CN108261861A - Clarifying smoke composition - Google Patents

Clarifying smoke composition Download PDF

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Publication number
CN108261861A
CN108261861A CN201810221740.6A CN201810221740A CN108261861A CN 108261861 A CN108261861 A CN 108261861A CN 201810221740 A CN201810221740 A CN 201810221740A CN 108261861 A CN108261861 A CN 108261861A
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parts
extract
weight
semen
smoke composition
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王婧宁
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Guorun Biotechnology (shenzhen) Co Ltd
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Guorun Biotechnology (shenzhen) Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D47/00Separating dispersed particles from gases, air or vapours by liquid as separating agent
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D47/00Separating dispersed particles from gases, air or vapours by liquid as separating agent
    • B01D47/06Spray cleaning
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
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  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
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  • Medicines Containing Plant Substances (AREA)

Abstract

Clarifying smoke composition in parts by weight, prepares raw material and includes:14 parts of seedling of xiongqiong extract, 1 1.5 parts of qinghaosu, 26 parts of mannosan, 14 parts of Herba Solani Lyrati extract, 23 parts of ethyl alcohol, 26 parts of Semen Cuscutae extract, 1.2 1.8 parts of turanose, 26 parts of Radix Morindae Officinalis extract, 14 parts of Gentrin Knotweed P.E, 0.2 0.8 parts of caffeine, 13 parts of 1,2 propylene glycol, 26 parts of aminoglycan, 26 parts of milkwort extract, 0.5 2 parts of rhamnose, 26 parts of tara gum, 6 10 parts of licorice, 26 parts of semen vaccariae extraction, 26 parts of Semen Plantaginis extract, 150 parts of deionized water.

Description

Clarifying smoke composition
Technical field
The present invention relates to clarifying smoke composition, further to a kind of clarifying smoke composition.
Background technology
Air is basic eco-environmental elements for the survival of mankind, and human lives are in atmospheric environment, and the moment is by its shadow It rings.But with the development of industry, urban population is intensive, coal and oil-fired swift and violent growth, and atmospheric environment is worsening, Atmosphere pollution oneself become one of Major risk factors for influencing global environment and human body health.Atmospheric particulates refer to liquid The metastable suspension system that dispersion is formed in air is hooked with solia particle.The ingredient of Atmospheric particulates is very complicated, main Its source, formation condition and particle diameter distribution are depended on, itself can be the carrier of noxious material or other pollutants. Wherein fine particle (PM2.5) refers to the particulate matter of aerodynamic diameter≤2.5 μm, it is easy to adsorb toxic in air Heavy metal, acidic oxide, organic pollution etc., and entered in vivo, and then go deep into alveolar and blood by breathing, so as to draw Play various diseases.
It is made of in flue dust containing a large amount of PM2.5, PM2.5 a variety of chemical compositions, complicated component can be mainly divided into water Soluble components and water insoluble ingredients two large divisions, wherein water soluble ingredient mainly include trace metal constituents and inorganic salts and A small amount of dissolved organic matter etc., and water insoluble ingredients are mainly organic pollution.Polycyclic aromatic hydrocarbon is then absorption on PM2.5 A kind of important dangerous organic matter, it be the environmental carcinogenesis class compound that is found earliest and at present quantity at most, point Cloth is most wide, endangers one of maximum and human relation's environmental carcinogenesis class compound the closest.
Invention content
In order to solve prior art problem, the first aspect of the present invention provides a kind of clarifying smoke composition, with parts by weight Meter, prepares raw material and includes:1-4 parts of seedling of xiongqiong extract, 1-1.5 parts of qinghaosu, 2-6 parts of mannosan, Herba Solani Lyrati extract 1-4 Part, 2-3 parts of ethyl alcohol, 2-6 parts of Semen Cuscutae extract, 1.2-1.8 parts of turanose, 2-6 parts of Radix Morindae Officinalis extract, Gentrin Knotweed P.E 1- 4 parts, 0.2-0.8 parts of caffeine, 1-3 parts of 1,2- propylene glycol, 2-6 parts of aminoglycan, 2-6 parts of milkwort extract, rhamnose 0.5-2 Part, 2-6 parts of tara gum, 6-10 parts of licorice, 2-6 parts of semen vaccariae extraction, 2-6 parts of Semen Plantaginis extract, deionization 150 parts of water.
In some embodiments, the clarifying smoke composition, prepares raw material and includes:2-4 parts of seedling of xiongqiong extract, 1.2-1.5 parts of qinghaosu, 2-4 parts of mannosan, 2-4 parts of Herba Solani Lyrati extract, 2.5-3 parts of ethyl alcohol, 2-4 parts of Semen Cuscutae extract, 1.2-1.5 parts of turanose, 2-4 parts of Radix Morindae Officinalis extract, 2-4 parts of Gentrin Knotweed P.E, 0.4-0.8 parts of caffeine, 1,2- propylene glycol 1-2.5 parts, 4-6 parts of aminoglycan, 2-4 parts of milkwort extract, 1-2 parts of rhamnose, 4-6 parts of tara gum, licorice 6-8 Part, 4-6 parts of semen vaccariae extraction, 2-4 parts of Semen Plantaginis extract, 150 parts of deionized water.
In some embodiments, the clarifying smoke composition, prepares raw material and includes:2 parts of seedling of xiongqiong extract, blueness 1.5 parts of artemisin, 4 parts of mannosan, 2 parts of Herba Solani Lyrati extract, 2.5 parts of ethyl alcohol, 4 parts of Semen Cuscutae extract, turanose 1.5 part, bar 2 parts of halberd day extract, 2 parts of Gentrin Knotweed P.E, 0.4 part of caffeine, 2.5 parts of 1,2- propylene glycol, 4 parts of aminoglycan, Radix Polygalae extraction 2 parts of object, 4 parts of tara gum, 8 parts of licorice, 6 parts of semen vaccariae extraction, 2 parts of Semen Plantaginis extract, is gone 1 part of rhamnose 150 parts of ionized water.
In some embodiments, the aminoglycan is selected from hyaluronic acid, chondroitin sulfate, Heparan sulfate, liver At least one of element.
In some embodiments, the aminoglycan is chondroitin sulfate.
In some embodiments, the weight ratio of the tara gum and mannosan is 1:1.
In some embodiments, the weight ratio of the turanose and rhamnose is 1.5:1.
The second aspect of the present invention provides a kind of preparation method of clarifying smoke composition, includes the following steps:
(1)In parts by weight, 2-6 parts of tara gums are added in 150 parts of deionized waters, stirred evenly, add 2-6 parts of sweet dews Glycan is heated to 85 DEG C, under stiring, adds in 1-4 parts of seedling of xiongqiong extract, 1-4 parts of Herba Solani Lyrati extract, Semen Cuscutae extract 2-6 Part, 2-6 parts of Radix Morindae Officinalis extract, 1-4 parts of Gentrin Knotweed P.E, 2-6 parts of aminoglycan, 2-6 parts of milkwort extract, licorice 6-10 parts, 2-6 parts of semen vaccariae extraction, 2-6 parts of Semen Plantaginis extract, stir 45 min, mixing speed be 420 rpm;
(2)60 DEG C are cooled to, sequentially adds 1-3 parts of 1,2-PD, 0.2-0.8 parts of caffeine, 1-1.5 parts of qinghaosu, second 2-3 parts of alcohol continues to stir 30 min, and mixing speed is 250 rpm;
(3)Stop heating, be cooled to room temperature, add 1.2-1.8 parts of turanose, 0.5-2 parts of rhamnose, stir evenly to get.
The third aspect of the present invention provides a kind of application method of clarifying smoke composition, is sprayed directly on air In.
The fourth aspect of the present invention provides a kind of application of clarifying smoke composition in environmental protection.
Specific embodiment
The detailed description for preferred implementation method of the invention below of participating in the election of and including embodiment this hair can be more easily understood Bright content.Unless otherwise defined, all technologies used herein and scientific terminology have common with fields of the present invention The normally understood identical meaning of technical staff.When there is a conflict, the definition in this specification shall prevail.
As used herein term " by ... prepare " it is synonymous with "comprising".Term "comprising" used herein, " comprising ", " having ", " containing " or its any other deformation, it is intended that cover including for non-exclusionism.For example, the combination comprising listed elements Object, step, method, product or device are not necessarily limited to those elements, but can include not expressly listed other elements or Such composition, step, method, product or the intrinsic element of device.
Conjunction " Consists of " excludes any element do not pointed out, step or component.If in claim, this Phrase will make claim be closed, it be made not include the material in addition to the material of those descriptions, but relative normal Except rule impurity.When being rather than immediately following after theme in the clause that phrase " Consists of " appears in claim main body, It is only limited to the element described in the clause;Other elements are not excluded except the claim as a whole.
Equivalent, concentration or other values or parameter are excellent with range, preferred scope or a series of upper limit preferred values and lower limit During the Range Representation that choosing value limits, this, which should be understood as, specifically discloses by any range limit or preferred value and any range All ranges that any pairing of lower limit or preferred value is formed, regardless of whether the range separately discloses.For example, when open During range " 1 to 5 ", described range should be interpreted as including range " 1 to 4 ", " 1 to 3 ", " 1 to 2 ", " 1 to 2 and 4 to 5 ", " 1 to 3 and 5 " etc..When numberical range is described herein, unless otherwise stated, otherwise range intention includes its end Value and all integers and score in the range.
Singulative includes plural number and object is discussed, unless the context clearly dictates otherwise." optional " or it is " arbitrary It is a kind of " refer to that the item described thereafter or event may or may not occur, and the description include situation that event occurs and The situation that event does not occur.
Approximate term in specification and claims is used for modifying quantity, represents specific the present invention is not limited to this Quantity further includes the modified part of the acceptable change without lead to related basic function close to the quantity.Phase It answers, modifies a numerical value with " about ", " about " etc., mean that the present invention is not limited to the exact numericals.In some examples, it is approximate Term likely corresponds to the precision of the instrument of measured value.In present specification and claims, range limits can be with It combines and/or exchanges, these ranges include all subranges contained therebetween if not stated otherwise.
In addition, indefinite article " one kind " before element of the present invention or component and "one" quantitative requirement to element or component (i.e. occurrence number) unrestriction.Therefore "one" or " one kind " should be read as including one or at least one, and odd number The element or component of form also include plural form, unless the apparent purport of the quantity refers to singulative.
The first aspect of the present invention provides a kind of clarifying smoke composition, in parts by weight, prepares raw material and includes:The seedling of xiongqiong 1-4 parts of extract, 1-1.5 parts of qinghaosu, 2-6 parts of mannosan, 1-4 parts of Herba Solani Lyrati extract, 2-3 parts of ethyl alcohol, Semen Cuscutae extraction 2-6 parts of object, 1.2-1.8 parts of turanose, 2-6 parts of Radix Morindae Officinalis extract, 1-4 parts of Gentrin Knotweed P.E, 0.2-0.8 parts of caffeine, 1, 1-3 parts of 2- propylene glycol, 2-6 parts of aminoglycan, 2-6 parts of milkwort extract, 0.5-2 parts of rhamnose, 2-6 parts of tara gum, Radix Glycyrrhizae carry Take 6-10 parts of object, 2-6 parts of semen vaccariae extraction, 2-6 parts of Semen Plantaginis extract, 150 parts of deionized water.
In some embodiments, the clarifying smoke composition, prepares raw material and includes:2-4 parts of seedling of xiongqiong extract, 1.2-1.5 parts of qinghaosu, 2-4 parts of mannosan, 2-4 parts of Herba Solani Lyrati extract, 2.5-3 parts of ethyl alcohol, 2-4 parts of Semen Cuscutae extract, 1.2-1.5 parts of turanose, 2-4 parts of Radix Morindae Officinalis extract, 2-4 parts of Gentrin Knotweed P.E, 0.4-0.8 parts of caffeine, 1,2- propylene glycol 1-2.5 parts, 4-6 parts of aminoglycan, 2-4 parts of milkwort extract, 1-2 parts of rhamnose, 4-6 parts of tara gum, licorice 6-8 Part, 4-6 parts of semen vaccariae extraction, 2-4 parts of Semen Plantaginis extract, 150 parts of deionized water.
In some embodiments, the clarifying smoke composition, prepares raw material and includes:2 parts of seedling of xiongqiong extract, blueness 1.5 parts of artemisin, 4 parts of mannosan, 2 parts of Herba Solani Lyrati extract, 2.5 parts of ethyl alcohol, 4 parts of Semen Cuscutae extract, turanose 1.5 part, bar 2 parts of halberd day extract, 2 parts of Gentrin Knotweed P.E, 0.4 part of caffeine, 2.5 parts of 1,2- propylene glycol, 4 parts of aminoglycan, Radix Polygalae extraction 2 parts of object, 4 parts of tara gum, 8 parts of licorice, 6 parts of semen vaccariae extraction, 2 parts of Semen Plantaginis extract, is gone 1 part of rhamnose 150 parts of ionized water.
Seedling of xiongqiong extract
The seedling of xiongqiong is the seedling leaf of samphire Rhizoma Chuanxiong.Perennial herb, high 40-70cm.Complete stool has enhanced aroma.Rhizome is in not advise Nodositas fist shape group port then, there are most fibrous roots in lower end.Stem is upright, and cylindrical, hollow, there is vertical straight flute line on surface.The lower portion of the stem Section expands discoid(It is commonly called as Siberian cocklebur), section more than middle part do not expand.The lower portion of the stem leaf has handle, the long 3-10cm of handle, and base portion is expanded into Sheath;Blade profile ovate triangle, long 12-15cm, wide 10-15cm go out formula pinniform and totally cleave for three to four times three, 4-5 pairs of accessory pinna, ovum Sliver wire lanceolar is returned to long avette in shape lanceolar, long 6-7cm, wide 5-6cm, end, and long 2-5mm, wide 1-2mm, top has small There is sparse pubescence on tip, only arteries and veins;Stem upper leaf gradually simplifies.Universal umbel basidixed or side life, phyllary 3-6 is linear, Long 0.5-2.5cm;Umbrella spoke 7-20, Length discrepancy, long 2-4cm;Umbellule has colored 10-24;Involucel piece 2-7, it is linear, slightly Purple, by pubescence, long 3-5mm;Calyx tooth agensis;Petal is in vain with obovate to ellipse, apex has short pointed projections, introversion; Stamen 5, anther light green;Style 2, long 2-3mm, downward contrary flexure.Two flat-sided pressure of young fruit, long 2-3mm, wide about 1mm;In heel slot There is oil pipe 1-5, there is oil pipe 2-3 in incline slot, there is oil pipe 6-8 in symphysis face.The month at florescence 7-8, the young fruit period 9-10 months.
Seedling of xiongqiong acrid flavour;It is warm-natured, Return liver, courage, the heart channel of Hang-Shaoyin.There is dispelling wind soothing the liver.Main wind is dizzy;Infantile convulsion;The eye of wind is shed tears;Head Wind headache.
The extracting method of seedling of xiongqiong extract is to clean the seedling of xiongqiong, decocts 30 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
Herba Solani Lyrati extract
Bittersweet is Solanaceae activity of Solanum Lyratum Thunb Solanum lyratum Thunb. [S. dulcamara L. var. lyratum (Thunb.) Sieb. et Zucc., S. Dulcamara L. var. pubescens Blume, S.Dulcamara L. var. chinense Dunal], it is used as medicine with herb or root.
Bittersweet is bitter in taste, is slightly cold.Channel tropism enters liver, stomach.Major function:It is clearing heat and detoxicating, inducing diuresis and reducing edema, anticancer.Herb:With In cold, fever, acute mastitis, malignant sore, jaundice with damp-heat pathogen, ascites, leukorrhea, nephritic dropsy;Carbuncle furuncle poison is controlled in external application.Root:Arthralgia pain due to rheumatism.
The extracting method of Herba Solani Lyrati extract is to clean bittersweet, decocts 45 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
Semen Cuscutae extract
Semen Cuscutae is the dry mature seed of Cuscuta chinensis Lam. Cuscuta chinensis Lam..Semen Cuscutae seed In spherical, 1~1.5mm of diameter.Surface taupe brown or yellowish-brown, have the dot of fine and closely woven protrusion, and there be linear kind of nick in one end Navel.Matter is solid, is not easy to crush with nail.Gas is micro-, lightly seasoned.
Semen Cuscutae seminality taste sweet, warm.Return liver, kidney, the spleen channel.With nourishing liver and kidney, astringent sperm contracting urine, tocolysis, improving eyesight, antidiarrheal The effect of.For impotence and seminal emission, dripping urination, enuresis frequent micturition, soreness and weakness of waist and knees, blurred vision tinnitus, vaginal bleeding due to deficiency of the kidney during pregnancy, fetal irritability, spleen Kidney deficiency is rushed down;Externally treating leucoderma.
Semen Cuscutae seed (quercetin) containing Quercetin, purple cloud (astragalin), hyperin (hyperin) and Mongolian oak Pi Su -3-O- β-D- galactolipins -7-O- β-glycoside (quercetin-3-O- β-D-galactoside-7-O- β - glucoside)。
The extracting method of Semen Cuscutae extract is to clean Semen Cuscutae and the salt of 0.1 times of weight mixes, fry to surface Become brown color, then 3 h decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
Radix Morindae Officinalis extract
Morinda officinalis is the dry root of madder wort Morinda officinalis Morinda officinalis How.Morinda offcinalis How Tiangeng is in oblate column Shape, slightly curved song, varying length, 0.5~2cm of diameter;Surface lark or dark gray, have longitudinal grin and transverse crack, and some skin zones are horizontal Expose woody part to dialysis;Matter is tough, and section skin zone is thick, and purple or lavender are easily removed with woody part;Woody part is hard, yellowish-brown or Huang White, 1~5mm of diameter.It is odorless, sweet in flavor and micro-puckery.Nature and flavor are sweet, pungent, tepor.Return kidney, Liver Channel.Kidney-replenishing, strengthening the bones and muscles, wind-dispelling It is wet.For impotence and seminal emission, uterus cold infertile, irregular menstruation, few abdomen crymodynia, arthralgia pain due to rheumatism, muscles and bones impotence.
Morinda offcinalis How Tiangeng contains anthraquinone component:Rubiadin (rubiadin), Rubiadin 1-methylether (rubiadin-1-methyl ether), Physcion (physcion), 2- hydroxyl methylol anthraquinones (2-hydroxy-3- Hydrox-ymethylanthraquinone), 1- hydroxy-anthraquiones (1-hydroxyanthraquinone), 1- hydroxy-2-methyl Anthraquinone (1-hydroxy-2-methyl anthraquinone), 1,6- dihydroxy -2,4- dimethoxy anthraquinone (1,6- Dihydroxy-2,4-dimethoxyan-thraquinone), 1,6- dihydroxy -2- methoxy anthraquinones (1,6-dihydroxy- 2-methoxyanthraquinone), 2-methylanthraquinone (2-methylanthraqui-none), also ingredient containing iridoid; Monotropein (monoTCMLIBopein), four acetyl asperulosides (asperuloside teTCMLIBaacetate).Contain again Glucose (glucose), mannose (mannose), cupreol (β-sitosterol), palmitic acid (palmitic acid). Vitamin (vitamin) C, nonadecane (nonadecane), 24- ethyls cholesterine (24-ethyl cholesterol).Root skin Containing 23 kinds of elements such as zinc, manganese, iron, chromium.
The extracting method of Radix Morindae Officinalis extract is to clean Morinda officinalis, grinds, and 1.5 h are decocted with the water of 10 times of weight, By decoction liquor be dried in vacuo to get.
Gentrin Knotweed P.E
Giant knotweed be polygonaceae plant giant knotweed Polygonum cuspidatum Sieb. et Zucc., dry rhizome and root.For Cylindrical short section or irregular sheet, long 1-7cm, diameter 0.5-2.5cm.Crust sepia has vertical wrinkle and mark of fibrous root, section Skin zone is relatively thin, and woody part is broad, brown color, ray irradiation shape, and skin zone is more easily separated with woody part.Have in rhizome marrow every or in cavity Shape.Matter is hard.Gas is micro-, mildly bitter flavor, puckery.Nature and flavor slight bitter, is slightly cold.Return liver, courage, lung channel.Major function expelling wind and removing dampness, the scattered stasis of blood are determined Bitterly, it is relieving cough and reducing sputum.For joint pain, jaundice with damp-heat pathogen, Amenorrhea, abdominal mass, scald, injury from falling down, carbuncle sore tumefacting virus, phlegm of coughing It is more.
Polygoni cuspidati,radix and rhizome match glucoside, predominantly rheum emodin containing dissociated anthraquinone and anthracene(emodin), Physcion (Physcion), Chrysophanol(chrysophanol), anthracene glucoside(anthraglycside)A, that is, Physcion (8-O- β-D- Portugals Grape glucoside(Physcion-8-O-β-D-glucoside), anthracene glucoside(anthraglycoside)B, that is, rheum emodin 8-O- β-D- grapes Glucoside(emodin-8-O-β-D-glucoside), fallacinol(fallacinol), 6- hydroxyl aloe-emodins (citreorsein), rheum emodin -8- methyl ethers(questin), 6- hydroxyl aloe-emodin -8- methyl ethers(questinol)Deng.Also Containing stilbene compound:Resveratrol(resveratrol)It is Resveratrol(3,4 ', 5-tri- hydroxystilbene), Polydatin(Polydatin)That is resveratrol 3-O- β-D-Glucose glucoside(rerveratrol-3-O- β-D-glucoside), and containing protocatechuic acid(Protocate-chuic acid), dextrorotation cachou extract(Catechin), 2,5- bis- Methyl -7- hydroxyl chromones(2,5-dimethyl-7-hydroxychromone), 7- hydroxyl -4- methoxyl group -5- methylcoumarins essence (7-hydroxyl-4-methoxy-5-methyl coumarin), 2- methoxyl group -6- acetyl group -7- methyl English walnuts match(2- methoxy-6-acetyl-7-methyljuglone), Cassia anthrone -8- glycosides(torachrysone-8-O-D- glucoside), cupreol glycoside(β-sitosterol glucoside).
The extracting method of Gentrin Knotweed P.E is to clean giant knotweed, slice, decocts 3 h with the water of 20 times of weight, filters, will Filter vacuum drying to get.
Milkwort extract
Radix Polygalae is milk wort Radix Polygalae Polygala tenuifolia Willd. or ovum leaf Radix Polygalae Polygala sibirica L. dry root.Spring, the excavation of two season of autumn, remove fibrous root and silt, dry.
Payta is cylinder, slightly curved song, long 3~15cm, 0.3~0.8cm of diameter.Surface lark has to taupe brown Horizontal wrinkle, vertical wrinkle and crackle closeer and get deeply stuck in, the horizontal wrinkle of old root is closeer more to be got deeply stuck in, slightly in nodositas.Matter is hard and crisp, easily It fractures, section skin zone brown color, woody part yellow-white, skin zone easily removes with woody part.Gas is micro-, and bitter, micro-pungent, what is chewed has throat hurt feeling.
Payta nature and flavor:It is bitter, pungent, warm.The thoughts of returning home, kidney, lung channel.With tranquilize the mind and promote the intelligence, the effect of eliminating phlegm and diminishing swelling.For heart kidney Caused insomnia and dreamful sleep is not handed over, and forgetful palpitation with fear is wandering, and expectoration is not well, sore swollen toxin, mastosis.
Payta contains saponin, and 2 sapogenins are obtained after hydrolysis:Presenegenin(tenuigenin)A and B is also isolated thin Leaf Radix Polygalae element(tenuifolin).Closely it is divided into obtain 7 triterpenoid saponins:Polygalin(onjisaponin)A, B, C, D, E, F, G, Also get 5 phenolic glycosides:Radix Polygalae glucoside(tenuifoliside)A, B, C, D and β-D-(3-O- mustard seed acyls)Furans fruit Glycosyl-a-D-(6-O- mustard seed acyls)Glucopyanoside [β-D-(3-O-sinapoyl)-fructofuranosyl-2-D-(6- O-sinapoyl)-glucopyranoside].Separately get 6 oligosaccharides:The few essence of Radix Polygalae(tenuifoliose)A、B、C、D、E、 F.Ketone compound containing xanthene again:6- hydroxyls -1,2,3,7- tetramethoxy xanthones(6-hydroxy-1,2,3,7- tetramethoxyxanthone), 1,2,3,7- tetramethoxy xanthone(1,2,3,7-tetramethoxyxanthone), 1, 2,3,6,7- five Shen oxygroup xanthones(1,2,3,6,7-pentamethoxyxanthone), 1,7- dihydroxy xanthone(1,7- dihydroxyxanthone), 1,7- dimethoxy xanthone(1,7-dimethoxyxanthone), 1,7- dihydroxy -2,3- Dimethoxy xanthone(1,7-dihydroxy-2,3-dimethoxyxanthone), 1- hydroxyl -3,7- dimethoxy xanthones (1-hydroxy-3,7-dimethoxyxanthone), 1,7- dimethoxy -2,3- methylene-dioxy xanthone(1,7- Dimethoxy-2,3-methylenedioxy-xanthone), Radix Polygalae xanthone(onjixanthone)I and II, 1,6- bis- Hydroxyl -3,7- dimethoxy xanthone(1,6-dihydroxy-3,7-dimethoxyxanthone), 1,7- dihydroxy -3- first Oxygroup xanthone(1,7-dihydroxy-3-methoxyxanthone), 1,6 dihydroxy -3,5,7- trimethoxy xanthones(1, 6-dihydroxy-3,5,7-trimethoxyxanthone), 1- hydroxyls -3,6,7- trimethoxy xanthones(1-hy-droxy- 3,6,7-trimethoxyxanthone), 1,3,6- trihydroxy -2,7- dimethoxy xanthone(1,3,6-trihydroxy-2, 7-dimethoxyxanthone).Also contain 3,4,5- trimethoxy cinnamic acids(3,4,5-trimethoxycinnamio acid), Polygalytol(polygalitol), N- acetate gucosamines(N-acetylglucosamine), tenuidine (tenuidine).
The extracting method of milkwort extract is to clean Radix Polygalae, segment, 3 h is decocted with the water of 5 times of weight, by decoction liquor Vacuum drying to get.
Licorice
Radix Glycyrrhizae is glycyrrhizic legume Glycyrrhiza uralensis Fisch., swollen fruit Radix Glycyrrhiza The dry root of inflata Bat. or glycyrrhiza glabra Glycyrrhiza glabra L..Spring, the excavation of two season of autumn, remove fibrous root, shine It is dry.Root is cylinder, long 25~100cm, 0.6~3.5cm of diameter.Crust is elastic to differ.Surface rufous or taupe brown, tool are aobvious Vertical wrinkle, rill, hole skin and the sparse radicula trace.Matter is solid, and section shows slightly fibroid, yellow-white, mealiness, cambium ring Significantly, ray irradiation shape, some have crack.Rhizome is cylinder, and there is bud scar on surface, has marrow in the middle part of section.Gas is micro-, sweet and special Very.It is distributed in the ground such as northeast, North China, Shaanxi, Gansu, Qinghai, Xinjiang, Shandong.With invigorating the spleen and benefiting qi, clearing heat and detoxicating, eliminating the phlegm stops The effect of cough, relieving spasm to stop pain, coordinating the drug actions of a prescription.It is usually used in weakness of the spleen and the stomach, lassitude hypodynamia, palpitation, coughing with a lot of sputum, gastral cavity abdomen, four Limb contraction urgency pain, carbuncle sore tumefacting virus alleviate drug toxicity, strong.
Licorice and root-like stock contain glycyrrhizin (glycyrrhizin), i.e. glycyrrhizic acid glycyrrhinic acid, C42H62O16) 6~14%, it is a kind of triterpenoid saponin for the sweet ingredient of Radix Glycyrrhizae.Glycyrrhizic acid hydrolysis generates a molecule enoxolone (glycyrrhetic acid, that is, glycyrrhetinic acid, C30H46O4) and two molecule glucose aldehydic acid (glycuronic acid,C6H10O7).And (i.e. liquiritin liquiritin, C containing a small amount of liquiritin21H22O9, it is a kind of flavanols flavanone Glucoside, glucoside member name glycyrrhizin liquiritigenin, C15H12O4With glycyramarin glycyamarin), isoliquiritin (iso-liquiritin,,C21H24O9), dihydroxy enoxolone (dihydroxyglycyrrhetic acid, that is, grabric acid,C30H46O5), licoricidin (licoricidin, C25H32O5, i.e. 3 ', 6- diisoamyl alkene -2 ', 4 ', 5- trihydroxies are different Flavane), glycyrol (glycyrol, C21H18O6), 5-0- methyl glycyrols (5-0-methyl glycerol, C22H20O6), it is different Glycyrol (iso-glycyrol, C21H18O6), in addition, still containing mannitol (mannite), glucose 3.8%, sucrose 2.4~ 6.5%th, malic acid, betulinic acid (betulicacid, C30H48O3), asparagine, Yan acid, life element (biotin, C10H16O3N2S) 296 micro- gram grams, trace volatile oil are the special odorous source of Radix Glycyrrhizae and starch etc..
The extracting method of licorice is to clean Radix Glycyrrhizae, grinds, adds in the ether of 10 times of weight, reflux 1.5 H is filtered, and the methanol of 10 times of weight is added in the dregs of a decoction, and flow back 1 h, filtering, and residue water dissolution is filtered, collection aqueous solution, By aqueous solution be dried in vacuo to get.
Semen vaccariae extraction
The seed of cowherb is pinkwort cow-fat Vaccaria segetalis(Neck.)The dry mature seed of Garcke. It is spherical in shape, diameter about 2mm.Surface black, slightly a small number of rufous, gloss have fine powder shape protrusion, and there is 1 recess in side Longitudinal furrow.Matter is hard.Endosperm white, embryo bending cyclization, cotyledon 2.Odorless, taste micro-puckery is bitter.It is bitter in taste, it puts down.Return liver, stomach.Function master Control invigorate blood circulation, lower breast detumescence.For agalactia, Amenorrhea, dysmenorrhoea, acute mastitis swelling and pain.
Seed of cowherb seed contains triterpenoid saponin, referred to as vacsedoside(vac-segoside)Have A, B, C, D4 kind, It is by gypsogenin(gypsogenin)Derivative polysaccharid glucoside.The saccharide part of glucoside A has D-Glucose aldehydic acid(D- glucuronic acid), D- galactolipins(D-galactose), L-arabinose(L-arabinose), D- xyloses(D- xylose), D- fucoses(D-fucose), L- rhamnoses(L-rhamnose), the saccharide part of glucoside D has D-Glucose aldehydic acid, D- Galactolipin, D- xyloses, D- fucoses, L- rhamnoses and D-Glucose(D-glucose).The hydrolysis of four kinds of saponins same king Places saponin is not stayed(vaccraoside), it is gypsogenin -3- β-D-Glucose aldehydic acid glucoside(gypsogenin-3-β-D- giucuronoside.Contain glycosides displayed again:Seed of cowherb glycosides displayed(vaccarin), isosaponaretin(isosaponarin).Also Containing phytin(phytin), phosphatide(phospholipid), stigmasterol(stigmasterol)Deng.
The extracting method of semen vaccariae extraction is to clean the seed of cowherb, and drying is fried with the method for frying to the white flower that pops, Decoct 1.5 h with the water of 10 times of weight again, filtering, by filter vacuum drying to get.
Semen Plantaginis extract
Plantain seed is plantago plant Chinese herbaceous peony Plantago asiatica L. or ordinary building Plantago depressa Willd. dry mature seed.Fruit ear is harvested when summer, two season of autumn seed maturity, is dried, rubs seed, removes impurity.Chinese herbaceous peony Sub- seed is oval, irregular oblong or triangular shape oblong, slightly flat, is about 2mm, wide about 1mm;Surface yellowish-brown is to black Brown, there is fine wrinkle, has canescence concave point shape hilum on one side, matter is hard, and gas is micro-, lightly seasoned;Nature and flavor are sweet, are slightly cold.It is Return liver, kidney, lung, small Intestines pass through.The effect of with reducing fever and causing diuresis, excreting dampness is treating stranguria, improving eyesight eliminating the phlegm.For oedema turgor, puckery pain of heat gonorrhea, summer heat damp diarrhea, hot eyes Swelling and pain, phlegm-heat cough.
Chinese herbaceous peony seed Aucubin containing the moon(aucubin), Chinese herbaceous peony mucopolysaccharide(plantago-mulilage)A, racemization- Plantagoside(plantago-side), all square rafter glucoside(geniposidic acid), plantenolic acid(plantenolic acid), succinic acid(succinic acid), adenine(adenine), choline(choline)And 10.43% fat oil, β- Sitosterol(β-sitosterol), cupreol -3-O- β-D- glucopyanosides(β-sitosteryl-3-O-β-D- glucopyranoside).Greater plantain seed contains Aucubin, Isoquercitrin(isoquercitrin), succinic acid, vitamin (vitamin)B1、A.
The extracting method of Semen Plantaginis extract is to clean plantain seed, segment, impregnates 24 h with 10wt% common salt aqueous solutions, Taking-up is dried, grinds, and 1.5 h are decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
In some embodiments, the aminoglycan is selected from hyaluronic acid, chondroitin sulfate, Heparan sulfate, liver At least one of element.
In some embodiments, the aminoglycan is chondroitin sulfate.
In some embodiments, the weight ratio of the tara gum and mannosan is 1:1.
In some embodiments, the weight ratio of the turanose and rhamnose is 1.5:1.
The present invention uses natural plant extracts, safe and non-toxic, of low cost.Each component cooperates, caffeine, tower Draw glue and mannosan that can improve composition and absorb gas pollutant and accelerate flue dust sedimentation, and composition can be allowed at low temperature Relatively stablize, the phenomenon that composition is not in layering when temperature is relatively low, extend storage life.Turanose and rhamnose can be adjusted The viscosity of composition adjusts the rheological property of composition.Qinghaosu has the function of sterilization, prevents composition from corruption occur and becomes Matter.
The second aspect of the present invention provides a kind of preparation method of clarifying smoke composition, includes the following steps:
(1)In parts by weight, 2-6 parts of tara gums are added in 150 parts of deionized waters, stirred evenly, add 2-6 parts of sweet dews Glycan is heated to 85 DEG C, under stiring, adds in 1-4 parts of seedling of xiongqiong extract, 1-4 parts of Herba Solani Lyrati extract, Semen Cuscutae extract 2-6 Part, 2-6 parts of Radix Morindae Officinalis extract, 1-4 parts of Gentrin Knotweed P.E, 2-6 parts of aminoglycan, 2-6 parts of milkwort extract, licorice 6-10 parts, 2-6 parts of semen vaccariae extraction, 2-6 parts of Semen Plantaginis extract, stir 45 min, mixing speed be 420 rpm;
(2)60 DEG C are cooled to, sequentially adds 1-3 parts of 1,2-PD, 0.2-0.8 parts of caffeine, 1-1.5 parts of qinghaosu, second 2-3 parts of alcohol continues to stir 30 min, and mixing speed is 250 rpm;
(3)Stop heating, be cooled to room temperature, add 1.2-1.8 parts of turanose, 0.5-2 parts of rhamnose, stir evenly to get.
Each component of composition can be stirred evenly, will not destroy plant extract by preparation method using the present invention Active ingredient in object, in the modest viscosity of each phase composition, be not in excessively sticky and the phenomenon that can not stir, together Stability of the Shi Tigao compositions during long-time preserves.
The third aspect of the present invention provides a kind of application method of clarifying smoke composition, is sprayed directly on air In.
The fourth aspect of the present invention provides a kind of application of clarifying smoke composition in environmental protection.
With reference to specific embodiment, the present invention is further explained.
Embodiment 1
Clarifying smoke composition in parts by weight, prepares raw material and includes:2 parts of seedling of xiongqiong extract, 1.5 parts of qinghaosu, sweet dew gather 4 parts of sugar, 2 parts of Herba Solani Lyrati extract, 2.5 parts of ethyl alcohol, 4 parts of Semen Cuscutae extract, 1.5 parts of turanose, 2 parts of Radix Morindae Officinalis extract, tiger 2 parts of cane extract, 0.4 part of caffeine, 2.5 parts of 1,2- propylene glycol, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, rhamnose 1 Part, 4 parts of tara gum, 8 parts of licorice, 6 parts of semen vaccariae extraction, 2 parts of Semen Plantaginis extract, 150 parts of deionized water.
The extracting method of seedling of xiongqiong extract is to clean the seedling of xiongqiong, decocts 30 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Herba Solani Lyrati extract is to clean bittersweet, decocts 45 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Semen Cuscutae extract is to clean Semen Cuscutae and the salt of 0.1 times of weight mixes, fry to surface Become brown color, then 3 h decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The extracting method of Radix Morindae Officinalis extract is to clean Morinda officinalis, grinds, and 1.5 h are decocted with the water of 10 times of weight, By decoction liquor be dried in vacuo to get.
The extracting method of Gentrin Knotweed P.E is to clean giant knotweed, slice, decocts 3 h with the water of 20 times of weight, filters, will Filter vacuum drying to get.
The extracting method of milkwort extract is to clean Radix Polygalae, segment, 3 h is decocted with the water of 5 times of weight, by decoction liquor Vacuum drying to get.
The extracting method of licorice is to clean Radix Glycyrrhizae, grinds, adds in the ether of 10 times of weight, reflux 1.5 H is filtered, and the methanol of 10 times of weight is added in the dregs of a decoction, and flow back 1 h, filtering, and residue water dissolution is filtered, collection aqueous solution, By aqueous solution be dried in vacuo to get.
The extracting method of semen vaccariae extraction is to clean the seed of cowherb, and drying is fried with the method for frying to the white flower that pops, Decoct 1.5 h with the water of 10 times of weight again, filtering, by filter vacuum drying to get.
The extracting method of Semen Plantaginis extract is to clean plantain seed, segment, impregnates 24 h with 10wt% common salt aqueous solutions, Taking-up is dried, grinds, and 1.5 h are decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The preparation method of clarifying smoke composition, includes the following steps:
(1)In parts by weight, 4 parts of tara gums are added in 150 parts of deionized waters, stirred evenly, added 4 parts of sweet dews and gather Sugar is heated to 85 DEG C, under stiring, adds in 2 parts of seedling of xiongqiong extract, 2 parts of Herba Solani Lyrati extract, 4 parts of Semen Cuscutae extract, Morinda officinalis 2 parts of extract, 2 parts of Gentrin Knotweed P.E, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 10 parts of licorice, the seed of cowherb carry 6 parts of object, 2 parts of Semen Plantaginis extract are taken, stirs 45 min, mixing speed is 420 rpm;
(2)60 DEG C are cooled to, sequentially adds 2.5 parts of 1,2-PD, 0.4 part of caffeine, 1.5 parts of qinghaosu, ethyl alcohol 2.5 Part, continue to stir 30 min, mixing speed is 250 rpm;
(3)Stop heating, be cooled to room temperature, add 1.5 parts of turanose, 1 part of rhamnose, stir evenly to get.
Embodiment 2
Clarifying smoke composition in parts by weight, prepares raw material and includes:1 part of seedling of xiongqiong extract, 1.5 parts of qinghaosu, sweet dew gather 4 parts of sugar, 1 part of Herba Solani Lyrati extract, 2.5 parts of ethyl alcohol, 2 parts of Semen Cuscutae extract, 1.5 parts of turanose, 6 parts of Radix Morindae Officinalis extract, tiger 1 part of cane extract, 0.4 part of caffeine, 2.5 parts of 1,2- propylene glycol, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, rhamnose 1 Part, 4 parts of tara gum, 10 parts of licorice, 2 parts of semen vaccariae extraction, 6 parts of Semen Plantaginis extract, 150 parts of deionized water.
The extracting method of seedling of xiongqiong extract is to clean the seedling of xiongqiong, decocts 30 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Herba Solani Lyrati extract is to clean bittersweet, decocts 45 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Semen Cuscutae extract is to clean Semen Cuscutae and the salt of 0.1 times of weight mixes, fry to surface Become brown color, then 3 h decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The extracting method of Radix Morindae Officinalis extract is to clean Morinda officinalis, grinds, and 1.5 h are decocted with the water of 10 times of weight, By decoction liquor be dried in vacuo to get.
The extracting method of Gentrin Knotweed P.E is to clean giant knotweed, slice, decocts 3 h with the water of 20 times of weight, filters, will Filter vacuum drying to get.
The extracting method of milkwort extract is to clean Radix Polygalae, segment, 3 h is decocted with the water of 5 times of weight, by decoction liquor Vacuum drying to get.
The extracting method of licorice is to clean Radix Glycyrrhizae, grinds, adds in the ether of 10 times of weight, reflux 1.5 H is filtered, and the methanol of 10 times of weight is added in the dregs of a decoction, and flow back 1 h, filtering, and residue water dissolution is filtered, collection aqueous solution, By aqueous solution be dried in vacuo to get.
The extracting method of semen vaccariae extraction is to clean the seed of cowherb, and drying is fried with the method for frying to the white flower that pops, Decoct 1.5 h with the water of 10 times of weight again, filtering, by filter vacuum drying to get.
The extracting method of Semen Plantaginis extract is to clean plantain seed, segment, impregnates 24 h with 10wt% common salt aqueous solutions, Taking-up is dried, grinds, and 1.5 h are decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The preparation method of clarifying smoke composition, includes the following steps:
(1)In parts by weight, 4 parts of tara gums are added in 150 parts of deionized waters, stirred evenly, added 4 parts of sweet dews and gather Sugar is heated to 85 DEG C, under stiring, adds in 1 part of seedling of xiongqiong extract, 1 part of Herba Solani Lyrati extract, 2 parts of Semen Cuscutae extract, Morinda officinalis 6 parts of extract, 1 part of Gentrin Knotweed P.E, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 10 parts of licorice, the seed of cowherb carry 2 parts of object, 6 parts of Semen Plantaginis extract are taken, stirs 45 min, mixing speed is 420 rpm;
(2)60 DEG C are cooled to, sequentially adds 2.5 parts of 1,2-PD, 0.4 part of caffeine, 1.5 parts of qinghaosu, ethyl alcohol 2.5 Part, continue to stir 30 min, mixing speed is 250 rpm;
(3)Stop heating, be cooled to room temperature, add 1.5 parts of turanose, 1 part of rhamnose, stir evenly to get.
Comparative example 1
Clarifying smoke composition in parts by weight, prepares raw material and includes:2 parts of seedling of xiongqiong extract, 1.5 parts of qinghaosu, sweet dew gather 4 parts of sugar, 2 parts of Herba Solani Lyrati extract, 2.5 parts of ethyl alcohol, 4 parts of Semen Cuscutae extract, 1.5 parts of turanose, 2 parts of Radix Morindae Officinalis extract, tiger 2 parts of cane extract, 2.5 parts of 1,2- propylene glycol, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 1 part of rhamnose, 4 parts of tara gum, 8 parts of licorice, 6 parts of semen vaccariae extraction, 2 parts of Semen Plantaginis extract, 150 parts of deionized water.
The extracting method of seedling of xiongqiong extract is to clean the seedling of xiongqiong, decocts 30 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Herba Solani Lyrati extract is to clean bittersweet, decocts 45 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Semen Cuscutae extract is to clean Semen Cuscutae and the salt of 0.1 times of weight mixes, fry to surface Become brown color, then 3 h decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The extracting method of Radix Morindae Officinalis extract is to clean Morinda officinalis, grinds, and 1.5 h are decocted with the water of 10 times of weight, By decoction liquor be dried in vacuo to get.
The extracting method of Gentrin Knotweed P.E is to clean giant knotweed, slice, decocts 3 h with the water of 20 times of weight, filters, will Filter vacuum drying to get.
The extracting method of milkwort extract is to clean Radix Polygalae, segment, 3 h is decocted with the water of 5 times of weight, by decoction liquor Vacuum drying to get.
The extracting method of licorice is to clean Radix Glycyrrhizae, grinds, adds in the ether of 10 times of weight, reflux 1.5 H is filtered, and the methanol of 10 times of weight is added in the dregs of a decoction, and flow back 1 h, filtering, and residue water dissolution is filtered, collection aqueous solution, By aqueous solution be dried in vacuo to get.
The extracting method of semen vaccariae extraction is to clean the seed of cowherb, and drying is fried with the method for frying to the white flower that pops, Decoct 1.5 h with the water of 10 times of weight again, filtering, by filter vacuum drying to get.
The extracting method of Semen Plantaginis extract is to clean plantain seed, segment, impregnates 24 h with 10wt% common salt aqueous solutions, Taking-up is dried, grinds, and 1.5 h are decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The preparation method of clarifying smoke composition, includes the following steps:
(1)In parts by weight, 4 parts of tara gums are added in 150 parts of deionized waters, stirred evenly, added 4 parts of sweet dews and gather Sugar is heated to 85 DEG C, under stiring, adds in 2 parts of seedling of xiongqiong extract, 2 parts of Herba Solani Lyrati extract, 4 parts of Semen Cuscutae extract, Morinda officinalis 2 parts of extract, 2 parts of Gentrin Knotweed P.E, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 10 parts of licorice, the seed of cowherb carry 6 parts of object, 2 parts of Semen Plantaginis extract are taken, stirs 45 min, mixing speed is 420 rpm;
(2)60 DEG C are cooled to, 2.5 parts of 1,2-PD, 1.5 parts of qinghaosu, 2.5 parts of ethyl alcohol is sequentially added, continues stirring 30 Min, mixing speed are 250 rpm;
(3)Stop heating, be cooled to room temperature, add 1.5 parts of turanose, 1 part of rhamnose, stir evenly to get.
Comparative example 2
Clarifying smoke composition in parts by weight, prepares raw material and includes:2 parts of seedling of xiongqiong extract, 1.5 parts of qinghaosu, bittersweet carry Take 2 parts of object, 2.5 parts of ethyl alcohol, 4 parts of Semen Cuscutae extract, 1.5 parts of turanose, 2 parts of Radix Morindae Officinalis extract, 2 parts of Gentrin Knotweed P.E, 0.4 part of caffeine, 2.5 parts of 1,2- propylene glycol, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 1 part of rhamnose, 4 parts of tara gum, 8 parts of licorice, 6 parts of semen vaccariae extraction, 2 parts of Semen Plantaginis extract, 150 parts of deionized water.
The extracting method of seedling of xiongqiong extract is to clean the seedling of xiongqiong, decocts 30 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Herba Solani Lyrati extract is to clean bittersweet, decocts 45 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Semen Cuscutae extract is to clean Semen Cuscutae and the salt of 0.1 times of weight mixes, fry to surface Become brown color, then 3 h decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The extracting method of Radix Morindae Officinalis extract is to clean Morinda officinalis, grinds, and 1.5 h are decocted with the water of 10 times of weight, By decoction liquor be dried in vacuo to get.
The extracting method of Gentrin Knotweed P.E is to clean giant knotweed, slice, decocts 3 h with the water of 20 times of weight, filters, will Filter vacuum drying to get.
The extracting method of milkwort extract is to clean Radix Polygalae, segment, 3 h is decocted with the water of 5 times of weight, by decoction liquor Vacuum drying to get.
The extracting method of licorice is to clean Radix Glycyrrhizae, grinds, adds in the ether of 10 times of weight, reflux 1.5 H is filtered, and the methanol of 10 times of weight is added in the dregs of a decoction, and flow back 1 h, filtering, and residue water dissolution is filtered, collection aqueous solution, By aqueous solution be dried in vacuo to get.
The extracting method of semen vaccariae extraction is to clean the seed of cowherb, and drying is fried with the method for frying to the white flower that pops, Decoct 1.5 h with the water of 10 times of weight again, filtering, by filter vacuum drying to get.
The extracting method of Semen Plantaginis extract is to clean plantain seed, segment, impregnates 24 h with 10wt% common salt aqueous solutions, Taking-up is dried, grinds, and 1.5 h are decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The preparation method of clarifying smoke composition, includes the following steps:
(1)In parts by weight, 4 parts of tara gums are added in 150 parts of deionized waters, are heated to 85 DEG C, under stiring, add in Mi Overgrown with weeds 2 parts of extract, 2 parts of Herba Solani Lyrati extract, 4 parts of Semen Cuscutae extract, 2 parts of Radix Morindae Officinalis extract, 2 parts of Gentrin Knotweed P.E, sulfuric acid 4 parts of chondroitin, 2 parts of milkwort extract, 10 parts of licorice, 6 parts of semen vaccariae extraction, 2 parts of Semen Plantaginis extract, stirring 45 min, mixing speed are 420 rpm;
(2)60 DEG C are cooled to, sequentially adds 2.5 parts of 1,2-PD, 0.4 part of caffeine, 1.5 parts of qinghaosu, ethyl alcohol 2.5 Part, continue to stir 30 min, mixing speed is 250 rpm;
(3)Stop heating, be cooled to room temperature, add 1.5 parts of turanose, 1 part of rhamnose, stir evenly to get.
Comparative example 3
Clarifying smoke composition in parts by weight, prepares raw material and includes:2 parts of seedling of xiongqiong extract, 1.5 parts of qinghaosu, sweet dew gather Sugar 4 parts, 2 parts of Herba Solani Lyrati extract, 2.5 parts of ethyl alcohol, 4 parts of Semen Cuscutae extract, 2 parts of Radix Morindae Officinalis extract, 2 parts of Gentrin Knotweed P.E, 0.4 part of caffeine, 2.5 parts of 1,2- propylene glycol, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 4 parts of tara gum, licorice 8 Part, 6 parts of semen vaccariae extraction, 2 parts of Semen Plantaginis extract, 150 parts of deionized water.
The extracting method of seedling of xiongqiong extract is to clean the seedling of xiongqiong, decocts 30 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Herba Solani Lyrati extract is to clean bittersweet, decocts 45 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Semen Cuscutae extract is to clean Semen Cuscutae and the salt of 0.1 times of weight mixes, fry to surface Become brown color, then 3 h decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The extracting method of Radix Morindae Officinalis extract is to clean Morinda officinalis, grinds, and 1.5 h are decocted with the water of 10 times of weight, By decoction liquor be dried in vacuo to get.
The extracting method of Gentrin Knotweed P.E is to clean giant knotweed, slice, decocts 3 h with the water of 20 times of weight, filters, will Filter vacuum drying to get.
The extracting method of milkwort extract is to clean Radix Polygalae, segment, 3 h is decocted with the water of 5 times of weight, by decoction liquor Vacuum drying to get.
The extracting method of licorice is to clean Radix Glycyrrhizae, grinds, adds in the ether of 10 times of weight, reflux 1.5 H is filtered, and the methanol of 10 times of weight is added in the dregs of a decoction, and flow back 1 h, filtering, and residue water dissolution is filtered, collection aqueous solution, By aqueous solution be dried in vacuo to get.
The extracting method of semen vaccariae extraction is to clean the seed of cowherb, and drying is fried with the method for frying to the white flower that pops, Decoct 1.5 h with the water of 10 times of weight again, filtering, by filter vacuum drying to get.
The extracting method of Semen Plantaginis extract is to clean plantain seed, segment, impregnates 24 h with 10wt% common salt aqueous solutions, Taking-up is dried, grinds, and 1.5 h are decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The preparation method of clarifying smoke composition, includes the following steps:
(1)In parts by weight, 4 parts of tara gums are added in 150 parts of deionized waters, stirred evenly, added 4 parts of sweet dews and gather Sugar is heated to 85 DEG C, under stiring, adds in 2 parts of seedling of xiongqiong extract, 2 parts of Herba Solani Lyrati extract, 4 parts of Semen Cuscutae extract, Morinda officinalis 2 parts of extract, 2 parts of Gentrin Knotweed P.E, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 10 parts of licorice, the seed of cowherb carry 6 parts of object, 2 parts of Semen Plantaginis extract are taken, stirs 45 min, mixing speed is 420 rpm;
(2)60 DEG C are cooled to, sequentially adds 2.5 parts of 1,2-PD, 0.4 part of caffeine, 1.5 parts of qinghaosu, ethyl alcohol 2.5 Part, continue to stir 30 min, mixing speed is 250 rpm;
(3)Stop heating, be cooled to room temperature, stir evenly to get.
Comparative example 4
Clarifying smoke composition in parts by weight, prepares raw material and includes:2 parts of seedling of xiongqiong extract, 4 parts of mannosan, bittersweet carry Take 2 parts of object, 2.5 parts of ethyl alcohol, 4 parts of Semen Cuscutae extract, 1.5 parts of turanose, 2 parts of Radix Morindae Officinalis extract, 2 parts of Gentrin Knotweed P.E, 0.4 part of caffeine, 2.5 parts of 1,2- propylene glycol, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 1 part of rhamnose, 4 parts of tara gum, 8 parts of licorice, 6 parts of semen vaccariae extraction, 2 parts of Semen Plantaginis extract, 150 parts of deionized water.
The extracting method of seedling of xiongqiong extract is to clean the seedling of xiongqiong, decocts 30 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Herba Solani Lyrati extract is to clean bittersweet, decocts 45 min with the water of 10 times of weight, filtering will filter Liquid vacuum drying to get.
The extracting method of Semen Cuscutae extract is to clean Semen Cuscutae and the salt of 0.1 times of weight mixes, fry to surface Become brown color, then 3 h decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The extracting method of Radix Morindae Officinalis extract is to clean Morinda officinalis, grinds, and 1.5 h are decocted with the water of 10 times of weight, By decoction liquor be dried in vacuo to get.
The extracting method of Gentrin Knotweed P.E is to clean giant knotweed, slice, decocts 3 h with the water of 20 times of weight, filters, will Filter vacuum drying to get.
The extracting method of milkwort extract is to clean Radix Polygalae, segment, 3 h is decocted with the water of 5 times of weight, by decoction liquor Vacuum drying to get.
The extracting method of licorice is to clean Radix Glycyrrhizae, grinds, adds in the ether of 10 times of weight, reflux 1.5 H is filtered, and the methanol of 10 times of weight is added in the dregs of a decoction, and flow back 1 h, filtering, and residue water dissolution is filtered, collection aqueous solution, By aqueous solution be dried in vacuo to get.
The extracting method of semen vaccariae extraction is to clean the seed of cowherb, and drying is fried with the method for frying to the white flower that pops, Decoct 1.5 h with the water of 10 times of weight again, filtering, by filter vacuum drying to get.
The extracting method of Semen Plantaginis extract is to clean plantain seed, segment, impregnates 24 h with 10wt% common salt aqueous solutions, Taking-up is dried, grinds, and 1.5 h are decocted with the water of 10 times of weight, by decoction liquor be dried in vacuo to get.
The preparation method of clarifying smoke composition, includes the following steps:
(1)In parts by weight, 4 parts of tara gums are added in 150 parts of deionized waters, stirred evenly, added 4 parts of sweet dews and gather Sugar is heated to 85 DEG C, under stiring, adds in 2 parts of seedling of xiongqiong extract, 2 parts of Herba Solani Lyrati extract, 4 parts of Semen Cuscutae extract, Morinda officinalis 2 parts of extract, 2 parts of Gentrin Knotweed P.E, 4 parts of chondroitin sulfate, 2 parts of milkwort extract, 10 parts of licorice, the seed of cowherb carry 6 parts of object, 2 parts of Semen Plantaginis extract are taken, stirs 45 min, mixing speed is 420 rpm;
(2)60 DEG C are cooled to, 2.5 parts of 1,2-PD, 0.4 part of caffeine, 2.5 parts of ethyl alcohol is sequentially added, continues stirring 30 Min, mixing speed are 250 rpm;
(3)Stop heating, be cooled to room temperature, add 1.5 parts of turanose, 1 part of rhamnose, stir evenly to get.
Evaluation test
1. stability
Embodiment 1-2 and comparative example 1-4 are sealed in transparent vessel respectively, is placed in insulating box and preserves, insulating box Temperature is set as 25 DEG C, 4 DEG C, preserves three months, sees whether muddy or layering occur, without muddy or layering note within three months For A, appearance in two months to three months is muddy or layering is denoted as B, muddiness occurs within one month to two months or be layered to be denoted as C, one Occur muddy or layering within month and be denoted as D.
2. biocidal property
S. aureus Inoculate is taken in broth bouillon, 18 h are cultivated at 37 DEG C.Take each bacterial strain battalion that 18 h are cultivated Broth culture is supported, nutrient broth is diluted to test.6 sterile test tubes are taken, every test tube adds in 1mL nutrient broth liquid Culture medium, then it is separately added into 1mL embodiments 1-2 or comparative example 1-4.24 h are cultivated at 37 DEG C, observes and whether occurs in test tube Muddiness is denoted as yes/no.
3. clarifying smoke is tested
Burning cigarette simulates flue dust, the concentration after cigarette combustion gasification in haze environment simulation case in haze environment simulation case For 550 μ g/m3.200mL embodiments 1-2 and comparative example 1-4 is sprayed into haze environment simulation case, required for record purge flue dust Time, unit min.Control group 1 sprays 200mL deionized waters, and control group 2 does not spray any reagent.
Test result is listed in the table below.
From test result, each ingredient of the invention can generate synergistic effect, and preferable purification can be generated to flue dust Effect, and being capable of long-time stable preservation.
Aforementioned example is merely illustrative, some features for explaining the present invention.Appended claim is intended to The range as wide as possible being contemplated that is sought, and embodiments as presented herein is only the combination according to all possible embodiment Selection embodiment explanation.Therefore, the purpose of applicant is the feature that appended claim is not illustrated the present invention Exemplary selectional restriction.And the progress in science and technology will be formed due to the inaccuracy that language is expressed it is not current The possible equivalent or son considered is replaced, and these variations should also be interpreted to be wanted by appended right in the conceived case Ask covering.

Claims (10)

1. clarifying smoke composition, which is characterized in that in parts by weight, prepare raw material and include:1-4 parts of seedling of xiongqiong extract, blueness 1-1.5 parts of artemisin, 2-6 parts of mannosan, 1-4 parts of Herba Solani Lyrati extract, 2-3 parts of ethyl alcohol, 2-6 parts of Semen Cuscutae extract, turanose 1.2-1.8 parts, 2-6 parts of Radix Morindae Officinalis extract, 1-4 parts of Gentrin Knotweed P.E, 0.2-0.8 parts of caffeine, 1-3 parts of 1,2- propylene glycol, 2-6 parts of aminoglycan, 2-6 parts of milkwort extract, 0.5-2 parts of rhamnose, 2-6 parts of tara gum, 6-10 parts of licorice, king are not Stay 2-6 parts of row extract, 2-6 parts of Semen Plantaginis extract, 150 parts of deionized water.
2. clarifying smoke composition as described in claim 1, which is characterized in that it prepares raw material and includes:Seedling of xiongqiong extract 2-4 Part, 1.2-1.5 parts of qinghaosu, 2-4 parts of mannosan, 2-4 parts of Herba Solani Lyrati extract, 2.5-3 parts of ethyl alcohol, Semen Cuscutae extract 2-4 Part, 1.2-1.5 parts of turanose, 2-4 parts of Radix Morindae Officinalis extract, 2-4 parts of Gentrin Knotweed P.E, 0.4-0.8 parts of caffeine, 1,2- the third two 1-2.5 parts of alcohol, 4-6 parts of aminoglycan, 2-4 parts of milkwort extract, 1-2 parts of rhamnose, 4-6 parts of tara gum, licorice 6-8 Part, 4-6 parts of semen vaccariae extraction, 2-4 parts of Semen Plantaginis extract, 150 parts of deionized water.
3. clarifying smoke composition as described in claim 1, which is characterized in that it prepares raw material and includes:Seedling of xiongqiong extract 2 Part, 1.5 parts of qinghaosu, 4 parts of mannosan, 2 parts of Herba Solani Lyrati extract, 2.5 parts of ethyl alcohol, 4 parts of Semen Cuscutae extract, turanose 1.5 Part, 2 parts of Radix Morindae Officinalis extract, 2 parts of Gentrin Knotweed P.E, 0.4 part of caffeine, 2.5 parts of 1,2- propylene glycol, 4 parts of aminoglycan, Radix Polygalae 2 parts of extract, 1 part of rhamnose, 4 parts of tara gum, 8 parts of licorice, 6 parts of semen vaccariae extraction, Semen Plantaginis extract 2 Part, 150 parts of deionized water.
4. clarifying smoke composition as described in claim 1, which is characterized in that the aminoglycan is selected from hyaluronic acid, sulphur At least one of aching and limp ossein, Heparan sulfate, heparin.
5. clarifying smoke composition as described in claim 1, which is characterized in that the aminoglycan is chondroitin sulfate.
6. clarifying smoke composition as described in claim 1, which is characterized in that the weight ratio of the tara gum and mannosan It is 1:1.
7. clarifying smoke composition as described in claim 1, which is characterized in that the weight ratio of the turanose and rhamnose is 1.5:1.
8. the preparation method of the clarifying smoke composition as described in any one of claim 1-7 claims, which is characterized in that Include the following steps:
(1)In parts by weight, 2-6 parts of tara gums are added in 150 parts of deionized waters, stirred evenly, add 2-6 parts of sweet dews Glycan is heated to 85 DEG C, under stiring, adds in 1-4 parts of seedling of xiongqiong extract, 1-4 parts of Herba Solani Lyrati extract, Semen Cuscutae extract 2-6 Part, 2-6 parts of Radix Morindae Officinalis extract, 1-4 parts of Gentrin Knotweed P.E, 2-6 parts of aminoglycan, 2-6 parts of milkwort extract, licorice 6-10 parts, 2-6 parts of semen vaccariae extraction, 2-6 parts of Semen Plantaginis extract, stir 45 min, mixing speed be 420 rpm;
(2)60 DEG C are cooled to, sequentially adds 1-3 parts of 1,2-PD, 0.2-0.8 parts of caffeine, 1-1.5 parts of qinghaosu, second 2-3 parts of alcohol continues to stir 30 min, and mixing speed is 250 rpm;
(3)Stop heating, be cooled to room temperature, add 1.2-1.8 parts of turanose, 0.5-2 parts of rhamnose, stir evenly to get.
9. the application method of the clarifying smoke composition as described in any one of claim 1-8 claims directly sprays it It spills in air.
10. application of the clarifying smoke composition as described in any one of claim 1-8 claims in environmental protection.
CN201810221740.6A 2018-03-18 2018-03-18 Clarifying smoke composition Withdrawn CN108261861A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1933744A (en) * 2004-02-19 2007-03-21 三荣源有限公司 Nicotine-reducing agent and nicotine reduction method
CN102057961A (en) * 2010-11-15 2011-05-18 赵正坤 Air purifying composition and preparation method and use thereof
CN103691314A (en) * 2013-12-30 2014-04-02 广州优克日用品有限公司 Deodorizing composition and application thereof
CN104910866A (en) * 2015-04-20 2015-09-16 广东工业大学 Novel spraying agent for reducing indoor haze, and application thereof
CN104958774A (en) * 2015-06-11 2015-10-07 北京清科慧谷科技发展有限公司 Air purification plant composition and making method thereof
CN107801738A (en) * 2017-11-28 2018-03-16 云南百叶集生物科技有限公司 A kind of plant composition and preparation method thereof, application

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1933744A (en) * 2004-02-19 2007-03-21 三荣源有限公司 Nicotine-reducing agent and nicotine reduction method
CN102057961A (en) * 2010-11-15 2011-05-18 赵正坤 Air purifying composition and preparation method and use thereof
CN103691314A (en) * 2013-12-30 2014-04-02 广州优克日用品有限公司 Deodorizing composition and application thereof
CN104910866A (en) * 2015-04-20 2015-09-16 广东工业大学 Novel spraying agent for reducing indoor haze, and application thereof
CN104958774A (en) * 2015-06-11 2015-10-07 北京清科慧谷科技发展有限公司 Air purification plant composition and making method thereof
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Application publication date: 20180710