CN108200912A - Mosquito repellent missible oil, mosquito expelling summer sleeping mat and preparation method thereof - Google Patents
Mosquito repellent missible oil, mosquito expelling summer sleeping mat and preparation method thereof Download PDFInfo
- Publication number
- CN108200912A CN108200912A CN201611187357.0A CN201611187357A CN108200912A CN 108200912 A CN108200912 A CN 108200912A CN 201611187357 A CN201611187357 A CN 201611187357A CN 108200912 A CN108200912 A CN 108200912A
- Authority
- CN
- China
- Prior art keywords
- mosquito
- missible oil
- summer sleeping
- sleeping mat
- mosquito repellent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/02—Processes; Apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/34—Organic impregnating agents
- B27K3/50—Mixtures of different organic impregnating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/20—Removing fungi, molds or insects
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Forests & Forestry (AREA)
- Dispersion Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of mosquito repellent missible oil, mosquito expelling summer sleeping mat and preparation method thereof.The mosquito repellent missible oil, is made of by weight percentage following components：Metadelphene 5 15%, sophoramine 2 4%, emulsifier 8 15%, surplus is organic solvent.The mosquito expelling summer sleeping mat is prepared using following methods：(1) after mosquito repellent missible oil being diluted with water 20 60 times, dip dyeing liquid for shell is formed；(2) by summer sleeping mat dip dyeing in the dip dyeing liquid for shell, drying, you can the mosquito expelling summer sleeping mat is made.The mosquito repellent missible oil of the present invention to safety of human and livestock, be not likely to produce drug resistance, be easy to degrade in natural environment, the mosquito expelling summer sleeping mat prepared by the present invention, the insect infestations ability such as mosquito expelling is strong, and repelling effect is lasting.
Description
Technical field
The present invention relates to a kind of missible oil, summer sleeping mat and preparation method thereof more particularly to mosquito repellent missible oil, mosquito expelling summer sleeping mat and its preparations
Method.
Background technology
The main harm of mosquito is to spread the disease.It was found that the disease of mosquitoes spread is up to as many as more than 80 kinds.On earth,
Which kind of animal there is the harm of bigger without to the mankind than mosquito again.
The pathophorous mosquito of energy is broadly divided into three classes in China：One kind is anopheles, popular name malarial mosquito, main propagation malaria.According to
Incomplete statistics, in 1 year of nineteen twenty-nine, the whole world about 200 ten thousand people lethal because suffering from malaria.It is another kind of to be culex, main propagation
Filariasis and Japanese Type-B encephalitis.Third class has black and white speckle, is called blackspot mosquito, main propagation is popular with it yellow-fever mosquito
Encephalitis B and dengue fever.
For a long time, people control mosquito using a variety of methods, but effect is unsatisfactory.
Invention content
For above-mentioned deficiency in the prior art, the first technical problem to be solved by the present invention provides a kind of mosquito repellent
Missible oil.
The second technical problem to be solved by the present invention is to provide a kind of preparation method of mosquito expelling summer sleeping mat.
The third technical problem to be solved by the present invention provides a kind of mosquito expelling summer sleeping mat.
The present invention seeks to what is be achieved through the following technical solutions：
A kind of mosquito repellent missible oil, is made of by weight percentage following components：Metadelphene 5-15%, sophoramine 2-4%, emulsification
Agent 8-15%, surplus are organic solvent.
The emulsifier is Tea Saponin and one kind or its mixture in agriculture breast 2201.Optimal, the emulsifier is by 20-
40wt% Tea Saponins and 60-80wt% agriculture breasts 2201 mix.
The organic solvent can be arene：Benzene,toluene,xylene；Fat hydrocarbon：Pentane, hexane, octane；Fat
Cyclic hydrocar-bons：Hexamethylene, cyclohexanone, toluene cyclohexanone；Halogenated hydrocarbons：Chlorobenzene, dichloro-benzenes, dichloromethane；Alcohols：Methanol, ethyl alcohol,
Isopropanol；Ethers：Ether, propylene oxide；Esters：Methyl acetate, ethyl acetate, propyl acetate；Ketone：Acetone, espeleton,
Methylisobutylketone, N-Methyl pyrrolidone；Diol, derivatives：Glycol monoethyl ether, ethylene glycol monoethyl ether, ethylene glycol monobutyl ether；
Other：Acetonitrile, pyridine, phenol, dimethyl sulfoxide (DMSO).
Preferably, the organic solvent is N-Methyl pyrrolidone, ethyl acetate, propyl acetate, dimethyl sulfoxide (DMSO), second two
One kind or its mixture in alcohol monomethyl ether, ethylene glycol monoethyl ether and ethylene glycol monobutyl ether.
Optimal, the organic solvent is ethylene glycol monoethyl ether.
Metadelphene also known as N, N- n,N-diethyl meta-toluamide, CAS accession number：134-62-3, English name：N,N-
Diethyl-3-methylbenzamide, referred to as：DEET.
Tea Saponin also known as tea saponin are a kind of candy glucoside compounds by being extracted in tea tree seed, are that a kind of performance is good
Good natural surfactant.Belong to triterpenes saponin with toil pungent, stimulation nasal membrane causes sneeze, and sterling is white
Color fine columnar crystal, hygroscopicity is strong, paramethyl red in acidity, be insoluble in absolute methanol, ethyl alcohol, insoluble in ether, acetone,
The organic solvents such as benzene, petroleum ether are soluble in aqueous methanol, hydrous ethanol and glacial acetic acid, aceticanhydride, pyridine etc..
Above-mentioned mosquito repellent missible oil may be used the general missible oil preparation method of the industry and be prepared, specifically, may be used
Following step：Metadelphene, sophoramine and emulsifier are added in organic solvent, 50-60 DEG C is heated to, is uniformly mixed, i.e.,
The mosquito repellent missible oil of the present invention can be made.
The mosquito repellent missible oil of the present invention, can spray after dilution, can rapid mosquito repellent.
The present invention also provides a kind of preparation methods of mosquito expelling summer sleeping mat, include the following steps：
(1) after the mosquito repellent missible oil being diluted with water 20-60 times, dip dyeing liquid for shell is formed；
(2) by summer sleeping mat dip dyeing in the dip dyeing liquid for shell, drying, you can the mosquito expelling summer sleeping mat of the present invention is made.
Preferably, the mass ratio of the summer sleeping mat and dip dyeing liquid for shell is 1:15-1:30, dip dyeing temperature is 50~90 DEG C, during dip dyeing
Between 10~60min.
Obviously, summer sleeping mat used can be commercially available without the processed summer sleeping mat of mosquito repellent in the present invention, such as bamboo mat, numb seat, grass
Seat or rattan seat.
Further, it the present invention also provides a kind of mosquito expelling summer sleeping mat, is prepared using the above method.
The insect infestations ability such as the mosquito expelling summer sleeping mat prepared by the present invention, mosquito expelling is strong, and repelling effect is lasting, mosquito repellent
Missible oil to safety of human and livestock, be not likely to produce drug resistance, be easy to degrade in natural environment.
Specific embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1：Prepare mosquito repellent missible oil
1 data of embodiment as corresponding to table 1 weigh each component, Metadelphene, sophoramine and emulsifier are added in organic molten
In agent, 50-60 DEG C is heated to, is uniformly mixed, you can the mosquito repellent missible oil of the present invention is made.
Table 1：Mosquito repellent emulsifiable concentrate formulation list position：Kilogram
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Metadelphene | 5 | 15 | 10 | 10 | 10 |
| Sophoramine | 4 | 2 | 3 | 3 | 3 |
| Tea Saponin | 8 | / | 10 | / | 3 |
| Agriculture breast 2201 | / | 15 | / | 10 | 7 |
| Ethylene glycol monoethyl ether | 83 | 68 | 77 | 77 | 77 |
Embodiment 2：Prepare mosquito repellent missible oil
2 data of embodiment as corresponding to table 1 weigh each component, Metadelphene, sophoramine and emulsifier are added in organic molten
In agent, 50-60 DEG C is heated to, is uniformly mixed, you can the mosquito repellent missible oil of the present invention is made.
Embodiment 3：Prepare mosquito repellent missible oil
3 data of embodiment as corresponding to table 1 weigh each component, Metadelphene, sophoramine and emulsifier are added in organic molten
In agent, 50-60 DEG C is heated to, is uniformly mixed, you can the mosquito repellent missible oil of the present invention is made.
Embodiment 4：Prepare mosquito repellent missible oil
4 data of embodiment as corresponding to table 1 weigh each component, Metadelphene, sophoramine and emulsifier are added in organic molten
In agent, 50-60 DEG C is heated to, is uniformly mixed, you can the mosquito repellent missible oil of the present invention is made.
Embodiment 5：Prepare mosquito repellent missible oil
5 data of embodiment as corresponding to table 1 weigh each component, Metadelphene, sophoramine and emulsifier are added in organic molten
In agent, 50-60 DEG C is heated to, is uniformly mixed, you can the mosquito repellent missible oil of the present invention is made.
Claims (6)
1. a kind of mosquito repellent missible oil, which is characterized in that be made of by weight percentage following components：Metadelphene 5-15%, sophoramine
2-4%, emulsifier 8-15%, surplus are organic solvent.
2. mosquito repellent missible oil as described in claim 1, it is characterised in that：The emulsifier is one in Tea Saponin and agriculture breast 2201
Kind or its mixture.
3. mosquito repellent missible oil as claimed in claim 2, it is characterised in that：The emulsifier is by 20-40wt% Tea Saponins and 60-
80wt% agriculture breasts 2201 mix.
4. mosquito repellent missible oil as described in claim 1, it is characterised in that：The organic solvent is N-Methyl pyrrolidone, acetic acid
One kind in ethyl ester, propyl acetate, dimethyl sulfoxide (DMSO), glycol monoethyl ether, ethylene glycol monoethyl ether and ethylene glycol monobutyl ether or its
Mixture.
5. a kind of preparation method of mosquito expelling summer sleeping mat, which is characterized in that include the following steps：
(1) after claim 1-4 any one of them mosquito repellent missible oil being diluted with water 20-60 times, dip dyeing liquid for shell is formed；
(2) by summer sleeping mat dip dyeing in the dip dyeing liquid for shell, drying.
6. the preparation method of mosquito expelling summer sleeping mat as claimed in claim 5, it is characterised in that：The mass ratio of the summer sleeping mat and dip dyeing liquid for shell
It is 1:15-1:30, dip dyeing temperature is 50~90 DEG C, 10~60min of immerged time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611187357.0A CN108200912A (en) | 2016-12-20 | 2016-12-20 | Mosquito repellent missible oil, mosquito expelling summer sleeping mat and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611187357.0A CN108200912A (en) | 2016-12-20 | 2016-12-20 | Mosquito repellent missible oil, mosquito expelling summer sleeping mat and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108200912A true CN108200912A (en) | 2018-06-26 |
Family
ID=62603613
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611187357.0A Pending CN108200912A (en) | 2016-12-20 | 2016-12-20 | Mosquito repellent missible oil, mosquito expelling summer sleeping mat and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108200912A (en) |
-
2016
- 2016-12-20 CN CN201611187357.0A patent/CN108200912A/en active Pending
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180626 |