CN108148552B - Efficient anti-icing and defogging agent and device - Google Patents
Efficient anti-icing and defogging agent and device Download PDFInfo
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- CN108148552B CN108148552B CN201711385440.3A CN201711385440A CN108148552B CN 108148552 B CN108148552 B CN 108148552B CN 201711385440 A CN201711385440 A CN 201711385440A CN 108148552 B CN108148552 B CN 108148552B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/18—Materials not provided for elsewhere for application to surfaces to minimize adherence of ice, mist or water thereto; Thawing or antifreeze materials for application to surfaces
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D83/00—Containers or packages with special means for dispensing contents
- B65D83/14—Containers or packages with special means for dispensing contents for delivery of liquid or semi-liquid contents by internal gaseous pressure, i.e. aerosol containers comprising propellant for a product delivered by a propellant
- B65D83/38—Details of the container body
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D83/00—Containers or packages with special means for dispensing contents
- B65D83/14—Containers or packages with special means for dispensing contents for delivery of liquid or semi-liquid contents by internal gaseous pressure, i.e. aerosol containers comprising propellant for a product delivered by a propellant
- B65D83/44—Valves specially adapted therefor; Regulating devices
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- Engineering & Computer Science (AREA)
- Dispersion Chemistry (AREA)
- Mechanical Engineering (AREA)
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- Detergent Compositions (AREA)
- Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)
Abstract
The invention discloses a high-efficiency anti-icing and demisting agent and a high-efficiency anti-icing and demisting agent device. The efficient anti-icing and demisting agent comprises the following components in parts by weight: 0.3 to 2 percent of water-based acrylic resin, 8 to 15 percent of organic silicon antifogging agent, 0.1 to 2 percent of organic siloxane coupling agent, 0.3 to 2 percent of polyethylene glycol and the balance of absolute ethyl alcohol. The efficient anti-icing defogging agent disclosed by the invention can resist icing, and has a good defogging effect and good defogging durability.
Description
Technical Field
The invention relates to the technical field of fog removing agents, in particular to a high-efficiency anti-icing fog removing agent and a high-efficiency anti-icing fog removing device.
Background
When the driver drives out, the glass in front can be cleaned by water. However, in rainy days or at low temperature, when a certain partial pressure of water vapor is cooled to the dew point, the water vapor reaches a saturated state, and is condensed to separate out tiny water drops, which are attached to the surface of the glass to generate an atomization phenomenon (fogging). The small water drops generate atomization, so that light is subjected to diffuse reflection, and the transparency of the glass is influenced to different degrees. This fogging affects the driving safety significantly.
In 2011, 21 thousands of road traffic accidents occur in China, 6 thousands of people die, 2 thousands of people are injured, and the property loss exceeds 9 hundred million yuan. Has far exceeded the average in developed countries. Among the causes of these traffic accidents, a considerable portion of the accidents occur in winter or rainy days, and the driver's sight line is blurred due to the fog on the windshield, thereby causing traffic accidents. Therefore, the potential hazard brought by the automobile glass aerosol is continuously amplified, and the automobile glass anti-fogging technology is in need.
The antifogging agent in the market at present mainly takes surfactants as main components, and the antifogging agent mainly comprises an oil surfactant, a solvent, a wetting agent and a dispersing agent. The antifogging agent has poor antifogging durability due to the fact that glass condenses water and a surfactant is lost, and the antifogging agent generally fails after being maintained for 2 days.
Disclosure of Invention
Based on the technical scheme, the efficient anti-icing and demisting agent provided by the invention can resist icing, has a good demisting effect and good demisting durability.
The invention also provides a high-efficiency anti-icing and defogging agent device.
In order to realize the purpose of the invention, the invention adopts the following technical scheme:
the efficient anti-icing and demisting agent comprises the following components in parts by weight: 0.3 to 2 percent of water-based acrylic resin, 8 to 15 percent of organic silicon antifogging agent, 0.1 to 2 percent of organic siloxane coupling agent, 0.3 to 2 percent of polyethylene glycol and the balance of absolute ethyl alcohol.
The efficient anti-icing and antifogging agent can form a polymer film on the surface of glass, the polymer film has hydrophilicity and stronger binding force with the glass, and cannot run off along with water binding of the glass, so that the antifogging durability is improved; the film can not frost on glass due to condensed moisture in the environment of-4 ℃ and above, and the defogging effect is further improved.
In some embodiments, the efficient anti-icing and defogging agent comprises the following components in parts by weight: 1% of water-based acrylic resin, 12% of organic silicon antifogging agent, 0.3% of organic siloxane coupling agent, 0.6% of polyethylene glycol and 86.1% of absolute ethyl alcohol.
In some embodiments, the efficient anti-icing and defogging agent comprises the following components in parts by weight: 1% of water-based acrylic resin, 8% of organic silicon antifogging agent, 0.5% of organic siloxane coupling agent, 0.7% of polyethylene glycol and 89.8% of absolute ethyl alcohol.
In some embodiments, the efficient anti-icing and defogging agent comprises the following components in parts by weight: 1% of water-based acrylic resin, 13% of organic silicon antifogging agent, 0.3% of organic siloxane coupling agent, 1% of polyethylene glycol and 84.7% of absolute ethyl alcohol.
The invention also adopts the following technical scheme:
the efficient anti-icing and demisting agent device comprises a spraying tank, an efficient anti-icing and demisting agent and a propellant, wherein the efficient anti-icing and demisting agent is filled in the spraying tank and comprises the following components in parts by weight: 0.3 to 2 percent of water-based acrylic resin, 8 to 15 percent of organic silicon antifogging agent, 0.1 to 2 percent of organic siloxane coupling agent, 0.3 to 2 percent of polyethylene glycol and the balance of absolute ethyl alcohol; the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1: 3-5.
In some of these embodiments, the propellant is propane and butane.
In some of these embodiments, the propane to butane mass ratio is 1/3-1: 1.
In some embodiments, the preparation method of the high-efficiency anti-icing and defogging agent device comprises the following steps:
providing 0.3-2% of water-based acrylic resin, 8-15% of organic silicon antifogging agent, 0.1-2% of organic siloxane coupling agent, 0.3-2% of polyethylene glycol, the balance of absolute ethyl alcohol, a spray can and a propellant;
mixing the water-based acrylic resin, the organic silicon antifogging agent, the organic siloxane coupling agent, the polyethylene glycol and the absolute ethyl alcohol, and uniformly stirring to obtain the high-efficiency anti-icing antifogging agent;
filling the efficient anti-icing and anti-fogging agent into the spray tank;
and adding a valve and a seal on the spray can, and finally filling the propellant.
In some of these embodiments, the propellant is propane and butane.
In some of these embodiments, the propane to butane mass ratio is 1/3-1: 1.
Detailed Description
In order that the invention may be more fully understood, reference will now be made to the following description. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention.
The efficient anti-icing and anti-fogging agent is used for rust removal and rust prevention on the surface of steel and prolongs the service life of the steel.
The efficient anti-icing and demisting agent comprises the following components in parts by weight: 0.3 to 2 percent of water-based acrylic resin, 8 to 15 percent of organic silicon antifogging agent, 0.1 to 2 percent of organic siloxane coupling agent, 0.3 to 2 percent of polyethylene glycol and the balance of absolute ethyl alcohol.
The efficient anti-icing and demisting agent has the following advantages:
the hydrophilicity of the antifogging coating and the water are utilized to generate a mixture with a low freezing point, so that the water does not generate fog frost under high temperature difference. And the coating has hydrophilicity, so that water drops condensed on the glass can be well spread, and fog and frost are not formed.
Hydrophilic macromolecules are used as carriers of the organic silicon antifogging agent, so that the antifogging agent forms an antifogging layer on glass, and the adhesion force of the hydrophilic macromolecules and the glass is enhanced due to the fact that the adhesion force of the hydrophilic macromolecules and the glass is not very strong and the water resistance is poor. The hydrophilic wetting agent polyethylene glycol is added, so that the hydrophilic polymer has better hydrophilicity, and the freezing point of condensed water can be reduced, so that the defogging agent is not easy to fog and frost.
In conclusion, the efficient anti-icing and defogging agent can form a polymer film on the surface of glass, and the polymer film has hydrophilicity and stronger binding force with the glass, cannot run off along with water binding of the glass, and improves the durability of antifogging; the film can not frost on glass due to condensed moisture in the environment of-4 ℃ and above, and the defogging effect is further improved.
The efficient anti-icing and demisting agent device adopting the efficient anti-icing and demisting agent comprises a spraying tank, and the efficient anti-icing and demisting agent and a propellant which are filled in the spraying tank; the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1: 3-5.
The propellant is propane or butane. Wherein the mass ratio of the propane to the butane is 1/3-1: 1.
The preparation method is that the high-efficiency anti-icing and anti-fogging agent is filled into a spray tank;
adding a valve and a seal on the spray can, and finally filling propellant.
The efficient anti-icing and defogging agent device adopts propane and butane which are mixed in a certain ratio as a propellant, so that the spray can quickly form a film.
The method of practicing the present invention will be further illustrated by the following examples.
Example one
The efficient anti-icing and demisting agent provided by the embodiment of the invention comprises the following components in parts by weight: 1% of water-based acrylic resin, 12% of organic silicon antifogging agent, 0.3% of organic siloxane coupling agent, 0.6% of polyethylene glycol and 86.1% of absolute ethyl alcohol.
The preparation method of the efficient anti-icing and demisting agent comprises the following steps: and mixing the components, and uniformly stirring to obtain the efficient anti-icing and demisting agent.
The efficient anti-icing and demisting agent device adopting the efficient anti-icing and demisting agent comprises a spraying tank, the efficient anti-icing and demisting agent and a propellant, wherein the efficient anti-icing and demisting agent and the propellant are filled into the spraying tank, the propellant is obtained by mixing butane and propane according to the proportion of 3:1, and the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1:3.
The preparation method of the high-efficiency anti-icing and defogging agent device comprises the following steps: the high-efficiency anti-icing and de-icing agent is filled into a spraying tank, a valve is arranged on the spraying tank, the spraying tank is sealed, and finally propellant is filled.
Example two
The efficient anti-icing and demisting agent provided by the embodiment of the invention comprises the following components in parts by weight: 1% of water-based acrylic resin, 8% of organic silicon antifogging agent, 0.5% of organic siloxane coupling agent, 0.7% of polyethylene glycol and 89.8% of absolute ethyl alcohol.
The preparation method of the efficient anti-icing and demisting agent comprises the following steps: and mixing the components, and uniformly stirring to obtain the efficient anti-icing and demisting agent.
The efficient anti-icing and demisting agent device adopting the efficient anti-icing and demisting agent comprises a spraying tank, the efficient anti-icing and demisting agent and a propellant, wherein the efficient anti-icing and demisting agent and the propellant are filled into the spraying tank, the propellant is obtained by mixing butane and propane according to the proportion of 2:1, and the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1: 4.
The preparation method of the high-efficiency anti-icing and defogging agent device comprises the following steps: the high-efficiency anti-icing and de-icing agent is filled into a spraying tank, a valve is arranged on the spraying tank, the spraying tank is sealed, and finally propellant is filled.
EXAMPLE III
The efficient anti-icing and demisting agent provided by the embodiment of the invention comprises the following components in parts by weight: 1% of water-based acrylic resin, 13% of organic silicon antifogging agent, 0.3% of organic siloxane coupling agent, 1% of polyethylene glycol and 84.7% of absolute ethyl alcohol.
The preparation method of the efficient anti-icing and demisting agent comprises the following steps: and mixing the components, and uniformly stirring to obtain the efficient anti-icing and demisting agent.
The efficient anti-icing and demisting agent device adopting the efficient anti-icing and demisting agent comprises a spraying tank, the efficient anti-icing and demisting agent and a propellant, wherein the efficient anti-icing and demisting agent and the propellant are filled into the spraying tank, the propellant is obtained by mixing butane and propane according to the proportion of 1:1, and the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1: 5.
The preparation method of the high-efficiency anti-icing and defogging agent device comprises the following steps: the high-efficiency anti-icing and de-icing agent is filled into a spraying tank, a valve is arranged on the spraying tank, the spraying tank is sealed, and finally propellant is filled.
Example four
The efficient anti-icing and demisting agent provided by the embodiment of the invention comprises the following components in parts by weight: 0.3 percent of water-based acrylic resin, 15 percent of organic silicon antifogging agent, 0.1 percent of organic siloxane coupling agent, 0.3 percent of polyethylene glycol and 84.3 percent of absolute ethyl alcohol.
The preparation method of the efficient anti-icing and demisting agent comprises the following steps: and mixing the components, and uniformly stirring to obtain the efficient anti-icing and demisting agent.
The efficient anti-icing and demisting agent device adopting the efficient anti-icing and demisting agent comprises a spraying tank, the efficient anti-icing and demisting agent and a propellant, wherein the efficient anti-icing and demisting agent and the propellant are filled into the spraying tank, the propellant is obtained by mixing butane and propane according to the proportion of 3:1, and the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1: 4.
The preparation method of the high-efficiency anti-icing and defogging agent device comprises the following steps: the high-efficiency anti-icing and de-icing agent is filled into a spraying tank, a valve is arranged on the spraying tank, the spraying tank is sealed, and finally propellant is filled.
EXAMPLE five
The efficient anti-icing and demisting agent provided by the embodiment of the invention comprises the following components in parts by weight: 2% of water-based acrylic resin, 10% of organic silicon antifogging agent, 2% of organic siloxane coupling agent, 2% of polyethylene glycol and 84% of absolute ethyl alcohol.
The preparation method of the efficient anti-icing and demisting agent comprises the following steps: and mixing the components, and uniformly stirring to obtain the efficient anti-icing and demisting agent.
The efficient anti-icing and demisting agent device adopting the efficient anti-icing and demisting agent comprises a spraying tank, the efficient anti-icing and demisting agent and a propellant, wherein the efficient anti-icing and demisting agent and the propellant are filled into the spraying tank, the propellant is obtained by mixing butane and propane according to the proportion of 2.5:1, and the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1: 3.5.
The preparation method of the high-efficiency anti-icing and defogging agent device comprises the following steps: the high-efficiency anti-icing and de-icing agent is filled into a spraying tank, a valve is arranged on the spraying tank, the spraying tank is sealed, and finally propellant is filled.
EXAMPLE six
The efficient anti-icing and demisting agent provided by the embodiment of the invention comprises the following components in parts by weight: 1.5 percent of water-based acrylic resin, 14 percent of organic silicon antifogging agent, 1.3 percent of organic siloxane coupling agent, 1.5 percent of polyethylene glycol and 81.7 percent of absolute ethyl alcohol.
The preparation method of the efficient anti-icing and demisting agent comprises the following steps: and mixing the components, and uniformly stirring to obtain the efficient anti-icing and demisting agent.
The efficient anti-icing and demisting agent device adopting the efficient anti-icing and demisting agent comprises a spraying tank, the efficient anti-icing and demisting agent and a propellant, wherein the efficient anti-icing and demisting agent and the propellant are filled into the spraying tank, the propellant is obtained by mixing butane and propane according to the proportion of 2:1, and the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1: 3.5.
The preparation method of the high-efficiency anti-icing and defogging agent device comprises the following steps: the high-efficiency anti-icing and de-icing agent is filled into a spraying tank, a valve is arranged on the spraying tank, the spraying tank is sealed, and finally propellant is filled.
Comparative example 1
A normal temperature type automobile glass fog remover comprises the following components:
0.02-0.05 wt% of surfactant; 0.01-0.02 wt% of film-forming agent; 0.001-0.002 wt% of defoaming agent; the rest is diluent; wherein the surfactant is a CH3O (CH3CH2CH2O) n (CH2CH2O) mCH3O type nonionic surfactant, wherein n is 2-6, and m is 5-10.
Comparative example No. two
The glass frost-removing and fog-removing agent comprises the following components in percentage by mass: 10-30% of medical ethanol, 0.5-3% of fatty alcohol-polyoxyethylene ether, 0.5-2% of menthol, 0.1-2% of polyethylene glycol, 1-8% of glycerol, 1-5% of spray and the balance of deionized water.
The defogging effects of the first to sixth examples and the comparative example were tested as follows.
1. Antifogging property
The antifogging agent of the present invention is sprayed or wiped on a clean 100mm x 100mm glass sheet, and after natural drying, the antifogging agent-coated glass sheet is fumigated for 2-5s with a household electric heating steam generator. The glass atomization phenomenon is observed, the glass naturally evaporates for 10min, and the glass still keeps transparent reflection, and the result is shown in the table I.
2. Durability of antifogging
And (3) uniformly spraying or wiping the antifogging agent on the glass test piece, clearly wiping the glass test piece by using a towel, and naturally drying for 5-10 min for later use. A250 ml beaker is filled with a certain amount of water, the temperature is kept constant at 50 ℃, the side of the glass test piece coated with the antifogging agent is covered on the beaker, the distance between the liquid level of the water and the glass test piece is kept at 25mm, and the time when the water mist appears on about 1/2 areas of the glass test piece is recorded, and the result is shown in the table I.
3. Anti-freezing property
Coating an antifogging agent on one surface of a clean double-sided mirror, wiping the double-sided mirror clearly by a towel, naturally drying the double-sided mirror for 5-10 min, placing the double-sided mirror in a refrigerator at minus 4 ℃ for standing for 30min, taking the double-sided mirror out of a room temperature environment, observing the aerial fog condition of the double-sided mirror, and observing the result that frost should not be formed, wherein the result is shown in the table I.
Watch 1
Test items | Antifogging property | Durability of antifogging | Anti-icing (-4 ℃, 30min) |
Example one | No fogging, and is transparent and clear | 180min | Ice-free cream |
Example two | No fogging, and is transparent and clear | 175min | Ice-free cream |
EXAMPLE III | No fogging, and is transparent and clear | 177min | Ice-free cream |
Example four | No fogging, and is transparent and clear | 168min | Ice-free cream |
EXAMPLE five | No fogging, and is transparent and clear | 180min | Ice-free cream |
EXAMPLE six | No fogging, and is transparent and clear | 180min | Ice-free cream |
Comparative example 1 | Little fog | 150min | Little frost |
Comparative example No. two | Fogging | 145min | With frost |
As can be seen from the table I, compared with the prior art, the efficient anti-icing and defogging agent disclosed by the embodiment of the invention has the advantages of better antifogging performance, high antifogging durability and lasting antifogging effect.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (10)
1. The efficient anti-icing and defogging agent for the automobile glass is characterized by comprising the following components in parts by weight: 0.3 to 2 percent of water-based acrylic resin, 8 to 15 percent of organic silicon antifogging agent, 0.1 to 2 percent of organic siloxane coupling agent, 0.3 to 2 percent of polyethylene glycol and the balance of absolute ethyl alcohol.
2. The efficient anti-icing and defogging agent for automobile glass as claimed in claim 1, which is characterized by comprising the following components in parts by weight: 1% of water-based acrylic resin, 12% of organic silicon antifogging agent, 0.3% of organic siloxane coupling agent, 0.6% of polyethylene glycol and 86.1% of absolute ethyl alcohol.
3. The efficient anti-icing and defogging agent for automobile glass as claimed in claim 1, which is characterized by comprising the following components in parts by weight: 1% of water-based acrylic resin, 8% of organic silicon antifogging agent, 0.5% of organic siloxane coupling agent, 0.7% of polyethylene glycol and 89.8% of absolute ethyl alcohol.
4. The efficient anti-icing and defogging agent for automobile glass as claimed in claim 1, which is characterized by comprising the following components in parts by weight: 1% of water-based acrylic resin, 13% of organic silicon antifogging agent, 0.3% of organic siloxane coupling agent, 1% of polyethylene glycol and 84.7% of absolute ethyl alcohol.
5. The efficient anti-icing and defogging agent device for the automobile glass is characterized by comprising a spraying tank, an efficient anti-icing and defogging agent and a propellant, wherein the efficient anti-icing and defogging agent is filled in the spraying tank and comprises the following components in parts by weight: 0.3 to 2 percent of water-based acrylic resin, 8 to 15 percent of organic silicon antifogging agent, 0.1 to 2 percent of organic siloxane coupling agent, 0.3 to 2 percent of polyethylene glycol and the balance of absolute ethyl alcohol; the weight ratio of the propellant to the efficient anti-icing and demisting agent is 1: 3-5.
6. The device as claimed in claim 5, wherein the propellant is propane and butane.
7. The device as claimed in claim 6, wherein the mass ratio of propane to butane is 1/3-1: 1.
8. The device as claimed in claim 5, wherein the device is prepared by the following steps:
providing 0.3-2% of water-based acrylic resin, 8-15% of organic silicon antifogging agent, 0.1-2% of organic siloxane coupling agent, 0.3-2% of polyethylene glycol, the balance of absolute ethyl alcohol, a spray can and a propellant;
mixing the water-based acrylic resin, the organic silicon antifogging agent, the organic siloxane coupling agent, the polyethylene glycol and the absolute ethyl alcohol, and uniformly stirring to obtain the high-efficiency anti-icing antifogging agent;
filling the efficient anti-icing and anti-fogging agent into the spray tank;
and adding a valve and a seal on the spray can, and finally filling the propellant.
9. The device as claimed in claim 8, wherein the propellant is propane and butane.
10. The device as claimed in claim 9, wherein the mass ratio of propane to butane is 1/3-1: 1.
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