CN108251914A - A kind of superfine notoginseng powder cellulose fibre preparation method - Google Patents
A kind of superfine notoginseng powder cellulose fibre preparation method Download PDFInfo
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- CN108251914A CN108251914A CN201810042603.6A CN201810042603A CN108251914A CN 108251914 A CN108251914 A CN 108251914A CN 201810042603 A CN201810042603 A CN 201810042603A CN 108251914 A CN108251914 A CN 108251914A
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- Prior art keywords
- notoginseng powder
- cellulose fibre
- bamboo
- bamboo pulp
- radix notoginseng
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/18—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from other substances
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacturing & Machinery (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Artificial Filaments (AREA)
Abstract
The invention discloses a kind of superfine notoginseng powder cellulose fibre preparation methods, comprise the technical steps that：Pretreatment, prepare spinning solution, spinning solution extrudes to form stoste thread from spinneret orifice, stoste thread is frozen into as-spun fibre, as-spun fibre is wrapped or is directly post-processed to obtain finished product, Radix Notoginseng powder is applied to functional fiber field, and combine the bamboo pulp of high mechanical strength, new cellulosic is made, this cellulose fibre is while holding bamboo pulp fiber original advantage, using the healthcare function of Radix Notoginseng medicinal powder compensate for bamboo pulp fiber in process bamboo natural characteristic by destroy the shortcomings that, so that the utility model cellulose fibre has deodorization, antibacterial, also there is healthcare function while anti-ultraviolet function, reasonable design of the present invention, more hommization, it is suitble to promote the use of.
Description
Technical field
The present invention relates to a kind of fiber producing processes, more particularly, to a kind of superfine notoginseng powder cellulose fibre preparation side
Method.
Background technology
Functional fiber refers in addition to physical mechanical property possessed by general fiber, also with certain specific function
Tencel.The appearance of functional fiber is the revolutionary mark of material science, its development and progress promotes traditional textile
Industry rises to high-tech industry.Functional fiber has property in physics, chemistry, medicine and biology etc.,
It is widely used to multiple fields.Existing functional fiber mainly uses and has functional component with fiber to fibre
It ties up progress chemical modification or will be provided with functional component and be attached directly on fiber, make it have certain property.
However often there is certain irritation to skin by the functional fiber after chemical modification, it is in direct contact people it is difficult to be prepared into
Body skin fabric can not compare with natural fiber.
The ingredient of Radix Notoginseng powder is as Radix Notoginseng main root, rich in notoginsenoside, notoginseng polysaccharide, dencichine, flavones active ingredient,
With hemostasis, promoting blood circulation and removing blood stasis, detumescence ding-tong, strengthening by means of tonics, antifatigue, resist oxygen lack, anti-aging, reducing blood lipid, blood pressure lowering, improve machine
The effects that body immunity function.Available for various inside and outside haemorrhages such as treatment traumatic hemorrhage, hemostasis, gastrorrhagia, hematurias；Expand blood
Pipe, thrombus improve microcirculation, and prevention and treatment hyperlipidemia, cholesterol increase, coronary heart diseases and angina pectoris, apoplexy sequela
Wait cardiovascular and cerebrovascular diseases；The hepatopathys such as fatty liver, liver fibrosis and lose blood, postpartum, physically weak disease caused by the reasons such as prolonged illness.Raw three
Seven have：The mass formed by blood stasis such as bruise hemostasis, traumatic hemorrhage, postpartum anemic fainting, haematemesis, bleeding from five sense organs or subcutaneous tissue, the heart and brain such as coronary heart disease, hyperlipidemia, hypertension
Vascular diseases；Ripe Radix Notoginseng has：For in poor health, loss of appetite, neurasthenia, over fatigue, lose blood, anaemia etc.；Ripe three
Seven powder have good effect to gynaecological diseases such as postoperative patient and menalgias.Bamboo pulp is with bamboo woods such as mao bamboon, bamboo, cizu
For raw material, commonly use sulfate process and soda processes etc. and be made.Also have tender bamboo through de- blueness, semi-mature material is pickled into lime.Fiber shape
State and length, between timber and grass fiber.Easily sizing, bamboo pulp is the paper pulp of moderate fiber length, thin and soft.Sheet pulp
Bulk, tearability are high, and pop strength and tensile strength are relatively low.There is higher mechanical strength.
Due to the various advantages of Radix Notoginseng powder, Radix Notoginseng powder is applied to functional fiber field, and combine high mechanical strength
New cellulosic is made in bamboo pulp, this cellulose fibre utilizes Radix Notoginseng medicinal powder while holding bamboo pulp fiber original advantage
Healthcare function compensate for the shortcomings that natural characteristic of bamboo pulp fiber bamboo in process is by destroying so that the utility model is fine
Also with healthcare function while cellulose fiber is with deodorization, antibacterial, anti-ultraviolet function.
Invention content
The present invention provides a kind of superfine notoginseng powder cellulose fibre preparation method, can effectively solve in above-mentioned background technology
The problem of.
Technical scheme of the present invention is summarized as follows：
A kind of superfine notoginseng powder cellulose fibre preparation method, comprises the technical steps that：
1st step, pretreatment, percentage take the Radix Notoginseng powder of 20-50%, add in the dispersant of 2-10%, add in
Deionized water obtains Radix Notoginseng powder dispersion liquid to 100%, by mixed system after being sufficiently mixed stirring；
2nd step, prepares spinning solution, and Radix Notoginseng powder dispersion liquid and a certain amount of bamboo pulp made from the 1st step are sufficiently mixed and are stirred
It mixes, and adds in adhesive, spinning solution is made；
Spinning solution made from 2nd step is extruded to form stoste thread from spinneret orifice by the 3rd step；
Stoste thread made from 3rd step is frozen into as-spun fibre by the 4th step；
5th step, as-spun fibre are wrapped or are directly post-processed to obtain finished product.
Preferably, the dispersant of the 1st step is polyoxyethylene alkylphenol base ether, dihydromethyl propionic acid, dicyandiamide, gathers
One or more of bicyclic pentyl ester of ammonium phosphate, methyl acid phosphate.
Preferably, the Radix Notoginseng powder dispersion liquid is equivalent to the 20-30% of bamboo pulp percentage by volume, in the 2nd step
Adhesive is carboxymethyl cellulose and the mixture of starch slurry.
Preferably, the bamboo pulp in the 2nd step is raw material by bamboo woods such as mao bamboon, bamboo, cizu, with sulfate process or burning
Alkaline process is made.
Preferably, the time being mixed in the 1st step is 2-4h, and whipping temp is 35-45 DEG C, the 2nd step
In mixing time for 3-6h, whipping temp is 40-60 DEG C.
Compared with prior art, the beneficial effects of the invention are as follows：
(1) Radix Notoginseng powder rich in notoginsenoside, notoginseng polysaccharide, dencichine, flavones active ingredient, have hemostasis, it is promoting blood circulation and removing blood stasis,
Detumescence ding-tong, antifatigue, resist oxygen lack, anti-aging, reducing blood lipid, blood pressure lowering, improves the effects that body's immunity at strengthening by means of tonics.
Available for various inside and outside haemorrhages such as treatment traumatic hemorrhage, hemostasis, gastrorrhagia, hematurias；Blood vessel is expanded, thrombus improves micro-
Cycle, the cardiovascular and cerebrovascular diseases such as prevention and treatment hyperlipidemia, cholesterol increase, coronary heart diseases and angina pectoris, apoplexy sequela；Fat
The hepatopathys such as fat liver, liver fibrosis and lose blood, postpartum, physically weak disease caused by the reasons such as prolonged illness, be applied to cellulose field,
Gradually improve human body constitution, keep fit and healthy, extend human life-span.
(2) bamboo pulp fiber form and length are easily glued between timber and grass fiber, and bamboo pulp is moderate fiber length
Paper pulp, thin and soft, sheet pulp bulk, tearability height, pop strength and tensile strength are relatively low, there is higher mechanical strength,
Bamboo pulp fiber has the function of deodorization, antibacterial, antiultraviolet, and bamboo pulp fiber and Radix Notoginseng powder are combined, and blend spinning original is made
Liquid is also added to the healthcare function of Radix Notoginseng powder while its deodorization, antibacterial, antiultraviolet advantage is kept, achieves many things at one stroke.
(3) carboxymethyl cellulose belongs to native cellulose, is that the polysaccharide most wide, content is most, source are distributed in nature
Very abundant.The modification technology of current fibre element is concentrated mainly on two aspect of etherificate and esterification.Carboxymethylation reaction is etherificate skill
One kind of art.Cellulose obtains carboxymethyl cellulose (CMC) after carboxy methylation, aqueous solution have thickening, film forming, gluing,
The effects that water tariff collection, colloid protection, emulsification and suspension, it is widely used in the industries such as oil, food, medicine, textile and paper,
It is one of most important cellulose ethers, adhesive is carboxymethyl cellulose and the mixture of starch slurry in the present invention, by bamboo pulp
It is bonded together with Radix Notoginseng powder dispersion liquid, conducive to spinning solution is made after its mixing.
Specific embodiment
The technical solution in the embodiment of the present invention is clearly and completely described below in conjunction with the embodiment of the present invention,
Obviously, described embodiment is only part of the embodiment of the present invention, instead of all the embodiments, based in the present invention
Embodiment, those of ordinary skill in the art's all other embodiments obtained without making creative work, all
Belong to the scope of protection of the invention.
Embodiment one
A kind of superfine notoginseng powder cellulose fibre preparation method, comprises the technical steps that：
1st step pre-processes, percentage, takes 20% Radix Notoginseng powder, adds in 2% dispersant, adds in deionization
Water obtains Radix Notoginseng powder dispersion liquid to 100%, by mixed system after being sufficiently mixed stirring；
2nd step, prepares spinning solution, and Radix Notoginseng powder dispersion liquid and a certain amount of bamboo pulp made from the 1st step are sufficiently mixed and are stirred
It mixes, and adds in adhesive, spinning solution is made；
Spinning solution made from 2nd step is extruded to form stoste thread from spinneret orifice by the 3rd step；
Stoste thread made from 3rd step is frozen into as-spun fibre by the 4th step；
5th step, as-spun fibre are wrapped or are directly post-processed to obtain finished product.
In this embodiment, the dispersant of the 1st step is polyoxyethylene alkylphenol base ether, dihydromethyl propionic acid, dicyandiamide, gathers
One or more of bicyclic pentyl ester of ammonium phosphate, methyl acid phosphate.
In this embodiment, Radix Notoginseng powder dispersion liquid is equivalent to the 20% of bamboo pulp percentage by volume, and the adhesive in the 2nd step is
The mixture of carboxymethyl cellulose and starch slurry.
In this embodiment, the bamboo pulp in the 2nd step is raw material by bamboo woods such as mao bamboon, bamboo, cizu, with sulfate process or burning
Alkaline process is made.
In this embodiment, the time being mixed in the 1st step is 2h, and whipping temp is 35 DEG C, and the mixing in the 2nd step is stirred
The time mixed is 3h, and whipping temp is 40 DEG C.
Embodiment two
A kind of superfine notoginseng powder cellulose fibre preparation method, comprises the technical steps that：
1st step, pretreatment, percentage, take 50% Radix Notoginseng powder, add in 10% dispersant, addition go from
Sub- water obtains Radix Notoginseng powder dispersion liquid to 100%, by mixed system after being sufficiently mixed stirring；
2nd step, prepares spinning solution, and Radix Notoginseng powder dispersion liquid and a certain amount of bamboo pulp made from the 1st step are sufficiently mixed and are stirred
It mixes, and adds in adhesive, spinning solution is made；
Spinning solution made from 2nd step is extruded to form stoste thread from spinneret orifice by the 3rd step；
Stoste thread made from 3rd step is frozen into as-spun fibre by the 4th step；
5th step, as-spun fibre are wrapped or are directly post-processed to obtain finished product.
In this embodiment, the dispersant of the 1st step is polyoxyethylene alkylphenol base ether, dihydromethyl propionic acid, dicyandiamide, gathers
One or more of bicyclic pentyl ester of ammonium phosphate, methyl acid phosphate.
In this embodiment, Radix Notoginseng powder dispersion liquid is equivalent to the 30% of bamboo pulp percentage by volume, and the adhesive in the 2nd step is
The mixture of carboxymethyl cellulose and starch slurry.
In this embodiment, the bamboo pulp in the 2nd step is raw material by bamboo woods such as mao bamboon, bamboo, cizu, with sulfate process or burning
Alkaline process is made.
In this embodiment, the time being mixed in the 1st step is 4h, and whipping temp is 45 DEG C, and the mixing in the 2nd step is stirred
The time mixed is 6h, and whipping temp is 60 DEG C.
Embodiment three
A kind of superfine notoginseng powder cellulose fibre preparation method, comprises the technical steps that：
1st step pre-processes, percentage, takes 35% Radix Notoginseng powder, adds in 6% dispersant, adds in deionization
Water obtains Radix Notoginseng powder dispersion liquid to 100%, by mixed system after being sufficiently mixed stirring；
2nd step, prepares spinning solution, and Radix Notoginseng powder dispersion liquid and a certain amount of bamboo pulp made from the 1st step are sufficiently mixed and are stirred
It mixes, and adds in adhesive, spinning solution is made；
Spinning solution made from 2nd step is extruded to form stoste thread from spinneret orifice by the 3rd step；
Stoste thread made from 3rd step is frozen into as-spun fibre by the 4th step；
5th step, as-spun fibre are wrapped or are directly post-processed to obtain finished product.
In this embodiment, the dispersant of the 1st step is polyoxyethylene alkylphenol base ether, dihydromethyl propionic acid, dicyandiamide, gathers
One or more of bicyclic pentyl ester of ammonium phosphate, methyl acid phosphate.
In this embodiment, Radix Notoginseng powder dispersion liquid is equivalent to the 25% of bamboo pulp percentage by volume, and the adhesive in the 2nd step is
The mixture of carboxymethyl cellulose and starch slurry.
In this embodiment, the bamboo pulp in the 2nd step is raw material by bamboo woods such as mao bamboon, bamboo, cizu, with sulfate process or burning
Alkaline process is made.
In this embodiment, the time being mixed in the 1st step is 3h, and whipping temp is 40 DEG C, and the mixing in the 2nd step is stirred
The time mixed is 4.5h, and whipping temp is 50 DEG C.
This kind of superfine notoginseng powder cellulose fibre preparation method, Technology design is completely compact, Radix Notoginseng powder rich in notoginsenoside,
Notoginseng polysaccharide, dencichine, flavones active ingredient have hemostasis, promoting blood circulation and removing blood stasis, detumescence ding-tong, strengthening by means of tonics, antifatigue, resistance to scarce
Oxygen, reducing blood lipid, blood pressure lowering, improves the effects that body's immunity at anti-aging.Go out available for treatment traumatic hemorrhage, hemostasis, stomach
The various inside and outside haemorrhages such as blood, hematuria；Blood vessel is expanded, thrombus improves microcirculation, prevention and treatment hyperlipidemia, cholesterol
Increase, the cardiovascular and cerebrovascular diseases such as coronary heart diseases and angina pectoris, apoplexy sequela；The hepatopathys such as fatty liver, liver fibrosis and lose blood,
Physically weak disease caused by the reasons such as postpartum, prolonged illness, is applied to cellulose field, gradually improves human body constitution, keep fit and healthy, prolong
Long human life-span；Bamboo pulp fiber form and length are easily glued between timber and grass fiber, and bamboo pulp is moderate fiber length
Paper pulp, thin and soft, sheet pulp bulk, tearability height, pop strength and tensile strength are relatively low, there is higher mechanical strength,
Bamboo pulp fiber has the function of deodorization, antibacterial, antiultraviolet, and bamboo pulp fiber and Radix Notoginseng powder are combined, and blend spinning original is made
Liquid is also added to the healthcare function of Radix Notoginseng powder while its deodorization, antibacterial, antiultraviolet advantage is kept, achieves many things at one stroke；Carboxylic first
Base cellulose belongs to native cellulose, is that the polysaccharide most wide, content is most, source very abundant are distributed in nature.It is current fine
The modification technology of dimension element is concentrated mainly on two aspect of etherificate and esterification.Carboxymethylation reaction is one kind of etherification technology.Cellulose
Carboxymethyl cellulose (CMC) is obtained after carboxy methylation, there is aqueous solution thickening, film forming, gluing, water tariff collection, colloid to protect
The effects that shield, emulsification and suspension, it is widely used in the industries such as oil, food, medicine, textile and paper, is most important fiber
One of plain ethers, mixture of the adhesive for carboxymethyl cellulose and starch slurry in the present invention, by bamboo pulp and Radix Notoginseng powder dispersion liquid
It is bonded together, conducive to spinning solution is made after its mixing, reasonable design of the present invention, more hommization are suitble to promote the use of.
Although the embodiments of the present invention have been disclosed as above, but its be not restricted in specification and embodiment it is listed
With it can be fully applied to various fields suitable for the present invention, for those skilled in the art, can be easily
Realize other modification, therefore without departing from the general concept defined in the claims and the equivalent scope, it is of the invention and unlimited
In specific details and embodiment shown here.
Claims (5)
1. a kind of superfine notoginseng powder cellulose fibre preparation method, which is characterized in that comprise the technical steps that：
1st step, pretreatment, percentage take the Radix Notoginseng powder of 20-50%, add in the dispersant of 2-10%, addition go from
Sub- water obtains Radix Notoginseng powder dispersion liquid to 100%, by mixed system after being sufficiently mixed stirring；
2nd step, prepares spinning solution, and Radix Notoginseng powder dispersion liquid and a certain amount of bamboo pulp made from the 1st step are sufficiently mixed stirring, and
Adhesive is added in, spinning solution is made；
Spinning solution made from 2nd step is extruded to form stoste thread from spinneret orifice by the 3rd step；
Stoste thread made from 3rd step is frozen into as-spun fibre by the 4th step；
5th step, as-spun fibre are wrapped or are directly post-processed to obtain finished product.
2. a kind of superfine notoginseng powder cellulose fibre preparation method according to claims 1, which is characterized in that described
The dispersant of 1 step is polyoxyethylene alkylphenol base ether, dihydromethyl propionic acid, dicyandiamide, ammonium polyphosphate, the bicyclic pentyl ester of methyl acid phosphate
One or more of.
3. a kind of superfine notoginseng powder cellulose fibre preparation method according to claims 1, which is characterized in that described three
Seven powder dispersion liquids are equivalent to the 20-30% of bamboo pulp percentage by volume, and the adhesive in the 2nd step is carboxymethyl cellulose and shallow lake
The mixture of slurry.
4. a kind of superfine notoginseng powder cellulose fibre preparation method according to claims 1, which is characterized in that described
Bamboo pulp in 2 steps is raw material by bamboo woods such as mao bamboon, bamboo, cizu, is made with sulfate process or soda processes.
5. a kind of superfine notoginseng powder cellulose fibre preparation method according to claims 1, which is characterized in that described
The time being mixed in 1 step is 2-4h, and whipping temp is 35-45 DEG C, and the time of the mixing in the 2nd step is 3-
6h, whipping temp are 40-60 DEG C.
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| CN201810042603.6A CN108251914A (en) | 2018-01-17 | 2018-01-17 | A kind of superfine notoginseng powder cellulose fibre preparation method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113699681A (en) * | 2021-08-28 | 2021-11-26 | 许玉梅 | Non-woven fabric manufacturing method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113699681A (en) * | 2021-08-28 | 2021-11-26 | 许玉梅 | Non-woven fabric manufacturing method |
| CN113699681B (en) * | 2021-08-28 | 2022-08-26 | 广东好念头医疗器械有限公司 | Non-woven fabric manufacturing method |
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Application publication date: 20180706 |