CN108260603A - A kind of pest of stored grain controlling agent of the repellant containing Java brucea - Google Patents
A kind of pest of stored grain controlling agent of the repellant containing Java brucea Download PDFInfo
- Publication number
- CN108260603A CN108260603A CN201611268404.4A CN201611268404A CN108260603A CN 108260603 A CN108260603 A CN 108260603A CN 201611268404 A CN201611268404 A CN 201611268404A CN 108260603 A CN108260603 A CN 108260603A
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- China
- Prior art keywords
- oil
- pest
- controlling agent
- brucea
- stored grain
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01M—CATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
- A01M29/00—Scaring or repelling devices, e.g. bird-scaring apparatus
- A01M29/12—Scaring or repelling devices, e.g. bird-scaring apparatus using odoriferous substances, e.g. aromas, pheromones or chemical agents
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
Abstract
The invention discloses a kind of preparation methods of the pest of stored grain controlling agent of pure plant source compounding, belong to field of pesticide preparation.The present invention is using brucea fruit oil as repellant, by being compounded according to a certain percentage with oil of badian, caryophyllus oil so as to obtain safe and environment-friendly, the free of contamination pest of stored grain controlling agent to pest of stored grain with good control ability.The present invention includes the raw material of following percentage composition：Brucea fruit oil 70% 85%；Oil of badian 10% 20%；Caryophyllus oil 5% 20%.
Description
Technical field
The invention belongs to pest of stored grain prevention and control fields, and in particular to a kind of pest of stored grain control of repellant containing Java brucea
Agent.
Background technology
Grain can cause more serious loss when infecting grain storage pest, not only result in weight in storage
The problems such as loss, quality decline, grain fever are gone mouldy, and frass and other excretas can reduce the edible quality of grain storage, add
Work quality, kind quality and technological quality or even the propagation for causing disease endanger the health of the mankind.The grain storage in China at present
Mostly using Chemical treatment during depositing, the chemical agent mode of action is more single, is easy to generate resistance, to people and animals, ring
Border can cause different degrees of pollution, and on stored grain quality, there is also undesirable influences, are badly in need of that safety and environmental protection, lasting period is wanted to grow
Chemical agent substitute product.
Method about foodstuff pest prevention more at present：
Chinese patent, application number：201510889588.5；Applicant：Agricultural University Of Anhui；Address：Hefei City, Anhui Province the Changjiang river
West Road 130；Denomination of invention：Application of the narrow leaved tea tree essential oil on prevention grain storage pest；Abstract：Narrow leaved tea tree essential oil is made
For a kind of application of plant pesticide on prevention grain storage pest, belong to biotechnology.The present invention combines foodstuff preservation and produces
It is practical, repellent is carried out to grain storage pest confused flour beetle and sitophilus zea-mais, is tagged, fumigation action, with disclosed patent
The 3 kinds of essential oil list product and its mixing formula reported in 201510340845.X are compared, the present invention to grain storage pest confused flour beetle and
The control effect of sitophilus zea-mais is more preferable, and especially fumigating insect killing action is notable, and the lasting period is long, is not likely to produce drug resistance.The present invention
Narrow leaved tea tree essential oil raw material resources enrich, it is at low cost, environmentally friendly, have exploitation for grain storage pest fumigant potential, storing up
There is boundless application prospect in terms of the prevention of grain pest.
Chinese patent, application number：201510753691.7；Applicant：Three agricultural science and technology Co., Ltd of Shangcai County；Ground
Location：The Zhumadian prefecture, Henan province city Shangcai County Dong Hong townshiies West Street west section south of road；Denomination of invention：A kind of stored-grain protectant and its application；It plucks
It will：The invention discloses a kind of stored-grain protectant and its application, which includes the component of following parts by weight：Pungent sulphur
0.8~1.0 part of phosphorus, 13~17 parts of Folium Meliae, 30~35 parts of talcum powder.The stored-grain protectant of the present invention, using phoxim or pungent
Sulphur Emulphors oil, Folium Meliae and talcum powder compound, and utilize the broad-spectrum insecticidal action of phoxim and the pest-resistant desinsection of the vegetalitas of Folium Meliae
Effect, the antibiotic bacteriostat suction-operated of talcum powder are combined, and three cooperates, coordinative role, and mixing compounding generates a kind of
Gas, foodstuff pest, livestock and poultry parasite and sanitary insect pest are respectively provided with tag, stomach toxicity and fumigation action, have it is good it is pest-resistant,
Insecticidal function, insecticidal spectrum is wide, can prevent plurality of cereals pest, livestock and poultry parasite and sanitary insect pest；Medicament residue is few, safely may be used
It leans on, it is at low cost, it is suitble to promote and apply.
Chinese patent, application number：201510118473.6；Applicant：Xiangyang Tian Wang insecticidal technologies development corporation, Ltd.；Ground
Location：Xiangfan City of Hubei Province fishgarth Zhou Luming islands；Denomination of invention：A kind of compounding fumigating insecticide for foodstuff pest prevention；It plucks
It will：A kind of compounding fumigating insecticide for foodstuff pest prevention, technical solution be by Celastrus angulatus and cinnamon oil in proportion
The compounding fumigating insecticide prevented for foodstuff pest is mixed and made into, component and content are：Celastrus angulatus 5%-30%, Chinese cassia tree
Oil 70% -95%.The compounding fumigating insecticide raw material of the present invention is mended short with long, and can reach increases desinsection intensity, reduce medication into
This, reduces environmental pollution, and alleviates drug resistance and other effects.Utilize the compounding fumigating insecticide described in the invention described above, it is especially useful in
The improvement of grain storage pest is fumigated, and is had：1. insecticidal range is wide；2. the lasting period is long；3. low toxicity, noresidue is nuisanceless, and environment is pacified
Entirely；4. using compound formulation, Celastrus angulatus, two kinds of insecticides of cinnamon oil have complementation and synergistic effect.
Chinese patent, application number：201510277123.4；Applicant：Close the bright spring；Address：Guangxi Zhuang Autonomous Region Nanning
City Heng County Heng Zhouzhen Liu Ming roads 80；Denomination of invention：A kind of grain insecticide containing cinnamon oil；Abstract：The invention belongs to grains
Storage technology field, and in particular to a kind of grain insecticide containing cinnamon oil includes the raw material of following percentage composition：Cinnamon oil
10%-14%；Galic essential oil 2%-5%；Neem oil 5%-8%；Turpentine oil 1%-4%；Citronella oil 1%-4%；Oil of badian 2%-5%；Rue
Essential oil 1%-4%；Remaining is the ethyl alcohol of volumetric concentration 75%.Grain insecticide of the present invention containing cinnamon oil is with natural plants essence
Oil is prepared for raw material, safe and environment-friendly, pollution-free and can effectively play the role of sterilization, desinsection.
Invention content
The object of the present invention is to provide a kind of pest of stored grain controlling agent of repellant containing Java brucea, the pest of stored grain controlling agents
It is to mix other plants essential oils with the natural brucea fruit oil of extraction to be prepared, safety and environmental protection holds the control of pest of stored grain
The effect phase is long.
In order to achieve the object of the present invention, the present invention adopts the following technical scheme that：A kind of storage grain of the repellant containing Java brucea
Agent for controlling noxious insect pests, which is characterized in that include the raw material of following percentage composition：
Brucea fruit oil：70%-85%
Oil of badian：10%-20%
Caryophyllus oil：5%-20%.
The preparation method of the pest of stored grain controlling agent of the above-mentioned repellant containing Java brucea, specifically includes following step：According to
The proportioning of above-mentioned percentage composition weighs brucea fruit oil；Oil of badian；Caryophyllus oil is sufficiently mixed it and uniformly can obtain this hair
The pest of stored grain controlling agent of the bright repellant containing Java brucea.
Brucea fruit oil is quassia Java brucea【Classification system】Brucea JavanicaFruit drying and crushing after
It is flaxen clear through physical squeezing or organic solvent, such as the fat oil of petroleum ether (60 ~ 90 DEG C), ethyl alcohol extraction
Clear liquid body.Containing abundant volatile oil component, such as australene, nopinene, β-myrcene, α-phellandrene, limonene, γ-pine
Oily alkene, terpinolene, β-linalool, 3- carenes, anethole, safrole, 1-ally-3,4-methy-lene dioxy benzene etc., these ingredients have certain sterilization
Activity, at the same have to Groton bug, lineae ablicantes Yi Wen, tyrophagus putrescentiae, dust mite, housefly, China fir octadentate bark beetle etc. it is good it is stifling,
Contact toxicity.
Oil of badian is from plant Chinese anise【Classification system】Illicium verum Hook.f.Fruit or branch
A kind of more complicated natural perfume material oil of ingredient for being extracted in leaf, main component is trans-anethole, limonene, australene,
Linalool, nerolidol, eucalyptol, terpinol etc..Star anise oil has preferable antibacterial, antibacterial action, while also has
Preferable insecticidal activity and antioxidative activity have the pests such as red flour beetle, lasioderma serricorne strong stifling and tag
Effect.
Caryophyllus oil is from plant of clove tree【Classification system】Syzygium aromaticum(L.) Merr. Et Perry
The extractions such as bud, leaf volatile oil, main component is eugenol, carypohyllene, epoxy carypohyllene, and experiment proves caryophyllus oil
There is good inhibiting effect to the growth of spoilage organisms and toxic bacteria common in food, have to pests such as lasioderma serricornes stronger
Tag and repellent action.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, before this, brucea fruit oil is chiefly used in field of medicaments, and plant protection art, which rarely has, to be referred to, and brucea fruit oil tool is found in testing
There is antifungal activity, and there is good fumigation, repellent activity, octagonal fennel to pests such as Groton bug, dust mite, tyrophagus putrescentiaes
The pests such as sesame oil, caryophyllus oil red flour beetle, lasioderma serricorne, rice weevil have good control effect, as long as various raw materials rationally assemble
It uses, can have the function that synergy, it being capable of effective protection storage grain safety and quality；
2nd, the ingredient of the pest of stored grain controlling agent of the repellant containing Java brucea of the invention is plant origin, natural environmental-protective, after use
Noresidue, pests are not easy to produce resistance, achievees the purpose that long-acting prevention and control pest of stored grain with repellent action by tagging；
3rd, the present invention has the characteristics of manufacturing cost is cheap, and preparation process is simple, easy to use and safe and efficient.
Specific embodiment：
To be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, with reference to specific
Embodiment, the present invention is further explained.
Embodiment 1：
A kind of pest of stored grain controlling agent of repellant containing Java brucea, the raw material percentage composition include：Brucea fruit oil 70% 8
Erect hypecoum oil 10%；Caryophyllus oil 20%.
A kind of preparation method of the pest of stored grain controlling agent of repellant containing Java brucea, specifically includes following step：According to upper
The proportioning for stating percentage composition weighs brucea fruit oil；Oil of badian；Caryophyllus oil can obtain courage containing crow of the invention after stirring evenly
The pest of stored grain controlling agent A of sub- repellant.
Embodiment 2：
A kind of pest of stored grain controlling agent of repellant containing Java brucea, the raw material percentage composition include：Brucea fruit oil 70% 8
Erect hypecoum oil 20%；Caryophyllus oil 10%.
A kind of preparation method of the pest of stored grain controlling agent of repellant containing Java brucea, specifically includes following step：According to upper
The proportioning for stating percentage composition weighs brucea fruit oil；Oil of badian；Caryophyllus oil can obtain courage containing crow of the invention after stirring evenly
The pest of stored grain controlling agent B of sub- repellant.
Embodiment 3：
A kind of pest of stored grain controlling agent of repellant containing Java brucea, the raw material percentage composition include：Brucea fruit oil 75% 8
Erect hypecoum oil 15%；Caryophyllus oil 10%.
A kind of preparation method of the pest of stored grain controlling agent of repellant containing Java brucea, specifically includes following step：According to upper
The proportioning for stating percentage composition weighs brucea fruit oil；Oil of badian；Caryophyllus oil can obtain courage containing crow of the invention after stirring evenly
The pest of stored grain controlling agent C of sub- repellant.
Embodiment 4：
A kind of pest of stored grain controlling agent of repellant containing Java brucea, the raw material percentage composition include：Brucea fruit oil 80% 8
Erect hypecoum oil 115%；Caryophyllus oil 5%.
A kind of preparation method of the pest of stored grain controlling agent of repellant containing Java brucea, specifically includes following step：According to upper
The proportioning for stating percentage composition weighs brucea fruit oil；Oil of badian；Caryophyllus oil can obtain courage containing crow of the invention after stirring evenly
The pest of stored grain controlling agent D of sub- repellant.
Embodiment 5：
A kind of pest of stored grain controlling agent of repellant containing Java brucea, the raw material percentage composition include：Brucea fruit oil 85% 8
Erect hypecoum oil 10%；Caryophyllus oil 5%.
A kind of preparation method of the pest of stored grain controlling agent of repellant containing Java brucea, specifically includes following step：According to upper
The proportioning for stating percentage composition weighs brucea fruit oil；Oil of badian；Caryophyllus oil can obtain courage containing crow of the invention after stirring evenly
The pest of stored grain controlling agent E of sub- repellant.
2nd, Application Example
Below using pest of stored grain controlling agent A, B, C, D, E to 1 to 5 gained of embodiment of Toxicity Determination method to corn
As the toxicity test example of, red flour beetle, the present invention will be described, but the present invention is not limited to following tool in practical applications
Body test example.
The indoor virulence test of the present invention is carried out in strict accordance with farm-chemical indoor determination test rule, with Abbott public affairs
Formula corrects the death rate of each processing, and LC50 and virulence regression equation are calculated with DPS softwares.
Test a kind of toxicity test of the pest of stored grain controlling agent to sitophilus zea-mais, red flour beetle of 1 repellant containing Java brucea.
Test worm：Red plan paddy steals sitophilus zea-mais.
Test method：Reference《People's Republic of China (PRC) agricultural industry criteria NY/T 1154.3-2006》Using conical flask method
Fumigation activity measure is carried out, repellent activity is measured using Y-shaped smell sensing apparatus.Processing time is 24 hours, sets 0.005mg/L,
Six concentration gradients of 0.01mg/L, 0.02mg/L, 0.04mg/L, 0.08mg/L.Specific method is as follows：First by 30 test worm adults
It is placed in wide-mouth bottle, then quantitative reagent is dropped on the filter paper item of long 7.5cm, width 2cm, be suspended from wide-mouth bottle, cover bottle cap.
Wide-mouth bottle is respectively placed in 25 DEG C again（Sitophilus zea-mais）With 28 DEG C（Red flour beetle）It is fumigated in dark culturing case, after 24 h, is beaten
It abroaches air-dispersing, checks stifling situation, record dead borer population, chemicals treatment is not added dropwise as control, each handle in triplicate.
1 is shown in Table to the stifling result of the test of corundum Sitophilusspp. imago
A kind of pest of stored grain controlling agent of 1 repellant containing Java brucea of table is to red flour beetle adult virulence result（24 h）.
A kind of pest of stored grain controlling agent of 2 repellant containing Java brucea of table is to corundum Sitophilusspp. imago virulence result（24 h）.
As can be seen from the above table, product of the present invention has good smoked kill effect to sitophilus zea-mais and red flour beetle, and adjoint
The content for brucea fruit oil rises and enhances, especially best with the combined effect in embodiment 4 in above 5 embodiments.
A kind of pest of stored grain controlling agent of repellant containing Java brucea measures the repellent action of sitophilus zea-mais, red flour beetle.
Test worm：Sitophilus zea-mais, red flour beetle adult.
Test method：With reference to the method for Liu Hui et al., the measure of repellent action is carried out using Y-shaped smell sensing apparatus.Specific method
It is as follows：Under the conditions of room temperature (26 ± 1) DEG C, relative humidity (65 ± 10) %, 140 Lux of intensity of illumination, by will
It asks and installs device, after outside air is purified via drying tower, moistened into water tower, two-way is divided to be connected respectively by silicone tube
Into sample measuring cell, the arm pipe that Y-shaped pipe is then connected by silicone tube enters supervisor, main tube gas's flow velocity be 20 ml/
Min is finally discharged by silicone tube.Every time measure when, with microsyringe draw 5 μ l 0.08mg/L A, B, D, D, E in
It on filter paper item, is put into the sample room of side, opposite side sample room is placed the not filter paper item of adding medicine and same size and compared, and beats
It opens vacuum pump, starts timing, be put into 20 test worm adults from throwing insect population after 20 s, test worm on record two-arm pipe after 24 h
Number.3 repetitions are set per sample treatment.Scattering ratio（%） =（（Control group test worm number-processing group test worm number）/（It is right
According to a group test worm number+processing group test worm number））× 100% .
Result of the test is as shown in table 3, table 4.
A kind of pest of stored grain controlling agent of 3 repellant containing Java brucea of table is to the repellent action reagent agent of sitophilus zea-mais.
A kind of pest of stored grain controlling agent of 4 repellant containing Java brucea of table is to the repellent action of red flour beetle.
By table 3, table 4 it is found that product of the present invention is respectively provided with good repellent effect in various embodiments above, and with
The raising of brucea fruit oil content and increase.Wherein embodiment 4 and 5 has reached 100% repellent effect.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (5)
1. a kind of pest of stored grain controlling agent of repellant containing Java brucea, it is characterised in that：Include the raw material of following percentage composition：
Brucea fruit oil：70%-85%
Oil of badian：10%-20%
Caryophyllus oil：5%-20%.
2. according to claim 1, the Java brucea repellant described in the pest of stored grain controlling agent of a repellant containing Java brucea be with
A kind of brucea fruit oil mixture as main component, the mixture refer to from fruit of khosam with squeezing, petroleum ether, ether,
The brucea fruit oil and its preparation of the organic solvents such as ethyl alcohol, methanol extraction gained, in an embodiment of the present invention, mainly with petroleum ether
Based on the brucea fruit oil of extraction.
3. a kind of preparation method of the pest of stored grain controlling agent of repellant containing Java brucea as described in claim 1 to 2, feature
It is：Proportional amount proportioning described in accordance with the claim 1 weighs brucea fruit oil, oil of badian and caryophyllus oil, and mixing is abundant
It can obtain.
4. the arbitrary suitable agricultural that the pest of stored grain controlling agent composition according to right 1 to 3 is processed into practical applications
On the dosage form that uses.
5. the pest of stored grain controlling agent composition described in any claim according to claims 1 to 4 is done harm in storage grain and storage
Application in worm control.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611268404.4A CN108260603A (en) | 2016-12-31 | 2016-12-31 | A kind of pest of stored grain controlling agent of the repellant containing Java brucea |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201611268404.4A CN108260603A (en) | 2016-12-31 | 2016-12-31 | A kind of pest of stored grain controlling agent of the repellant containing Java brucea |
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| CN108260603A true CN108260603A (en) | 2018-07-10 |
Family
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| CN201611268404.4A Pending CN108260603A (en) | 2016-12-31 | 2016-12-31 | A kind of pest of stored grain controlling agent of the repellant containing Java brucea |
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Cited By (3)
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| CN109006841A (en) * | 2018-08-01 | 2018-12-18 | 华南农业大学 | It is a kind of can in plant transporting antifeedant for insect |
| CN112931496A (en) * | 2021-01-27 | 2021-06-11 | 仲恺农业工程学院 | Special pesticide containing brucea javanica oil for flying defense and preparation method thereof |
| CN116406662A (en) * | 2023-04-13 | 2023-07-11 | 西北农林科技大学 | Plant source mixed microemulsion and preparation method and application thereof |
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| CN104886183A (en) * | 2015-05-27 | 2015-09-09 | 闭炳春 | Cinnamon oil contained insect repelling mildew preventive for grain storage |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109006841A (en) * | 2018-08-01 | 2018-12-18 | 华南农业大学 | It is a kind of can in plant transporting antifeedant for insect |
| CN109006841B (en) * | 2018-08-01 | 2021-05-04 | 华南农业大学 | Insect antifeedant capable of being transported in plant body |
| CN112931496A (en) * | 2021-01-27 | 2021-06-11 | 仲恺农业工程学院 | Special pesticide containing brucea javanica oil for flying defense and preparation method thereof |
| CN116406662A (en) * | 2023-04-13 | 2023-07-11 | 西北农林科技大学 | Plant source mixed microemulsion and preparation method and application thereof |
| CN116406662B (en) * | 2023-04-13 | 2024-04-09 | 西北农林科技大学 | Plant source mixed microemulsion and preparation method and application thereof |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180710 |