CN108271874A - High DHA content antarctic krill oil reconciliation health-care oil and preparation method thereof - Google Patents
High DHA content antarctic krill oil reconciliation health-care oil and preparation method thereof Download PDFInfo
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- CN108271874A CN108271874A CN201810020523.0A CN201810020523A CN108271874A CN 108271874 A CN108271874 A CN 108271874A CN 201810020523 A CN201810020523 A CN 201810020523A CN 108271874 A CN108271874 A CN 108271874A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
- A23D9/013—Other fatty acid esters, e.g. phosphatides
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Abstract
The present invention provides a kind of antarctic krill oil of high DHA content reconciliation health-care oils；It counts in parts by weight, including following several components：5 95 parts of high DHA greases, 5 95 parts of krill oils and 0 0.5 parts of auxiliary elements.The high DHA grease is the grease that DHA content is more than EPA, specially DHA algal oil, one or more of isolate and purify DHA triglycerides, DHA phosphatide and DHA ethyl ester.Since there are DHA algal oil itself a little fragrants to have no fishlike smell, therefore the unhappy smell of krill oil can be diluted and be mitigated after krill oil mixing is added, while retain good mouthfeel.In addition, being more than the grease of EPA by the way that DHA content is added, DHA concentration in oil product is significantly improved, the low defect of DHA content in antarctic krill oil is improved；Meanwhile the ratio of EPA and DHA in health-care oil is can be adjusted according to the needs, to expand the suitable group of krill oil.
Description
Technical field
The invention belongs to field of food, and in particular to oil processing field, more particularly to it is a kind of by high DHA content grease and
Health-care oil and preparation method thereof made of antarctic krill oil allotment.
Background technology
Krill is the food that the numerous fish in the Antarctic Continent, seabird, sea dog, penguin and cetacean are depended on for existence, it
It is played a very important role in Southern Oceans food chain.Krill is the fourth-largest money in area after grain, oil, coal
Source, reserves are very surprising, and nutritive value is high.Antarctic krill oil is that powder is made by the krill for being grown in the South Pole in groups,
Again from powder extract oil and obtain.Have containing abundant omega-3 aliphatic acid, phosphatide, choline and astaxanthin etc. in antarctic krill oil
Beneficial ingredient.Currently, at abroad, edible krill oil has the history of decades.In American-European countries, krill oil is as a kind of new resources
Food, the mass selling on the market in the form of dietary supplements, obtains the approval of official of American-European countries for many years.
Scientific investigations showed that increasing intake and the antithrombotic of krill oil omega-3 aliphatic acid, anti-arrhythmia cordis, anti-dynamic
Arteries and veins hardens and anti-inflammatory functional correlation.Omega-3 in krill oil have been demonstrated to releive with the relevant mood of premenstrual syndrome and
Physical problems, moreover it is possible to adjust blood fat health, increase high density cholesterol (HDL) and reduce low density cholesterol (LDL), reduce heart
And hepatic fat content.Scientific investigations showed that compared with the omega-3 aliphatic acid in three acid esters form of typical glycerol, krill oil
In in the form of Phospholipids existing for omega-3 aliphatic acid be easier to be absorbed by the body, transformation efficiency higher is more suitable for human body
Nutritional supplement.However, fixed in the fishy odor having due to antarctic krill oil and its omega-3 aliphatic acid contained
Eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA) proportion relation, limit its scope of application and audience.Root
According to the literature, EPA content is far above DHA content in conventional antarctic krill oil, is not suitable for infant, pregnant woman and wet nurse et al.
Group.
Application for a patent for invention 201210280323.1 discloses " edible blend oil of addition antarctic krill oil ".The invention is special
In the edible blend oil of profit application, antarctic krill oil is 0.1%~99.9%, edible vegetable oil or its tune by weight percentage
It is 0.1%~99.9% with oil.Wherein, the vegetable oil or its reconciliation that antarctic krill oil weight percent is 90%~99.9%
Oil, and be added in antarctic krill oil as diluent as the grease of principal mode using triglycerides and be used for as raw materials for production
Semi-finished product；Antarctic krill oil account for 0.1%~10.0% so that people while daily edible oil, can also absorb it is abundant not
Saturated fatty acid and high-quality phosphatide so that edible oil is healthier, plays the role of nutrition and health care.However, the application for a patent for invention
Only krill oil is added in oil with common edible, although improving unsaturated fatty acid in edible oil and high-quality phosphatide
Content, but still without changing the intrinsic fishlike smell of antarctic krill oil and it is not suitable for the crowds such as infant, pregnant woman and wet nurse
The problem of.
Invention content
For problem and shortage existing for current antarctic krill oil, the present invention provides a kind of South Pole phosphorus of high DHA content
Shrimp sauce reconciliation health-care oil.The antarctic krill oil reconciliation health-care oil not only effectively improves the intrinsic flavor of antarctic krill oil, also
EPA and DHA ratios in health-care oil can be adjusted, the absorptivity of DHA, expands the suitable group of krill oil during enhancing is oily.
Technical scheme of the present invention：
The antarctic krill oil reconciliation health-care oil of high DHA content, is counted, including following several components in parts by weight：5-95 parts
High DHA grease, 5-95 parts of krill oils and 0-0.5 parts of auxiliary elements.
Grease of the high DHA grease for DHA content more than EPA, specially DHA algal oil isolate and purify DHA glycerine three
One or more of fat, DHA phosphatide and DHA ethyl ester.The high DHA grease is all made of commercial goods.Due to DHA algal oil itself
Fishlike smell is had no with a little fragrants, therefore can dilute and mitigate the unhappy smell of krill oil after krill oil mixing is added, simultaneously
Retain good mouthfeel.In addition, being more than the grease of EPA by the way that DHA content is added, DHA concentration in oil product is significantly improved, is improved
The low defect of DHA content in antarctic krill oil；Meanwhile the ratio of EPA and DHA in health-care oil is can be adjusted according to the needs, from
And expand the suitable group of krill oil.
The auxiliary element is natural VE, ascorbic acid, tea polyphenols, bamboo-leaves flavones, Vitwas E, anti-bad
One or more of hematic acid palmitate, astaxanthin and rosemary.
Preferably, in the reconciliation health-care oil, the weight ratio of DHA and EPA are 0.8-76.
Preferably, in the reconciliation health-care oil, the weight ratio of DHA and EPA are 1-64.
Preferably, in the reconciliation health-care oil, the weight ratio of DHA and EPA are 3-50.
Preferably, in the reconciliation health-care oil, the weight ratio of DHA and EPA are 5-50.
Preferably, in the reconciliation health-care oil, the weight ratio of DHA and EPA are 10-40.
Preferably, in the reconciliation health-care oil, the weight ratio of DHA and EPA are 20-40.
The preparation method of the antarctic krill oil reconciliation health-care oil of high DHA content, includes the following steps：
(1) weigh the high DHA grease of 5-95 parts by weight, the krill oil of 5-95 parts by weight, the auxiliary of 0-0.5 parts by weight at
Point；The high DHA grease is DHA algal oil, one or more of isolates and purifies DHA triglycerides, DHA phosphatide and DHA ethyl ester；
The auxiliary element is natural VE, ascorbic acid, tea polyphenols, bamboo-leaves flavones, Vitwas E, ascorbic acid palm
One or more of acid esters, astaxanthin and rosemary；
(2) component for weighing step (1) under nitrogen protection, under 20-60 DEG C of temperature condition stirring to be uniformly mixed,
Obtain the antarctic krill oil reconciliation health-care oil of high DHA content.The speed of the stirring is 30-60 revs/min, the stirring
Time is 20-30min.
Beneficial effects of the present invention：
1. flavored oils of the present invention can effectively improve the absorptivity of DHA in oil product；Due to main in antarctic krill oil
It is the phosphatide utilized that is easily absorbed by the body to want ingredient, therefore, increases the absorption of DHA in ready-mixed oil under synergistic mechanism effect
Rate.
2. ready-mixed oil of the present invention substantially increases the concentration of DHA, a small amount of edible DHA that can meet recommends to take the photograph daily
Enter the requirement of amount；Mouthfeel and flavor can also be taken into account simultaneously.
3. ready-mixed oil of the present invention can carry out personalized collocation, flexible modulation DHA according to area and eating habit
Intake and total grease intake, the most of market demand can be met, have a vast market foreground and huge
Economic benefit.
Specific implementation mode
With reference to embodiment, the present invention is described further.
Table 1.DHA algae oils at being grouped as
The main component of 2. antarctic krill oil of table forms
Embodiment 1：
Parts by weight meter, by 5 parts of antarctic krill oil, 95 parts of DHA algal oil (based on containing pure DHA 45%), and natural dimension life
0.2 part of plain E is sufficiently mixed.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 20 minutes, mixing speed is 60 turns per minute, is mixed
It is 60 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 43.4%, DHA in this ready-mixed oil:EPA ratios are 29.The main fat of ready-mixed oil
Fat acid forms and content is as shown in table 3.
Embodiment 2：
It counts in parts by weight, it is fully mixed by 95 parts of antarctic krill oil, 5 parts of DHA algal oil (based on containing pure DHA 50%)
It closes.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 30 minutes, mixing speed is 30 turns per minute, is mixed
It is 20 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 15.2%, DHA in this ready-mixed oil:EPA ratios are 0.8.Ready-mixed oil is main
Aliphatic acid forms and content is as shown in table 3.
Embodiment 3：
It counts in parts by weight, by 6 parts of antarctic krill oil, 93.9 parts of DHA ethyl ester (based on containing pure DHA 60%), and it is natural
0.05 part of vitamin E, 0.02 part of Vitwas E, 0.03 part of ascorbyl palmitate, is sufficiently mixed.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 25 minutes, mixing speed is 60 turns per minute, is mixed
It is 50 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 55.7%, DHA in this ready-mixed oil:EPA ratios are 50.The main fat of ready-mixed oil
Fat acid forms and content is as shown in table 3.
Embodiment 4：
It counts in parts by weight, by 24.8 parts of antarctic krill oil, 75 parts of DHA ethyl ester (based on containing pure DHA 50%) and day
Right 0.1 part of vitamin E, 0.1 part of rosemary are sufficiently mixed.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 30 minutes, mixing speed is 40 turns per minute, is mixed
It is 40 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 38.9%, DHA in this ready-mixed oil:EPA ratios are 10.The main fat of ready-mixed oil
Fat acid forms and content is as shown in table 3.
Embodiment 5：
It counts in parts by weight, by 6.8 parts of antarctic krill oil, 53 parts of DHA algal oil (based on containing pure DHA 55%), DHA phosphorus
0.1 part of 40 parts of fat (based on containing pure DHA 55%) and natural VE, 0.05 part of ascorbic acid, 0.05 part of tea polyphenols fill
Divide mixing.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 30 minutes, mixing speed is 50 turns per minute, is mixed
It is 55 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 52.1%, DHA in this ready-mixed oil:EPA ratios are 40.The main fat of ready-mixed oil
Fat acid forms and content is as shown in table 3.
Embodiment 6：
It counts in parts by weight, 94.5 parts of DHA algal oil (based on containing DHA 60%), 5 parts of antarctic krill oil and natural dimension are given birth to
0.2 part of plain E, 0.1 part of ascorbic acid, 0.05 part of rosemary, 0.05 part of Vitwas E, ascorbyl palmitate 0.1
Part, it is sufficiently mixed.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 30 minutes, mixing speed is 30 turns per minute, is mixed
It is 35 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 57.4%, DHA in this ready-mixed oil:EPA ratios are 76.The main fat of ready-mixed oil
Fat acid forms and content is as shown in table 3.
Embodiment 7：
It counts in parts by weight, by 5.84 parts of antarctic krill oil, 94 parts of DHA algal oil (based on containing DHA 60%), and it is natural
0.05 part of vitamin E, 0.1 part of ascorbic acid, 0.01 part of astaxanthin are sufficiently mixed.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 30 minutes, mixing speed is 30 turns per minute, is mixed
It is 25 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 56.8%, DHA in this ready-mixed oil:EPA ratios are 64.The main fat of ready-mixed oil
Fat acid forms and content is as shown in table 3.
Embodiment 8：
It counts in parts by weight, by 79.8 parts of antarctic krill oil, 20 parts of DHA algal oil (based on containing DHA 55%), and it is natural
0.1 part of vitamin E, 0.05 part of ascorbic acid, 0.05 part of ascorbyl palmitate are sufficiently mixed.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 30 minutes, mixing speed is 30 turns per minute, is mixed
It is 55 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 15.8%, DHA in this ready-mixed oil:EPA ratios are 1.The main fat of ready-mixed oil
Fat acid forms and content is as shown in table 3.
Embodiment 9：
It counts in parts by weight, by 54.9 parts of antarctic krill oil, 45 parts of DHA algal oil (based on containing DHA 55%), and it is natural
0.1 part of vitamin E is sufficiently mixed.
The preparation method of nutrition oil of the present invention, includes the following steps：
The above components are mixed after the assay was approved, are then stirred 30 minutes, mixing speed is 30 turns per minute, is mixed
It is 55 DEG C to close temperature, and nitrogen is filled in mixed process and is protected.Product oil is obtained after the completion of stirring, and product oil is filled into food
In grade packaged bucket, quantitative sealed.It is filled with nitrogen during packing, prevents its contact with oxygen.
It calculates as mass fraction, DHA content is 28.1%, DHA in this ready-mixed oil:EPA ratios are 3.The main fat of ready-mixed oil
Fat acid forms and content is as shown in table 3.
Embodiment 10：
It counts in parts by weight, by 30.8 parts of antarctic krill oil, 69 parts of DHA phosphatide (based on containing DHA 55%), and it is natural
0.1 part of vitamin E, 0.05 part of ascorbic acid, 0.05 part of ascorbyl palmitate are sufficiently mixed, and are stirred 30 minutes, stirring
Speed is 30 turns per minute, and mixing temperature is 50 DEG C, and nitrogen is filled in mixed process and is protected.Finished product is obtained after the completion of stirring
Product oil is filled into food-grade pail pack, quantitative sealed by oil.It is filled with nitrogen during packing, prevents itself and oxygen
Contact.
It calculates as mass fraction, DHA content is 41.9%, DHA in this ready-mixed oil:EPA ratios are 6.8.Ready-mixed oil is main
Aliphatic acid forms and content is as shown in table 3.
3. embodiment 1-10 of table prepares primary fat acid content in ready-mixed oil
As seen from the results in Table 3, the ready-mixed oil DHA concentration that prepared by embodiment 1-10 is high, can also take into account mouthfeel and wind simultaneously
Taste, it is a small amount of to eat the requirement that meet the daily recommended intakes of DHA and EPA, and be easy to be absorbed by the body.In addition, the south
Pole krill oil reconciliation health-care oil can also be realized according to area and personal eating habit on-demand customization, to solve Chinese residents per capita
The relatively low problem of DHA intakes provides a kind of convenience, flexible DHA supplies mode, has a vast market foreground and huge
Business potential.
Claims (10)
1. the antarctic krill oil reconciliation health-care oil of high DHA content, it is characterised in that：It counts in parts by weight, including following several groups
Part：5-95 parts of high DHA greases, 5-95 parts of krill oils and 0-0.5 parts of auxiliary elements.
2. the antarctic krill oil reconciliation health-care oil of high DHA content according to claim 1, it is characterised in that：The high DHA
Grease is the grease that DHA content is more than EPA.
3. the antarctic krill oil reconciliation health-care oil of high DHA content according to claim 2, it is characterised in that：The high DHA
Grease is DHA algal oil, one or more of isolates and purifies DHA triglycerides, DHA phosphatide and DHA ethyl ester.
4. the antarctic krill oil reconciliation health-care oil of high DHA content according to claim 1, it is characterised in that：The auxiliary
Ingredient is natural VE, ascorbic acid, tea polyphenols, bamboo-leaves flavones, Vitwas E, ascorbyl palmitate, shrimp
One or more of green element and rosemary.
5. the antarctic krill oil reconciliation health-care oil of the high DHA content according to any one of claim 1-4, feature exist
In：In the reconciliation health-care oil, the weight ratio of DHA and EPA are 0.8-76.
6. the antarctic krill oil reconciliation health-care oil of the high DHA content according to any one of claim 1-4, feature exist
In：In the reconciliation health-care oil, the weight ratio of DHA and EPA are 1-64.
7. the antarctic krill oil reconciliation health-care oil of the high DHA content according to any one of claim 1-4, feature exist
In：In the reconciliation health-care oil, the weight ratio of DHA and EPA are 3-50.
8. the antarctic krill oil reconciliation health-care oil of the high DHA content according to any one of claim 1-4, feature exist
In：In the reconciliation health-care oil, the weight ratio of DHA and EPA are 10-40.
9. the preparation method of the antarctic krill oil reconciliation health-care oil of high DHA content, it is characterised in that：Include the following steps：(1) claim
Take the high DHA grease of 5-95 parts by weight, the krill oil of 5-95 parts by weight, the auxiliary element of 0-0.5 parts by weight；(2) by step (1)
The component weighed under nitrogen protection, under 20-60 DEG C of temperature condition stirring to being uniformly mixed to get to the south of high DHA content
Pole krill oil reconciliation health-care oil.
10. the preparation method of the antarctic krill oil reconciliation health-care oil of high DHA content according to claim 9, feature exist
In：The high DHA grease is DHA algal oil, high DHA fish oil, isolates and purifies in DHA triglycerides, DHA phosphatide and DHA ethyl ester
It is one or more of；The auxiliary element be natural VE, ascorbic acid, tea polyphenols, bamboo-leaves flavones, Vitwas E,
One or more of ascorbyl palmitate, astaxanthin and rosemary；The speed of the stirring is 30-60 revs/min, institute
The time for stating stirring is 20-30min.
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| CN110564787A (en) * | 2019-08-02 | 2019-12-13 | 大渔华创(广州)海洋生物科技有限公司 | Polyunsaturated fatty acid-rich blood phospholipid composition and preparation method thereof |
| CN113115843A (en) * | 2019-12-30 | 2021-07-16 | 丰益(上海)生物技术研发中心有限公司 | Structured emulsions containing algal oil |
| TWI765535B (en) * | 2021-01-18 | 2022-05-21 | 健茂生物科技股份有限公司 | Health product composition containing plant-based oils |
| CN114748553A (en) * | 2022-03-30 | 2022-07-15 | 大连工业大学 | Composition with auxiliary blood fat reducing and antioxidant functions |
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| CN105211326A (en) * | 2014-06-25 | 2016-01-06 | 中国科学院青岛生物能源与过程研究所 | A kind of health care seasoning oil being rich in DHA and preparation method thereof |
| CN106360437A (en) * | 2016-11-30 | 2017-02-01 | 广州康琪莱生物科技有限公司 | Krill oil microcapsule with antioxidation effect and preparation process thereof |
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| US9610298B1 (en) * | 2011-06-15 | 2017-04-04 | Ronald E Rosedale | Omega-3 fatty acid nutriceutical composition and optimization method |
| CN105211326A (en) * | 2014-06-25 | 2016-01-06 | 中国科学院青岛生物能源与过程研究所 | A kind of health care seasoning oil being rich in DHA and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110564787A (en) * | 2019-08-02 | 2019-12-13 | 大渔华创(广州)海洋生物科技有限公司 | Polyunsaturated fatty acid-rich blood phospholipid composition and preparation method thereof |
| CN110564787B (en) * | 2019-08-02 | 2023-02-21 | 大渔华创(广州)海洋生物科技有限公司 | Polyunsaturated fatty acid-rich blood phospholipid composition and preparation method thereof |
| CN113115843A (en) * | 2019-12-30 | 2021-07-16 | 丰益(上海)生物技术研发中心有限公司 | Structured emulsions containing algal oil |
| CN113115843B (en) * | 2019-12-30 | 2023-12-19 | 丰益(上海)生物技术研发中心有限公司 | Structured emulsions containing algae oil |
| TWI765535B (en) * | 2021-01-18 | 2022-05-21 | 健茂生物科技股份有限公司 | Health product composition containing plant-based oils |
| CN114748553A (en) * | 2022-03-30 | 2022-07-15 | 大连工业大学 | Composition with auxiliary blood fat reducing and antioxidant functions |
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