CN108142918A - 一种番茄红素微囊粉及其制备方法 - Google Patents
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Abstract
本发明公开了一种番茄红素微囊粉及其制备方法，由番茄红素、水解明胶、蔗糖、D‑Vc钠、吐温‑80、混合生育酚六种物质制备得到，具体是将水解明胶、蔗糖、D‑Vc钠加入热水中充分搅拌，冷却后加入吐温‑80、混合生育酚及番茄红素；经砂磨机搅拌研磨后继续用高压均质机均质一次使粒径更加均匀；将均质好的番茄红素乳液经喷雾干燥机干燥后得到番茄红素微囊粉。采用本发明方法得到的番茄红素微囊粉稳定性好且包埋率高达99％。
Description
技术领域
本发明属于保健食品领域，具体涉及一种番茄红素微囊粉及其制备方法。
背景技术
番茄红素是一种不含氧的类胡萝卜素。其分子式为C40H56，分子量为536.85，是迄今为止自然界中被发现的最强抗氧化剂之一，对防治前列腺疾病、前列腺癌、肺癌、胃癌、乳癌有奇效，有效抑制癌细胞的扩散和复制，被西方国家称为“植物黄金”。纯品为针状深红色晶体，在分子结构上有11个共轭双键和2个非共轭双键组成的直链型碳氢化合物，所以番茄红素易被氧化变质，大大影响其在食品、制药工业中的应用。现在市场上的番茄红素产品以番茄红素油树脂产品为主，其在加工终端产品时应用面有限，终端产品单一。鉴于以上问题，以及微囊技术可以解决番茄红素稳定性差、应用范围窄、生物利用度低等技术难题。故经过多次研究实验，不断的创新改良，设计出此次的制备方法。
现有技术仅使用高压均质机，即使多次均质，很难使颗粒均匀分散。
发明内容
本发明的目的是克服上述不足之处，提供一种具有高包埋率的番茄红素微囊粉。
本发明还有一个目的是提供上述番茄红素微囊粉的制备方法。
本发明的目的是通过以下方式实现的：
一种番茄红素微囊粉，该番茄红素微囊粉由以下重量份的组分制成：
水解明胶25～40份、蔗糖36～50份、D-Vc钠1～4份、番茄红素5～15份、吐温-80 1～4份、混合生育酚1～4份。
上述番茄红素微囊粉的生产方法包括如下操作步骤：
步骤一：将水解明胶、蔗糖、D-Vc钠加入60℃～80℃热水中搅拌充分；
步骤二：冷却后加入吐温-80、混合生育酚及番茄红素，搅拌均匀；
步骤三：将搅拌均匀的番茄红素水溶液加入到砂磨机中，充分研磨制成番茄红素初乳液；
步骤四：将番茄红素初乳液加入高压均质机中进行一次高压均质，制备成番茄红素乳液；
步骤五：将番茄红素乳液加入喷雾干燥机中喷雾干燥后得到番茄红素微囊粉。
上述番茄红素微囊粉的工艺生产方法的步骤三中，砂磨机转速为1500rpm～2000rpm。
上述步骤四中，高压均质压力为30～60MPa。
上述步骤五中，喷雾干燥设备进风温度160～180℃，进料温度40～60℃，出风温度70～90℃。
上述番茄红素微囊粉的制备方法具体为：
(1)将水解明胶25～40份、蔗糖36～50份、D-Vc钠1～4份加入到60℃～80℃热水中搅拌充分；
(2)冷却后加入吐温-80 1～4份、混合生育酚1～4份及番茄红素5～15份，搅拌均匀；
(3)将搅拌均匀的番茄红素水溶液加入到砂磨机中，1500rpm～2000rpm下充分研磨制成番茄红素初乳液；
(4)将番茄红素初乳液加入高压均质机中用压力为30～60MPa进行一次高压均质，制备成番茄红素乳液；
(5)将番茄红素乳液加入喷雾干燥机中干燥后得到番茄红素微囊粉，干燥条件为进风温度160～180℃，进料温度40～60℃，出风温度70～90℃。
研磨制成番茄红素初乳液的时间可以为10-60min。
与现有技术比较，本发明的有益效果：
(1)本发明方法先通过砂磨机研磨获得番茄红素初乳液，此时的初乳液均匀度较好，通过高压均质机均质后，颗粒粒度减小并且均匀度一致，形成更加稳定的乳液。
(2)本发明方法选用水解明胶和蔗糖作为壁材和填充剂，壁材水解明胶属于多肽类物质，能够将番茄红素包埋于其空间结构中。但是仅明胶的空间结构不严密，仍有部分氧气能进入其内部使番茄红素氧化变质，所以加入蔗糖作为填充物，填充其孔道，使网状结构更加严密。同时明胶分子中的氨基与蔗糖分子中的醛基可以发生交联反应，使膜具有更高的致密性，提高番茄红素微囊的效率。而只有在两者比例最佳时，包埋最紧密，如果增加蔗糖的比例，那么水解明胶的比例就要相应减少，此时部分番茄红素无法得到包埋，导致微囊化的效率降低。因此要严格控制二者的比例。添加少量吐温-80时，可取代界面膜上的部分多肽，从而降低乳液粒径，如果进一步加大吐温-80的量，界面膜上多肽属于劣势，膜强度降低，导致乳液的稳定性下降。本发明方法得到的番茄红素微囊粉稳定性好且包埋率可达99％。
下面将结合具体实施方式进一步说明本发明，但本发明要求保护的范围并不局限于下列实施方式。
具体实施方式
以下通过具体实施例进一步说明本发明。但实施例的具体细节仅用于解释本发明，不应理解为对本发明总的技术方案的限定。
实施例1：
番茄红素5重量份、水解明胶25重量份、蔗糖36重量份、D-Vc钠1重量份、吐温-801重量份、混合生育酚1重量份。
制备方法为：
(1)将水解明胶、蔗糖、D-Vc钠加入60℃～80℃热水中充分搅拌；
(2)冷却后加入吐温-80、混合生育酚及番茄红素，搅拌均匀；
(3)将搅拌均匀的番茄红素水溶液加入到砂磨机中，1500rpm下研磨20min制成番茄红素初乳液；
(4)将番茄红素初乳液加入高压均质机中用压力为30MPa进行一次高压均质，制备成番茄红素乳液；
(5)将番茄红素乳液加入喷雾干燥机中干燥后得到番茄红素微囊粉，喷雾干燥条件为进风温度160℃，进料温度40℃，出风温度70℃，得到粒径200目的微囊粉。
使用高效液相色谱法对得到的番茄红素微囊粉的包埋率进行检测，包埋率为99％。
实施例2：
番茄红素15重量份、水解明胶32重量份、蔗糖41重量份、D-Vc钠3重量份、吐温-803重量份、混合生育酚3重量份。
制备方法为：
(1)将水解明胶32份、蔗糖41份、D-Vc钠3份加入60℃～80℃热水中充分搅拌；
(2)冷却后加入吐温-80 3份、混合生育酚3份及番茄红素15份，搅拌均匀；
(3)将搅拌均匀的番茄红素水溶液加入到砂磨机中，1900rpm下研磨15min制成番茄红素初乳液；
(4)将番茄红素初乳液加入高压均质机中用压力为50MPa进行一次高压均质，制备成番茄红素乳液；
(5)将番茄红素乳液加入喷雾干燥机中干燥后得到番茄红素微囊粉，干燥条件为进风温度175℃，进料温度50℃，出风温度80℃，得到粒径120目的微囊粉。
使用高效液相色谱法对得到的番茄红素微囊粉的包埋率进行检测，包埋率为99％。
实施例3：
番茄红素10份、水解明胶40份、蔗糖50份、D-Vc钠4份、吐温-80 4份、混合生育酚4份。
制备方法为：
(1)将水解明胶40份、蔗糖50份、D-Vc钠4份加入60℃～80℃热水中充分搅拌；
(2)冷却后加入吐温-80 4份、混合生育酚4份及番茄红素10份，搅拌均匀；
(3)将搅拌均匀的番茄红素水溶液加入到砂磨机中，2000rpm下充分研磨制成番茄红素初乳液；
(4)将番茄红素初乳液加入高压均质机中用压力为60MPa进行一次高压均质，制备成番茄红素乳液；
(5)将番茄红素乳液加入喷雾干燥机中干燥后得到番茄红素微囊粉，干燥条件为进风温度180℃，进料温度60℃，出风温度90℃，得到粒径60目的微囊粉。
使用高效液相色谱法对得到的番茄红素微囊粉的包埋率进行检测，包埋率为99％。
Claims (5)
1.一种番茄红素微囊粉，其特征在于该番茄红素微囊粉由以下重量份的组分制成：
水解明胶25～40份、蔗糖36～50份、D-Vc钠1～4份、番茄红素5～15份、吐温-80 1～4份、混合生育酚1～4份。
2.一种权利要求1所述的番茄红素微囊粉的生产方法，其特征在于该包括如下操作步骤：
步骤一：将水解明胶、蔗糖、D-Vc钠加入60℃～80℃热水中搅拌充分；
步骤二：冷却后加入吐温-80、混合生育酚及番茄红素，搅拌均匀；
步骤三：将搅拌均匀的番茄红素水溶液加入到砂磨机中，充分研磨制成番茄红素初乳液；
步骤四：将番茄红素初乳液加入高压均质机中进行一次高压均质，制备成番茄红素乳液；
步骤五：将番茄红素乳液喷雾干燥后得到番茄红素微囊粉。
3.根据权利要求1所述的番茄红素微囊粉的工艺生产方法，其特征在于：所述步骤三中，砂磨机转速为1500rpm～2000rpm。
4.根据权利要求1所述的番茄红素微囊粉的工艺生产方法，其特征在于：所述步骤四中，高压均质压力为30～60MPa。
5.根据权利要求1所述的番茄红素微囊粉的工艺生产方法，其特征在于：所述步骤五中，喷雾干燥条件为：进风温度160～180℃，进料温度40～60℃，出风温度70～90℃。
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| CN101151300A (zh) * | 2005-05-31 | 2008-03-26 | 格利达股份公司 | 用于制备低分子量明胶水解产物的方法和明胶水解产物组合物 |
| CN103284290A (zh) * | 2013-05-24 | 2013-09-11 | 肇庆巨元生化有限公司 | 一种良好的类胡萝卜素的微囊化方法 |
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| CN101151300A (zh) * | 2005-05-31 | 2008-03-26 | 格利达股份公司 | 用于制备低分子量明胶水解产物的方法和明胶水解产物组合物 |
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