CN108192416A - A kind of silk-screen fission ink and preparation method thereof - Google Patents
A kind of silk-screen fission ink and preparation method thereof Download PDFInfo
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- CN108192416A CN108192416A CN201810202627.3A CN201810202627A CN108192416A CN 108192416 A CN108192416 A CN 108192416A CN 201810202627 A CN201810202627 A CN 201810202627A CN 108192416 A CN108192416 A CN 108192416A
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- silk
- screen
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- diacrylate
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/101—Inks specially adapted for printing processes involving curing by wave energy or particle radiation, e.g. with UV-curing following the printing
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of silk-screen fission ink, it is characterized in that, its formula includes following components, respectively epoxy modification acrylate, urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein the mass ratio of above-mentioned each component is epoxy modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:Amine aided initiating:Antifoaming agent=(10‑20):(30‑50):(20‑40):(3‑10):(10‑20):(0.5‑2).The ink is imprinted on stock surface using silk-screen printing technique means, after special condition curing, printing can generate a kind of solid, uniformly the high-grade exquisite article packaging such as the visual effect as skin lines, extensive utilization to Yan Bao, wine packet.
Description
Technical field
The present invention relates to ink areas, and in particular to a kind of silk-screen fission ink and preparation method thereof.
Background technology
With the development and improvement of living standard of commodity economy, people drill printing to packaging dress and propose higher want
It asks.Since lithographic plate, intaglio plate, letterpress have the limitation of its own, and silk-screen printing is with layer of ink is thick, coining is small, the space of a whole page is soft
Soft, the features such as printable fabric is extensive, has played advantage in top grade packs product.Especially in recent years in cigarette, wine gift wrap
In employ etching, frost flower, refractive power (radium-shine) screen printing method, have qualitative leap, feature compared with traditional printing packaging
It is beautiful in colour, luxurious, elegant, is the perfect package method of high-grade famous-brand and high-quality goods.At present, pseud metal-etching, frost flower texture, folding
The wire marks series package box such as light (radium-shine) market is had an optimistic view of, and is still expanding.Simultaneously, because the exploitation of fabrography and equipment and materials and
It introduces, if some domestic wire mark producers can utilize new technology development new product, wire mark technology of the package is made to be gradually improved, exquisite net
Print is packaged to be the accreditation of consumer, and it is also undisputed that more packaging markets are captured in silk-screen printing.
With constantly popularizing for imitative metal wire mark packing box, the novel ink and fabrography of a kind of grain effect of fissioning are again
It has been pushed to market.Such UV silk-screens fission ink is special imitative metal ink, using silk-screen printing technique means by ink
Stock surface is imprinted on, after special condition curing, printing can generate a kind of solid, uniformly as skin lines
Visual effect, the high-grade exquisite article packaging such as extensive utilization to Yan Bao, wine packet.
Invention content
The purpose of the present invention is to provide a kind of completely new silk-screen fission ink and preparation method thereof, to split in printing
Become effect more to enrich, increase the three-dimensional sense of printing.
To achieve the above object, the present invention provides following technical solution:
A kind of silk-screen is fissioned ink, which is characterized in that it, which is formulated, includes following components, respectively epoxy modification acrylate, gather
Urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein above-mentioned each group
The mass ratio divided is epoxy modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:
Amine aided initiating:Antifoaming agent=(10-20):(30-50):(20-40):(3-10):(10-20):(0.5-2).
Silk-screen fission ink according to an embodiment of the invention can be further arranged to epoxy-modified acrylic acid in formula
Ester, urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent each component
Mass ratio is 16:36:27:6:14:1.
Silk-screen fission ink according to an embodiment of the invention can be further arranged to epoxy-modified acrylic acid in formula
Ester, urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent each component
Mass ratio is 20:44:32:8:16:1.2.
Silk-screen fission ink according to an embodiment of the invention can be further arranged to epoxy-modified acrylic acid in formula
Ester, urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent each component
Mass ratio is 13:35:25:5:13:0.9.
According to preparation method of the another object of the present invention for silk-screen fission ink, which is characterized in that include the following steps:
S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure
Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1200-1800 revs/min, stirred tank cylinder temperature rises, highest
Temperature must not be higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;
S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears
Infusion, wherein the rotating speed of the dispersion machine is controlled at 500-700 revs/min, the time of dispersion should be controlled at 15-20 minutes;
S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process
Aided initiating, wherein the rotating speed control of the dispersion machine, at 400-600 revs/min, the time of dispersion should be controlled at 25-40 points
Clock;
S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
The preparation method of silk-screen fission ink according to an embodiment of the invention can be further arranged in S1 steps
The rotating speed of blender is controlled at 1500 revs/min.
The preparation method of silk-screen fission ink according to an embodiment of the invention can be further arranged in S2 steps
The rotating speed of the dispersion machine is controlled at 700 revs/min, and the time of dispersion should be controlled at 15 minutes.
The preparation method of silk-screen fission ink according to an embodiment of the invention can be further arranged in S3 steps
The rotating speed of the dispersion machine is controlled at 500 revs/min, and the time of dispersion should be controlled at 30 minutes.
Compared with prior art, beneficial effects of the present invention are as follows:
The principle of the silk-screen fission ink of the present invention is that UV wet films have certain thickness, ultraviolet wavelength more in short-term, organic
Penetrability in film is poorer, and low pressure mercury lamp mainly emits 254nm light, is just absorbed totally, can not be worn in moisture membrane surface substantially
Black bottom is arrived thoroughly, and curing certainly only occurs in film surface layer, surface layer cure shrinkage, and entire layer of ink shrinks uneven, generation fission effect
Fruit, then radiated with conventional UV lamp(Based on wavelength 365nm), long wave UV is worn to film bottom, thorough to cure, and is consolidated by above-mentioned condition
After change, printing can generate a kind of solid, uniformly the visual effect as skin lines, extensive utilization to Yan Bao, Jiu Bao
Deng high-grade exquisite article packaging.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical solution in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, those of ordinary skill in the art's all other embodiments obtained without making creative work, all
Belong to the scope of protection of the invention.
The silk-screen fission ink formulations include following components, respectively epoxy modification acrylate, urethane acrylate,
Tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein the mass ratio of above-mentioned each component is
Epoxy modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:Amine aided initiating:
Antifoaming agent=(10-20):(30-50):(20-40):(3-10):(10-20):(0.5-2).
The preparation method of silk-screen fission ink includes the following steps:
S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure
Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1200-1800 revs/min, stirred tank cylinder temperature rises, highest
Temperature must not be higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;
S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears
Infusion, wherein the rotating speed of the dispersion machine is controlled at 500-700 revs/min, the time of dispersion should be controlled at 15-20 minutes;
S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process
Aided initiating, wherein the rotating speed control of the dispersion machine, at 400-600 revs/min, the time of dispersion should be controlled at 25-40 points
Clock;
S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
During silk-screen fission ink is used, using cured in stages twice, first consolidated using low pressure mercury lamp
Change, then cured using the radiation of conventional UV lamp.Wherein low pressure mercury lamp transmitting 254nm light, and the radiation of conventional UV lamp then with
Based on wavelength 365nm.
Embodiment 1
Silk-screen fission ink formulations include following components, respectively epoxy modification acrylate, urethane acrylate, two contractings
Tripropylene glycol diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein the mass ratio of above-mentioned each component is epoxy
Modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:Amine aided initiating:Defoaming
Agent=16:36:27:6:14:1.
The preparation method of silk-screen fission ink includes the following steps:
S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure
Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1500 revs/min, stirred tank cylinder temperature rises, and the highest temperature is not
It obtains higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;
S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears
Infusion, wherein the rotating speed of the dispersion machine is controlled at 700 revs/min, the time of dispersion should be controlled at 15 minutes;
S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process
Aided initiating, wherein the rotating speed of the dispersion machine is controlled at 500 revs/min, the time of dispersion should be controlled at 30 minutes;
S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
Embodiment 2
Silk-screen fission ink formulations include following components, respectively epoxy modification acrylate, urethane acrylate, two contractings
Tripropylene glycol diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein the mass ratio of above-mentioned each component is epoxy
Modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:Amine aided initiating:Defoaming
Agent=20:44:32:8:16:1.2.
The preparation method of silk-screen fission ink includes the following steps:
S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure
Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1200-1800 revs/min, stirred tank cylinder temperature rises, highest
Temperature must not be higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;
S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears
Infusion, wherein the rotating speed of the dispersion machine is controlled at 650 revs/min, the time of dispersion should be controlled at 18 minutes;
S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process
Aided initiating, wherein the rotating speed of the dispersion machine is controlled at 600 revs/min, the time of dispersion should be controlled at 20 minutes;
S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
Embodiment 3
Silk-screen fission ink formulations include following components, respectively epoxy modification acrylate, urethane acrylate, two contractings
Tripropylene glycol diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein the mass ratio of above-mentioned each component is epoxy
Modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:Amine aided initiating:Defoaming
Agent=13:35:25:5:13:0.9.
The preparation method of silk-screen fission ink includes the following steps:
S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure
Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1200-1800 revs/min, stirred tank cylinder temperature rises, highest
Temperature must not be higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;
S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears
Infusion, wherein the rotating speed of the dispersion machine is controlled at 700 revs/min, the time of dispersion should be controlled at 15 minutes;
S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process
Aided initiating, wherein the rotating speed of the dispersion machine is controlled at 400 revs/min, the time of dispersion should be controlled at 40 minutes;
S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
Embodiment 4
Silk-screen fission ink formulations include following components, respectively epoxy modification acrylate, urethane acrylate, two contractings
Tripropylene glycol diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein the mass ratio of above-mentioned each component is epoxy
Modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:Amine aided initiating:Defoaming
Agent=10:30:20:3:10:0.5.
The preparation method of silk-screen fission ink includes the following steps:
S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure
Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1600 revs/min, stirred tank cylinder temperature rises, and the highest temperature is not
It obtains higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;
S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears
Infusion, wherein the rotating speed of the dispersion machine is controlled at 600 revs/min, the time of dispersion should be controlled at 18 minutes;
S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process
Aided initiating, wherein the rotating speed of the dispersion machine is controlled at 500 revs/min, the time of dispersion should be controlled at 30 minutes;
S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
Embodiment 5
Silk-screen fission ink formulations include following components, respectively epoxy modification acrylate, urethane acrylate, two contractings
Tripropylene glycol diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein the mass ratio of above-mentioned each component is epoxy
Modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:Amine aided initiating:Defoaming
Agent=20:50:40:10:20:2.
The preparation method of silk-screen fission ink includes the following steps:
S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure
Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1600 revs/min, stirred tank cylinder temperature rises, and the highest temperature is not
It obtains higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;
S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears
Infusion, wherein the rotating speed of the dispersion machine is controlled at 600 revs/min, the time of dispersion should be controlled at 20 minutes;
S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process
Aided initiating, wherein the rotating speed of the dispersion machine is controlled at 450 revs/min, the time of dispersion should be controlled at 35 minutes;
S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
Embodiment 6
Silk-screen fission ink formulations include following components, respectively epoxy modification acrylate, urethane acrylate, two contractings
Tripropylene glycol diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein the mass ratio of above-mentioned each component is epoxy
Modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:Photoinitiator:Amine aided initiating:Defoaming
Agent=20:45:27:9:16:1.5.
The preparation method of silk-screen fission ink includes the following steps:
S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure
Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1800 revs/min, stirred tank cylinder temperature rises, and the highest temperature is not
It obtains higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;
S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears
Infusion, wherein the rotating speed of the dispersion machine is controlled at 700 revs/min, the time of dispersion should be controlled at 15 minutes;
S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process
Aided initiating, wherein the rotating speed of the dispersion machine is controlled at 500 revs/min, the time of dispersion should be controlled at 40 minutes;
S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
The silk-screen fission ink prepared according to embodiment 1-6 formulas and technique is carried out, using test, utilizing silk-screen printing
Ink is imprinted on stock surface by process means, and passes through special curing process, it is found that embodiment 1 is formulated and is prepared by technique
Ink generates fission best results after curing process, and three-dimensional sense is most strong, while abrasion resistant effect is best.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (8)
- The ink 1. a kind of silk-screen is fissioned, which is characterized in that it, which is formulated, includes following components, respectively epoxy modification acrylate, Urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent, wherein above-mentioned each The mass ratio of component is epoxy modification acrylate:Urethane acrylate:Tri (propylene glycol) diacrylate:It is light-initiated Agent:Amine aided initiating:Antifoaming agent=(10-20):(30-50):(20-40):(3-10):(10-20):(0.5-2).
- 2. a kind of silk-screen fission ink according to claim 1, which is characterized in that epoxy modification acrylate in formula, Urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent each component matter Amount is than being 16:36:27:6:14:1.
- 3. a kind of silk-screen fission ink according to claim 1, which is characterized in that epoxy modification acrylate in formula, Urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent each component matter Amount is than being 20:44:32:8:16:1.2.
- 4. a kind of silk-screen fission ink according to claim 1, which is characterized in that epoxy modification acrylate in formula, Urethane acrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, antifoaming agent each component matter Amount is than being 13:35:25:5:13:0.9.
- 5. a kind of silk-screen fission ink according to any one of claims 1-4, which is characterized in that preparation method includes Following steps:S1, tri (propylene glycol) diacrylate, epoxy modification acrylate and light are drawn according to recipe ratio under room temperature, normal pressure Hair agent is previously added stirred tank and is stirred, and improves rotating speed to 1200-1800 revs/min, stirred tank cylinder temperature rises, highest Temperature must not be higher than 60 DEG C, up to stirring and dissolving to transparent grainless state;S2, the mixed liquor that S1 is obtained is placed in dispersion machine, and adds in dispersion process the urethane acrylate of recipe ratio, disappears Infusion, wherein the rotating speed of the dispersion machine is controlled at 500-700 revs/min, the time of dispersion should be controlled at 15-20 minutes;S3, continued to be dispersed in the mixed liquor obtained in S2 steps with dispersion machine, and the amine of recipe ratio is added in dispersion process Aided initiating, wherein the rotating speed control of the dispersion machine, at 400-600 revs/min, the time of dispersion should be controlled at 25-40 points Clock;S4, the mixed liquor obtained in S3 steps is filtered, packaging just obtains finished product.
- A kind of 6. silk-screen fission ink according to claim 5, which is characterized in that silk-screen fission ink preparation method S1 steps The rotating speed of blender is controlled at 1500 revs/min in rapid.
- A kind of 7. silk-screen fission ink according to claim 6, which is characterized in that silk-screen fission ink preparation method S2 steps The rotating speed of dispersion machine described in rapid is controlled at 700 revs/min, and the time of dispersion should be controlled at 15 minutes.
- A kind of 8. silk-screen fission ink according to claim 7, which is characterized in that silk-screen fission ink preparation method S3 steps The rotating speed of dispersion machine described in rapid is controlled at 500 revs/min, and the time of dispersion should be controlled at 30 minutes.
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CN201810202627.3A CN108192416A (en) | 2018-03-13 | 2018-03-13 | A kind of silk-screen fission ink and preparation method thereof |
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CN109608934A (en) * | 2019-01-29 | 2019-04-12 | 浙江银鹿新材料有限公司 | A kind of ultraviolet light solidification silk-screen fission ink |
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