CN108165086A - A kind of gravure snowflake printing ink and preparation method thereof - Google Patents
A kind of gravure snowflake printing ink and preparation method thereof Download PDFInfo
- Publication number
- CN108165086A CN108165086A CN201810110149.3A CN201810110149A CN108165086A CN 108165086 A CN108165086 A CN 108165086A CN 201810110149 A CN201810110149 A CN 201810110149A CN 108165086 A CN108165086 A CN 108165086A
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- China
- Prior art keywords
- gravure
- diacrylate
- printing ink
- dispersion
- photoinitiator
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/101—Inks specially adapted for printing processes involving curing by wave energy or particle radiation, e.g. with UV-curing following the printing
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/103—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds of aldehydes, e.g. phenol-formaldehyde resins
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Epoxy Resins (AREA)
Abstract
The invention discloses a kind of gravure snowflake printing inks, it is characterized in that, its formula includes epoxy modification acrylate, aldehyde ketone resin liquid, 1,6 hexanediyl esters, tri (propylene glycol) diacrylate and photoinitiator, amine aided initiating, levelling agent, antifoaming agent, wherein epoxy modification acrylate, aldehyde ketone resin liquid, 1,6 hexanediyl esters, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, levelling agent, antifoaming agent mass ratio be（5‑15）：（30‑40）：（10‑20）：（10‑20）：（5‑15）：（10‑18）：（0.5‑2）：（0.5‑2）.The ink, which passes through, adjusts internal formula, reasonable preparation auxiliary agent so that rocketing by ignition cures the texture for showing the glittering and translucent texture as winter snowflake and greatly enhance, while enhance the solar heat protection of ink, moisture-proof ability.
Description
Technical field
The present invention relates to ink areas, and in particular to a kind of gravure snowflake printing ink and preparation method thereof.
Background technology
Ultraviolet light curing gravure snowflake printing is a kind of special process of printed matter surface processing, can be in the color printing of printed matter
The figure line of transparent stereo is generated on pattern, makes the novel high-grade decoration result of printed patterns performance.Ultraviolet light cures silk-screen snowflake
Ink is first printed on the patterned surfaces of printed matter by printing machine by ink, shows winter snowflake using the ignition curing that rockets
As glittering and translucent texture texture process, be crystallization, fission type special process ink.
Invention content
The purpose of the present invention is to provide a kind of completely new gravure snowflake printing inks and preparation method thereof, rocket to improve ignition
Curing shows the texture of the glittering and translucent texture as winter snowflake.
To achieve the above object, the present invention provides following technical solution：
A kind of gravure snowflake printing ink, which is characterized in that its be formulated include epoxy modification acrylate, aldehyde ketone resin liquid, 1,6- oneself
Omega-diol diacrylate, tri (propylene glycol) diacrylate and photoinitiator, amine aided initiating, levelling agent, antifoaming agent,
Wherein epoxy modification acrylate, aldehyde ketone resin liquid, 1,6 hexanediol diacrylate, tri (propylene glycol) diacrylate,
Photoinitiator, amine aided initiating, levelling agent, antifoaming agent mass ratio be（5-15）：（30-40）：（10-20）：（10-20）：
（5-15）：（10-18）：（0.5-2）：（0.5-2）.
Gravure snowflake printing ink according to an embodiment of the invention can be further arranged to epoxy modification acrylate, aldehyde ketone
Resin liquid, 1,6 hexanediol diacrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, levelling
Agent, antifoaming agent mass ratio be 10：34：16：16：10：12：1：1.
Epoxy modification acrylate, aldehyde can be further arranged to according to the gravure snowflake printing ink of another embodiment of the invention
Ketone resin liquid, 1,6 hexanediol diacrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, stream
Flat agent, antifoaming agent mass ratio be 8：32：16：16：12：12：1：1.
Epoxy modification acrylate, aldehyde can be further arranged to according to the gravure snowflake printing ink of another embodiment of the invention
Ketone resin liquid, 1,6 hexanediol diacrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, stream
Flat agent, antifoaming agent mass ratio be 12：38：18：20：15：15：1.5：1.5.
According to the preparation method that another object of the present invention is gravure snowflake printing ink, which is characterized in that include the following steps：
S1, under room temperature, normal pressure according to the 1,6 hexanediol diacrylate of recipe ratio, tri (propylene glycol) diacrylate,
Epoxy modification acrylate and photoinitiator are previously added stirred tank and are stirred, and improve rotating speed to 1400-1600 revs/min,
Up to stirring and dissolving to transparent grainless state；
S2, the mixed liquor obtained in S1 steps is placed in dispersion machine, the aldehyde ketone resin liquid of recipe ratio is added in dispersion process, is disappeared
At 500-700 revs/min, the time of dispersion should be controlled at 15-20 points for the rotating speed control of infusion, levelling agent agent, while dispersion machine
Clock；
S3, the mixed liquor obtained in S2 steps is placed in dispersion machine and continues to disperse, and recipe ratio is added in dispersion process
Amine aided initiating, at 500-800 revs/min, the time of dispersion should be controlled at 20-30 points for the rotating speed control of the dispersion machine
Clock.
S4, the mixed liquor obtained in S2 steps is filtered, packaging just obtains finished product.
The preparation method of gravure snowflake printing ink according to an embodiment of the invention can be further arranged in S1 steps
The rotating speed of blender is controlled at 1500 revs/min, and stirred tank cylinder temperature rises, and the highest temperature must not be higher than 60 DEG C.
The preparation method of gravure snowflake printing ink according to an embodiment of the invention can be further arranged in S2 steps
The rotating speed of dispersion machine is controlled at 700 revs/min, and the time of dispersion should be controlled at 15 minutes.
The preparation method of gravure snowflake printing ink according to an embodiment of the invention can be further arranged in S3 steps
The rotating speed of dispersion machine is controlled at 500 revs/min, and the time of dispersion should be controlled at 30 minutes.
Compared with prior art, beneficial effects of the present invention are as follows：
The gravure snowflake printing ink of the present invention be particle in UV solidification process, ink due to contact or close proximity, cause phase
Mutually attract, quickly to entity intermediate aggregate, a kind of texture of exquisiteness is formed on layer of ink surface, similar to the dot of protrusion.The oil
Ink, which passes through, adjusts internal formula, reasonable preparation auxiliary agent so that rocket by ignition cure show it is sparkling and crystal-clear as winter snowflake
The texture of exquisitely carved texture greatly enhances, while enhances the solar heat protection of ink, moisture-proof ability.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical solution in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, those of ordinary skill in the art's all other embodiments obtained without making creative work, all
Belong to the scope of protection of the invention.
The formula of the gravure snowflake printing ink includes epoxy modification acrylate, aldehyde ketone resin liquid, two propylene of 1,6-HD
Acid esters, tri (propylene glycol) diacrylate and photoinitiator, amine aided initiating, levelling agent, antifoaming agent, wherein epoxy change
Property acrylate, aldehyde ketone resin liquid, 1,6 hexanediol diacrylate, tri (propylene glycol) diacrylate, photoinitiator, amine
Class aided initiating, levelling agent, antifoaming agent mass ratio be（5-15）：（30-40）：（10-20）：（10-20）：（5-15）：（10-
18）：（0.5-2）：（0.5-2）.
By optimizing its formula, the preparation method of gravure snowflake printing ink is adjusted, substantially reduces the complexity of its preparation, is adjusted
Whole preparation method includes the following steps：
S1, under room temperature, normal pressure according to the 1,6 hexanediol diacrylate of recipe ratio, tri (propylene glycol) diacrylate,
Epoxy modification acrylate and photoinitiator are previously added stirred tank and are stirred, and improve rotating speed to 1400-1600 revs/min,
Up to stirring and dissolving to transparent grainless state；
S2, the mixed liquor obtained in S1 steps is placed in dispersion machine, the aldehyde ketone resin liquid of recipe ratio is added in dispersion process, is disappeared
At 500-700 revs/min, the time of dispersion should be controlled at 15-20 points for the rotating speed control of infusion, levelling agent agent, while dispersion machine
Clock；
S3, the mixed liquor obtained in S2 steps is placed in dispersion machine and continues to disperse, and recipe ratio is added in dispersion process
Amine aided initiating, at 500-800 revs/min, the time of dispersion should be controlled at 20-30 points for the rotating speed control of the dispersion machine
Clock.
S4, the mixed liquor obtained in S2 steps is filtered, packaging just obtains finished product.
Embodiment 1
The formula of the gravure snowflake printing ink include epoxy modification acrylate, aldehyde ketone resin liquid, 1,6 hexanediol diacrylate,
Tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, levelling agent, antifoaming agent, the mass ratio of above-mentioned each component
It is 10：34：16：16：10：12：1：1.
Corresponding preparation method includes the following steps：
S1, under room temperature, normal pressure according to the 1,6 hexanediol diacrylate of recipe ratio, tri (propylene glycol) diacrylate,
Epoxy modification acrylate and photoinitiator are previously added stirred tank and are stirred, and improve rotating speed to 1500 revs/min, and stir
Kettle cylinder temperature rises, and the highest temperature must not be higher than 60 DEG C, up to stirring and dissolving to transparent grainless state；
S2, the mixed liquor obtained in S1 steps is placed in dispersion machine, the aldehyde ketone resin liquid of recipe ratio is added in dispersion process, is disappeared
The rotating speed of infusion, levelling agent agent, while dispersion machine is controlled at 500 revs/min, and the time of dispersion should be controlled at 20 minutes；
S3, the mixed liquor obtained in S2 steps is placed in dispersion machine and continues to disperse, and recipe ratio is added in dispersion process
Amine aided initiating, the rotating speed of the dispersion machine are controlled at 800 revs/min, and the time of dispersion should be controlled at 20 minutes.
S4, the mixed liquor obtained in S2 steps is filtered, packaging just obtains finished product.
Embodiment 2
The formula of the gravure snowflake printing ink include epoxy modification acrylate, aldehyde ketone resin liquid, 1,6 hexanediol diacrylate,
Tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, levelling agent, antifoaming agent, the mass ratio of above-mentioned each component
It is 8：32：16：16：12：12：1：1.
Corresponding preparation method includes the following steps：
S1, under room temperature, normal pressure according to the 1,6 hexanediol diacrylate of recipe ratio, tri (propylene glycol) diacrylate,
Epoxy modification acrylate and photoinitiator are previously added stirred tank and are stirred, and improve rotating speed to 1500 revs/min, and stir
Kettle cylinder temperature rises, and the highest temperature must not be higher than 60 DEG C, up to stirring and dissolving to transparent grainless state；
S2, the mixed liquor obtained in S1 steps is placed in dispersion machine, the aldehyde ketone resin liquid of recipe ratio is added in dispersion process, is disappeared
At 500-700 revs/min, the time of dispersion should be controlled at 15-20 points for the rotating speed control of infusion, levelling agent agent, while dispersion machine
Clock；
S3, the mixed liquor obtained in S2 steps is placed in dispersion machine and continues to disperse, and recipe ratio is added in dispersion process
Amine aided initiating, at 500-800 revs/min, the time of dispersion should be controlled at 20-30 points for the rotating speed control of the dispersion machine
Clock.
S4, the mixed liquor obtained in S2 steps is filtered, packaging just obtains finished product.
Embodiment 3
The formula of the gravure snowflake printing ink include epoxy modification acrylate, aldehyde ketone resin liquid, 1,6 hexanediol diacrylate,
Tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, levelling agent, antifoaming agent, the mass ratio of above-mentioned each component
It is 12：38：18：20：15：15：1.5：1.5.
Corresponding preparation method includes the following steps：
S1, under room temperature, normal pressure according to the 1,6 hexanediol diacrylate of recipe ratio, tri (propylene glycol) diacrylate,
Epoxy modification acrylate and photoinitiator are previously added stirred tank and are stirred, and improve rotating speed to 1400 revs/min, and stir
Kettle cylinder temperature rises, and the highest temperature must not be higher than 60 DEG C, up to stirring and dissolving to transparent grainless state；
S2, the mixed liquor obtained in S1 steps is placed in dispersion machine, the aldehyde ketone resin liquid of recipe ratio is added in dispersion process, is disappeared
The rotating speed of infusion, levelling agent agent, while dispersion machine is controlled at 700 revs/min, and the time of dispersion should be controlled at 15 minutes；
S3, the mixed liquor obtained in S2 steps is placed in dispersion machine and continues to disperse, and recipe ratio is added in dispersion process
Amine aided initiating, the rotating speed of the dispersion machine are controlled at 500 revs/min, and the time of dispersion should be controlled at 30 minutes.
S4, the mixed liquor obtained in S2 steps is filtered, packaging just obtains finished product.
The gravure snowflake printing ink of above-described embodiment 1-3 is tested, wherein glittering and translucent texture in the snowflake of embodiment 1
Texture is best, which can be used as high-grade cigarette outer case to print ink and use.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (8)
1. a kind of gravure snowflake printing ink, which is characterized in that its formula includes epoxy modification acrylate, aldehyde ketone resin liquid, 1,6-
Hexanediyl ester, tri (propylene glycol) diacrylate and photoinitiator, amine aided initiating, levelling agent, defoaming
Agent, wherein epoxy modification acrylate, aldehyde ketone resin liquid, 1,6- hexanediyl esters, tripropylene glycol diacrylate
Ester, photoinitiator, amine aided initiating, levelling agent, antifoaming agent mass ratio be（5-15）：（30-40）：（10-20）：（10-
20）：（5-15）：（10-18）：（0.5-2）：（0.5-2）.
2. a kind of gravure snowflake printing ink according to claim 1, which is characterized in that epoxy modification acrylate, aldehyde ketone tree
Fat liquid, 1,6 hexanediol diacrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, levelling
Agent, antifoaming agent mass ratio be 10：34：16：16：10：12：1：1.
3. a kind of gravure snowflake printing ink according to claim 1, which is characterized in that epoxy modification acrylate, aldehyde ketone tree
Fat liquid, 1,6 hexanediol diacrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, levelling
Agent, antifoaming agent mass ratio be 8：32：16：16：12：12：1：1.
4. a kind of gravure snowflake printing ink according to claim 1, which is characterized in that epoxy modification acrylate, aldehyde ketone tree
Fat liquid, 1,6 hexanediol diacrylate, tri (propylene glycol) diacrylate, photoinitiator, amine aided initiating, levelling
Agent, antifoaming agent mass ratio be 12：38：18：20：15：15：1.5：1.5.
A kind of 5. gravure snowflake printing ink according to any one of claims 1 to 4, which is characterized in that the gravure snowflake printing ink
Preparation method include the following steps：
S1, under room temperature, normal pressure according to the 1,6 hexanediol diacrylate of recipe ratio, tri (propylene glycol) diacrylate,
Epoxy modification acrylate and photoinitiator are previously added stirred tank and are stirred, and improve rotating speed to 1400-1600 revs/min,
Up to stirring and dissolving to transparent grainless state；
S2, the mixed liquor obtained in S1 steps is placed in dispersion machine, the aldehyde ketone resin liquid of recipe ratio is added in dispersion process, is disappeared
At 500-700 revs/min, the time of dispersion should be controlled at 15-20 points for the rotating speed control of infusion, levelling agent agent, while dispersion machine
Clock；
S3, the mixed liquor obtained in S2 steps is placed in dispersion machine and continues to disperse, and recipe ratio is added in dispersion process
Amine aided initiating, at 500-800 revs/min, the time of dispersion should be controlled at 20-30 points for the rotating speed control of the dispersion machine
Clock.
S4, the mixed liquor obtained in S2 steps is filtered, packaging just obtains finished product.
A kind of 6. gravure snowflake printing ink according to claim 5, which is characterized in that the rotating speed control of blender in S1 steps
System is at 1500 revs/min, and stirred tank cylinder temperature rises, and the highest temperature must not be higher than 60 DEG C.
A kind of 7. gravure snowflake printing ink according to claim 6, which is characterized in that the rotating speed control of dispersion machine in S2 steps
At 700 revs/min, the time of dispersion should control at 15 minutes system.
A kind of 8. gravure snowflake printing ink according to claim 7, which is characterized in that the rotating speed control of dispersion machine in S3 steps
At 500 revs/min, the time of dispersion should control at 30 minutes system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810110149.3A CN108165086A (en) | 2018-02-05 | 2018-02-05 | A kind of gravure snowflake printing ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810110149.3A CN108165086A (en) | 2018-02-05 | 2018-02-05 | A kind of gravure snowflake printing ink and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108165086A true CN108165086A (en) | 2018-06-15 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810110149.3A Pending CN108165086A (en) | 2018-02-05 | 2018-02-05 | A kind of gravure snowflake printing ink and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112094531A (en) * | 2020-08-25 | 2020-12-18 | 浙江美浓材料科技有限公司 | UV offset printing snowflake ink and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1580149A (en) * | 2004-05-17 | 2005-02-16 | 深圳市立美特环保油墨有限公司 | Ultraviolet light curable ink |
| CN102229762A (en) * | 2011-06-09 | 2011-11-02 | 深圳市科彩印务有限公司 | Water-based ultraviolet (UV) curing silk screening snowflake ink |
| CN103395305A (en) * | 2013-06-24 | 2013-11-20 | 贵州劲嘉新型包装材料有限公司 | Rotary wheel gravure method and equipment achieving process simulating silk screen snowflake printing ink effect |
| CN104073057A (en) * | 2014-07-11 | 2014-10-01 | 王景泉 | Waterproof UV snowflake printing ink and preparation method thereof |
-
2018
- 2018-02-05 CN CN201810110149.3A patent/CN108165086A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1580149A (en) * | 2004-05-17 | 2005-02-16 | 深圳市立美特环保油墨有限公司 | Ultraviolet light curable ink |
| CN102229762A (en) * | 2011-06-09 | 2011-11-02 | 深圳市科彩印务有限公司 | Water-based ultraviolet (UV) curing silk screening snowflake ink |
| CN103395305A (en) * | 2013-06-24 | 2013-11-20 | 贵州劲嘉新型包装材料有限公司 | Rotary wheel gravure method and equipment achieving process simulating silk screen snowflake printing ink effect |
| CN104073057A (en) * | 2014-07-11 | 2014-10-01 | 王景泉 | Waterproof UV snowflake printing ink and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112094531A (en) * | 2020-08-25 | 2020-12-18 | 浙江美浓材料科技有限公司 | UV offset printing snowflake ink and preparation method thereof |
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| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180615 |
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