 that the raw material components of cosmetics, which include mass ratio,：100 work
Property component and helper component.Active component includes：15 parts by weight of jasmine flower extract, red do not have 2 parts by weight of Flos Buddlejae extract
10 parts by weight of medicine alcohol, 2 parts by weight of ethylhexyl palmitate, 3 parts by weight of lanolin, 2 parts by weight of SEMEN SINAPIS ALBAE, 00.8 parts by weight of asafoetide
With 10 parts by weight of glycerine；The preparation method of active component is：It is uniformly mixed after raw material components are weighed in proportion, obtains activearm
Point；The preparation method of jasmine flower extract includes：Jasmine is subjected to refluxing extraction at 105 DEG C, filters and collects filtrate, obtain
To jasmine flower extract；The preparation method of Flos Buddlejae extract includes：Butterflybush flower is extracted using supercritical carbon dioxide,
It is 7.5 to collect filtrate and adjust pH value, obtains Flos Buddlejae extract.Helper component includes：500 parts by weight of water, 2 weight of atoleine
Measure part, 1 parts by weight of propylene glycol, 0.5 parts by weight of titanium dioxide, 1 parts by weight of ring five dimethyl silicone polymer, 5 weight of isohexadecane
Part, 2 parts by weight of dimethyl silicone polymer, 2 parts by weight of vaseline, 1 parts by weight of cera alba, 3 parts by weight of magnesium stearate, methoxycinnamate
0.2 parts by weight of sour ethylhexyl, two (lauramide glutamine) Sodium lysinates, 3 parts by weight, 2 parts by weight of Octocrilene, methylene
Base pair -2 parts by weight of benzotriazole base tetramethyl butyl phenol, 1 parts by weight of butylmethoxydibenzoylmethane, C12-15 alcohol benzene
5 parts by weight of formic acid esters, 3 parts by weight of tocopherol, 5 parts by weight of 1,2- hexylene glycols, 1 parts by weight of parahydroxyacet-ophenone, 3 weight of Phenoxyethanol
Measure part, 3 parts by weight of 0.1 parts by weight of magnesium sulfate and xanthans.
In addition, according to preparation method provided by the invention, full photoprotection cosmetics are prepared, are included the following steps：
S101：The each raw material component in helper component is weighed in proportion, ultrasonic agitation processing is carried out, in 4000r/ after cooling
5min is centrifuged under min, is removed sediment, is obtained helper component；
S102：Helper component is heated to 60 DEG C, active component is added and is uniformly mixed, full photoprotection cosmetics are obtained.
Comparative example three
This comparative example provides a kind of full photoprotection cosmetics, and it is 30 that the raw material components of cosmetics, which include mass ratio,：100 work
Property component and helper component.Active component includes：15 parts by weight of jasmine flower extract, red do not have 2 parts by weight of Flos Buddlejae extract
10 parts by weight of medicine alcohol, 2 parts by weight of ethylhexyl palmitate, 3 parts by weight of lanolin, 2 parts by weight of SEMEN SINAPIS ALBAE, 00.8 parts by weight of asafoetide
With 10 parts by weight of glycerine；The preparation method of active component is：It is uniformly mixed after raw material components are weighed in proportion, obtains activearm
Point；The preparation method of jasmine flower extract and Flos Buddlejae extract is：Raw material Jasmine or raw material butterflybush flower are used into quality
The sodium hydrate aqueous solution that percentage concentration is 0.01% impregnates, and carries out refluxing extraction at 105 DEG C later, filters and collect filter
Liquid obtains jasmine flower extract or Flos Buddlejae extract.Helper component includes：500 parts by weight of water, 2 parts by weight of atoleine, third
1 parts by weight of glycol, 0.5 parts by weight of titanium dioxide, 1 parts by weight of ring five dimethyl silicone polymer, 5 parts by weight of isohexadecane, poly- two
2 parts by weight of methylsiloxane, 2 parts by weight of vaseline, 1 parts by weight of cera alba, 3 parts by weight of magnesium stearate, methoxy cinnamic acid ethyl
0.2 parts by weight of own ester, two (lauramide glutamine) Sodium lysinates, 3 parts by weight, 2 parts by weight of Octocrilene, di-2-ethylhexylphosphine oxide-benzene
And 2 parts by weight of triazolyl tetramethyl butyl phenol, 1 parts by weight of butylmethoxydibenzoylmethane, C12-15 alcohol benzoic ethers 5
Parts by weight, 3 parts by weight of tocopherol, 5 parts by weight of 1,2- hexylene glycols, 1 parts by weight of parahydroxyacet-ophenone, 3 parts by weight of Phenoxyethanol, sulphur
3 parts by weight of 0.1 parts by weight of sour magnesium and xanthans.
In addition, according to preparation method provided by the invention, full photoprotection cosmetics are prepared, are included the following steps：
S101：The each raw material component in helper component is weighed in proportion, ultrasonic agitation processing is carried out, in 4000r/ after cooling
5min is centrifuged under min, is removed sediment, is obtained helper component；
S102：Helper component is heated to 60 DEG C, active component is added and is uniformly mixed, full photoprotection cosmetics are obtained.
In addition, the effect of in order to preferably evaluate each embodiment full photoprotection cosmetics, carry out following experiment：
One, toxicity test
It is the small white mouse 70 (each 35 of male and female) of 18~22g to select weight, is divided into 7 groups, each 5 of every group of male and female, small white mouse
Back unhairing exposes exocuticle, unhairing range 2cm × 2cm, and first group to the 7th group is smeared various embodiments of the present invention and right respectively
The full photoprotection cosmetics that ratio is prepared, dosage 5g, successive administration 30 days.When during administration and 1 week after being discontinued,
Observe white mouse growth conditions and activity and diet, identification hematology, blood biochemical analysis, organ tissue structure and routine urinalysis etc..Knot
Fruit finds the health existence of all small white mouses, without any side effects；Blood picture, liver function, each organs and tissues state is dissected and observed,
The indifference compared with normal small white mouse.It is demonstrated experimentally that full photoprotection cosmetics provided by the invention are nontoxic, drug safety is reliable.
Two, the anti-blue light performance detection of the full photoprotection cosmetics of each embodiment
Detection method：By using the survival rate of cell of CellTiter96 (MTS) detections with metabolic activity, proliferation
Rate come study blue light to the damage of people's epidermal keratinocyte (HEK) and human dermis' fibrocyte (HDF) and the present invention makeup
Protective action of the product to the damage.
Specifically：Cell is cultivated in 96- microwell plates, the cell quantity in each microwell plate is identical.People's table will be housed
The micropore of chrotoplast and human dermis' fibrocyte is covered by a packaged flat bottom sterile plate for having cosmetic sample solution of the present invention,
Top apart from culture dish 30cm carries out LED (476nm, 1900lux) blue light illumination 9h, then use CellTiter96 (MTS) into
Row cell survival rate measures.
Blank control：(37 DEG C) cell is not exposed under blue light at room temperature.Sample solution is respectively：By each embodiment and right
The cosmetics of ratio are dissolved in the solution in dimethyl sulfoxide (DMSO)；Specific data are shown in Table 1.
The anti-blue light performance of the full photoprotection cosmetics of 1 each embodiment of table
| People's epidermal keratinocyte activity/% | Human dermis' fibrocyte activity/% | |
| Embodiment one | 90 | 93 |
| Embodiment two | 92 | 93 |
| Embodiment three | 99 | 100 |
| Example IV | 97 | 98 |
| Comparative example one | 66 | 59 |
| Comparative example two | 72 | 67 |
| Comparative example three | 70 | 46 |
Three, the uvioresistant performance detection of the full photoprotection cosmetics of each embodiment
Specifically, female volunteers 70 are collected, are divided into 10 groups, try out each embodiment and comparative example cosmetics respectively；
UV light skin detectors are used to detect the uvioresistant performance data of each cosmetics, and skin whitening effects test data moral later
State's CK companies dermal melanin and haematochrome test probe MX 1 are tested.Each group of data is averaged, specifically such as 2 institute of table
Show.
The uvioresistant performance of the full photoprotection cosmetics of 2 each embodiment of table
| Before use | It uses 2 weeks | It uses 4 weeks | |
| Embodiment one | 356 | 321 | 298 |
| Embodiment two | 369 | 320 | 295 |
| Embodiment three | 350 | 302 | 286 |
| Example IV | 393 | 306 | 280 |
| Comparative example one | 372 | 365 | 350 |
| Comparative example two | 368 | 359 | 352 |
| Comparative example three | 353 | 350 | 345 |
Four, the antioxidation of the full photoprotection cosmetics of each embodiment
(1) Scavenging activity on hydroxyl free radical measures：Take the Phen solution 1ml of 0.75mmol/L in 10ml tool plug test tubes
In, 2ml0.2mmol/L is sequentially added, the ferrous sulfate of PBS buffer solution, 1ml0.75mmol/L that pH is 7.5 is uniformly mixed, adds
Enter 1ml sample solutions, the hydrogen peroxide of 1ml0.01% is added after mixing, with deionized water constant volume, 37 DEG C of heating water bath 60min,
Go out to measure its absorbance value in 510nm.The clearance rate of hydroxy radical is calculated as follows：Clearance rate=[(A1-A0)/(A2-A0)]
× 100%；Wherein, A1For absorbance when hydrogen peroxide and sample is added；A0For the suction for hydrogen peroxide being added but when being not added with sample
Luminosity；A2For hydrogen peroxide and the sample not absorbance of added-time.In addition, the configuration method of sample solution is：Take 5g each respectively
The full photoprotection cosmetics of embodiment are added after 100ml deionized waters in 7 beakers in 45 DEG C of microwave heating 60min, cooling
The required sample solution of the present invention is obtained after to room temperature.
(2) measurement of DPPH clearance rates：Each 2ml of above-mentioned sample solution is taken, the DPPH that 2ml 0.1mmol/L are added is molten
Liquid is uniformly mixed, and after being protected from light 30min, absorbance value A1 is measured at 217nm；Blank group replaces sample solution with DPPH,
Control group replaces sample solution with isometric distilled water.Clearance rate is calculated as follows：Clearance rate=[1- (A1-A0)/A2]×
100%；Wherein, A1For the absorbance of sample sets；A0For the absorbance of blank group；A2For the absorbance of control group.Each embodiment
The antioxidative specific experiment data of cosmetic are as shown in table 3：
The antioxidation of the full photoprotection cosmetics of 3 each embodiment of table
| Scavenging action to hydroxyl free radical/% | Measurement/% of DPPH clearance rates | |
| Embodiment one | 92 | 90 |
| Embodiment two | 90 | 91 |
| Embodiment three | 98 | 96 |
| Example IV | 97 | 94 |
| Comparative example one | 76 | 69 |
| Comparative example two | 83 | 87 |
| Comparative example three | 79 | 78 |
Certainly, the case where being enumerated in addition to embodiment one to example IV, the type and weight percent of other raw material components,
Condition and parameter in preparation process etc. are also possible.
Full photoprotection cosmetics provided by the invention select the plant extract containing active skull cap components to form, and contain a variety of
Ingredient is nourished, slim and graceful ventilative, fine and smooth texture, soft and moist nourishing can form clear separation layer in skin surface, play excellent resist
Blue light, UV resistance and anti-oxidant and other effects, protect skin from interference such as dust, haze, color make-ups, constantly take good care of delicate flesh
Skin provides all-weather protective for skin.In addition, full photoprotection cosmetic industry provided by the invention is notable, stability is good, uses
Conveniently, universality is strong, is with a wide range of applications.
In the description of this specification, it is to be understood that reference term " one embodiment ", " is shown " some embodiments "
The description of example ", " specific example " or " some examples " etc. mean specific features described in conjunction with this embodiment or example, structure,
Material or feature are included at least one embodiment or example of the invention.In the present specification, above-mentioned term is shown
The statement of meaning property is necessarily directed to identical embodiment or example.Moreover, specific features, structure, material or the spy of description
Point may be combined in any suitable manner in any one or more of the embodiments or examples.In addition, without conflicting with each other,
Those skilled in the art can be by different embodiments or examples described in this specification and different embodiments or examples
Feature is combined.
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example
Property, it is not considered as limiting the invention, those skilled in the art within the scope of the invention can be to above-mentioned
Embodiment is changed, changes, replacing and modification.
Claims (9)
1. a kind of full photoprotection active component, which is characterized in that raw material components include：
It is one or more in jasmine flower extract, Flos Buddlejae extract, chamomile extract and glycerine.
2. full photoprotection active component according to claim 1, which is characterized in that raw material components by weight, including：
5~15 parts by weight of jasmine flower extract, 2~6 parts by weight of Flos Buddlejae extract, 5~10 parts by weight of chamomile extract and
10~20 parts by weight of glycerine.
3. full photoprotection active component according to claim 2, which is characterized in that further include：
2~5 parts by weight of ethylhexyl palmitate, 1~3 parts by weight of lanolin, 2~5 parts by weight of SEMEN SINAPIS ALBAE and asafoetide 0.5~0.8
Parts by weight.
4. full photoprotection active component according to claim 2, it is characterised in that：
The preparation method of the jasmine flower extract includes：By Jasmine use mass percentage concentration for 0.01%~1% hydrogen
Aqueous solution of sodium oxide impregnates, and carries out refluxing extraction at 90~105 DEG C later, filters and collect filtrate, obtains Jasmine extraction
Object；
The preparation method of the Flos Buddlejae extract includes：Butterflybush flower is extracted using supercritical carbon dioxide, collects filter
Liquid and adjust pH value be 7.5~8.5, obtain Flos Buddlejae extract；
The chamomile extract specifically selects bisabolol.
5. a kind of preparation method of full photoprotection active component, which is characterized in that include the following steps：
Claims 1 to 4 any one of them raw material components are weighed in proportion, are uniformly mixed later, it is anti-to obtain the full light
Protect active component.
6. any one of Claims 1 to 4 full photoprotection active component is in UV resistance, anti-blue light, slim and graceful ventilative, replenishing water and preserving moisture
Cosmetics and/or cosmetic additive agent in application.
7. a kind of full photoprotection cosmetics, which is characterized in that the raw material components of the cosmetics include：
Claims 1 to 4 any one of them active component and helper component；Wherein, the active component and the auxiliary
The mass ratio of component is (1~50)：100.
8. full photoprotection cosmetics according to claim 7, it is characterised in that：
The raw material components of the helper component by weight, including：500~2000 parts by weight of water, 1~2 weight of atoleine
Part, 1~3 parts by weight of propylene glycol, 0.1~0.5 parts by weight of titanium dioxide, 1~2 parts by weight of ring five dimethyl silicone polymer, different ten
Six alkane, 1~5 parts by weight, 2~5 parts by weight of dimethyl silicone polymer, 1~2 parts by weight of vaseline, 1~5 parts by weight of cera alba, tristearin
1~3 parts by weight of sour magnesium, 0.2~2 parts by weight of ethylhexyl methoxy cinnamate, two (lauramide glutamine) Sodium lysinates 1
~3 parts by weight, 2~5 parts by weight of Octocrilene, 1~2 parts by weight of methylene bis-benzotriazolyl tetramethyl butyl phenol, butyl first
1~5 parts by weight of oxygroup dibenzoyl methane, 1~5 parts by weight of C12-15 alcohol benzoic ethers, 3~8 parts by weight of tocopherol, 1,2-
1~5 parts by weight of hexylene glycol, 1~2 parts by weight of parahydroxyacet-ophenone, 1~3 parts by weight of Phenoxyethanol, 0.1~0.8 weight of magnesium sulfate
Part and 1~3 parts by weight of xanthans.
9. the preparation method of the full photoprotection cosmetics described in claim 7 or 8, which is characterized in that include the following steps：
S101：Weigh each raw material component in helper component in proportion, carry out ultrasonic agitation processing, it is cooling after in 2500~
5~20min is centrifuged under 4000r/min, is removed sediment, is obtained the helper component；
S102：The helper component is heated to 50 DEG C~60 DEG C, the active component is added and is uniformly mixed, is obtained described complete
Photoprotection cosmetics.
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| CN109464308A (en) * | 2018-11-15 | 2019-03-15 | 广东轻工职业技术学院 | A kind of essential oil composition and application with anti-blue light skin-care effect |
| WO2020152577A1 (en) * | 2019-01-21 | 2020-07-30 | University Of Pretoria | Anticancer activity of buddleja saligna compositions |
| CN109674720A (en) * | 2019-01-24 | 2019-04-26 | 广州市瓷颜化妆品有限公司 | A kind of anti-blue light frost and preparation method thereof |
| CN109674720B (en) * | 2019-01-24 | 2021-06-25 | 广州市瓷颜化妆品有限公司 | Blue light resisting cream and preparation method thereof |
| CN109771353A (en) * | 2019-03-29 | 2019-05-21 | 广东芭薇生物科技股份有限公司 | A kind of anti-blue light and infrared composition and its cosmetics |
| CN109771353B (en) * | 2019-03-29 | 2021-08-13 | 广东芭薇生物科技股份有限公司 | Blue light and infrared prevention composition and cosmetics thereof |
| CN110292543A (en) * | 2019-06-14 | 2019-10-01 | 上海科颜生物科技有限公司 | It is a kind of substitute ultraviolet absorbing agent biological composition and its application |
| CN110292543B (en) * | 2019-06-14 | 2022-04-01 | 上海科颜生物科技有限公司 | Biological composition for replacing ultraviolet absorbent and application thereof |
| CN110840794A (en) * | 2019-12-12 | 2020-02-28 | 广州卡迪莲化妆品科技有限公司 | Blue-light-resistant and infrared-resistant sunscreen composition and application thereof |
| CN110840794B (en) * | 2019-12-12 | 2021-11-26 | 广州卡迪莲化妆品科技有限公司 | Blue-light-resistant and infrared-resistant sunscreen composition and application thereof |
| CN113197793A (en) * | 2021-04-15 | 2021-08-03 | 广州天玺生物科技有限公司 | Blue light resistant composition and preparation method and application thereof |
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Application publication date: 20180713 |