CN108143697A - A kind of whitening mask and preparation method thereof - Google Patents
A kind of whitening mask and preparation method thereof Download PDFInfo
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- CN108143697A CN108143697A CN201810223642.6A CN201810223642A CN108143697A CN 108143697 A CN108143697 A CN 108143697A CN 201810223642 A CN201810223642 A CN 201810223642A CN 108143697 A CN108143697 A CN 108143697A
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- whitening
- whitening mask
- mask
- beeswax
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses a kind of whitening mask and preparation method thereof.The whitening mask includes following component：Bamboo-leaves flavones 0.01 ~ 2%, ganoderma spore polysaccharide 0.01 ~ 5%, beeswax 0.01 ~ 1%, vitamin E 0.01 ~ 5%, ursin 0.05 ~ 5%, resorcinol derivatives 0.01 ~ 2%, liquid fatty 0.1 ~ 10%, surfactant 0.1% ~ 15%, polyalcohol 0.1 ~ 15% and surplus physiological seawater.The whitening mask of the present invention moistens delaying skin aging, and antiallergy, whitening effect are notable, easy to use suitable for various skin crowds.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of whitening mask and preparation method thereof.
Background technology
With the development of society, the improvement of people's living standards, requirement of the women to cosmetics also becomes higher and higher, perhaps
The people more to like to be beautiful be to the care of oneself skin it is careful to the utmost.It is ultraviolet in dust dirty air, sunlight but in metropolis
Line, computer radiate, the coloured and dazzling color make-up that also we change daily, are all the formidable enemies of delicate skin, accelerate declining for skin
Always, make skin dark yellow.Periodically skin is maintained, is capable of the aging of effective delaying skin, plays the glossy effect of skin health
Fruit.
Facial mask currently on the market is mostly MASQUE APAISANT HYDRATANT or whitening mask.And more extensive whitening is used in whitening mask
Additive mainly has ursin, resorcinol and its derivative etc., they are typically by inhibiting melanocyte proliferation, inhibiting junket
The correlation speed limit enzymatic activity such as propylhomoserin enzyme and the transfer for inhibiting melanin, so as to reach whitening effect.However, these whitenings are added
Agent is affected to external environments such as light, heat and pH value, more due to the shakiness of these whitening compositions in the whitening mask of preparation
It is fixed, cause whitening effect poor.
Invention content
In view of this, the present invention provides a kind of whitening mask, the whitening composition in the whitening mask is stablized, by environment
Influence is smaller, is capable of providing permanent whitening moisturizing effect.Simultaneously also be able to balance skin water and oil balance, delaying skin aging,
Improve the multi-efficiencies such as skin water moistens, exquisiteness is soft.The present invention also provides the preparation methods of above-mentioned whitening mask.
Technical scheme is as follows：
A kind of whitening mask, comprising following weight percentage components：Bamboo-leaves flavones 0.01~2%, ganoderma spore polysaccharide
0.01~5%, beeswax 0.01~1%, vitamin E 0.01~5%, ursin 0.05~5%, resorcinol derivatives 0.01
~2%, the physiological sea of liquid fatty 0.1~10%, surfactant 0.1%~15%, polyalcohol 0.1~15% and surplus
Water.
Preferably, whitening mask of the invention, comprising following weight percentage components：Bamboo-leaves flavones 0.2~1%, spirit
Ganoderma lucidum spore polysaccharide 0.2~2%, beeswax 0.05~0.8%, vitamin E 0.1~4%, ursin 0.1~4%, resorcinol spread out
Biological 0.5~2%, the physiological of liquid fatty 0.3~8%, surfactant 1%~10%, polyalcohol 2~10% and surplus
Seawater.
Preferably, the resorcinol derivatives include hexyl resorcin, Symwhite-337, dimethoxy-p
The mixture of one or more of base -4- propyl diphenol.
Preferably, the liquid fatty includes myristic acid glyceride, isopropyl myristate, Caprylic Capric three
Ester, polyethylene glycol glyceryl laurate ester, glyceryl linoleate, Sefsol 218, two pungent capric acid propylene glycol esters, decanedioic acid two
The mixture of one or more of ethyl ester, isononyl isononanoate, propylene glycol dipelargonate and octyl dodecanol myristinate.
Preferably, the surfactant includes sorbitan laurate, Crodaret, polyoxyethylene fat
The mixture of one or more of fat acid esters, castor oil polyoxyethylene ether and polyoxyethylene sorbitan fatty acid ester.
Preferably, the polyalcohol is included in polyethylene glycol, propylene glycol, glycerine, 1,3-BDO and 1,2- pentanediol
One or more of mixtures.
The invention also includes the preparation methods of whitening mask described in any of the above-described technical solution, include the following steps：
A. by physiological seawater high-temperature sterilization, when greenhouse cooling is to 65-85 DEG C, beeswax is dissolved thereto；
B. surfactant and polyalcohol are stirred 15-20 minutes at 80-85 DEG C；
C. the dissolving feed liquid step a obtained homogeneous together with the mixture that step b is obtained；
D. the material after homogeneous is cooled to 48-55 DEG C, add in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin,
Hydroquinone derivatives and vitamin E, stir evenly, and adjust pH value to 5~7, are down to room temperature.
Preferably, the step of high-temperature sterilization is that the physiological seawater is kept stirring to 15-20 points at 90-95 DEG C
Clock.
Preferably, mixing speed is 40-50 revs/min in the step b.
Preferably, homogeneous speed described in step c is 1200-1800 revs/min, and homogenizing time is 3-5 minutes.
Relative to the prior art, the present invention has the following advantages：
Contain in whitening mask of the present invention there are many ingredient the effect of whitening antioxidation, it is more including bamboo-leaves flavones, Reishi sporule
The anti-oxidant whitening composition such as sugared, beeswax and physiological seawater and ursin, resorcinol derivatives and vitamin E.The present invention
The ingredients such as bamboo-leaves flavones, ganoderma spore polysaccharide, beeswax collaboration skin whitening effect is played during the use of facial mask, improve
The whitening effect of facial mask plays skin the repairing effect of comprehensive anti-ageing whitening.
The present invention adds in bamboo-leaves flavones and vitamin E in facial mask, melanin is inhibited to be formed in facial mask whitening composition same
When, already oxidised melanin is restored, has played synergistic effect, it will be apparent that enhance white-skinned face function.Ganoderma spore polysaccharide and bee
Wax has certain protective effect to the stability of ursin and resorcinol derivatives, improves ursin and resorcinol spreads out
Biology ensure that the whitening effect of facial mask of the present invention, extend the shelf of facial mask of the present invention to the tolerance of light, temperature and pH value
Phase.
The use of physiological seawater improves the various trace elements in facial mask, also has sterilization, antiallergy and anti-inflammatory
Effect improves the isolation effect of facial mask, and the facial mask of the present invention is made to be equally applicable to sensitive skin, improves facial mask of the present invention
Safety in utilization and target user.
The whitening mask of the present invention complies fully with country's promulgation《Cosmetics health specification》Items in (2007 editions) refer to
Mark, does not contain any noxious material.It can individually use coated on skin, the mask matrixes such as non-woven fabrics can be also soaked in facial mask,
Coated on skin, it is mainly used for facial and neck take.The whitening mask of the present invention moistens delaying skin aging, antiallergy,
Whitening effect is notable, easy to use suitable for various skin crowds.
Specific embodiment
The present invention provides a kind of whitening mask, comprising following weight percentage components：Bamboo-leaves flavones 0.01~2%,
Ganoderma spore polysaccharide 0.01~5%, beeswax 0.01~1%, vitamin E 0.01~5%, ursin 0.05~5%, isophthalic two
Amphyl 0.01~2%, liquid fatty 0.1~10%, surfactant 0.1%~15%, polyalcohol 0.1~15% and remaining
The physiological seawater of amount.
The whitening mask of the present invention includes 0.01~2% bamboo-leaves flavones that mass percentage is, preferably 0.2~
1%, more preferably 0.3~0.8%.Bamboo-leaves flavones are a kind of safe and efficient biological anti-oxidants, can remove human skin
Active oxidation free radical prevents biomembrane lipid from being aoxidized by superoxide radical and hydroxyl radical free radical, plays effective antioxidant and anti-aging
Effect.Meanwhile the high-efficiency antioxidant of bamboo-leaves flavones, it is compounded with ganoderma spore polysaccharide, its antioxidant activity can be enhanced, added
Speed inhibits the melanin reduction of formation and the oxidation of melanin, plays the effect of collaboration whitening.The present invention is to bamboo-leaves flavones
Source is not particularly limited, and commercially available bamboo-leaves flavones are voluntarily extracted or used using the conventional method in this field.
The whitening mask of the present invention includes 0.01~5% ganoderma spore polysaccharide that mass percentage is, preferably
0.2~2%, more preferably 0.3~1.5%.Ganoderma spore polysaccharide has excellent moistening effect, and performance of keeping humidity will be due to saturating
Bright matter acid.In the present invention, ganoderma spore polysaccharide is other than its performance of keeping humidity, also for the whitening unstable to external environment
Ingredient ursin and resorcinol derivatives have certain protective effect, slow down ursin and resorcinol derivatives not
Loss of activity in good environment ensure that the whitening effect of whitening mask of the present invention.Meanwhile ganoderma spore polysaccharide also has centainly
Antiphlogistic effects, certain protective effect is played to sensitive skin.The present invention does not have special limit to the source of ganoderma spore polysaccharide
It is fixed, commercially available Reishi sporule is voluntarily extracted or used using the conventional method in this field.
The whitening mask of the present invention includes mass percentage for 0.01~1% beeswax, preferably 0.05~
0.8%, more preferably 0.1~0.5%.The nutrition of beeswax energy and improvement subcutaneous tissue situation, activate its elastic fibers, prevent that it is hard
Change, promote skin soft and moist, reduce wrinkle.Since beeswax has temperature very strong tolerance, bee is added in the facial mask of the present invention
Wax, can effectively keep the state of active ingredient and the tolerance to temperature in facial mask, especially can effectively maintain facial mask beautiful
Labile element in Bai Chengfen such as ursin and resorcinol derivatives, improves guarantor of the active constituent in storage
The matter phase ensures the whitening effect of facial mask of the present invention.The beeswax of the present invention is preferably commercially available beeswax product.
The whitening mask of the present invention includes mass percentage for 0.01~5% vitamin E, preferably 0.1~
4%, more preferably 1~3%.Vitamin E can react with free radical, provide hydrogen ion to free radical, realize anti-oxidant
Effect, can will be restored back by the melanin aoxidized, realize the gradually whitening of skin.In addition to having very strong inoxidizability
Outside, it can also moisturize the skin, promote skin metabolism.
The whitening mask of the present invention includes mass percentage for 0.05~5% ursin, and preferably 0.1~4%,
More preferably 1~3%.Ursin can prevent the generation of melanin, so as to reduce by inhibiting the activity of internal tyrosinase
Skin pigmentation, dispelling stain and freckle, while also have the effect of sterilization, anti-inflammatory.But ursin is more sensitive to pH value,
It is easily decomposed under alkaline condition.Beeswax is added in the facial mask of the present invention, can effectively maintain the pH stable of facial mask 5~7
In the range of, it effectively prevent the decomposition of ursin.
The whitening mask of the present invention includes the resorcinol derivatives that mass percentage is 0.01~2%, preferably
0.1~1%, more preferably 0.2~0.5%.In the present invention, the resorcinol derivatives preferably include hexyl resorcin,
The mixture of one or more of Symwhite-337, dimethoxy-p base -4- propyl diphenol.In the present invention
In, to the mass ratioes of resorcinol derivatives various in mixture there is no limit.Resorcinol derivatives have excellent whitening
Effect is one of highest tyrosinase inhibitor of activity having been reported that, and then inhibits the formation of melanin.But due to isophthalic
To light, thermally labile, resorcinol derivatives content can reduce rapidly two amphyls in storage is prepared, and can not play
Its effect.The present invention has delayed shakiness of the resorcinol to light, heat by being added to ganoderma spore polysaccharide and beeswax in facial mask
It is qualitative, it ensure that the whitening effect of facial mask Resorcino derivative in storage.
The whitening mask of the present invention includes mass percentage for 0.1%~10% liquid fatty, preferably 0.3%~
8%, more preferably 0.5%~4%.In the present invention, the liquid fatty preferably includes myristic acid glyceride, myristic acid
It is isopropyl ester, Miglyol 812N, polyethylene glycol glyceryl laurate ester, glyceryl linoleate, Sefsol 218, two pungent
In capric acid propylene glycol ester, diethyl sebacate, isononyl isononanoate, propylene glycol dipelargonate and octyl dodecanol myristinate
One or more of mixtures.In the present invention, to the mass ratio of liquid fatties various in mixture, there is no limit.The present invention
Liquid fatty select in Long carbon chain aliphatic acid and middle Long carbon chain unsaturated alcohol generation esters, have natural moisture preserving and repair
Effect, and suitable for a plurality of types of skin.Some physicochemical properties of liquid fatty are very similar to the object on human skin surface layer
Matter can well be mixed with the lipid in skin, reduced the water loss of skin surface and then kept humidity of skin.The present invention is right
The source of liquid fatty does not limit, using commercial liquid lipid.
Whitening mask provided by the invention includes the surfactant that mass percentage is 0.1%~15.0%, excellent
It is selected as 1%~10%, more preferably 2%~8%.In the present invention, the surfactant includes sorbitan laurate, gathers
Ethylene oxide rilanit special, polyoxyethylene fatty acid ester, castor oil polyoxyethylene ether, polyoxyethylene sorbitan fatty acid ester
One or more of mixture.In the present invention, to the mass ratio of surfactants various in mixture, there is no limit.This
Surfactant in invention selects nonionic surface active agent, and, small toxicity small to skin irritation increases functional component
Dissolubility during making face mask improves the content of functional component.The permeability of facial mask can also be enhanced simultaneously, promote work(
Effect ingredient enters skin, and then plays anti-ageing skin whitening effect.
Whitening mask provided by the invention includes mass percentage for 0.1%~15.0% polyalcohol, and preferably 1%
~10%, more preferably 3%~8%.In the present invention, the polyalcohol preferably includes polyethylene glycol, propylene glycol, glycerine, 1,
The mixture of one or more of 3- butanediols and 1,2- pentanediols.In the present invention, to polyalcohols various in mixture
There is no limit for mass ratio.Polyalcohol has good solubilizing effect to functional component, can improve the content of functional component in facial mask.
In addition polyalcohol can adsorb the polar end in surfactant, can also be embedded in the chain of surfactant, live so as to enhance surface
Property the film that is formed in oil-water interfaces of agent, and then enhance the stability of facial mask.
Whitening mask provided by the invention further includes the physiological seawater of surplus.The use of physiological seawater improves facial mask
In various trace elements, also there is the effect of sterilization, antiallergy and anti-inflammatory, the facial mask of the present invention is made to be equally applicable to sensitive flesh
Skin improves safety in utilization and the target user of facial mask of the present invention.
The present invention also provides the preparation methods of whitening mask described in above-mentioned technical proposal, include the following steps：
A. by physiological seawater high-temperature sterilization, when greenhouse cooling is to 65-85 DEG C, beeswax is dissolved thereto；
B. the liquid fatty, surfactant and polyalcohol are stirred 15-20 minutes at 80-85 DEG C；
C. the dissolving feed liquid step a obtained homogeneous together with the mixture that step b is obtained；
D. the material after homogeneous is cooled to 48-55 DEG C, add in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin,
Hydroquinone derivatives and vitamin E, stir evenly, and adjust pH value to 5~7, are down to room temperature.
In the present invention, the physiological seawater high-temperature sterilization is preferably a step the physiological seawater at 90-95 DEG C
It is kept stirring 15-20 minutes, is stirred 16~18 minutes more preferably at 92-93 DEG C.The temperature of preferably physiological seawater of the invention
When degree is down to 70~80 DEG C, beeswax is dissolved.
The liquid fatty, surfactant and polyalcohol are mixed the present invention, preferably stir 16- at 81-84 DEG C
18 minutes.It is preferred that the speed stirred is 40-50 revs/min, more preferably 43~48 revs/min.Mixture is obtained after stirring.
Present invention homogeneous together with the mixture that step b is obtained by dissolving feed liquid that step a is obtained.The present invention is to homogeneous
Method is not particularly limited, preferably described homogeneous speed be 1200-1800 revs/min, more preferably 1400-1700 revs/min,
Homogenizing time is preferably 3-5 minutes, more preferably 4 minutes.
Material after homogeneous of the present invention preferably cools to 50~53 DEG C, adds in bamboo-leaves flavones, ganoderma spore polysaccharide, black bearberry
Glycosides, resorcinol derivatives and vitamin E, stir evenly, and after adjusting pH value to 5~7, more preferably 5.5~6.5, are down to
Room temperature to get to the present invention whitening mask.
The whitening mask of the present invention has both the effect of anti-ageing, moisturizing and whitening, and repairing for comprehensive whitening is played to skin
Multiple effect, safe to use, adaptation population is wide.
Below in conjunction with the embodiment in the present invention, the technical solution in the embodiment of the present invention is carried out clearly and completely
Description, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based on this hair
Embodiment in bright, the every other implementation that those of ordinary skill in the art are obtained without making creative work
Example, shall fall within the protection scope of the present invention.
Embodiment 1：
A kind of whitening mask by weight percentage, includes following component：
Between bamboo-leaves flavones 1%, ganoderma spore polysaccharide 3%, beeswax 0.5%, vitamin E 0.05%, ursin 2%, hexyl
Benzenediol 1%, myristic acid glyceride 5%, polyoxyethylene fatty acid ester 10%, polyethylene glycol 4%, glycerine 4%, surplus is made a living
Rationality seawater.
Preparation method includes the following steps：
A. physiological seawater is put into agitated kettle, mixing speed is 42 revs/min, is heated to 95 DEG C, is kept stirring 15
Minute；The water of agitated kettle is cooled to 65 DEG C, addition beeswax, which is stirred to, to be completely dissolved；
B. myristic acid glyceride, polyoxyethylene fatty acid ester, polyethylene glycol and glycerine are mixed, 15 is stirred at 80 DEG C
Minute.
C. the dissolving feed liquid that step a is obtained, homogeneous, homogenizer speed are 1500 together with the mixture that step b is obtained
Rev/min, homogeneous 5 minutes.
D. the material after homogeneous is cooled to 50 DEG C, adds in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin, isophthalic
Two amphyls and vitamin E, stir evenly, and adjust pH value to 6.0, are down to room temperature.
Embodiment 2：
A kind of whitening mask by weight percentage, includes following component：
Bamboo-leaves flavones 2%, ganoderma spore polysaccharide 5%, beeswax 1%, vitamin E 5%, ursin 5%, phenethyl isophthalic
Diphenol 2%, Miglyol 812N 5%, glyceryl linoleate 5%, sorbitan laurate 8%, polyoxyethylene sorbitan mountain
Pears alcohol fatty acid ester 7%, propylene glycol 10%, 1,3-BDO 5%, surplus are physiological seawater.
Preparation method includes the following steps：
A. physiological seawater is put into agitated kettle, mixing speed is 50 revs/min, is heated to 90 DEG C, is kept stirring 20
Minute；The water of agitated kettle is cooled to 75 DEG C, addition beeswax, which is stirred to, to be completely dissolved；
B. Miglyol 812N, glyceryl linoleate, sorbitan laurate, polyoxyethylene sorbitan fat
Fat acid esters, propylene glycol and 1,3-BDO mixing, are stirred 20 minutes at 85 DEG C.
C. the dissolving feed liquid that step a is obtained, homogeneous, homogenizer speed are 1800 together with the mixture that step b is obtained
Rev/min, homogeneous 2 minutes.
D. the material after homogeneous is cooled to 53 DEG C, adds in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin, isophthalic
Two amphyls and vitamin E, stir evenly, and adjust pH value to 5.5, are down to room temperature.
Embodiment 3
A kind of whitening mask by weight percentage, includes following component：
Bamboo-leaves flavones 0.5%, ganoderma spore polysaccharide 1%, beeswax 0.2%, vitamin E 0.01%, ursin 0.1%, two
Methoxy methyl phenyl -4- propyls diphenol 0.05%, propylene glycol dipelargonate 0.5%, gathers Sefsol 218 0.5%
Ethylene oxide rilanit special 2%, 1,2- pentanediols 1%, surplus are physiological seawater.
Preparation method includes the following steps：
A. physiological seawater is put into agitated kettle, mixing speed is 45 revs/min, is heated to 92 DEG C, is kept stirring 18
Minute；The water of agitated kettle is cooled to 85 DEG C, addition beeswax, which is stirred to, to be completely dissolved；
B. Sefsol 218, propylene glycol dipelargonate, Crodaret and 1,2- pentanediol are mixed,
It is kept stirring at 82 DEG C 18 minutes.
C. the dissolving feed liquid that step a is obtained, homogeneous, homogenizer speed are 1200 together with the mixture that step b is obtained
Rev/min, homogeneous 4 minutes.
D. the material after homogeneous is cooled to 48 DEG C, adds in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin, isophthalic
Two amphyls and vitamin E, stir evenly, and adjust pH value to 6.5, are down to room temperature.
Comparative example 1
Whitening mask, in addition to beeswax is not contained, remaining component is same as Example 1.
Comparative example 2
Whitening mask, in addition to ganoderma spore polysaccharide and beeswax is not contained, remaining component is same as Example 1.
Comparative example 3
Whitening foundation emulsion, in addition to bamboo-leaves flavones and beeswax are not contained, remaining component is same as Example 1.
Comparative example 4
Whitening mask, in addition to bamboo-leaves flavones, ganoderma spore polysaccharide and beeswax is not contained, remaining component is same as Example 1.
Comparative example 5
Physiological seawater in embodiment 1 is replaced with deionized water by whitening mask, remaining component and preparation method and reality
It is identical to apply example 1.
The ingredient contrast table of 1 embodiment 1 of table and comparative example 1~5
| Bamboo-leaves flavones | Ganoderma spore polysaccharide | Beeswax | Water | |
| Embodiment 1 | √ | √ | √ | Physiological seawater |
| Comparative example 1 | √ | √ | Physiological seawater | |
| Comparative example 2 | √ | Physiological seawater | ||
| Comparative example 3 | √ | Physiological seawater | ||
| Comparative example 4 | Physiological seawater | |||
| Comparative example 5 | √ | √ | √ | Deionized water |
Embodiment 4
Functional component stability experiment in whitening mask
The whitening mask that embodiment 1 and comparative example 1~4 are obtained is placed 60 days in closed container, under room temperature, is used
The content of functional component ursin, resorcinol derivatives, vitamin E, real in high performance liquid chromatography (HPLC) detection sample
Test that the results are shown in Table 2.
The functional component content results of 60 days in 2 whitening mask of table
As shown in Table 2, whitening mask of the invention in closed container, under room temperature place 60 days after, functional component bear
Fruit glycosides, resorcinol derivatives and content of vitamin E without significant change, in comparative example 1~4 due to do not have to add bamboo-leaves flavones,
It is one or more in ganoderma spore polysaccharide and beeswax, in whitening mask of the white-skinned face function component content relative to embodiment 1
Content is low.Therefore, whitening mask provided by the invention is with good stability.
Embodiment 5
Whitening mask tests cutaneous sensibility
Whitening mask prepared by Example 1 and comparative example 1~5 carries out skin irritation test.
Take healthy rabbits 39, weight (2.0 ± 0.2) kg is randomly divided into 13 groups, every group of animal 3, before experiment for 24 hours
By rabbit skin of back both sides unhairing, check whether skin of unhairing is injured, and compromised skin is unfit to do skin irritation for 24 hours after unhairing
Experiment.The whitening mask 3 times using embodiment 1 and comparative example 1~5 is smeared daily, it is continuous to smear 7 days, observe skin condition, examination
It tests and the results are shown in Table 2.
The irritation test result of 3 whitening mask of table
"+" rabbit dermohemia, redness；" ++ " represents that congested, red and swollen phenomenon still exists, but have increase trend；"-" represents
Without congested, red and swollen phenomenon.
As shown in Table 3, the whitening mask and the whitening mask of comparative example 1~4 that embodiment 1 is prepared are due to being added to life
Rationality seawater reduces the stimulation of functional component in facial mask, improves tolerance of the skin to facial mask.And in comparative example 5 due to
Deionized water is used, the phenomenon that skin sensitivity occurs in continuous smear the 5th day, illustrates whitening mask provided by the invention
There is no irritation to sensitive skin.
Embodiment 6
The whitening effect experiment of whitening mask
The whitening mask of Example 1 and comparative example 1~5 carries out skin whitening efficacy evaluation test.
Choose 130 skin healths, without cosmetic allergic contact dermatitis history, volunteer of the age between 20~35 as subject,
Arm skin is divided into 13 groups, every group of 10 people are smeared obtained using embodiment 1 and comparative example 1~4 respectively as experimental subjects
Whitening mask.3 times a day, it is continuous to smear 60 days, skin whiteness is detected, result of the test is shown in Table 4.
The whitening result of the test of 4 whitening mask of table
The addition of bamboo-leaves flavones, ganoderma spore polysaccharide grade beeswax contained in the whitening mask of the present invention, it is effective to improve
The whitening effect of whitening mask.Wherein bamboo-leaves flavones have excellent tyrosinase activity inhibiting effect, high-efficiency antioxidant
Effect inhibits the activity of melanocyte and the generation of melanin well, while also is able to make the melanin of oxidation to restore, and improves
Whitening effect.Ganoderma spore polysaccharide effectively raises the anti-oxidant whitening of bamboo-leaves flavones while moistening effect is provided
Effect plays effective collaboration antioxidation.Ganoderma spore polysaccharide and beeswax can stablize the ursin in whitening mask
And the content of resorcinol derivatives, it is played the effect of ursin and resorcinol derivatives in whitening mask so as to ensure that,
Improve whitening effect.
As shown in Table 4, after whitening mask provided by the invention is applied to human skin, after long-time service, skin whiteness with
The extension of usage time and gradually increase, have apparent whitening effect.Due to being added to bamboo-leaves flavones and spirit in comparative example 1
Ganoderma lucidum spore polysaccharide, whitening mask obtained have preferable whitening effect, but have lacked the protection taste of beeswax relative to embodiment 1
Moisten effect, whitening effect is not as good as embodiment 1.Bamboo-leaves flavones are added in comparative example 2, leaf of bamboo Huang is not added with relative to embodiment 3
For ketone, whitening effect is preferable, but still unlike with embodiment 1 and comparative example 1.Ganoderma spore polysaccharide is added in comparative example 3, it is right
Ursin, resorcinol derivatives and vitamin E have certain protective role, to there is preferable whitening for comparative example 4
Effect.
To sum up, in whitening mask of the invention, bamboo-leaves flavones, ganoderma spore polysaccharide and beeswax are during the use of facial mask
Collaboration skin whitening effect is played, improves the whitening effect of facial mask, the reparation effect of comprehensive anti-ageing whitening is played to skin
Fruit.
It can be that professional and technical personnel in the field realize or use that the above embodiment, which is intended to illustrate the present invention, to above-mentioned
Embodiment is modified and be will be apparent for those skilled in the art, therefore the present invention includes but not limited to
The above embodiment, it is any to meet the claims or specification description, meet with principles disclosed herein and novelty,
The method of inventive features, technique, product, each fall within protection scope of the present invention.
Claims (10)
1. a kind of whitening mask, which is characterized in that comprising following weight percentage components：Bamboo-leaves flavones 0.01 ~ 2%, ganoderma lucidum spore
Sub- polysaccharide 0.01 ~ 5%, beeswax 0.01 ~ 1%, vitamin E 0.01 ~ 5%, ursin 0.05 ~ 5%, resorcinol derivatives 0.01 ~
2%th, liquid fatty 0.1 ~ 10%, surfactant 0.1% ~ 15%, polyalcohol 0.1 ~ 15% and surplus are physiological seawater.
2. whitening mask according to claim 1, which is characterized in that comprising following weight percentage components：The leaf of bamboo is yellow
Ketone 0.2 ~ 1%, ganoderma spore polysaccharide 0.2 ~ 2%, beeswax 0.05 ~ 0.8%, vitamin E 0.1 ~ 4%, ursin 0.1 ~ 4%, isophthalic two
Amphyl 0.1 ~ 1%, liquid fatty 0.3 ~ 8%, surfactant 1% ~ 10%, polyalcohol 1 ~ 10% and surplus physiological seawater.
3. whitening mask according to claim 1 or 2, which is characterized in that the resorcinol derivatives are included between hexyl
The mixture of one or more of benzenediol, Symwhite-337, dimethoxy-p base -4- propyl diphenol.
4. whitening mask according to claim 1 or 2, which is characterized in that the liquid fatty includes myristic acid glycerine
Ester, isopropyl myristate, Miglyol 812N, polyethylene glycol glyceryl laurate ester, glyceryl linoleate, propylene glycol list
Caprylate, two pungent capric acid propylene glycol esters, diethyl sebacate, isononyl isononanoate, propylene glycol dipelargonate and octyl dodecanol
The mixture of one or more of myristinate.
5. whitening mask according to claim 1 or 2, which is characterized in that the surfactant includes sorbierite bay
Acid esters, Crodaret, polyoxyethylene fatty acid ester, castor oil polyoxyethylene ether and polyoxyethylene sorbitan
The mixture of one or more of aliphatic ester.
6. whitening mask according to claim 1 or 2, which is characterized in that the polyalcohol includes polyethylene glycol, the third two
The mixture of one or more of alcohol, glycerine, 1,3 butylene glycol and 1,2- pentanediols.
7. the preparation method of any one of the claim 1-6 whitening mask, which is characterized in that include the following steps：
A. by physiological seawater high-temperature sterilization, when greenhouse cooling is to 65-85 DEG C, beeswax is dissolved thereto；
B. the liquid fatty, surfactant and polyalcohol are stirred 15-20 minutes at 80-85 DEG C；
C. the dissolving feed liquid step a obtained homogeneous together with the mixture that step b is obtained；
D. the material after homogeneous is cooled to 48-55 DEG C, adds in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin, isophthalic two
Amphyl and vitamin E, stir evenly, and adjust pH value to 5 ~ 7, are down to room temperature.
8. the preparation method of whitening mask according to claim 7, which is characterized in that for by institute the step of the high-temperature sterilization
Physiological seawater is stated to be kept stirring at 90-95 DEG C 15-20 minutes.
9. the preparation method of whitening mask according to claim 7, which is characterized in that the mixing speed of the step b is 40-
50 revs/min.
10. the preparation method of whitening mask according to claim 7, which is characterized in that homogeneous speed described in step c is
1200-1800 revs/min, homogenizing time is 3-5 minutes.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810223642.6A CN108143697A (en) | 2018-03-19 | 2018-03-19 | A kind of whitening mask and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810223642.6A CN108143697A (en) | 2018-03-19 | 2018-03-19 | A kind of whitening mask and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108938504A (en) * | 2018-09-30 | 2018-12-07 | 广西秀美壮乡能源环保有限公司 | A kind of Skin whitening care cosmetics and preparation method thereof |
| US20220370311A1 (en) * | 2021-05-24 | 2022-11-24 | Hangzhou shanshangshui Technology Co., Ltd | Application of hydrogen ion water and a mask containing hydrogen ion water |
-
2018
- 2018-03-19 CN CN201810223642.6A patent/CN108143697A/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108938504A (en) * | 2018-09-30 | 2018-12-07 | 广西秀美壮乡能源环保有限公司 | A kind of Skin whitening care cosmetics and preparation method thereof |
| CN108938504B (en) * | 2018-09-30 | 2021-05-07 | 台州中知英健机械自动化有限公司 | Whitening skin care product and preparation method thereof |
| US20220370311A1 (en) * | 2021-05-24 | 2022-11-24 | Hangzhou shanshangshui Technology Co., Ltd | Application of hydrogen ion water and a mask containing hydrogen ion water |
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Application publication date: 20180612 |