CN108136361B - 使用振荡流混合反应器合成有机过氧化物 - Google Patents

使用振荡流混合反应器合成有机过氧化物 Download PDF

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Publication number
CN108136361B
CN108136361B CN201680062469.5A CN201680062469A CN108136361B CN 108136361 B CN108136361 B CN 108136361B CN 201680062469 A CN201680062469 A CN 201680062469A CN 108136361 B CN108136361 B CN 108136361B
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flow
flow channel
reactor
oscillating
fluid communication
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Chinese (zh)
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CN108136361A (zh
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A.布卢姆
P.马吉
S.胡布
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Arkema France SA
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Arkema France SA
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/241—Stationary reactors without moving elements inside of the pulsating type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00033—Continuous processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)
CN201680062469.5A 2015-10-26 2016-10-26 使用振荡流混合反应器合成有机过氧化物 Active CN108136361B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1560186 2015-10-26
FR1560186A FR3042793B1 (fr) 2015-10-26 2015-10-26 Synthese de peroxydes organiques a l'aide d'un reacteur agite a ecoulement oscillatoire
PCT/EP2016/075834 WO2017072190A1 (en) 2015-10-26 2016-10-26 Synthesis of organic peroxydes using an oscillatory flow mixing reactor

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CN108136361A CN108136361A (zh) 2018-06-08
CN108136361B true CN108136361B (zh) 2020-07-07

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US (1) US10449509B2 (enExample)
EP (2) EP3368209B1 (enExample)
JP (1) JP6854802B2 (enExample)
CN (1) CN108136361B (enExample)
FR (1) FR3042793B1 (enExample)
MX (1) MX2018004424A (enExample)
WO (1) WO2017072190A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109553560A (zh) 2017-08-12 2019-04-02 上海惠和化德生物科技有限公司 一种由醇或烷烃直接制备有机过氧化物的在线全连续流生产工艺
WO2019034006A1 (zh) * 2017-08-12 2019-02-21 上海惠和化德生物科技有限公司 一种由醇或烷烃直接制备有机过氧化物的在线全连续流生产工艺
BE1026312B1 (nl) 2018-05-25 2019-12-23 Ajinomoto Omnichem Doorstroomreactor en gebruik ervan
GB201811402D0 (en) * 2018-07-12 2018-08-29 Alconbury Weston Ltd Liquid process assembly
JP7143257B2 (ja) * 2018-07-12 2022-09-28 株式会社神戸製鋼所 反応器及びこれを備えた反応器システム
US10807947B2 (en) * 2018-12-05 2020-10-20 Saudi Arabian Oil Company Controlled catalytic oxidation of MEROX process by-products in integrated refinery process
CN109541248B (zh) * 2018-12-11 2023-09-15 苏州英赛斯智能科技有限公司 一种流动注射反应池装置和用于此装置的换向流体单元
CN109776376B (zh) * 2019-03-15 2024-12-06 湘潭大学 连续合成4-溴-2-对氯-5-三氟甲基吡咯-3-腈的装置及合成方法
CN121623650B (zh) * 2026-02-05 2026-04-14 东营华泰化工集团有限公司 一种适用于dtbp微反应的多原料精准配比混合装置

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4444961A (en) * 1980-10-30 1984-04-24 The Dow Chemical Company Process and apparatus for preparing uniform size polymer beads
WO2012095176A1 (en) * 2011-01-13 2012-07-19 Dsm Ip Assets B.V. Oscillating flow minireactor
CN103562145A (zh) * 2010-12-06 2014-02-05 塔邦生物系统公司 生物制品的连续加工方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3167395A (en) * 1958-08-26 1965-01-26 Union Carbide Corp Resonating pulse reactor
US4075236A (en) * 1976-09-30 1978-02-21 Pennwalt Corporation Continuous manufacture of peroxyesters
DD128663A1 (de) 1976-12-13 1977-11-30 Dietmar Rossner Verfahren zur kontinuierlichen herstellung von perestern
CA1123578A (en) 1979-11-20 1982-05-18 Frank Souhrada Process and apparatus for the prevention of solids deposits in a tubular reactor
EP0540180B1 (en) * 1991-10-26 1995-12-13 The British Petroleum Company P.L.C. Process for producing polyolefins
DE19634450A1 (de) * 1996-08-26 1998-03-05 Basf Ag Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen
AU3720099A (en) 1998-04-28 1999-11-16 Heriot-Watt University Method and apparatus for phase separated synthesis
JP5069827B2 (ja) * 2001-02-28 2012-11-07 株式会社ダイセル 反応制御方法および制御装置
EE200400060A (et) * 2004-02-25 2005-10-17 Nordic Alternative Energy OÜ Meetod ja seade karboksüülhapete estrite pidevaprotsessiliseks transesterifikatsioonikssuperkriitilises monovalentses alkoholis
DE102005009322A1 (de) 2005-03-01 2006-09-14 Degussa Ag Durchmischungsreaktor
DE102005049294C5 (de) * 2005-10-14 2012-05-03 Ehrfeld Mikrotechnik Bts Gmbh Verfahren zur Herstellung organischer Peroxide mittels Mikroreaktionstechnik
EP1852418A1 (en) 2006-04-27 2007-11-07 Arkema France Process for synthesizing selected organic peroxides
DE102006032165A1 (de) * 2006-07-12 2008-01-24 Evonik Degussa Gmbh Kontinuierliches Verfahren zur Herstellung von Acylperoxiden
DE102006032166B4 (de) * 2006-07-12 2018-08-02 Evonik Degussa Gmbh Verfahren zur Herstellung von Acylperoxiden
JP5109004B1 (ja) * 2011-11-11 2012-12-26 マイクロ波化学株式会社 化学反応装置
DE102012216945A1 (de) * 2012-09-21 2014-05-28 Ehrfeld Mikrotechnik Bts Gmbh Verfahren und Vorrichtung zur Herstellung organischer Peroxide mittels Millireaktionstechnik
US9550731B2 (en) * 2014-05-22 2017-01-24 Honeywell Federal Manufacturing & Technologies, Llc Method for phase transfer synthesis of organic peroxides

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4444961A (en) * 1980-10-30 1984-04-24 The Dow Chemical Company Process and apparatus for preparing uniform size polymer beads
CN103562145A (zh) * 2010-12-06 2014-02-05 塔邦生物系统公司 生物制品的连续加工方法
CN105107228A (zh) * 2010-12-06 2015-12-02 颇尔公司 生物制品的连续加工方法
WO2012095176A1 (en) * 2011-01-13 2012-07-19 Dsm Ip Assets B.V. Oscillating flow minireactor

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Publication number Publication date
JP2018538234A (ja) 2018-12-27
JP6854802B2 (ja) 2021-04-07
FR3042793A1 (enExample) 2017-04-28
MX2018004424A (es) 2018-05-11
EP3368209B1 (en) 2021-03-17
WO2017072190A1 (en) 2017-05-04
FR3042793B1 (fr) 2019-12-27
CN108136361A (zh) 2018-06-08
EP3368209A1 (en) 2018-09-05
US20180304227A1 (en) 2018-10-25
US10449509B2 (en) 2019-10-22
EP3838399A1 (en) 2021-06-23

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