CN108254458A - Textile sense of taste style measuring device and measuring method - Google Patents

Textile sense of taste style measuring device and measuring method Download PDF

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Publication number
CN108254458A
CN108254458A CN201711435717.9A CN201711435717A CN108254458A CN 108254458 A CN108254458 A CN 108254458A CN 201711435717 A CN201711435717 A CN 201711435717A CN 108254458 A CN108254458 A CN 108254458A
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finger
bionic finger
sample
bionic
sampling
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CN108254458B (en
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杜赵群
孙懿
何玲娥
张明月
仵玉芝
龚占江
邵青青
李涵
余卫东
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Donghua University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation

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  • Life Sciences & Earth Sciences (AREA)
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  • General Health & Medical Sciences (AREA)
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  • Sampling And Sample Adjustment (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)

Abstract

The present invention relates to a kind of textile sense of taste style measuring device and measuring methods, light source and bionic finger are equipped in textile sense of taste generating means, bionic finger carries out reciprocating friction to fabric sample, heat supply bionic finger heats fabric sample, feed flow bionic finger is soaked to fabric sample feed flow, sampling bionic finger connect extracting liq sample with fluid sampling device, and liquid sample imports liquid chromatography mass combined instrument and is connected to signal-data processing unit.Measuring method includes:Place fabric sample;Open light source, heat supply bionic finger electrified regulation;Feed flow bionic finger feed flow soaks fabric sample;Driving bionic finger makees fabric sample chewing type reciprocating friction;Sampling imports liquid chromatography mass combined instrument and is detected, and signal-data processing unit carries out data analysis.The present invention is based on dynamic with liquid, heating and simulate mouth chew it is automatic, quickly and accurately the sense of taste style of textile is detected.

Description

Textile sense of taste style measuring device and measuring method
Technical field
The invention belongs to the technical fields that textile sense of taste style measures, and are surveyed more particularly to a kind of textile sense of taste style Measure device and measuring method.
Background technology
With the raising that people's environmental protection and safety and sanitation are realized, the mankind have the quality of textile more comprehensive Understanding.Traditional practicability, aesthetics and durability far can not meet the requirement of consumers in general, weaving It increasingly attracts people's attention with the presence or absence of the toxicant that may damage consumer health in product.Especially into 21 Century, advocating for the ideas such as " green consumption ", " ecological safety ", " ecological textile " just continuous promote textile product safety It improves, to meet consumer to textile increasing requirement safely.So many governments of developed country and world's authority's group It knits and issues law and technical standard in succession and be controlled come the safety to textile.Oeko-Tex Standard 100 and I State's standard GB/T/T1888-2002 ecological textiles technology require all to the residue limits of harmful substances various in textile into Clear stipulaties are gone.
Textile will be related to the use of formaldehyde during resin arranges.In order to reach the mesh such as wrinkle resistant, shrinkproof, fire-retardant , stamp, the durability dyed are kept, improves feel, formaldehyde need to be added in auxiliary agent.Textile containing formaldehyde, wears in people And use during, can gradually disengage free formaldehyde, pass through human respiratory tract and skin contact and cause respiratory inflammation and skin Skin inflammation can also generate stimulation to eyes, and formaldehyde can also cause allergy or even can induce cancer.Perfluor organic matter has chemistry The excellent performance of inertia and heat resistance.Due to the characteristic of hydrophobic oleophobic, be commonly used as in textile water-refusing oil-refusing finishing agent with And surface soiling inorganic agent.Perfluorooctane sulfonyl compound (PFOS) and perfluoro caprylic acid (PFOA) are at present in China's textile industry Use scope it is particularly extensive, PFCs has the characteristic of persistence, degradation difficulty big, toxicity and bioaccumulation, to environment The health of biology and the mankind generate the influence of chronicity.Azo dyes extensively should due to its chromatic colour and the performance stablized For weaving, food, papermaking and leather industry.Forbidding azo dyes are mainly sensitization dyestuff and carcinogenicity dyestuff.In the market Nearly 70% is azo dyes in the synthetic dyestuffs of circulation, wherein about 210 kinds of carcinogenic aromatic amine may be restored.
Textile plays important role in daily life, and textile from raw material to product among plus It needs to use various TEXTILE CHEMICALSs (dyestuff and auxiliary agent) in work dyeing process.Contained harmful substance is generally in textile Micro or even trace level range, but poisonous and harmful substance is remained on textile clothes with human body Long Term Contact, and health is made Into harm.
Gustometry device, design visualization taste sensor, using sensitive material to liquid are had existed in the prior art So as to identify food agricultural product flavor characteristic, (yellow star is grand, and South Korea is triumphant, opens with color response for micro- trace chemical in body sample Avenge Ke, patent of invention, application number:201710540958.3 the applying date:2017.07.05);There is Patent design micro spectrometer pair Food is scanned, and is measured the ingredient and content of food, is compared with database, and food is collected through mini fan, heating unit Object smell (Lou Baodong, patent of invention, application number:201710666004.7 the applying date:2017.08.04);It is fast using electronic tongues The acid of speed detection food liquid, sweet tea, hardship, the intensity of salty four kinds of basic taste sensations, carry out macro operation to test result, can obtain difference Concentration basic taste sensation substance in electronic tongues relative intensity relationship (Li Zhi's space, Feng Tao, Xiao Zuobing, Hou Chun, Tian Huaixiang, Mao Deshou, Wangkai, patent of invention, application number:201210411946.8 the applying date:2012.12.25).Scope described in these patented technologies is only It is related to the flavor characteristic of food and the research of Taste Signals analysis, but is not directed to textile sense of taste research and provided by the present invention Textile sense of taste style measuring device, be especially not directed to it is provided by the present invention it is a kind of simulate human body chew generate the sense of taste spinning Fabric sense of taste generating means and method.
Here the textile sense of taste style proposed is not merely comprising traditional bitter, salty, sour, sweet tea, fresh five kinds of bases This taste perception, the oral cavity for also referring to people are contacted with respiratory tract with textile with the presence or absence of harmful substance threat health, such as Among Children, which can be caught in its mouth, chews clothes, and toxic chemical substance can then cause children certain harm on textile.Therefore it weaves Product need to be detected using highly sensitive and high accuracy Modern Analytical Instrument with people.Liquid chromatography is because of its strong separation Ability and high-resolution and the detection for being usually applied to textile.Higher boiling, thermal stability are poor, relative molecular weight is big (is more than More than 400) organic matter all can carry out separation analysis using high performance liquid chromatography in principle.Not only liquid-phase chromatographic analysis has Have the advantages that analyze speed is fast, highly sensitive, separation efficiency is high, automation, and liquid chromatogram and other instruments combination can be with Being complementary to one another more rapidly can accurately detect harmful substance.Have become the important means of textile analysis detection.
Invention content
The technical problems to be solved by the invention are to provide a kind of textile sense of taste style measuring device and measuring method, base In dynamic with liquid, heating and simulate mouth chew it is automatic, quickly and accurately the sense of taste style of textile is detected.
The technical solution adopted by the present invention to solve the technical problems is to provide a kind of textile sense of taste style measuring device, It is described including textile sense of taste generating means, fluid sampling device, liquid chromatography mass combined instrument and signal-data processing unit Several light sources, heat supply bionic finger, feed flow bionic finger and sampling bionic finger are equipped in textile sense of taste generating means, it is described Heat supply bionic finger, feed flow bionic finger and sampling bionic finger try textile by the driving of textile sense of taste generating means Sample carries out reciprocating friction, and the heat supply bionic finger heats fabric sample, and the feed flow bionic finger is to textile Sample provides liquid wetting, and the sampling bionic finger connect the liquid sample progress to fabric sample with fluid sampling device Extraction, the liquid sample import liquid chromatography mass combined instrument, the importing liquid chromatography mass by fluid sampling device Combined instrument is connected to signal-data processing unit.
The feed flow bionic finger and sampling bionic finger are arranged in parallel in textile sense of taste generating means, the heat supply Bionic finger is set to feed flow bionic finger with sampling the top position among bionic finger.
The textile sense of taste generating means includes first driving means, the second driving device and third driving device, institute State heat supply bionic finger drives progress to move back and forth back and forth horizontally and/or vertically by first driving means, and the feed flow is bionical Finger driven by the second driving device carry out back and forth horizontally and/or it is vertical move back and forth, the sampling bionic finger passes through the Three driving devices, which drive, move back and forth back and forth horizontally and/or vertically;
First telecontrol equipment includes the first stepper motor and first connecting rod, and the first connecting rod lower end and heat supply are bionical Finger connects, and the first stepper motor driving first connecting rod drives heat supply bionic finger back and forth to rub in fabric sample upper surface It wipes;
Second telecontrol equipment includes the second stepper motor and second connecting rod, and the second connecting rod lower end and feed flow are bionical Finger connects, and the second stepper motor driving second connecting rod drives feed flow bionic finger back and forth to rub in fabric sample lower surface It wipes;
The third telecontrol equipment includes third stepper motor and third connecting rod, and the third connecting rod lower end is bionical with sampling Finger connects, and the third stepper motor driving third connecting rod drives sampling bionic finger back and forth to rub in fabric sample lower surface It wipes.
Four corner positions of the textile sense of taste generating means are respectively equipped with light source, and four light sources are xenon long-arc lamp light One or more of source, xenon short-act lamp light source, fluorescent light source, halogen light source and ultraviolet light source.
The heat supply bionic finger includes the first silica gel finger and heater, and the first silica gel finger is humanoid hand Refer to, the heater is the thin slice heater being sleeved on the first silica gel finger, and the heat supply temperature of the heater is 20 DEG C~250 ℃。
The feed flow bionic finger includes the second silica gel finger and sample feeding pipe, and the second silica gel finger is humanoid hand Refer to, the sample feeding pipe outer end is connect with syringe, inner end is placed in the second silica gel finger interior and liquid outlet is set to the second silica gel The surface of finger.
The sampling bionic finger includes third silica gel finger and probe tube, and the third silica gel finger is humanoid hand Refer to, the probe tube outer end is connected to fluid sampling device, inner end is placed in third silica gel finger interior and inlet is set to the The surface of three silica gel fingers.
The surface of the heat supply bionic finger, feed flow bionic finger and sampling bionic finger is equipped with rough lines, The relative altitude of the lines is 50~5000 microns, relative spacing is 10~1000 microns.
The fluid sampling device includes sampling bottle, the first conduit, the second conduit and negative pressure device, and the sampling bottle passes through Second conduit is connect with negative pressure device, and the sampling bottle connect extracting liq sample by the first conduit with sampling bionic finger, The sampling bottle is connect by third conduit with liquid chromatography mass combined instrument imports liquid sample.
Another technical solution is to provide a kind of above-mentioned textile sense of taste wind used by the present invention solves its technical problem The measuring method of lattice measuring device, includes the following steps:
A) fabric sample is positioned between heat supply bionic finger, feed flow bionic finger and sampling bionic finger;
B) light source is opened, heat supply bionic finger is powered, fabric sample is carried out being heated to measuring predetermined temperature;
C) fabric sample is soaked to fabric sample feed flow by feed flow bionic finger;
D) start textile sense of taste generating means, driving heat supply bionic finger, feed flow bionic finger and sampling bionic finger Make chewing type reciprocating friction to fabric sample;
E) start liquid sampler and liquid chromatography mass combined instrument, pass through under the suction function of fluid sampling device Sample the liquid sample that bionic finger draws fabric sample, import liquid chromatography mass combined instrument to the component of liquid sample and Content is detected, and is passed through signal-data processing unit and carried out data analysis acquisition textile sense of taste style.
Advantageous effect
First, the present invention is innovatively devised a kind of textile sense of taste style for being matched liquid and heating based on dynamic and measures dress It puts, is the bionical action chewed based on human body, obtain the sense of taste degree of textile, be by being based on textile sense of taste generating means Exploitation, with reference to the application of liquid chromatography mass combined instrument, simulation human body chews the physiology course for generating the sense of taste, realizes textile Sense of taste style measures;
Second, the present invention in for soak textile liquid can be and human body fluid and the relevant liquid of saliva, mould Intend sense of taste style of the textile under the effects that saliva, sweat stain, physiological saline, restore environmental condition in human oral cavity, simulate people The sense of taste style of crunching textile or even harmful substance can also evaluate the harm of human body;
Third, the present invention can complete to different textiles under the conditions of illumination and high temperature ageing sense of taste style it is multiple fast Speed, qualitative and quantitative detection analysis, realize textile sense of taste style with the use of textile and the measure of the change of chew time;
4th, online data real-time display of the invention can accurate Characterization textile sense of taste style;
5th, the device of the invention is easy to operate, and repeatability is excellent, it can be achieved that measuring state that is automatic, easy, stablizing.
Description of the drawings
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is the structure diagram of textile sense of taste generating means of the present invention.
Fig. 3 is the structure diagram that heat supply bionic finger of the present invention is connect with first driving means.
Fig. 4 is the structure diagram that feed flow of the present invention (sampling) bionic finger is connect with second (third) driving device.
Fig. 5 is the dimensional structure diagram of bionic finger relative position of the present invention.
Fig. 6 is the planar structure schematic diagram of bionic finger relative position of the present invention.
Wherein:1- textile sense of taste generating means;2- light sources;11- chamber doors;12- first driving means;13- second Driving device;14- third driving devices;15- fabric samples;16- syringes;31- heat supply bionic fingers;32- feed flows Bionic finger;33- samples bionic finger;311- the first silica gel fingers;312- heaters;321- the second silica gel fingers; 322- sample feeding pipes;331- third silica gel fingers;332- probe tubes;41- sampling bottles;The first conduits of 42-;43- second is led Pipe;44- third conduits;5- vacuum pumps;6- liquid chromatography mass combined instruments, 7- signal-data processing units.
Specific embodiment
With reference to specific embodiment, the present invention is further explained.It should be understood that these embodiments are merely to illustrate the present invention Rather than it limits the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, people in the art Member can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited Range.
A kind of textile sense of taste style measuring device as shown in Figure 1, takes including textile sense of taste generating means 1, liquid Sampling device, liquid chromatography mass combined instrument 6 and signal-data processing unit 7.
As shown in Fig. 2, textile sense of taste generating means 1 is equipped with chamber door 11, and it is convenient that fabric sample 15 is replaced, it is interior Portion sets there are four light source 2, heat supply bionic finger 31, feed flow bionic finger 32 and samples bionic finger 33.
Four light sources 2 are respectively arranged at four corner positions of textile sense of taste generating means 1, and four light sources 2 are long arc It is one or more in xenon source, xenon short-act lamp light source, fluorescent light source, halogen light source and ultraviolet light source.Pass through light The aging action for simulating solarization and lights illumination is irradiated in source 2, by long-time irradiation and the control of irradiation level, can also add The ageing process of fast fabric sample 15, the sense of taste style of the textile under the conditions of simulation chewing for a long time.
As shown in Figure 5 and Figure 6, feed flow bionic finger 32 and sampling bionic finger 33 are arranged in parallel in the generation of the textile sense of taste In device 1, heat supply bionic finger 31 is set to feed flow bionic finger 32 with sampling the top position among bionic finger 33, weaving Product sample 15 rides on feed flow bionic finger 32 and sampling bionic finger 33 and is passed through from 31 bottom of heat supply bionic finger.Heat supply is imitated Green hand refers to 31, feed flow bionic finger 32 and sampling bionic finger 33 by the driving of textile sense of taste generating means 1 to textile Sample 15 carries out by chew formula reciprocating friction, and simulation mouth is to the chew of textile.
First driving means 12, the second driving device 13 and third driving are additionally provided with inside textile sense of taste generating means 1 Device 14.
As shown in figure 3, heat supply bionic finger 31 includes the first silica gel finger 311 and heater 312.First silica gel finger 311 be humanoid finger, a diameter of 15~20mm, a length of 24~30mm, a height of 14~18mm.Heater 312 is is sleeved on first Thin slice heater on silica gel finger 311, with certain flexibility and with good thermal conductivity, the heat supply temperature of heater 312 It is 20 DEG C~250 DEG C.First telecontrol equipment 12 includes the first stepper motor 121 and first connecting rod 122.122 lower end of first connecting rod It is connect with the rear end of heat supply bionic finger 31, the first stepper motor 121 driving first connecting rod 122 drives heat supply bionic finger 31 to exist Make horizontal-vertical parallel reciprocating friction in 15 upper surface of fabric sample.It rubs in heat supply bionic finger 31 and fabric sample 15 Temperature in mouth mastication processes during wiping is provided, higher temperature is provided in particular in and passes through for analyzing fabric sample 15 The sense of taste style of long-time mastication.
As shown in figure 4, feed flow bionic finger 32 includes the second silica gel finger 321 and sample feeding pipe 322.Second silica gel finger 321 be humanoid finger, a diameter of 15~20mm, a length of 24~30mm, a height of 14~18mm.Sample feeding pipe 322 is L-type conduit, A diameter of 4~6mm, a length of 35~40mm, outer end are connect with syringe 16, and inner end is placed in 321 inside of the second silica gel finger and goes out Liquid mouth is set to the upper surface of the second silica gel finger 321.Second telecontrol equipment 13 includes the second stepper motor 131 and second connecting rod 132.132 lower end of second connecting rod is connect with the rear end of feed flow bionic finger 32, the second stepper motor 131 driving second connecting rod 132 drive feed flow bionic finger 32 to make horizontal-vertical parallel reciprocating friction in 15 lower surface of fabric sample.Pass through syringe The liquid of 16 injections is delivered to by sample feeding pipe 322 on the surface of second silica gel finger 321, to being connect on the second silica gel finger 321 Tactile 15 feed flow of fabric sample wetting.Saliva, acid sweat stain, alkaline sweat stain, physiological saline, rain can be included by injecting liquid Water, deionized water and breast milk etc..
As shown in figure 4, sampling bionic finger 33 includes third silica gel finger 331 and probe tube 332.Third silica gel finger 331 be humanoid finger, a diameter of 15~20mm, a length of 24~30mm, a height of 14~18mm.Probe tube 332 is L-type conduit, Material is polypropylene, a diameter of 4~6mm, a length of 35~40mm, and outer end is connected to fluid sampling device, and inner end is placed in third silicon 331 inside of glue finger and inlet are set to the upper surface of third silica gel finger 331.Third telecontrol equipment 14 includes third stepping Motor 141 and third connecting rod 142.142 lower end of third connecting rod is connect with sampling the rear end of bionic finger 34, third stepper motor It is horizontal-vertical parallel reciprocal that 141 driving third connecting rods 142 drive sampling bionic fingers 33 to make in 15 lower surface of fabric sample Friction.
The surface of heat supply bionic finger 31, feed flow bionic finger 32 and sampling bionic finger 33 is equipped with rough thick Rough lines, the relative altitude of lines are 50~5000 microns, and relative spacing is 10~1000 microns, lines according to mouth lip Lines is designed.
Fluid sampling device includes sampling bottle 41, the first conduit 42, the second conduit 43 and negative pressure device 5.Sampling bottle 41 is logical It crosses the second conduit 43 to connect with negative pressure device 5, negative pressure device 5 uses vacuum pump, provides the negative pressure drawn needed for liquid sample.It takes 41 upper end of sample bottle is connect by the first conduit 42 with sampling the probe tube 332 of bionic finger 33, and extraction fabric sample 15 is through old The liquid sample that change and friction generate.41 upper end of sampling bottle connects additionally by third conduit 44 and liquid chromatography mass combined instrument 6 It connects, liquid sample is imported to liquid chromatography mass combined instrument 6 by third conduit 44.Liquid chromatography mass combined instrument 6 is connected to Signal-data processing unit 7, liquid chromatography mass combined instrument 6 detect the fluid sample that textile sense of taste generating means 1 generates, warp Signal-data processing unit 7 is analyzed, and obtains the sense of taste style of fabric sample 15.
A kind of measuring method of above-mentioned textile sense of taste style measuring device is provided below, includes the following steps:
A) by fabric sample 15 be positioned over heat supply bionic finger 31, feed flow bionic finger 32 and sampling bionic finger 33 it Between;
B) light source 2 is opened, the heater 312 of heat supply bionic finger 31 is powered, by heat supply bionic finger 31 to weaving Product sample 15 carries out being heated to measuring predetermined temperature;
C) liquid is drawn with syringe 16, injects sample feeding pipe 322, supplied by feed flow bionic finger 32 to fabric sample 15 Liquid soaks fabric sample 15;
D) start the first stepper motor 121, the second stepper motor 131 and third stepper motor 141, drive heat supply bionic hand Refer to 31, feed flow bionic finger 32 and sampling bionic finger 33 makees chewing type reciprocating friction to fabric sample 15;
E) start vacuum pump and liquid chromatography mass combined instrument 6, pass through sampling under the suction function of fluid sampling device Bionic finger 33 draws the liquid sample of fabric sample 15, imports component of the liquid chromatography mass combined instrument 6 to liquid sample It is detected with content, and passes through signal-data processing unit 7 and carry out data analysis acquisition textile sense of taste style.
The present apparatus can be completed based on textile sense of taste style measuring device of the dynamic with liquid and heating to different textiles The measurement evaluation of sense of taste style, is provided below ten specific embodiments:Embodiment 1 is commented for the measurement of mask sample sense of taste style Valency;Embodiment 2 is evaluated for the measurement of towel sample sense of taste style;Embodiment 3 is evaluated for the measurement of tissue sample sense of taste style; Embodiment 4 is evaluated for the measurement of home textile sample sense of taste style;Embodiment 5 is evaluated for the measurement of nightwear sample sense of taste style;Implement Example 6 is evaluated for the measurement of underwear sample sense of taste style;Embodiment 7 is evaluated for the measurement of automotive trim sample sense of taste style;Implement Example 8 is evaluated for the measurement of bib sample sense of taste style for baby;Embodiment 9 is the measurement of yam-like Molars rod sample sense of taste style Evaluation;Embodiment 10 is evaluated for the measurement of stroller cloth sample sense of taste style.
Embodiment 1
Mask sample is positioned between bionic finger;Start textile sense of taste generating means 1, it is ultraviolet to open roof four Heater 312 is powered by lamp source 2, and mask sample is carried out by heat supply bionic finger 31 to be heated to 35 DEG C;With syringe 16 Saliva solution is drawn, injects sample feeding pipe 322, into 32 surface of feed flow bionic finger, soaks mask sample;Start the first stepping electricity Machine 121, the second stepper motor 131 and third stepper motor 141 drive heat supply bionic finger 31, feed flow bionic finger 32 and sampling Bionic finger 33 makees mask sample the compound reciprocating friction of horizontal vertical of chewing type;Open vacuum pump and liquid chromatography mass connection With instrument 6, under fluid sampling device effect, liquid sample on mask sample is drawn by sampling bionic finger 33, by the Three conduits 44 import liquid chromatography mass combined instrument 6, analyze the component and content of liquid sample.Gained textile sense of taste style etc. Grade is as shown in table 1.
Embodiment 2
Towel sample is positioned between bionic finger 3;Start textile sense of taste generating means 1, open four purples of roof Outer lamp source 2, heater 312 is powered, and towel sample is carried out by heat supply bionic finger 31 to be heated to 80 DEG C;Use syringe 16 draw normal saline solution, inject sample feeding pipe 322, into 32 surface of feed flow bionic finger, soak towel sample;Start first Stepper motor 121, the second stepper motor 131 and third stepper motor 141 drive heat supply bionic finger 31, feed flow bionic finger 32 Make the compound reciprocating friction of horizontal vertical of chewing type to towel sample with sampling bionic finger 33;Open vacuum pump and liquid chromatogram Mass spectrometer 6, under fluid sampling device effect, by sampling the liquid sample on the absorption towel sample of bionic finger 33, Liquid chromatography mass combined instrument 6 is imported by third conduit 44, analyzes the component and content of liquid sample.The gained textile sense of taste Style grade is as shown in table 1.
Embodiment 3
Between tissue sample is positioned over bionic finger, start textile sense of taste generating means 1, open four day of roof Heater 312 is powered by light lamp source 2, and tissue sample is carried out by heat supply bionic finger 31 to be heated to 35 DEG C;With injection Device 16 draws normal saline solution, injects sample feeding pipe 322, into 32 surface of feed flow bionic finger, soaks tissue sample;Start First stepper motor 121, the second stepper motor 131 and third stepper motor 141 drive heat supply bionic finger 31, feed flow bionic hand Refer to 32 and sample the horizontal reciprocating friction that bionic finger 33 makees tissue sample chewing type;Open vacuum pump and liquid chromatogram matter Combined instrument 6 is composed, under fluid sampling device effect, by sampling the liquid sample on the absorption tissue sample of bionic finger 33, Liquid chromatography mass combined instrument 6 is imported by third conduit 44, analyzes the component and content of liquid sample.The gained textile sense of taste Style grade is as shown in table 1.
Embodiment 4
Between home textile sample is positioned over bionic finger, start textile sense of taste generating means 1, open four long arcs of roof Heater 312 is powered by xenon source 2, home textile sample is carried out by heat supply bionic finger 31 to be heated to 100 DEG C, with injection Device 16 draws sweat stain solution, injects sample feeding pipe 322, into 32 surface of feed flow bionic finger, soaks home textile sample;Start the first step Stepper motor 121, the second stepper motor 131 and third stepper motor 141 drive heat supply bionic finger 31,32 and of feed flow bionic finger Sampling bionic finger 33 makees home textile sample the compound reciprocating friction of horizontal vertical of chewing type;Open vacuum pump and liquid chromatogram matter Combined instrument 6 is composed, under fluid sampling device effect, by sampling the liquid sample on the absorption home textile sample of bionic finger 33, is led to It crosses third conduit 44 and imports liquid chromatography mass combined instrument 6, analyze the component and content of liquid sample.Gained textile sense of taste wind Lattice grade is as shown in table 1.
Embodiment 5
Between nightwear sample is positioned over bionic finger, start textile sense of taste generating means 1, it is ultraviolet to open roof four Heater 312 is powered by lamp source 2, nightwear sample is carried out by heat supply bionic finger 31 to be heated to 80 DEG C, with syringe 16 Sweat stain solution is drawn, injects sample feeding pipe 322, into 32 surface of feed flow bionic finger, soaks nightwear sample;Start the first stepping electricity Machine 121, the second stepper motor 131 and third stepper motor 141 drive heat supply bionic finger 31, feed flow bionic finger 32 and sampling Bionic finger 33 makees nightwear sample 15 the compound reciprocating friction of horizontal vertical of chewing type;Open vacuum pump and liquid chromatography mass Combined instrument 6 under fluid sampling device effect, by sampling the liquid sample on the absorption nightwear sample of bionic finger 33, passes through Third conduit 44 imports liquid chromatography mass combined instrument 6, analyzes the component and content of liquid sample.Gained textile sense of taste style Grade is as shown in table 1.
Embodiment 6
Between underwear sample is positioned over bionic finger, start textile sense of taste generating means 1, it is ultraviolet to open roof four Heater 312 is powered by lamp source 2, underwear sample is carried out by heat supply bionic finger 31 to be heated to 50 DEG C, with syringe 16 Sweat stain solution is drawn, sample feeding pipe 322 is injected, into 32 surface of feed flow bionic finger, wetting undergarments sample;Start the first stepping electricity Machine 121, the second stepper motor 131 and third stepper motor 141 drive heat supply bionic finger 31, feed flow bionic finger 32 and sampling Bionic finger 33 makees underwear sample 15 the compound reciprocating friction of horizontal vertical of chewing type;Open vacuum pump and liquid chromatography mass Combined instrument 6 under fluid sampling device effect, by sampling the liquid sample on the absorption underwear sample of bionic finger 33, passes through Third conduit 44 imports liquid chromatography mass combined instrument 6, analyzes the component and content of liquid sample.Gained textile sense of taste style Grade is as shown in table 1.
Embodiment 7
Automotive trim sample is positioned between bionic finger;Start textile sense of taste generating means 1, open roof four Heater 312 is powered by xenon long-arc lamp light source 2, and automotive trim sample is carried out by heat supply bionic finger 31 to be heated to 250 ℃;Normal saline solution is drawn with syringe 16, injects sample feeding pipe 322, into 32 surface of feed flow bionic finger, is soaked in automobile Adorn sample;Start the first stepper motor 121, the second stepper motor 131 and third stepper motor 141 and drive heat supply bionic finger 31st, feed flow bionic finger 32 and sampling bionic finger 33 make automotive trim sample the horizontal vertical of chewing type and compound back and forth rub It wipes;Vacuum pump and liquid chromatography mass combined instrument 6 are opened, under fluid sampling device effect, is inhaled by sampling bionic finger 33 The liquid sample on automotive trim sample is taken, liquid chromatography mass combined instrument 6 is imported by third conduit 44, analyzes liquid sample Component and content.Gained textile sense of taste style grade is as shown in table 1.
Embodiment 8
Bib sample for baby is positioned between bionic finger;Start textile sense of taste generating means 1, open roof four A ultraviolet light source 2, heater 312 is powered, and bib sample for baby is carried out being heated to 80 by heat supply bionic finger 31 ℃;Saliva solution is drawn with syringe 16, sample feeding pipe 322 is injected, into 32 surface of feed flow bionic finger, soaks bib for baby Sample;Start the first stepper motor 121, the second stepper motor 131 and third stepper motor 141 drive heat supply bionic finger 31, Horizontal vertical that feed flow bionic finger 32 and sampling bionic finger 33 make chewing type to bib sample 15 for baby is compound back and forth to rub It wipes;Vacuum pump and liquid chromatography mass combined instrument 6 are opened, under the effect of fluid sampling device 4, is inhaled by sampling bionic finger 33 The liquid sample on bib sample for baby is taken, liquid chromatography mass combined instrument 6 is imported by third conduit 44, analyzes liquid-like This component and content.Gained textile sense of taste style grade is as shown in table 1.
Embodiment 9
Yam-like Molars rod sample is positioned between bionic finger 3;Start textile sense of taste generating means 1, open top Four fluorescent light sources 2 of wall, heater 312 is powered, and yam-like Molars rod sample is added by heat supply bionic finger 31 Heat is to 35 DEG C;Saliva solution is drawn with syringe 16, injects sample feeding pipe 322, into 32 surface of feed flow bionic finger, soaks yarn Shape Molars rod sample;Starting the first stepper motor 121, the second stepper motor 131 and third stepper motor 141 drives heat supply bionical Finger 31, feed flow bionic finger 32 and sampling bionic finger 33 make the vertically reciprocating of chewing type to yam-like Molars rod sample and rub It wipes;Vacuum pump and liquid chromatography mass combined instrument 6 are opened, under fluid sampling device effect, is inhaled by sampling bionic finger 33 The liquid sample on yam-like Molars rod sample is taken, liquid chromatography mass combined instrument 6 is imported by third conduit 44, analyzes liquid The component and content of sample.Gained textile sense of taste style grade is as shown in table 1.
Embodiment 10
Stroller cloth sample is positioned between bionic finger 3;Start textile sense of taste generating means 1, open top Four ultraviolet light sources 2 of wall, heater 312 is powered, and stroller cloth sample is added by heat supply bionic finger 31 Heat is to 200 DEG C;Normal saline solution is drawn with syringe 16, injects sample feeding pipe 322, into 32 surface of feed flow bionic finger, profit Wet stroller cloth sample;Start the first stepper motor 121, the second stepper motor 131 and the driving of third stepper motor 141 to supply Hot bionic finger 31, feed flow bionic finger 32 and sampling bionic finger 33 make stroller cloth sample 15 level of chewing type Vertical compound reciprocating friction;Vacuum pump and liquid chromatography mass combined instrument 6 are opened, under fluid sampling device effect, by taking Sample bionic finger 33 draws the liquid sample on stroller cloth sample, and importing liquid chromatography mass by third conduit 44 joins With instrument 6, the component and content of liquid sample are analyzed.Gained textile sense of taste style grade is as shown in table 1.
Table 1

Claims (10)

1. a kind of textile sense of taste style measuring device, it is characterised in that:It is taken including textile sense of taste generating means (1), liquid Sampling device, liquid chromatography mass combined instrument (6) and signal-data processing unit (7), the textile sense of taste generating means (1) are interior Equipped with several light sources (2), heat supply bionic finger (31), feed flow bionic finger (32) and sampling bionic finger (33), the heat supply The drive that bionic finger (31), feed flow bionic finger (32) and sampling bionic finger (33) pass through textile sense of taste generating means (1) Dynamic to carry out reciprocating friction to fabric sample (15), the heat supply bionic finger (31) heats fabric sample (15), The feed flow bionic finger (32) provides liquid wetting to fabric sample (15), and the sampling bionic finger (33) takes with liquid Sampling device connection extracts the liquid sample of fabric sample (15), and the liquid sample is imported by fluid sampling device Liquid chromatography mass combined instrument (6), the importing liquid chromatography mass combined instrument (6) are connected to signal-data processing unit (7).
2. a kind of textile sense of taste style measuring device according to claim 1, it is characterised in that:The feed flow bionic hand Refer to (32) and sampling bionic finger (33) is arranged in parallel in textile sense of taste generating means (1), the heat supply bionic finger (31) it is set to feed flow bionic finger (32) top position intermediate with sampling bionic finger (33).
3. a kind of textile sense of taste style measuring device according to claim 1 or 2, it is characterised in that:The textile Sense of taste generating means (1) includes first driving means (12), the second driving device (13) and third driving device (14), the confession Hot bionic finger (31) is driven by first driving means (12) move back and forth back and forth horizontally and/or vertically, the feed flow Bionic finger (32) is driven by the second driving device (13) move back and forth back and forth horizontally and/or vertically, and the sampling is imitative Green hand refers to (33) and progress is driven to move back and forth back and forth horizontally and/or vertically by third driving device (14);
First telecontrol equipment (12) includes the first stepper motor (121) and first connecting rod (122), the first connecting rod (122) lower end is connect with heat supply bionic finger (31), and the first stepper motor (121) driving first connecting rod (122), which drives, to supply Hot bionic finger (31) is in fabric sample (15) upper surface reciprocating friction;
Second telecontrol equipment (13) includes the second stepper motor (131) and second connecting rod (132), the second connecting rod (132) lower end is connect with feed flow bionic finger (32), and the second stepper motor (131) driving second connecting rod (132), which drives, to supply Liquid bionic finger (32) is in fabric sample (15) lower surface reciprocating friction;
The third telecontrol equipment (14) includes third stepper motor (141) and third connecting rod (142), the third connecting rod (142) lower end is connect with sampling bionic finger (34), and third stepper motor (141) the driving third connecting rod (142), which drives, to be taken Sample bionic finger (33) is in fabric sample (15) lower surface reciprocating friction.
4. a kind of textile sense of taste style measuring device according to claim 1, it is characterised in that:The textile sense of taste Four corner positions of generating means (1) are respectively equipped with light source (2), and four light sources (2) are xenon long-arc lamp light source, xenon short-act lamp light One or more of source, fluorescent light source, halogen light source and ultraviolet light source.
5. a kind of textile sense of taste style measuring device according to claim 1, it is characterised in that:The heat supply bionic hand Refer to (31) and include the first silica gel finger (311) and heater (312), the first silica gel finger (311) is humanoid finger, institute It is the thin slice heater being sleeved on the first silica gel finger (311) to state heater (312), the heat supply temperature of the heater (312) It is 20 DEG C~250 DEG C.
6. a kind of textile sense of taste style measuring device according to claim 1, it is characterised in that:The feed flow bionic hand Refer to (32) and include the second silica gel finger (321) and sample feeding pipe (322), the second silica gel finger (321) is humanoid finger, institute State that sample feeding pipe (322) outer end is connect with syringe (16), inner end is placed in that the second silica gel finger (321) is internal and liquid outlet is set to The surface of second silica gel finger (321).
7. a kind of textile sense of taste style measuring device according to claim 1, it is characterised in that:The sampling bionic hand Refer to (33) and include third silica gel finger (331) and probe tube (332), the third silica gel finger (331) is humanoid finger, institute State that probe tube (332) outer end is connected to fluid sampling device, inner end is placed in that third silica gel finger (331) is internal and inlet is set In the surface of third silica gel finger (331).
8. a kind of textile sense of taste style measuring device according to claim 1,5,6 or 7, it is characterised in that:The confession The surface of hot bionic finger (31), feed flow bionic finger (32) and sampling bionic finger (33) is equipped with rough lines, institute The relative altitude for stating lines is 50~5000 microns, relative spacing is 10~1000 microns.
9. a kind of textile sense of taste style measuring device according to claim 1, it is characterised in that:The liquid sampling dress It puts including sampling bottle (41), the first conduit (42), the second conduit (43) and negative pressure device (5), the sampling bottle (41) passes through Two conduits (43) are connect with negative pressure device (5), and the sampling bottle (41) passes through the first conduit (42) and sampling bionic finger (33) Extracting liq sample is connected, the sampling bottle (41) is connect by third conduit (44) with liquid chromatography mass combined instrument (6) leads Enter liquid sample.
10. a kind of measuring method of textile sense of taste style measuring device described in claim 1, includes the following steps:
A) fabric sample (15) is positioned over heat supply bionic finger (31), feed flow bionic finger (32) and sampling bionic finger (33) between;
B) light source (2) is opened, heat supply bionic finger (31) energization is carried out being heated to measuring pre- constant temperature to fabric sample (15) Degree;
C) fabric sample (15) is soaked to fabric sample (15) feed flow by feed flow bionic finger (32);
D) start textile sense of taste generating means (1), driving heat supply bionic finger (31), feed flow bionic finger (32) and sampling are imitative Green hand refers to (33) and makees chewing type reciprocating friction to fabric sample (15);
E) start liquid sampler and liquid chromatography mass combined instrument (6), pass through under the suction function of fluid sampling device The liquid sample that bionic finger (33) draws fabric sample (15) is sampled, imports liquid chromatography mass combined instrument (6) to liquid The component and content of sample are detected, and are passed through signal-data processing unit (7) and carried out the data analysis acquisition textile sense of taste Style.
CN201711435717.9A 2017-12-26 2017-12-26 Textile taste style measuring device and measuring method Expired - Fee Related CN108254458B (en)

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