CN108158879A - A kind of no silicone oil shampoo and preparation method thereof - Google Patents
A kind of no silicone oil shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN108158879A CN108158879A CN201711434553.8A CN201711434553A CN108158879A CN 108158879 A CN108158879 A CN 108158879A CN 201711434553 A CN201711434553 A CN 201711434553A CN 108158879 A CN108158879 A CN 108158879A
- Authority
- CN
- China
- Prior art keywords
- silicone oil
- preparation
- oil shampoo
- mixture
- shampoo
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of no silicone oil shampoos and preparation method thereof.This no silicone oil shampoo is made of following raw material：Silver birch extract, Millettia extract, Radix Ampelopsis extract, Echinacea Purpurea Herb P.E, Extracts of Mallotus apelta, amino acid, collagen, citric acid, sodium chloride and water.Also disclose the preparation method of this no silicone oil shampoo.The present invention uses draft not add the additives such as silicone oil for raw material, and add nutrient needed for the epidermises such as amino acid, collagen, so as to which a kind of no silicone oil shampoo be prepared.This no silicone oil shampoo can solve the problems, such as that baby pregnant woman's postpartum washes shield using additive, and have cleaning, oil-control effect well.
Description
Technical field
The present invention relates to a kind of no silicone oil shampoos and preparation method thereof.
Background technology
Silicone oil shampoo is not suitable for oily hair crowd, and oily hair crowd fat secretion is excessive, be easy to cause pore blocks up
Plug.Silicate-containing oil shampoo is used for a long time, silicone oil can gather on hair upper strata, cause hair it is unnatural, it is greasy, thick and heavy, cave in, do
It is withered short-tempered.
No silicone oil shampoo is increasingly becoming the research topic of a hot spot in recent years, excellent with mild, environmental protection, health etc.
The extensive concern by consumer is put, and has been achieved with part successfully business application and popularization.At present, no silicone oil shampoo master
If the surfactant of some smooth dose of silicone oil of substitution is added, such as alkanoyl propylhomoserin salt, alkyl sulfo succinate and alkane
Sulfonylmethyl alanine salt etc..But there are still viscosity is relatively low, foam is insufficient, condiment difference etc. in existing no silicone oil shampoo
Problem needs further to improve.
Invention content
The purpose of the present invention is to provide a kind of no silicone oil shampoos and preparation method thereof.
The technical solution used in the present invention is：
A kind of no silicone oil shampoo, is made of the raw material of following mass percent：
Preferably, a kind of no silicone oil shampoo, is made of the raw material of following mass percent：
Without in silicone oil shampoo, amino acid is glutamic acid, arginine, serine, cystine, glycine, alanine, figured silk fabrics ammonia
Acid, leucine, isoleucine, phenylalanine, tyrosine, tryptophan, proline, threonine, aspartic acid, lysine, group ammonia
At least one of acid, cysteine, methionine, citrulling.
The preparation method of this no silicone oil shampoo, includes the following steps：
1) raw material is weighed by above-mentioned composition；
2) by silver birch extract, Millettia extract, Radix Ampelopsis extract, Echinacea Purpurea Herb P.E, Extracts of Mallotus apelta, ammonia
Base acid, collagen and water are uniformly mixed, and the mixture of gained, which is placed in reaction kettle, to be stirred to react；
3) pH value of mixture is adjusted with citric acid, the viscosity of mixture is adjusted with sodium chloride, filling discharging obtains no silicon
Oil wash floods.
In the step 2) of preparation method, the temperature of reaction is 50 DEG C~70 DEG C, and the reaction time is 1h~3h.
In the step 2) of preparation method, the speed of agitator of reaction kettle is 40r/min~50r/min, and homogeneous rotating speed is
2500r/min~3000r/min.
In the step 3) of preparation method, the pH value for adjusting mixture is 5~7.
In the step 3) of preparation method, the viscosity for adjusting mixture is 4000cP~6000cP at 25 DEG C.
The beneficial effects of the invention are as follows：
The present invention uses draft not add the additives such as silicone oil for raw material, and add the epidermises such as amino acid, collagen
Required nutrient, so as to which a kind of no silicone oil shampoo be prepared.This no silicone oil shampoo can solve baby pregnant woman's production
The problem of washing shield using additive afterwards, and have cleaning, oil-control effect well.
Specific embodiment
A kind of no silicone oil shampoo, is made of the raw material of following mass percent：
Preferably, a kind of no silicone oil shampoo, is made of the raw material of following mass percent：
Preferably, in no silicone oil shampoo, amino acid is glutamic acid, arginine, serine, cystine, glycine, the third ammonia
Acid, leucine, isoleucine, phenylalanine, tyrosine, tryptophan, proline, threonine, aspartic acid, relies ammonia at valine
At least one of acid, histidine, cysteine, methionine, citrulling.
The preparation method of this no silicone oil shampoo, includes the following steps：
1) raw material is weighed by above-mentioned composition；
2) by silver birch extract, Millettia extract, Radix Ampelopsis extract, Echinacea Purpurea Herb P.E, Extracts of Mallotus apelta, ammonia
Base acid, collagen and water are uniformly mixed, and the mixture of gained, which is placed in reaction kettle, to be stirred to react；
3) pH value of mixture is adjusted with citric acid, the viscosity of mixture is adjusted with sodium chloride, filling discharging obtains no silicon
Oil wash floods.
Preferably, in the step 2) of preparation method, the temperature of reaction is 50 DEG C~70 DEG C, and the reaction time is 1h~3h.
Preferably, in the step 2) of preparation method, the speed of agitator of reaction kettle is 40r/min~50r/min, homogeneous rotating speed
For 2500r/min~3000r/min.
Preferably, in the step 3) of preparation method, the pH value for adjusting mixture is 5~7.
Preferably, in the step 3) of preparation method, the viscosity for adjusting mixture is 4000cP~6000cP at 25 DEG C.
Some raw material function and effect used in the present invention are described as follows：
Silver birch extract is white birch leaf and the extract of bark, and the protein in hair fiber can be inhibited molten
Solution restores damaged hair gloss and accelerates natural on-off cycles of hair growth.
Millettia extract, which has, enriches blood, invigorates blood circulation and dredging collateral and other effects.
Alopecia caused by Radix Ampelopsis extract can prevent hormone vigorous promotes natural on-off cycles of hair growth.
The main ingredient of Echinacea Purpurea Herb P.E is Cichoric acid, has the function of antibacterial, strengthen immunity.
Extracts of Mallotus apelta has the function of antipruritic and sterilization.
Present disclosure is described in further detail below by way of specific embodiment, it is former used in embodiment
Material can be obtained from routine business approach.
Embodiment 1：
The shampoo preparation method of embodiment 1 is as follows：
1) radix ampelopsis of the silver birch extract of 8 mass parts, the Millettia extract of 5 mass parts, 0.5 mass parts is extracted
Object, the Echinacea Purpurea Herb P.E of 0.5 mass parts, the Extracts of Mallotus apelta of 0.5 mass parts, 8 mass parts amino acid (including 1.5 matter
Measure part glutamic acid, 0.5 mass parts arginine, 1 mass parts alanine, 1 mass parts leucine, 0.5 mass parts phenylalanine, 1 matter
Measure part tyrosine, 1 mass parts tryptophan, 1 mass parts aspartic acid and 0.5 mass parts methionine), the collagen eggs of 3 mass parts
White and 73 mass parts water are uniformly mixed, and are fed the mixture into shampoo special reactor and are stirred to react 2h for 60 DEG C, wherein instead
The speed of agitator for answering kettle is 50r/min, and homogeneous rotating speed is 2800r/min；
2) pH value of mixture is adjusted with the citric acid of 0.5 mass parts to 6.5, mixing is adjusted with the sodium chloride of 1 mass parts
The viscosity of object is to 5000cP (at 25 DEG C), filling discharging, obtain embodiment 1 without silicone oil shampoo.
Embodiment 2：
The shampoo preparation method of embodiment 2 is as follows：
1) by the silver birch extract of 5 mass parts, the Millettia extract of 8 mass parts, 1 mass parts Radix Ampelopsis extract,
The Echinacea Purpurea Herb P.E of 0.5 mass parts, the Extracts of Mallotus apelta of 0.5 mass parts, the amino acid of 5 mass parts are (smart including 1 mass parts
Propylhomoserin, 0.5 mass parts cystine, 0.5 mass parts valine, 0.5 mass parts isoleucine, 0.5 mass parts phenylalanine, 0.5
Mass parts proline, 0.5 mass parts threonine, 0.5 mass parts histidine, 0.5 mass parts citrulling), the collagen eggs of 4 mass parts
White and 74 mass parts water are uniformly mixed, and are fed the mixture into shampoo special reactor and are stirred to react 1h for 70 DEG C, wherein instead
The speed of agitator for answering kettle is 50r/min, and homogeneous rotating speed is 2800r/min；
2) pH value of mixture is adjusted with the citric acid of 0.8 mass parts to 6, mixing is adjusted with the sodium chloride of 1.2 mass parts
The viscosity of object is to 6000cP (at 25 DEG C), filling discharging, obtain embodiment 2 without silicone oil shampoo.
Embodiment 3：
The shampoo preparation method of embodiment 3 is as follows：
1) radix ampelopsis of the silver birch extract of 3 mass parts, the Millettia extract of 6 mass parts, 0.5 mass parts is extracted
Object, the Echinacea Purpurea Herb P.E of 0.5 mass parts, the Extracts of Mallotus apelta of 0.5 mass parts, 6 mass parts amino acid (including 1 mass
Part glutamic acid, 1 mass parts valine, 1 mass parts serine, half Guang of 1 mass parts glycine, 1 mass parts lysine and 1 mass parts
Propylhomoserin), the water of the collagen of 2 mass parts and 80 mass parts be uniformly mixed, feed the mixture into shampoo special reactor
50 DEG C are stirred to react 3h, and the wherein speed of agitator of reaction kettle is 50r/min, and homogeneous rotating speed is 2800r/min；
2) pH value of mixture is adjusted with the citric acid of 1 mass parts to 5.5, mixing is adjusted with the sodium chloride of 0.5 mass parts
The viscosity of object is to 4000cP (at 25 DEG C), filling discharging, obtain embodiment 3 without silicone oil shampoo.
Performance evaluation：
It is tested by the shampoo for providing the embodiment of the present invention 1~3 to volunteer, the test number of each embodiment
It is 30 people, men and women is fifty-fifty, and the age is 18 to 60 years old, average age 38 years old.Volunteer is continuously made using the shampoo of the present invention
After 2 weeks, evaluated.Represent that score is 0~5 according to the effect scoring after using, score is higher to represent that effect is better.0
Divide and indicate no positive effect, 5 points represent that effects are very notable.To investigation, results are averaged, as shown in table 1.
The Evaluation results of 1 embodiment of table
| Survey item | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Wet comb performance | 4.4 | 4.2 | 4.0 |
| Dry comb performance | 4.6 | 4.5 | 4.2 |
| Feel after hair shaft | 4.1 | 3.8 | 4.0 |
From the point of view of the test result of table 1, most of volunteer is higher (more using scoring after the shampoo of the embodiment of the present invention
Number at 4 points and more than), illustrate the embodiment of the present invention has excellent wet comb performance and dry comb performance without silicone oil shampoo product,
The phenomenon that in carding process without apparent tangled up and knotted, and good hand touch after hair shaft.
In addition, the shampoo of embodiment 1 is issued to 10 pregnant woman volunteers using continuous one week, and evaluated.It comments
Valency is divided into three gears：No positive effect (being not improved using front and rear) is effective (to improve before the experiment of hair oily gum, hair quality is soft
Along easily comb), have positive effect (hair without grease and soapy feeling, it is smooth, relatively test before significantly improve).Rating result is as follows：Have
Positive effect accounts for 2, and effective accounts for 7, and no positive effect accounts for 1, total effective rate 90%.
Thus, shampoo of the invention works well, and has wide application value and market prospects.
Claims (8)
1. a kind of no silicone oil shampoo, it is characterised in that：It is made of the raw material of following mass percent：
2. a kind of no silicone oil shampoo according to claim 1, it is characterised in that：By the raw material group of following mass percent
Into：
3. a kind of no silicone oil shampoo according to claim 1 or 2, it is characterised in that：Amino acid is glutamic acid, smart ammonia
Acid, serine, cystine, glycine, alanine, valine, leucine, isoleucine, phenylalanine, tyrosine, tryptophan,
At least one of proline, threonine, aspartic acid, lysine, histidine, cysteine, methionine, citrulling.
4. a kind of preparation method of no silicone oil shampoo, it is characterised in that：Include the following steps：
1) composition as described in claim 1 or 2 weighs raw material；
2) by silver birch extract, Millettia extract, Radix Ampelopsis extract, Echinacea Purpurea Herb P.E, Extracts of Mallotus apelta, amino
Acid, collagen and water are uniformly mixed, and the mixture of gained, which is placed in reaction kettle, to be stirred to react；
3) pH value of mixture is adjusted with citric acid, the viscosity of mixture is adjusted with sodium chloride, filling discharging obtains no silicone oil and washes
Shampoo.
5. a kind of preparation method of no silicone oil shampoo according to claim 4, it is characterised in that：In step 2), reaction
Temperature for 50 DEG C~70 DEG C, the reaction time is 1h~3h.
6. a kind of preparation method of no silicone oil shampoo according to claim 4, it is characterised in that：In step 2), reaction
The speed of agitator of kettle is 40r/min~50r/min, and homogeneous rotating speed is 2500r/min~3000r/min.
7. a kind of preparation method of no silicone oil shampoo according to claim 4, it is characterised in that：In step 3), adjust
The pH value of mixture is 5~7.
8. a kind of preparation method of no silicone oil shampoo according to claim 4, it is characterised in that：In step 3), adjust
The viscosity of mixture is 4000cP~6000cP at 25 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711434553.8A CN108158879A (en) | 2017-12-26 | 2017-12-26 | A kind of no silicone oil shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711434553.8A CN108158879A (en) | 2017-12-26 | 2017-12-26 | A kind of no silicone oil shampoo and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108158879A true CN108158879A (en) | 2018-06-15 |
Family
ID=62521428
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711434553.8A Pending CN108158879A (en) | 2017-12-26 | 2017-12-26 | A kind of no silicone oil shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108158879A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112089666A (en) * | 2020-10-26 | 2020-12-18 | 广州环亚化妆品科技有限公司 | Antioxidant composition and preparation method and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103948519A (en) * | 2014-04-16 | 2014-07-30 | 陈建婷 | Multifunctional shampoo |
| CN104306182A (en) * | 2014-09-30 | 2015-01-28 | 青岛叁鼎卫生制品有限公司 | Weak acid amino acid liquid shampoo |
| CN105326655A (en) * | 2015-11-24 | 2016-02-17 | 北京斯利安制药有限公司 | Silicone-oil-free folic acid shampoo and preparation method thereof |
| CN106580726A (en) * | 2016-11-11 | 2017-04-26 | 珠海伊斯佳科技股份有限公司 | Silicone-oil-free liquid shampoo containing amino acid and preparation method of silicone-oil-free liquid shampoo |
| CN106727114A (en) * | 2016-12-12 | 2017-05-31 | 德阳力久云智知识产权运营有限公司 | One kind is without silicone oil shampoo and preparation method thereof |
-
2017
- 2017-12-26 CN CN201711434553.8A patent/CN108158879A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103948519A (en) * | 2014-04-16 | 2014-07-30 | 陈建婷 | Multifunctional shampoo |
| CN104306182A (en) * | 2014-09-30 | 2015-01-28 | 青岛叁鼎卫生制品有限公司 | Weak acid amino acid liquid shampoo |
| CN105326655A (en) * | 2015-11-24 | 2016-02-17 | 北京斯利安制药有限公司 | Silicone-oil-free folic acid shampoo and preparation method thereof |
| CN106580726A (en) * | 2016-11-11 | 2017-04-26 | 珠海伊斯佳科技股份有限公司 | Silicone-oil-free liquid shampoo containing amino acid and preparation method of silicone-oil-free liquid shampoo |
| CN106727114A (en) * | 2016-12-12 | 2017-05-31 | 德阳力久云智知识产权运营有限公司 | One kind is without silicone oil shampoo and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 王建新等: "《化妆品植物原料大全》", 30 June 2012 * |
| 裘炳毅等: "《现代化妆品科学与技术 下》", 31 March 2016 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112089666A (en) * | 2020-10-26 | 2020-12-18 | 广州环亚化妆品科技有限公司 | Antioxidant composition and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106750361B (en) | A kind of lignin sulfonate modified object and its application and the shampoo comprising the modifier | |
| CN106580726A (en) | Silicone-oil-free liquid shampoo containing amino acid and preparation method of silicone-oil-free liquid shampoo | |
| CN103263372B (en) | Natural flower petal and cosmetic adopting same | |
| CN102885254B (en) | Stone-milled black soybean health-maintaining dried noodles | |
| CN103796630A (en) | Shampoo composition | |
| CN103892199B (en) | A kind of muskmelon taste noodles and preparation method thereof | |
| CN107550795A (en) | Nourish reparation, black hair anticreep camellia oleifera fruit shampoo and preparation method thereof | |
| CN103735457B (en) | Toner containing herbal components and preparation method thereof | |
| CN103735467A (en) | Natural plant shower gel and preparation method thereof | |
| CN108158879A (en) | A kind of no silicone oil shampoo and preparation method thereof | |
| CN106361636A (en) | Skincare composition and application thereof in skin whitening | |
| CN106047517A (en) | Woolen sweater washing liquid containing snail extracting solution | |
| CN102188330B (en) | Use of bacterial cellulose wet membrane in hair-care products | |
| CN104365890A (en) | Tea leaf preparing process | |
| CN104705805B (en) | A kind of beauty mask moisturizing panty hose and preparation method thereof | |
| CN103820250A (en) | Skin care soap containing Spina Gleditsiae and Mythic Fungus, and its making method | |
| CN102919790A (en) | Soup blend and preparation method thereof | |
| CN108785137A (en) | A kind of hair conditioner and preparation method thereof | |
| CN108004060A (en) | A kind of intestines Enteromorpha skin care soap and preparation method thereof | |
| CN109953918A (en) | A kind of facial mask of the light speckles, beautification and white of anti-acne | |
| CN104771346A (en) | Lemongrass liquid soap and preparation method thereof | |
| CN109793681A (en) | It is a kind of containing educating the shampoo composite for sending out hair loss composite reactive Essence anti- | |
| CN107334679A (en) | Shampoo prepared by a kind of gleditsia sinensis and preparation method thereof | |
| CN108324589A (en) | A kind of composition for whitening skin and preparation method thereof | |
| CN101152136B (en) | Multifunctional shampoo of Chinese yam and method of preparing the same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180615 |