CN108245555A - A kind of preparation method of Chinese medicinal material - Google Patents
A kind of preparation method of Chinese medicinal material Download PDFInfo
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- CN108245555A CN108245555A CN201810218633.8A CN201810218633A CN108245555A CN 108245555 A CN108245555 A CN 108245555A CN 201810218633 A CN201810218633 A CN 201810218633A CN 108245555 A CN108245555 A CN 108245555A
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- fleece
- flower root
- auxiliary material
- extractive
- juice
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/704—Polygonum, e.g. knotweed
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Alternative & Traditional Medicine (AREA)
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- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses a kind of preparation method of Chinese medicinal material, are related to Chinese medicine processing technique field.A kind of preparation method of Chinese medicinal material, S1:Auxiliary material makes, and takes 1 part of Semen sesami nigrum, boils 3 hours, filtration, just 1.2~1.8 parts of extractive is obtained, then Semen sesami nigrum is boiled 2 hours, filtration obtains time 0.8~1.2 part of extractive, merge just extractive and time extractive obtains juice auxiliary material, juice auxiliary material is concentrated or add water, obtain 2~3 parts of juice auxiliary materials;S2:Bored profit takes 10 parts of fleece-flower root block piece, is mixed thoroughly with the juice auxiliary material, is put into container and stands;S3:Vacuum processing makes fleece-flower root surface generate fine and closely woven sand holes;S4:It steams, auxiliary material is made further to moisturize the fleece-flower root.This programme not only enhances the drug effect of the fleece-flower root, reduces traditional processing process, further reduces " poison " property of the fleece-flower root.
Description
Technical field
The present invention relates to Chinese medicine processing technique field, more particularly to a kind of preparation method of Chinese medicinal material.
Background technology
The fleece-flower root be few section's Plant-Polygonum Polygonum multiflorum Thunb. dried root, bitter, it is sweet,
Puckery, slightly warm in nature, Return liver, the heart, kidney channel have removing toxic substances, the carbuncle that disappears, preventing malaria, relax bowel and other effects, prepared fleece flower root with filling liver kidney,
Benefiting essence-blood, strengthening the bones and muscles, changes turbid lipid-loweringing and other effects at black beard and hair.
But the fleece-flower root is directly edible to have the phenomenon that cause is let out, therefore the method for using " processing " from ancient times to the present, how first removal is
" poison " property that this cause of crow is let out.
Fleece-flower root successive dynasties concocting method has net system, cutting, is not added with auxiliary material system, adds auxiliary material system, more than 20 kinds of several major class of concoction system
Concocting method.The auxiliary material system of being not added with includes boiling, steaming, exposing, frying, processing, roasting etc. heating the concocting method processed merely, adds auxiliary material
System is processed with auxiliary material simply, more than two tastes or two tastes.
Modern times carry out the fleece-flower root composition Study discovery, and anthraquinone analog compound, anthraquinone analog compound tool are contained in the fleece-flower root
Under playing the role of hemostasis, antibacterial, rushing down, diuresis.In the fleece-flower root, Anthraquinones include " combined anthraquinone " and " dissociated anthraquinone " again, wherein
It is caused by " combined anthraquinone " to cause " poison " property let out.
Invention content
The shortcomings that technical problems to be solved by the invention are, overcome the prior art provides a kind of preparation method of Chinese medicinal material,
By the way that auxiliary material is added to be processed, the content of " combined anthraquinone " in the fleece-flower root is reduced.
In order to solve the above technical problems, the present invention provides a kind of preparation method of Chinese medicinal material,
S1:Auxiliary material makes, and takes Semen sesami nigrum 10kg, boils 3 hours, filtration, extractive about 15kg, Semen sesami nigrum tanning 2 is small
When, filtration, extractive about 10kg merges juice, concentrates or adds water, it is 25kg to make juice total amount.
S2:Bored profit takes net fleece-flower root block piece 100kg, is mixed thoroughly, is put in stainless steel barrel with boiled Semen sesami nigrum juice, bored profit,
Treat that juice exhausts.
S3:Vacuum processing, the fleece-flower root sabot that will be moisturized, sabot 3~5cm of thickness are put in reduced vacuum drying box, are taken out true
Sky keeps vacuum degree 0.08 or so, about 1.5 hours, fleece-flower root piece is made to generate fine and closely woven sand holes, slowly discharges vacuum.
S4:It steams, the fleece-flower root after reduced pressure treatment is put in digester, is heated with steam, vapor (steam) temperature 110~120
DEG C, digester pressure normal pressure is started the clock after upper vapour, is steamed 8 hours, 80 DEG C of dryings.
The beneficial effects of the invention are as follows:
(1) score in the present invention refers to mass fraction, and the function of the fleece-flower root is filling liver kidney, benefiting essence-blood, black beard and hair, strong tight
Gu, change turbid lipid-loweringing.The effect of Semen sesami nigrum mainly filling liver kidney, benefiting essence-blood.Therefore it does auxiliary material with Semen sesami nigrum and processes the fleece-flower root, it can be with
The effect of enhancing fleece-flower root filling liver kidney, benefiting essence-blood.And Semen sesami nigrum is food and medicament dual-purpose medicinal material, non-toxic and side effect, therefore completely
It may be used as processing the auxiliary material of the fleece-flower root
(2) present invention makes medicinal material generate fine and closely woven sand holes, is conducive to auxiliary material juice and penetrates into medicine with reduced vacuum facture
Material central part makes processed product inside and outside color evenly, and quality is more stable;
(3) present invention steam during steaming is easier to enter inside medicinal material, and the fleece-flower root is made to be heated evenly, will not be produced
The phenomenon that raw outer dilute inner hard, the shape of processed product is more complete.
(4) present invention can reach processing effect in the case where reduction steams number, shorten the production cycle, reduce
Energy consumption.In addition, do the effect of auxiliary material can enhance prepared fleece flower root filling liver kidney, benefiting essence-blood using Semen sesami nigrum.
Specific embodiment
Embodiment 1:
A kind of preparation method of Chinese medicinal material provided in this embodiment,
S1:Auxiliary material makes, and takes Semen sesami nigrum 10kg, boils 3 hours, and filtration obtains extractive 15kg, and Semen sesami nigrum is being boiled 2
Hour, filtration obtains extractive 10kg, merges juice, concentrates or adds water, it is 25kg to make juice total amount.
S2:Bored profit takes net fleece-flower root block piece 100kg, is mixed thoroughly, is put in stainless steel barrel with boiled Semen sesami nigrum juice, bored profit,
Treat that juice exhausts.
S3:Vacuum processing, the fleece-flower root sabot that will be moisturized, sabot 4 ± 0.5cm of thickness are put in reduced vacuum drying box, are taken out
Vacuum keeps 0.08 ± 0.01Mpa of vacuum degree, after 1.5 hours, fleece-flower root piece is made to generate fine and closely woven sand holes, slowly discharges vacuum.
S4:It steams, the fleece-flower root after reduced pressure treatment is put in digester, is heated with steam, 115 DEG C of vapor (steam) temperature, boiling
Pot pressure normal pressure, starts the clock after upper vapour, steams 8 hours, is placed in 80 DEG C of environment dry.
Score in this programme refers to mass fraction, and the function of the fleece-flower root is filling liver kidney, benefiting essence-blood, black beard and hair, strong fastening, changes
Turbid lipid-loweringing.The effect of Semen sesami nigrum mainly filling liver kidney, benefiting essence-blood.Therefore it does auxiliary material with Semen sesami nigrum and processes the fleece-flower root, can enhance
The effect of fleece-flower root filling liver kidney, benefiting essence-blood.And Semen sesami nigrum is food and medicament dual-purpose medicinal material, non-toxic and side effect, therefore completely can be with
As the auxiliary material for processing the fleece-flower root.With reduced vacuum facture, medicinal material is made to generate fine and closely woven sand holes, be conducive to the infiltration of auxiliary material juice
To medicinal material central part, make processed product inside and outside color evenly, quality is more stable;Steam is easier to enter during steaming
Inside medicinal material, the fleece-flower root is made to be heated evenly, the phenomenon that outer dilute inner hard will not be generated, the shape of processed product is more complete.It is reducing
It can reach processing effect in the case of steaming number, shorten the production cycle, reduce energy consumption.In addition, it is done using Semen sesami nigrum
Auxiliary material can enhance the effect of prepared fleece flower root filling liver kidney, benefiting essence-blood.
Using the present embodiment finished product fleece-flower root piece manufactured secondary in three batches be denoted as respectively No. 2 samples, No. 3 samples, No. 4
Sample.
The fleece-flower root processes Historic Evolution
Now steaming method (CP method), decoction of black soybean Traditional Method (nine, which steam nine, shines) big gun are mixed with steamed method (CP method), decoction of black soybean respectively
Prepared fleece flower root, and obtain No. 5 samples, No. 6 samples, No. 7 samples.
No. 5 sample makings, steamed method (CP method):
Net fleece-flower root block piece 100kg is taken, is mixed thoroughly, is put in stainless steel barrel with clear water about 25kg, bored profit moisturizes.By what is moisturized
The fleece-flower root is put in digester, is heated with steam, 110~120 DEG C of vapor (steam) temperature, and digester pressure normal pressure starts to count after upper vapour
Evaluation time steams 8 hours, until surface, section take out in sepia, digester inner liquid medicine are drenched and is dipped into fleece-flower root surface, 80
DEG C drying.
No. 6 sample makings, decoction of black soybean mix steaming method (CP method):
Black soya bean 10kg is taken, is boiled 4 hours, filtration, extractive about 15kg, then black soya bean is boiled 3 hours, filtration, extractive is about
10kg merges juice, concentrates or adds water, it is 25kg to make juice total amount.Net fleece-flower root block piece 100kg is taken, with boiled black soya bean
Juice is mixed thoroughly, is put in stainless steel barrel, bored profit, treats that juice exhausts.The fleece-flower root moisturized is put in digester, is heated with steam, steam
110~120 DEG C of temperature, digester pressure normal pressure, starts the clock after upper vapour, steams 8 hours, until surface, section are in
Sepia is taken out, and the leaching of digester inner liquid medicine is dipped into fleece-flower root surface, 80 DEG C of dryings.
No. 7 sample makings, decoction of black soybean Traditional Method (nine, which steam nine, shines):
Fleece-flower root medicine materical crude slice 100kg is taken, is first soaked 24 hours with water in which rice has been washed, in wooden one layer of black soya bean of rice steamer middle berth, spreads one layer of tuber of multiflower knotweed, then
One layer of black soya bean is spread, one layer of tuber of multiflower knotweed is alternate layer by layer, face upper berth beans, beans is gone to dry for degree so that beans are ripe, the raw black soya bean of method before secondary sunshine
It steams, steams 9 times repeatedly again, shine 9 times, discard black soya bean, 80 DEG C of dryings.As No. 7 samples.
No. 1 sample making:
The fresh fleece-flower root is taken, is cleaned, is sliced, it is dry, obtain Radix Polygoni Multiflori.
To 1~No. 7 sample respectively according to《Chinese Pharmacopoeia》Version in 2000, defined method measures free under prepared fleece flower root item
The content of anthraquinone, combined anthraquinone and Stibene-glucoside, and following table is made:
Different concocting method Anthraquinones, Stibene-glucoside comparision contents (%):
As can be seen from the above table, concocting method of the invention, the content of Stibene-glucoside is apparently higher than in processed product《China
Pharmacopeia》Defined decoction of black soybean mixes steaming method and steamed method, is only second to tradition nine and steams nine solarization methods, the decline degree of combined anthraquinone and free
The rising degree of anthraquinone is better than CP method.And reduce the number steamed in technique, reach and preferably process effect.
In addition to the implementation, the present invention can also have other embodiment;It is all to use equivalent substitution or equivalent transformation shape
Into technical solution, all fall within the present invention claims protection domain.
Claims (2)
1. a kind of preparation method of Chinese medicinal material, it is characterised in that:
S1:Auxiliary material makes, and takes 1 part of Semen sesami nigrum, boils 3 hours, and filtration obtains just 1.2~1.8 parts of extractive, then Semen sesami nigrum is endured
System 2 hours, filtration obtain time 0.8~1.2 part of extractive, merge just extractive and time extractive obtains juice auxiliary material, to juice auxiliary material into
Row concentration adds water, obtains 2~3 parts of juice auxiliary materials;
S2:Bored profit takes 10 parts of fleece-flower root block piece, is mixed thoroughly with the juice auxiliary material, is put into container and stands;
S3:Vacuum processing takes out the fleece-flower root piece of bored profit from the container, and the fleece-flower root piece is placed on vessel,
Then the vessel are put into confined space, the space is carried out after sealing to take out air decompression, protects the pressure in the space
It holds in 0.06~0.1Mpa, the retention time is 1~2 hour, fleece-flower root piece is made to generate fine and closely woven sand holes, then to the confined space
In be filled with air to standard atmospheric pressure;
S4:It steams, the fleece-flower root piece with sand holes is put into digester, is heated with steam, vapor (steam) temperature 110~120
DEG C, pressure is 1Mpa in digester, and the timing since " upper vapour " is steamed 7~9 hours, then taken out, in 70~90 DEG C of environment
In be dried to obtain finished product.
2. a kind of preparation method of Chinese medicinal material according to claim 1, it is characterised in that:
S2:Bored profit, the container are stainless steel barrel.
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CN201810218633.8A CN108245555B (en) | 2018-03-16 | 2018-03-16 | Processing method of polygonum multiflorum |
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CN201810218633.8A CN108245555B (en) | 2018-03-16 | 2018-03-16 | Processing method of polygonum multiflorum |
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CN108245555A true CN108245555A (en) | 2018-07-06 |
CN108245555B CN108245555B (en) | 2021-05-14 |
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Citations (1)
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CN107773586A (en) * | 2017-11-15 | 2018-03-09 | 贵州大学 | A kind of processing procedure of black soya bean slurry prepared fleece flower root |
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CN107773586A (en) * | 2017-11-15 | 2018-03-09 | 贵州大学 | A kind of processing procedure of black soya bean slurry prepared fleece flower root |
Non-Patent Citations (2)
Title |
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国家药典委员会编: "《中国人民共和国药典临床用药须知:2015年版.中药饮片卷》", 30 September 2017 * |
陆兔林等主编: "《中药炮制学实验》", 31 January 2015 * |
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