CN108136361B - 使用振荡流混合反应器合成有机过氧化物 - Google Patents
使用振荡流混合反应器合成有机过氧化物 Download PDFInfo
- Publication number
- CN108136361B CN108136361B CN201680062469.5A CN201680062469A CN108136361B CN 108136361 B CN108136361 B CN 108136361B CN 201680062469 A CN201680062469 A CN 201680062469A CN 108136361 B CN108136361 B CN 108136361B
- Authority
- CN
- China
- Prior art keywords
- flow
- flow channel
- reactor
- oscillating
- fluid communication
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/241—Stationary reactors without moving elements inside of the pulsating type
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/248—Reactors comprising multiple separated flow channels
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00027—Process aspects
- B01J2219/00033—Continuous processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00164—Controlling or regulating processes controlling the flow
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1560186A FR3042793B1 (fr) | 2015-10-26 | 2015-10-26 | Synthese de peroxydes organiques a l'aide d'un reacteur agite a ecoulement oscillatoire |
| FR1560186 | 2015-10-26 | ||
| PCT/EP2016/075834 WO2017072190A1 (en) | 2015-10-26 | 2016-10-26 | Synthesis of organic peroxydes using an oscillatory flow mixing reactor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108136361A CN108136361A (zh) | 2018-06-08 |
| CN108136361B true CN108136361B (zh) | 2020-07-07 |
Family
ID=55135339
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201680062469.5A Active CN108136361B (zh) | 2015-10-26 | 2016-10-26 | 使用振荡流混合反应器合成有机过氧化物 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10449509B2 (OSRAM) |
| EP (2) | EP3838399A1 (OSRAM) |
| JP (1) | JP6854802B2 (OSRAM) |
| CN (1) | CN108136361B (OSRAM) |
| FR (1) | FR3042793B1 (OSRAM) |
| MX (1) | MX2018004424A (OSRAM) |
| WO (1) | WO2017072190A1 (OSRAM) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109553560A (zh) | 2017-08-12 | 2019-04-02 | 上海惠和化德生物科技有限公司 | 一种由醇或烷烃直接制备有机过氧化物的在线全连续流生产工艺 |
| WO2019034006A1 (zh) * | 2017-08-12 | 2019-02-21 | 上海惠和化德生物科技有限公司 | 一种由醇或烷烃直接制备有机过氧化物的在线全连续流生产工艺 |
| BE1026312B1 (nl) * | 2018-05-25 | 2019-12-23 | Ajinomoto Omnichem | Doorstroomreactor en gebruik ervan |
| WO2020013022A1 (ja) * | 2018-07-12 | 2020-01-16 | 株式会社神戸製鋼所 | 反応器及びこれを備えた反応器システム |
| GB201811402D0 (en) * | 2018-07-12 | 2018-08-29 | Alconbury Weston Ltd | Liquid process assembly |
| US10807947B2 (en) * | 2018-12-05 | 2020-10-20 | Saudi Arabian Oil Company | Controlled catalytic oxidation of MEROX process by-products in integrated refinery process |
| CN109541248B (zh) * | 2018-12-11 | 2023-09-15 | 苏州英赛斯智能科技有限公司 | 一种流动注射反应池装置和用于此装置的换向流体单元 |
| CN109776376B (zh) * | 2019-03-15 | 2024-12-06 | 湘潭大学 | 连续合成4-溴-2-对氯-5-三氟甲基吡咯-3-腈的装置及合成方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4444961A (en) * | 1980-10-30 | 1984-04-24 | The Dow Chemical Company | Process and apparatus for preparing uniform size polymer beads |
| WO2012095176A1 (en) * | 2011-01-13 | 2012-07-19 | Dsm Ip Assets B.V. | Oscillating flow minireactor |
| CN103562145A (zh) * | 2010-12-06 | 2014-02-05 | 塔邦生物系统公司 | 生物制品的连续加工方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3167395A (en) * | 1958-08-26 | 1965-01-26 | Union Carbide Corp | Resonating pulse reactor |
| US4075236A (en) * | 1976-09-30 | 1978-02-21 | Pennwalt Corporation | Continuous manufacture of peroxyesters |
| DD128663A1 (de) | 1976-12-13 | 1977-11-30 | Dietmar Rossner | Verfahren zur kontinuierlichen herstellung von perestern |
| CA1123578A (en) | 1979-11-20 | 1982-05-18 | Frank Souhrada | Process and apparatus for the prevention of solids deposits in a tubular reactor |
| EP0540180B1 (en) * | 1991-10-26 | 1995-12-13 | The British Petroleum Company P.L.C. | Process for producing polyolefins |
| DE19634450A1 (de) * | 1996-08-26 | 1998-03-05 | Basf Ag | Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen |
| US6429268B1 (en) | 1998-04-28 | 2002-08-06 | Heriot-Watt University | Method and apparatus for phase separated synthesis |
| JP5069827B2 (ja) * | 2001-02-28 | 2012-11-07 | 株式会社ダイセル | 反応制御方法および制御装置 |
| EE200400060A (et) * | 2004-02-25 | 2005-10-17 | Nordic Alternative Energy OÜ | Meetod ja seade karboksüülhapete estrite pidevaprotsessiliseks transesterifikatsioonikssuperkriitilises monovalentses alkoholis |
| DE102005009322A1 (de) | 2005-03-01 | 2006-09-14 | Degussa Ag | Durchmischungsreaktor |
| DE102005049294C5 (de) * | 2005-10-14 | 2012-05-03 | Ehrfeld Mikrotechnik Bts Gmbh | Verfahren zur Herstellung organischer Peroxide mittels Mikroreaktionstechnik |
| EP1852418A1 (en) | 2006-04-27 | 2007-11-07 | Arkema France | Process for synthesizing selected organic peroxides |
| DE102006032165A1 (de) | 2006-07-12 | 2008-01-24 | Evonik Degussa Gmbh | Kontinuierliches Verfahren zur Herstellung von Acylperoxiden |
| DE102006032166B4 (de) * | 2006-07-12 | 2018-08-02 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Acylperoxiden |
| JP5109004B1 (ja) * | 2011-11-11 | 2012-12-26 | マイクロ波化学株式会社 | 化学反応装置 |
| DE102012216945A1 (de) * | 2012-09-21 | 2014-05-28 | Ehrfeld Mikrotechnik Bts Gmbh | Verfahren und Vorrichtung zur Herstellung organischer Peroxide mittels Millireaktionstechnik |
| US9550731B2 (en) * | 2014-05-22 | 2017-01-24 | Honeywell Federal Manufacturing & Technologies, Llc | Method for phase transfer synthesis of organic peroxides |
-
2015
- 2015-10-26 FR FR1560186A patent/FR3042793B1/fr active Active
-
2016
- 2016-10-26 CN CN201680062469.5A patent/CN108136361B/zh active Active
- 2016-10-26 US US15/768,684 patent/US10449509B2/en active Active
- 2016-10-26 JP JP2018504154A patent/JP6854802B2/ja not_active Expired - Fee Related
- 2016-10-26 EP EP21156602.1A patent/EP3838399A1/en not_active Withdrawn
- 2016-10-26 MX MX2018004424A patent/MX2018004424A/es unknown
- 2016-10-26 EP EP16787846.1A patent/EP3368209B1/en active Active
- 2016-10-26 WO PCT/EP2016/075834 patent/WO2017072190A1/en not_active Ceased
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4444961A (en) * | 1980-10-30 | 1984-04-24 | The Dow Chemical Company | Process and apparatus for preparing uniform size polymer beads |
| CN103562145A (zh) * | 2010-12-06 | 2014-02-05 | 塔邦生物系统公司 | 生物制品的连续加工方法 |
| CN105107228A (zh) * | 2010-12-06 | 2015-12-02 | 颇尔公司 | 生物制品的连续加工方法 |
| WO2012095176A1 (en) * | 2011-01-13 | 2012-07-19 | Dsm Ip Assets B.V. | Oscillating flow minireactor |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2017072190A1 (en) | 2017-05-04 |
| FR3042793B1 (fr) | 2019-12-27 |
| EP3368209B1 (en) | 2021-03-17 |
| US10449509B2 (en) | 2019-10-22 |
| MX2018004424A (es) | 2018-05-11 |
| EP3838399A1 (en) | 2021-06-23 |
| EP3368209A1 (en) | 2018-09-05 |
| JP6854802B2 (ja) | 2021-04-07 |
| CN108136361A (zh) | 2018-06-08 |
| US20180304227A1 (en) | 2018-10-25 |
| FR3042793A1 (OSRAM) | 2017-04-28 |
| JP2018538234A (ja) | 2018-12-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108136361B (zh) | 使用振荡流混合反应器合成有机过氧化物 | |
| US7968753B2 (en) | Method for the production of organic peroxides by means of a microreaction technique | |
| Bianchi et al. | Oscillatory flow reactors for synthetic chemistry applications | |
| McGlone et al. | Oscillatory flow reactors (OFRs) for continuous manufacturing and crystallization | |
| US20100036152A1 (en) | Continuous Method for Producing Acyl Peroxides | |
| US6838061B1 (en) | Reactor for carrying out gas-liquid, liquid, liquid-liquid or gas-liquid-solid chemical reactions | |
| CN101479239A (zh) | 用于合成选定的有机过氧化物的方法 | |
| CA2733326C (en) | Parallelized jet loop reactors | |
| CA2658018C (en) | Mixing apparatus and process | |
| CA2693422C (en) | System and process for production of polyvinyl chloride | |
| EA024431B1 (ru) | Способ и система получения полимеров, в частности полиэтилена и полипропилена | |
| US7410620B2 (en) | Apparatus for continuous production of polymers in carbon dioxide | |
| EP1248807A1 (en) | Continuous process for making polymers in carbon dioxide | |
| US20090005608A1 (en) | High shear process for cyclohexanol production | |
| EP2010575B1 (en) | Process of free-radical polymerization or crosslinking in the presence of a selected organic peroxide prepared by an ex situ process | |
| WO2018145660A1 (zh) | 一种2-甲基-1,4-萘醌的全连续流合成工艺 | |
| US9550731B2 (en) | Method for phase transfer synthesis of organic peroxides | |
| Ala et al. | A comprehensive study on the synthesis of highly pure dicetyl peroxydicarbonate in a microreactor | |
| CN114426459A (zh) | 一种环己烷氧化制ka油的装置和方法 | |
| JPH03103408A (ja) | 塩化ビニル樹脂の重合装置および製造方法 | |
| CN117510388A (zh) | 一种利用微反应器连续合成二叔丁基过氧化物的方法 | |
| CN114555218A (zh) | 醛醇缩合反应用连续搅拌釜反应器 | |
| WO2020230491A1 (ja) | 小流量フロー反応に適した化学反応システム及び装置 | |
| de Souza | Continuous flow: a transformative technology | |
| Loewe | Synthesis of Ionic Liquids in Microstructured Reactors–a Brief Introduction |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |