CN108193313A - A kind of preparation process of textile material for adding amino silane and its application - Google Patents
A kind of preparation process of textile material for adding amino silane and its application Download PDFInfo
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- CN108193313A CN108193313A CN201711481768.5A CN201711481768A CN108193313A CN 108193313 A CN108193313 A CN 108193313A CN 201711481768 A CN201711481768 A CN 201711481768A CN 108193313 A CN108193313 A CN 108193313A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/06—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyolefin as constituent
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Preparation process and its application the invention discloses a kind of textile material for adding amino silane, this method is used polypropylene fiber, silk fiber, barium metaborate, ball-milled mixtures are made by ball-milling treatment in zirconium sulfate, again by dimethyl double hexadecyl ammonium chloride, amino silane, epoxy propane butyl ether, drying obtains stirring mixture after absolute ethyl alcohol is mixed, then the two is put into reaction kettle jointly, add in stabilizer, high-temperature stirring after adhesive, obtain thermal reaction mixture, thermal reaction mixture is finally sent into double screw extruder, product is squeezed out, plastotype, last drying obtains the textile material of finished product addition amino silane.The textile material of addition amino silane being prepared, intensity is high, wear-resisting, stain resistant, has a good application prospect in household textiles.
Description
Technical field
The present invention relates to this technical fields of textile material, are related specifically to a kind of textile material for adding amino silane
Preparation process and its application.
Background technology
Textile material refers to fiber and fibre, is embodied in fiber, yarn, fabric and its compound.Fiber is
The basic unit of textile material, fiber are by sources divided into two major class of natural fiber and chemical fibre with custom.According to the object of fiber
Natural fiber is divided into plant fiber, animal origin and mineral fibres by matter source attribute.By raw material, processing method and constituent
Difference, and regenerated fiber, synthetic fibers and inorfil three classes can be divided into.With the yarn that textile fabric is process in various
Property, yarn presses its system, there is yarn, silk, line；It is formed by fiber, is divided into pure yarn, scribbled, with yarn；It presses
The distribution of composite fibre is divided into uniform blended yarns, variation blended yarns, combination or complex yarn.Fabric, abbreviation cloth are
The main species of fibre are the citation forms of textile.Textile presses the difference of the mode of production, can broadly be divided into yarn
The classes such as class, band class, rope class, woven fabric, knitted fabric, braided fabric and non-woven cloth.
Natural fiber has the characteristics that higher intensity, at low cost, low density, and when regularity is good, the intensity of yarn is high,
Uniformly, any surface finish, filoplume are few, and therefore, spinning property is good.But textile material made of natural fiber is often in performance
Cannot meet the needs of growing, it is multiple made of natural fiber and high molecular material with the continuous development of scientific research
Condensation material can overcome the defects of natural fiber, be successfully applied to each field.
Amino silane is a kind of chemical substance, commonly used in fiberglass, coating, casting, plastics, adhesive, fluid sealant, spinning
It knits in all trades and professions such as printing and dyeing, is the tackifier of RTV silicon rubber, and weaving material is given by adding amino silane in textile material
Material self performance brings improved research to have not been reported.
Invention content
In order to solve the above technical problems, the present invention provide it is a kind of add amino silane textile material preparation process and its
Using, this method is used is made ball-milled mixtures by polypropylene fiber, silk fiber, barium metaborate, zirconium sulfate by ball-milling treatment,
It dries and obtains after dimethyl double hexadecyl ammonium chloride, amino silane, epoxy propane butyl ether, absolute ethyl alcohol are mixed again
Mixture is stirred, then puts into the two in reaction kettle jointly, adds in high-temperature stirring after stabilizer, adhesive, is obtained hot anti-
Mixture is answered, thermal reaction mixture is finally sent into double screw extruder, product is squeezed out, plastotype, last drying is obtained into
Product add the textile material of amino silane.The textile material of addition amino silane being prepared, intensity is high, wear-resisting, resistance to be stained with
Dirt has a good application prospect in household textiles.
The purpose of the present invention can be achieved through the following technical solutions：
A kind of preparation process for the textile material for adding amino silane, includes the following steps：
(1) 32-36 parts of polypropylene fiber, 27-29 parts of silk fiber, 6-10 parts of barium metaborate, 5-7 parts of zirconium sulfate are placed in ball
Ball-milling treatment is carried out in grinding machine, obtains ball-milled mixtures；
(2) by 7-9 parts of dimethyl double hexadecyl ammonium chloride, 4-6 parts of amino silane, 4-6 parts of epoxy propane butyl ether, nothing
50-60 parts of mixing of water-ethanol, stir 150min with the rotating speed of 350-400r/min in magnetic stirrer, then dry in an oven
Dry, drying temperature is 50-60 DEG C, obtains stirring mixture；
(3) the stirring mixture that the ball-milled mixtures for obtaining step (1) are obtained with step (2) puts into reaction kettle jointly
In, 3-5 parts of stabilizer, 3-5 parts of adhesive are then added in, reaction kettle is then heated, reaction temperature is made to be promoted to 110-120 DEG C,
The mixing speed for keeping reaction kettle is 1200-1300r/min, persistently stirs 60min, obtains thermal reaction mixture；
(4) thermal reaction mixture for obtaining step (3) is sent into double screw extruder, product is squeezed out, plastotype, most passed through afterwards
Drying obtains the textile material of finished product addition amino silane.
Further, the ratio of grinding media to material of ball mill is 15 in the step (1):1, drum's speed of rotation 250-300r/min,
Ball-milling Time is 80-90min.
Further, the stabilizer in the step (3) is arbitrary in orange osmanthus acid esters, moon calcium silicates, barium naphthanate
It is a kind of.
Further, the adhesive in the step (3) is in polyacrylate, sulfenamide, chlorine Bezalip Tablets
Any one.
Further, the screw speed of double screw extruder is 230r/min in the step (4), and each area's temperature is：One
185 DEG C of area's temperature, two 215 DEG C of area's temperature, three 210 DEG C of area's temperature, four 190 DEG C of area's temperature.
Further, the textile material the invention also discloses the addition amino silane obtained by the preparation process exists
Application in waterproof barrier material field.
Compared with prior art, the present invention advantage is：
(1) preparation process of the textile material of addition amino silane of the invention is used polypropylene fiber, silk fiber, partially
Ball-milled mixtures are made by ball-milling treatment in barium borate, zirconium sulfate, then by dimethyl double hexadecyl ammonium chloride, amino silane,
Drying obtains stirring mixture after epoxy propane butyl ether, absolute ethyl alcohol are mixed, and the two is then put into reaction jointly
In kettle, high-temperature stirring after stabilizer, adhesive is added in, obtains thermal reaction mixture, thermal reaction mixture is finally sent into double spiral shells
Bar extruder squeezes out product, plastotype, and last drying obtains the textile material of finished product addition amino silane.It is prepared
The textile material of amino silane is added, intensity is high, wear-resisting, stain resistant, has a good application prospect in household textiles.
(2) present invention employs dimethyl double hexadecyl ammonium chloride, amino silane, epoxy propane butyl ether is these types of
Drying obtains stirring mixture after raw material is mixed with absolute ethyl alcohol, is then total to stirring mixture with ball-milled mixtures
With thermal response is carried out, effective performance boost is carried out to textile material, although these materials are not first Application in weaving material
In material, but it is aided with corresponding processing mode after amount combination according to a certain ratio, to the addition amino silane being finally prepared
Textile material brings increasing substantially in performance, this is never to report in previous research, for realizing
The technique effect of the present invention plays the role of conclusive.
Specific embodiment
The technical solution of invention is described in detail with reference to specific embodiment.
Embodiment 1
(1) 32 parts of polypropylene fiber, 27 parts of silk fiber, 6 parts of barium metaborate, 5 parts of zirconium sulfate are placed in ball mill and carried out
Ball-milling treatment, the ratio of grinding media to material of ball mill is 15:1, drum's speed of rotation 250r/min, Ball-milling Time 80min obtain ball milling and mix
Close object；
(2) by 7 parts of dimethyl double hexadecyl ammonium chloride, 4 parts of amino silane, 4 parts of epoxy propane butyl ether, absolute ethyl alcohol
50 parts of mixing, stir 150min with the rotating speed of 350r/min in magnetic stirrer, then dry in an oven, drying temperature is
50 DEG C, obtain stirring mixture；
(3) the stirring mixture that the ball-milled mixtures for obtaining step (1) are obtained with step (2) puts into reaction kettle jointly
In, 3 parts of orange osmanthus acid esters, 3 parts of polyacrylate are then added in, then heats reaction kettle, reaction temperature is made to be promoted to 110 DEG C, is protected
The mixing speed for holding reaction kettle is 1200r/min, persistently stirs 60min, obtains thermal reaction mixture；
(4) thermal reaction mixture for obtaining step (3) is sent into double screw extruder, the screw speed of double screw extruder
For 230r/min, each area's temperature is：One 185 DEG C of area's temperature, two 215 DEG C of area's temperature, three 210 DEG C of area's temperature, four area's temperature 190
DEG C, product is squeezed out using double screw extruder, plastotype, last drying obtains the textile material of finished product addition amino silane.
The performance test results of the textile material of addition amino silane obtained are as shown in table 1.
Embodiment 2
(1) 34 parts of polypropylene fiber, 28 parts of silk fiber, 8 parts of barium metaborate, 6 parts of zirconium sulfate are placed in ball mill and carried out
Ball-milling treatment, the ratio of grinding media to material of ball mill is 15:1, drum's speed of rotation 275r/min, Ball-milling Time 85min obtain ball milling and mix
Close object；
(2) by 8 parts of dimethyl double hexadecyl ammonium chloride, 5 parts of amino silane, 5 parts of epoxy propane butyl ether, absolute ethyl alcohol
55 parts of mixing, stir 150min with the rotating speed of 375r/min in magnetic stirrer, then dry in an oven, drying temperature is
55 DEG C, obtain stirring mixture；
(3) the stirring mixture that the ball-milled mixtures for obtaining step (1) are obtained with step (2) puts into reaction kettle jointly
In, 4 parts of moon calcium silicates, 4 parts of sulfenamide are then added in, then heats reaction kettle, reaction temperature is made to be promoted to 115 DEG C, is kept
The mixing speed of reaction kettle is 1250r/min, persistently stirs 60min, obtains thermal reaction mixture；
(4) thermal reaction mixture for obtaining step (3) is sent into double screw extruder, the screw speed of double screw extruder
For 230r/min, each area's temperature is：One 185 DEG C of area's temperature, two 215 DEG C of area's temperature, three 210 DEG C of area's temperature, four area's temperature 190
DEG C, product is squeezed out using double screw extruder, plastotype, last drying obtains the textile material of finished product addition amino silane.
The performance test results of the textile material of addition amino silane obtained are as shown in table 1.
Embodiment 3
(1) 36 parts of polypropylene fiber, 29 parts of silk fiber, 10 parts of barium metaborate, 7 parts of zirconium sulfate are placed in ball mill and carried out
Ball-milling treatment, the ratio of grinding media to material of ball mill is 15:1, drum's speed of rotation 300r/min, Ball-milling Time 90min obtain ball milling and mix
Close object；
(2) by 9 parts of dimethyl double hexadecyl ammonium chloride, 6 parts of amino silane, 6 parts of epoxy propane butyl ether, absolute ethyl alcohol
60 parts of mixing, stir 150min with the rotating speed of 400r/min in magnetic stirrer, then dry in an oven, drying temperature is
60 DEG C, obtain stirring mixture；
(3) the stirring mixture that the ball-milled mixtures for obtaining step (1) are obtained with step (2) puts into reaction kettle jointly
In, 5 parts of barium naphthanate, 5 parts of chlorine Bezalip Tablets are then added in, reaction kettle is then heated, reaction temperature is made to be promoted to 120 DEG C,
The mixing speed for keeping reaction kettle is 1300r/min, persistently stirs 60min, obtains thermal reaction mixture；
(4) thermal reaction mixture for obtaining step (3) is sent into double screw extruder, the screw speed of double screw extruder
For 230r/min, each area's temperature is：One 185 DEG C of area's temperature, two 215 DEG C of area's temperature, three 210 DEG C of area's temperature, four area's temperature 190
DEG C, product is squeezed out using double screw extruder, plastotype, last drying obtains the textile material of finished product addition amino silane.
The performance test results of the textile material of addition amino silane obtained are as shown in table 1.
Comparative example 1
(1) 34 parts of polypropylene fiber, 28 parts of silk fiber, 8 parts of barium metaborate, 6 parts of zirconium sulfate are placed in ball mill and carried out
Ball-milling treatment, the ratio of grinding media to material of ball mill is 15:1, drum's speed of rotation 275r/min, Ball-milling Time 85min obtain ball milling and mix
Close object；
(2) by 5 parts of amino silane, 5 parts of epoxy propane butyl ether, the mixing of 55 parts of absolute ethyl alcohol, in magnetic stirrer with
The rotating speed stirring 150min of 375r/min, is then dried in an oven, and drying temperature is 55 DEG C, obtains stirring mixture；
(3) the stirring mixture that the ball-milled mixtures for obtaining step (1) are obtained with step (2) puts into reaction kettle jointly
In, 4 parts of moon calcium silicates, 4 parts of sulfenamide are then added in, then heats reaction kettle, reaction temperature is made to be promoted to 115 DEG C, is kept
The mixing speed of reaction kettle is 1250r/min, persistently stirs 60min, obtains thermal reaction mixture；
(4) thermal reaction mixture for obtaining step (3) is sent into double screw extruder, the screw speed of double screw extruder
For 230r/min, each area's temperature is：One 185 DEG C of area's temperature, two 215 DEG C of area's temperature, three 210 DEG C of area's temperature, four area's temperature 190
DEG C, product is squeezed out using double screw extruder, plastotype, last drying obtains the textile material of finished product addition amino silane.
The performance test results of textile material obtained are as shown in table 1.
Comparative example 2
(1) 34 parts of polypropylene fiber, 28 parts of silk fiber, 8 parts of barium metaborate, 6 parts of zirconium sulfate are placed in ball mill and carried out
Ball-milling treatment, the ratio of grinding media to material of ball mill is 15:1, drum's speed of rotation 275r/min, Ball-milling Time 85min obtain ball milling and mix
Close object；
(2) 8 parts of dimethyl double hexadecyl ammonium chloride, 5 parts of epoxy propane butyl ether, 55 parts of absolute ethyl alcohol are mixed,
150min is stirred with the rotating speed of 375r/min in magnetic stirrer, is then dried in an oven, drying temperature is 55 DEG C, is stirred
Mix mixture；
(3) the stirring mixture that the ball-milled mixtures for obtaining step (1) are obtained with step (2) puts into reaction kettle jointly
In, 4 parts of moon calcium silicates, 4 parts of sulfenamide are then added in, then heats reaction kettle, reaction temperature is made to be promoted to 115 DEG C, is kept
The mixing speed of reaction kettle is 1250r/min, persistently stirs 60min, obtains thermal reaction mixture；
(4) thermal reaction mixture for obtaining step (3) is sent into double screw extruder, the screw speed of double screw extruder
For 230r/min, each area's temperature is：One 185 DEG C of area's temperature, two 215 DEG C of area's temperature, three 210 DEG C of area's temperature, four area's temperature 190
DEG C, product is squeezed out using double screw extruder, plastotype, last drying obtains the textile material of finished product addition amino silane.
The performance test results of textile material obtained are as shown in table 1.
Comparative example 3
(1) 34 parts of polypropylene fiber, 28 parts of silk fiber, 8 parts of barium metaborate, 6 parts of zirconium sulfate are placed in ball mill and carried out
Ball-milling treatment, the ratio of grinding media to material of ball mill is 15:1, drum's speed of rotation 275r/min, Ball-milling Time 85min obtain ball milling and mix
Close object；
(2) it by 55 parts of 8 parts of dimethyl double hexadecyl ammonium chloride, 5 parts of amino silane, absolute ethyl alcohol mixing, is stirred in magnetic force
It mixes in machine and 150min is stirred with the rotating speed of 375r/min, then dry in an oven, drying temperature is 55 DEG C, is stirred
Object；
(3) the stirring mixture that the ball-milled mixtures for obtaining step (1) are obtained with step (2) puts into reaction kettle jointly
In, 4 parts of moon calcium silicates, 4 parts of sulfenamide are then added in, then heats reaction kettle, reaction temperature is made to be promoted to 115 DEG C, is kept
The mixing speed of reaction kettle is 1250r/min, persistently stirs 60min, obtains thermal reaction mixture；
(4) thermal reaction mixture for obtaining step (3) is sent into double screw extruder, the screw speed of double screw extruder
For 230r/min, each area's temperature is：One 185 DEG C of area's temperature, two 215 DEG C of area's temperature, three 210 DEG C of area's temperature, four area's temperature 190
DEG C, product is squeezed out using double screw extruder, plastotype, last drying obtains the textile material of finished product addition amino silane.
The performance test results of textile material obtained are as shown in table 1.
The textile material obtained of embodiment 1-3 and comparative example 1-3 is subjected to the tensile strength, coefficient of kinetic friction, resistance to respectively
Contamination grade (GB/T30159.1-2013) this several performance tests.
Table 1
| Tensile strength (MPa) | The coefficient of kinetic friction | Stain resistance (grade) | |
| Embodiment 1 | 196 | 0.1086 | 5 |
| Embodiment 2 | 203 | 0.1035 | 5 |
| Embodiment 3 | 201 | 0.1064 | 5 |
| Comparative example 1 | 188 | 0.1233 | 4 |
| Comparative example 2 | 183 | 0.1259 | 4 |
| Comparative example 3 | 185 | 0.1237 | 4 |
The preparation process of the textile material of the addition amino silane of the present invention is used polypropylene fiber, silk fiber, inclined boron
Ball-milled mixtures are made by ball-milling treatment in sour barium, zirconium sulfate, then by dimethyl double hexadecyl ammonium chloride, amino silane, ring
Drying obtains stirring mixture after Ethylene Oxide butyl ether, absolute ethyl alcohol are mixed, and the two is then put into reaction kettle jointly
In, high-temperature stirring after stabilizer, adhesive is added in, thermal reaction mixture is obtained, thermal reaction mixture is finally sent into twin-screw
Extruder squeezes out product, plastotype, and last drying obtains the textile material of finished product addition amino silane.What is be prepared adds
The textile material of base silane is ammoniated, intensity is high, wear-resisting, stain resistant, has a good application prospect in household textiles.And
And present invention employs by dimethyl double hexadecyl ammonium chloride, amino silane, epoxy propane butyl ether these types raw material and nothing
Drying obtains stirring mixture after water-ethanol is mixed, and stirring mixture is then carried out heat jointly with ball-milled mixtures
Reaction, effective performance boost has been carried out to textile material, although these materials be not first Application in textile material, press
After being combined according to certain proportional quantity, it is aided with corresponding processing mode, to the textile material of addition amino silane being finally prepared
Increasing substantially in performance is brought, this is never to report in previous research, for realizing the present invention's
Technique effect plays the role of conclusive.
The foregoing is merely the embodiment of the present invention, are not intended to limit the scope of the invention, every to utilize this hair
The equivalent structure or equivalent flow shift that bright description is made directly or indirectly is used in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (6)
1. a kind of preparation process for the textile material for adding amino silane, which is characterized in that include the following steps：
(1) 32-36 parts of polypropylene fiber, 27-29 parts of silk fiber, 6-10 parts of barium metaborate, 5-7 parts of zirconium sulfate are placed in ball mill
Middle carry out ball-milling treatment, obtains ball-milled mixtures；
(2) by 7-9 parts of dimethyl double hexadecyl ammonium chloride, 4-6 parts of amino silane, 4-6 parts of epoxy propane butyl ether, anhydrous second
50-60 parts of mixing of alcohol, stir 150min with the rotating speed of 350-400r/min in magnetic stirrer, then dry in an oven,
Drying temperature is 50-60 DEG C, obtains stirring mixture；
(3) the stirring mixture that the ball-milled mixtures for obtaining step (1) are obtained with step (2) is put into reaction kettle jointly, with
3-5 parts of stabilizer, 3-5 parts of adhesive are added in afterwards, then heats reaction kettle, reaction temperature is made to be promoted to 110-120 DEG C, keep anti-
The mixing speed for answering kettle is 1200-1300r/min, persistently stirs 60min, obtains thermal reaction mixture；
(4) thermal reaction mixture for obtaining step (3) is sent into double screw extruder, product is squeezed out, plastotype, last drying
Obtain the textile material of finished product addition amino silane.
2. the preparation process of the textile material of addition amino silane according to claim 1, which is characterized in that the step
(1) ratio of grinding media to material of ball mill is 15 in:1, drum's speed of rotation 250-300r/min, Ball-milling Time 80-90min.
3. the preparation process of the textile material of addition amino silane according to claim 1, which is characterized in that the step
(3) any one of stabilizer in orange osmanthus acid esters, moon calcium silicates, barium naphthanate in.
4. the preparation process of the textile material of addition amino silane according to claim 1, which is characterized in that the step
(3) any one of adhesive in polyacrylate, sulfenamide, chlorine Bezalip Tablets in.
5. the preparation process of the textile material of addition amino silane according to claim 1, which is characterized in that the step
(4) screw speed of double screw extruder is 230r/min in, and each area's temperature is：One 185 DEG C of area's temperature, two 215 DEG C of area's temperature,
Three 210 DEG C of area's temperature, four 190 DEG C of area's temperature.
6. the textile material of the addition amino silane according to obtained by claim 1-5 any one of them preparation processes is in household
Application in textile.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111871071A (en) * | 2020-06-17 | 2020-11-03 | 吉祥三宝高科纺织有限公司 | High-temperature-resistant and corrosion-resistant microporous membrane material for processing mask filter layer |
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