CN108125901A - A kind of whitening foundation emulsion with anti-ageing effect and preparation method thereof - Google Patents
A kind of whitening foundation emulsion with anti-ageing effect and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses a kind of whitening foundation emulsions with anti-ageing effect and preparation method thereof.The whitening foundation emulsion includes following component:Bamboo-leaves flavones 0.01 ~ 2%, ganoderma spore polysaccharide 0.01 ~ 5%, beeswax 0.01 ~ 1%, vitamin E 0.01 ~ 5%, ursin 0.05 ~ 5%, resorcinol derivatives 0.01 ~ 2%, liquid fatty 0.1 ~ 10%, surfactant 0.1% ~ 15%, polyalcohol 0.1 ~ 15%, Nano pearl powder 1 ~ 15%, chromatic timing powder 0.1 ~ 5% and surplus physiological seawater.The whitening foundation emulsion of the present invention moistens delaying skin aging, and antiallergy, whitening effect are notable, easy to use suitable for various skin crowds.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of whitening foundation emulsion and its preparation with anti-ageing effect
Method.
Background technology
With the development of society, the improvement of people's living standards, requirement of the women to cosmetics also becomes higher and higher, perhaps
The people more to like to be beautiful be to the care of oneself skin it is careful to the utmost.It is ultraviolet in dust dirty air, sunlight but in metropolis
Line, computer radiate, the coloured and dazzling color make-up that also we change daily, are all the formidable enemies of delicate skin, accelerate declining for skin
Always.Therefore, many women usually smear one layer of foundation emulsion when going out in face, and these above-mentioned pollution sources " insulation ", from
And delayed the aging of skin, play the role of maintenance.It also is able to cover the flaw of face, face is made to seem clean and tidy beautiful.
The existing foundation emulsion frost effects focused on isolation and hide the flaw, prolonged isolation also prevent skin from normally exhaling more
It inhales, leads to a variety of skin problems, it is such as dry, coarse, do not have elastic, dim mute, the coarse skin disorder of pore the synthesis of the colour of skin
Problem.Although skin care item in the market are very abundant, it can not always be solved well in face of this global question, make skin
Increasingly tend to aging.
Invention content
Based on whitening foundation emulsion in the prior art there are the problem of, the present invention provides a kind of whitenings with anti-ageing effect
Foundation emulsion, the whitening foundation emulsion is while being isolated and hiding the flaw, additionally it is possible to which balance skin water and oil balance, carries delaying skin aging
The multi-efficiencies such as high skin water profit, fine and smooth soft, long-acting persistently moist whitening effect.The present invention also provides above-mentioned whitening foundation creams
The preparation method of liquid.
Technical scheme is as follows:
A kind of whitening foundation emulsion with anti-ageing effect, comprising following weight percentage components:Bamboo-leaves flavones 0.01~
2%th, ganoderma spore polysaccharide 0.01~5%, beeswax 0.01~1%, vitamin E 0.01~5%, ursin 0.05~5%,
Hydroquinone derivatives 0.01~2%, liquid fatty 0.1~10%, surfactant 0.1%~15%, polyalcohol 0.1~
15%th, the physiological seawater of Nano pearl powder 1~15%, chromatic timing powder 0.1~5% and surplus.
Preferably, whitening foundation emulsion of the invention, comprising following weight percentage components:Bamboo-leaves flavones 0.2~1%,
Ganoderma spore polysaccharide 0.2~2%, beeswax 0.05~0.8%, vitamin E 0.1~4%, ursin 0.1~4%, resorcinol
Derivative 0.5~2%, liquid fatty 0.3~8%, surfactant 1%~10%, polyalcohol 2~10%, Nano pearl powder 5
~10%, chromatic timing powder 0.5~2% and the physiological seawater of surplus.
Preferably, the resorcinol derivatives include hexyl resorcin, Symwhite-337, dimethoxy-p
The mixture of one or more of base -4- propyl diphenol.
Preferably, the liquid fatty includes myristic acid glyceride, isopropyl myristate, Caprylic Capric three
Ester, polyethylene glycol glyceryl laurate ester, glyceryl linoleate, Sefsol 218, two pungent capric acid propylene glycol esters, decanedioic acid two
The mixture of one or more of ethyl ester, isononyl isononanoate, propylene glycol dipelargonate and octyl dodecanol myristinate.
Preferably, the surfactant includes sorbitan laurate, Crodaret, polyoxyethylene fat
The mixture of one or more of fat acid esters, castor oil polyoxyethylene ether and polyoxyethylene sorbitan fatty acid ester.
Preferably, the polyalcohol is included in polyethylene glycol, propylene glycol, glycerine, 1,3-BDO and 1,2- pentanediol
One or more of mixtures.
The invention also includes the preparation methods of whitening foundation emulsion described in any of the above-described technical solution, include the following steps:
A. by physiological seawater high-temperature sterilization, when greenhouse cooling is to 65-85 DEG C, beeswax is dissolved thereto;
B. after the Nano pearl powder and chromatic timing powder mixing milling, with the liquid fatty, surfactant and polynary
Alcohol stirs 15-20 minutes at 80-85 DEG C;
C. the dissolving feed liquid step a obtained homogeneous together with the mixture that step b is obtained;
D. the material after homogeneous is cooled to 48-55 DEG C, add in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin,
Hydroquinone derivatives and vitamin E, stir evenly, and are down to room temperature.
Preferably, the step of high-temperature sterilization is that the physiological seawater is kept stirring to 15-20 points at 90-95 DEG C
Clock.
Preferably, mixing speed is 40-50 revs/min in the step b.
Preferably, homogeneous speed described in step c is 1200-1800 revs/min, and homogenizing time is 3-5 minutes.
Relative to the prior art, the present invention has the following advantages:
Whitening composition and the benefit with moisturizing effect there are many containing in whitening foundation emulsion of the invention with anti-ageing effect
Water antioxidant content, wherein, whitening composition includes ursin, resorcinol derivatives, vitamin E and Nano pearl powder, moisturizing
Antioxidant content includes bamboo-leaves flavones, ganoderma spore polysaccharide, beeswax, vitamin E and physiological seawater.The moisturizing antioxygen of the present invention
Chemical conversion divides the ingredients such as bamboo-leaves flavones, ganoderma spore polysaccharide to play collaboration skin whitening effect during the use of foundation emulsion, carries
The high whitening effect of foundation emulsion plays skin the repairing effect of comprehensive anti-ageing whitening.
In the whitening composition of foundation emulsion of the present invention, ursin and resorcinol derivatives are unstable to light, temperature and pH value,
Easy in inactivation and then its effect can not be played during storage.Bamboo-leaves flavones and vitamin E are added in foundation emulsion, in foundation emulsion
While whitening composition inhibits melanin formation, already oxidised melanin is restored, has played synergistic effect, it will be apparent that enhance
White-skinned face function.Ganoderma spore polysaccharide and beeswax there is certain protection to make the stability of ursin and resorcinol derivatives
With improving the tolerance of ursin and resorcinol derivatives to light, temperature and pH value, ensure that U.S. of foundation emulsion of the present invention
White effect extends the shelf life of foundation emulsion of the present invention.
The use of physiological seawater improves the various trace elements in foundation emulsion, also has sterilization, antiallergy and anti-inflammatory
Effect, improve the isolation effect of foundation emulsion, the foundation emulsion of the present invention made to be equally applicable to sensitive skin, improves the present invention
The safety in utilization of foundation emulsion and target user.
The whitening foundation emulsion of the present invention complies fully with country's promulgation《Cosmetics health specification》Items in (2007 editions)
Index does not contain any noxious material.It can individually be used coated on skin, be mainly used for face and neck.The whitening powder of the present invention
Bottom liquid moistens delaying skin aging, and antiallergy, whitening effect are notable, easy to use suitable for various skin crowds.
Specific embodiment
The present invention provides a kind of whitening foundation emulsion with anti-ageing effect, comprising following weight percentage components:Bamboo
Leaf flavones 0.01~2%, ganoderma spore polysaccharide 0.01~5%, beeswax 0.01~1%, vitamin E 0.01~5%, ursin
0.05~5%, resorcinol derivatives 0.01~2%, liquid fatty 0.1~10%, surfactant 0.1%~15%, more
First alcohol 0.1~15%, Nano pearl powder 1~15%, chromatic timing powder 0.1~5% and surplus physiological seawater.
The whitening foundation emulsion of the present invention includes 0.01~2% bamboo-leaves flavones that mass percentage is, preferably 0.2~
1%, more preferably 0.3~0.8%.Bamboo-leaves flavones are a kind of safe and efficient biological anti-oxidants, can remove human skin
Active oxidation free radical prevents biomembrane lipid from being aoxidized by superoxide radical and hydroxyl radical free radical, plays effective antioxidant and anti-aging
Effect.Meanwhile the high-efficiency antioxidant of bamboo-leaves flavones, it is compounded with ganoderma spore polysaccharide, its antioxidant activity can be enhanced, added
The effect of collaboration whitening is played in the melanin reduction of speed oxidation.The present invention is not particularly limited the source of bamboo-leaves flavones, uses
Commercially available bamboo-leaves flavones are voluntarily extracted or used to conventional method in this field.
The whitening foundation emulsion of the present invention includes 0.01~5% ganoderma spore polysaccharide that mass percentage is, preferably
It is 0.2~2%, more preferably 0.3~1.5%.Ganoderma spore polysaccharide has excellent moistening effect, and performance of keeping humidity will be due to
Hyaluronic acid.In the present invention, ganoderma spore polysaccharide is other than its performance of keeping humidity, also for U.S. unstable to external environment
Bai Chengfen ursin and resorcinol derivatives have certain protective effect, slow down ursin and resorcinol derivatives exist
Loss of activity in poor environment ensure that the whitening effect of whitening foundation emulsion of the present invention.The present invention is to ganoderma spore polysaccharide
Source is not particularly limited, and commercially available Reishi sporule is voluntarily extracted or used using the conventional method in this field.
The whitening foundation emulsion of the present invention includes mass percentage for 0.01~1% beeswax, preferably 0.05~
0.8%, more preferably 0.1~0.5%.The nutrition of beeswax energy and improvement subcutaneous tissue situation, activate its elastic fibers, prevent that it is hard
Change, promote skin soft and moist, reduce wrinkle.Since beeswax has temperature very strong tolerance, added in the foundation emulsion of the present invention
Beeswax can effectively keep the state of active ingredient and the tolerance to temperature in foundation emulsion, especially can effectively maintain powder
Labile element in the liquid whitening composition of bottom such as ursin and resorcinol derivatives, improves the active constituent in storage
In shelf-life, ensure the whitening effect of foundation emulsion of the present invention.The beeswax of the present invention is preferably commercially available beeswax product.
The whitening foundation emulsion of the present invention includes mass percentage for 0.01~5% vitamin E, preferably 0.1~
4%, more preferably 1~3%.Vitamin E can react with free radical, provide hydrogen ion to free radical, realize anti-oxidant
Effect, can will be restored back by the melanin aoxidized, realize the gradually whitening of skin.In addition to having very strong inoxidizability
Outside, it can also moisturize the skin, promote skin metabolism.
The whitening foundation emulsion of the present invention includes mass percentage for 0.05~5% ursin, preferably 0.1~
4%, more preferably 1~3%.Ursin can prevent the generation of melanin by inhibiting the activity of internal tyrosinase, so as to
Skin pigmentation, dispelling stain and freckle are reduced, while also has the effect of sterilization, anti-inflammatory.But ursin is quicker to pH value
Sense is easily decomposed under alkaline condition.Beeswax is added in the foundation emulsion of the present invention, can effectively maintain the pH stable of foundation emulsion
In the range of 5~7, it effectively prevent the decomposition of ursin.
The whitening foundation emulsion of the present invention includes the resorcinol derivatives that mass percentage is 0.01~2%, preferably
It is 0.1~1%, more preferably 0.2~0.5%.In the present invention, the resorcinol derivatives preferably include hexylresorcinol two
The mixture of one or more of phenol, Symwhite-337, dimethoxy-p base -4- propyl diphenol.In this hair
In bright, to the mass ratioes of resorcinol derivatives various in mixture there is no limit.Resorcinol derivatives have excellent U.S.
White effect is one of highest tyrosinase inhibitor of activity having been reported that, and then inhibits the formation of melanin.But due to
Hydroquinone derivatives are to light, thermally labile, and resorcinol derivatives content can reduce rapidly in storage is prepared, Wu Fafa
Wave its effect.The present invention has delayed resorcinol to light, heat by being added to ganoderma spore polysaccharide and beeswax in foundation emulsion
Unstability ensure that the whitening effect of foundation emulsion Resorcino derivative in storage.
The whitening foundation emulsion of the present invention includes mass percentage for 0.1%~10% liquid fatty, and preferably 0.3%
~8%, more preferably 0.5%~4%.In the present invention, the liquid fatty preferably includes myristic acid glyceride, nutmeg
Isopropyl propionate, Miglyol 812N, polyethylene glycol glyceryl laurate ester, glyceryl linoleate, Sefsol 218, two
Pungent capric acid propylene glycol ester, diethyl sebacate, isononyl isononanoate, propylene glycol dipelargonate and octyl dodecanol myristinate
One or more of mixture.In the present invention, to the mass ratio of liquid fatties various in mixture, there is no limit.This hair
Long carbon chain aliphatic acid and the esters of middle Long carbon chain unsaturated alcohol generation, have natural moisture preserving and reparation during bright liquid fatty is selected
Effect, and suitable for a plurality of types of skin.Some physicochemical properties of liquid fatty are very similar to human skin surface layer
Substance can well be mixed with the lipid in skin, reduced the water loss of skin surface and then kept humidity of skin.The present invention
The source of liquid fatty is not limited, using commercial liquid lipid.
Whitening foundation emulsion provided by the invention includes the surfactant that mass percentage is 0.1%~15.0%,
Preferably 1%~10%, more preferably 2%~8%.In the present invention, the surfactant include sorbitan laurate,
Crodaret, polyoxyethylene fatty acid ester, castor oil polyoxyethylene ether, polyoxyethylene sorbitan aliphatic acid
The mixture of one or more of ester.In the present invention, to the mass ratio of surfactants various in mixture, there is no limit.
Surfactant in the present invention selects nonionic surface active agent, small toxicity small to skin irritation, increase effect into
Divide the dissolubility in foundation emulsion manufacturing process, improve the content of functional component.The permeability of foundation emulsion can also be enhanced simultaneously,
Functional component is promoted to enter skin, and then plays anti-ageing skin whitening effect.
Whitening foundation emulsion provided by the invention includes the polyalcohol that mass percentage is 0.1%~15.0%, preferably
1%~10%, more preferably 3%~8%.In the present invention, the polyalcohol preferably include polyethylene glycol, propylene glycol, glycerine,
The mixture of one or more of 1,3 butylene glycol and 1,2- pentanediols.In the present invention, to polyalcohols various in mixture
Mass ratio there is no limit.Polyalcohol has good solubilizing effect to functional component, can improve functional component in foundation emulsion
Content.In addition polyalcohol can adsorb the polar end in surfactant, can also be embedded in the chain of surfactant, so as to enhance table
The film that face activating agent is formed in oil-water interfaces, and then enhance the stability of foundation emulsion.
Whitening foundation emulsion provided by the invention includes the Nano pearl powder that mass percentage is 1%~15%, preferably
5%~10%, more preferably 6%~9%.Amino acid and mineral matter element there are many containing in Nano pearl powder, pass through enhancement of SOD
Activity play the role of anti-aging, allow skin refreshing it is soft and smooth, it is pale can people.Nano pearl powder uses commercially available receiving in this field
Rice pearl powder.
Whitening foundation emulsion provided by the invention includes the chromatic timing powder that mass percentage is 0.1%~5%, preferably
0.5%~2%, more preferably 1%~1.5%.Chromatic timing powder is used to adjust the coloration of foundation emulsion, is suitable for foundation emulsion different
The colour of skin.Chromatic timing powder uses the commercial goods of this field.
Whitening foundation emulsion provided by the invention further includes the physiological seawater of surplus.The use of physiological seawater improves powder
Various trace elements in the liquid of bottom also have the effect of sterilization, antiallergy and anti-inflammatory, improve the isolation effect of foundation emulsion, make
The foundation emulsion of the present invention is equally applicable to sensitive skin, improves safety in utilization and the target user of foundation emulsion of the present invention.
The present invention also provides the preparation methods of whitening foundation emulsion described in above-mentioned technical proposal, include the following steps:
A. by physiological seawater high-temperature sterilization, when greenhouse cooling is to 65-85 DEG C, beeswax is dissolved thereto;
B. after the Nano pearl powder and chromatic timing powder mixing milling, with the liquid fatty, surfactant and polynary
Alcohol stirs 15-20 minutes at 80-85 DEG C;
C. the dissolving feed liquid step a obtained homogeneous together with the mixture that step b is obtained;
D. the material after homogeneous is cooled to 48-55 DEG C, add in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin,
Hydroquinone derivatives and vitamin E, stir evenly, and are down to room temperature.
In the present invention, the physiological seawater high-temperature sterilization is preferably a step the physiological seawater at 90-95 DEG C
It is kept stirring 15-20 minutes, is stirred 16~18 minutes more preferably at 92-93 DEG C.The temperature of preferably physiological seawater of the invention
When degree is down to 70~80 DEG C, beeswax is dissolved.
The present invention is by Nano pearl powder and chromatic timing powder mixing milling.The present invention is not particularly limited the mode of milling, adopts
With the conventional milling mode in this field.It is preferred that by Nano pearl powder and chromatic timing powder 1~5min of milling in colloid mill, more
Preferably 2~4min.The mixed powder that milling is obtained is mixed with the liquid fatty, surfactant and polyalcohol, excellent
81-84 DEG C is selected in stir 16-18 minutes.It is preferred that the speed stirred is 40-50 revs/min, more preferably 43~48 revs/min.
Present invention homogeneous together with the mixture that step b is obtained by dissolving feed liquid that step a is obtained.The present invention is to homogeneous
Method is not particularly limited, preferably described homogeneous speed be 1200-1800 revs/min, more preferably 1400-1700 revs/min,
Homogenizing time is preferably 3-5 minutes, more preferably 4 minutes.
Material after homogeneous of the present invention preferably cools to 50~53 DEG C, adds in bamboo-leaves flavones, ganoderma spore polysaccharide, black bearberry
Glycosides, resorcinol derivatives and vitamin E, stir evenly, be down to room temperature to get to the present invention whitening foundation emulsion.
The whitening foundation emulsion of the present invention has both isolation, hides the flaw, anti-ageing and whitening effect, and comprehensive resist is played to skin
Decline the repairing effect of whitening, and adaptation population is wide.
Below in conjunction with the embodiment in the present invention, the technical solution in the embodiment of the present invention is carried out clearly and completely
Description, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based on this hair
Embodiment in bright, the every other implementation that those of ordinary skill in the art are obtained without making creative work
Example, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of whitening foundation emulsion by weight percentage, includes following component:
Between bamboo-leaves flavones 1%, ganoderma spore polysaccharide 3%, beeswax 0.5%, vitamin E 0.05%, ursin 2%, hexyl
Benzenediol 1%, myristic acid glyceride 5%, polyoxyethylene fatty acid ester 10%, polyethylene glycol 4%, glycerine 4%, nano-pearl
Powder 8%, chromatic timing powder 1%, surplus are physiological seawater.
Preparation method includes the following steps:
A. physiological seawater is put into agitated kettle, mixing speed is 42 revs/min, is heated to 95 DEG C, is kept stirring 15
Minute;The water of agitated kettle is cooled to 65 DEG C, addition beeswax, which is stirred to, to be completely dissolved;
B. after Nano pearl powder and chromatic timing powder being mixed myristic acid glycerine is put into after 3 minutes through colloid mill, cycle milling
Ester, polyoxyethylene fatty acid ester, polyethylene glycol and glycerine stir 15 minutes at 80 DEG C.
C. the dissolving feed liquid that step a is obtained, homogeneous, homogenizer speed are 1500 together with the mixture that step b is obtained
Rev/min, homogeneous 5 minutes.
D. the material after homogeneous is cooled to 50 DEG C, adds in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin, isophthalic
Two amphyls and vitamin E, stir evenly, and are down to room temperature.
Embodiment 2:
A kind of whitening foundation emulsion by weight percentage, includes following component:
Bamboo-leaves flavones 2%, ganoderma spore polysaccharide 5%, beeswax 1%, vitamin E 5%, ursin 5%, phenethyl isophthalic
Diphenol 2%, Miglyol 812N 5%, glyceryl linoleate 5%, sorbitan laurate 8%, polyoxyethylene sorbitan mountain
Pears alcohol fatty acid ester 7%, propylene glycol 10%, 1,3-BDO 5%, Nano pearl powder 2%, chromatic timing powder 0.5%, surplus are physiology
Property seawater.
Preparation method includes the following steps:
A. physiological seawater is put into agitated kettle, mixing speed is 50 revs/min, is heated to 90 DEG C, is kept stirring 20
Minute;The water of agitated kettle is cooled to 75 DEG C, addition beeswax, which is stirred to, to be completely dissolved;
B. after Nano pearl powder and chromatic timing powder being mixed Caprylic Capric is put into after 1 minute through colloid mill, cycle milling
Three esters, glyceryl linoleate, sorbitan laurate, polyoxyethylene sorbitan fatty acid ester, propylene glycol and 1,3- fourths two
Alcohol stirs 20 minutes at 85 DEG C.
C. the dissolving feed liquid that step a is obtained, homogeneous, homogenizer speed are 1800 together with the mixture that step b is obtained
Rev/min, homogeneous 2 minutes.
D. the material after homogeneous is cooled to 53 DEG C, adds in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin, isophthalic
Two amphyls and vitamin E, stir evenly, and are down to room temperature.
Embodiment 3
A kind of whitening foundation emulsion by weight percentage, includes following component:
Bamboo-leaves flavones 0.5%, ganoderma spore polysaccharide 1%, beeswax 0.2%, vitamin E 0.01%, ursin 0.1%, two
Methoxy methyl phenyl -4- propyls diphenol 0.05%, propylene glycol dipelargonate 0.5%, gathers Sefsol 218 0.5%
Ethylene oxide rilanit special 2%, 1,2- pentanediols 1%, Nano pearl powder 15%, chromatic timing powder 4%, surplus are physiological seawater.
Preparation method includes the following steps:
A. physiological seawater is put into agitated kettle, mixing speed is 45 revs/min, is heated to 92 DEG C, is kept stirring 18
Minute;The water of agitated kettle is cooled to 85 DEG C, addition beeswax, which is stirred to, to be completely dissolved;
B. after Nano pearl powder and chromatic timing powder being mixed after five minutes, propylene glycol list octanoic acid is put into through colloid mill, cycle milling
Ester, propylene glycol dipelargonate, Crodaret and 1,2- pentanediol are kept stirring 18 minutes at 82 DEG C.
C. the dissolving feed liquid that step a is obtained, homogeneous, homogenizer speed are 1200 together with the mixture that step b is obtained
Rev/min, homogeneous 4 minutes.
D. the material after homogeneous is cooled to 48 DEG C, adds in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin, isophthalic
Two amphyls and vitamin E, stir evenly, and are down to room temperature.
Comparative example 1
Whitening foundation emulsion, in addition to beeswax is not contained, remaining component is same as Example 1.
Comparative example 2
Whitening foundation emulsion, in addition to ganoderma spore polysaccharide and beeswax is not contained, remaining component is same as Example 1.
Comparative example 3
Whitening foundation emulsion, in addition to bamboo-leaves flavones and beeswax are not contained, remaining component is same as Example 1.
Comparative example 4
Whitening foundation emulsion, in addition to bamboo-leaves flavones, ganoderma spore polysaccharide and beeswax is not contained, remaining component and 1 phase of embodiment
Together.
Comparative example 5
Physiological seawater in embodiment 1 is replaced with deionized water by whitening foundation emulsion, remaining component and preparation method with
Embodiment 1 is identical.
The ingredient contrast table of 1 embodiment 1 of table and comparative example 1~5
Bamboo-leaves flavones | Ganoderma spore polysaccharide | Beeswax | Water | |
Embodiment 1 | √ | √ | √ | Physiological seawater |
Comparative example 1 | √ | √ | Physiological seawater | |
Comparative example 2 | √ | Physiological seawater | ||
Comparative example 3 | √ | Physiological seawater | ||
Comparative example 4 | Physiological seawater | |||
Comparative example 5 | √ | √ | √ | Deionized water |
Embodiment 4
Functional component stability experiment in whitening foundation emulsion
The whitening foundation emulsion that embodiment 1 and comparative example 1~4 are obtained is placed 60 days in closed container, under room temperature, is adopted
The content of functional component ursin, resorcinol derivatives, vitamin E in sample is detected with high performance liquid chromatography (HPLC),
Experimental result is as shown in table 2.
The functional component content results of 60 days in 2 whitening foundation emulsion of table
As shown in Table 2, whitening foundation emulsion of the invention in closed container, under room temperature place 60 days after, functional component
Ursin, resorcinol derivatives and content of vitamin E are yellow due to not having to add the leaf of bamboo in comparative example 1~4 without significant change
It is one or more in ketone, ganoderma spore polysaccharide and beeswax, white-skinned face function component content relative to embodiment 1 whitening foundation cream
Content is low in liquid.Therefore, whitening foundation emulsion provided by the invention is with good stability.
Embodiment 5
Whitening foundation emulsion tests cutaneous sensibility
Whitening foundation emulsion prepared by Example 1 and comparative example 1~5 carries out skin irritation test.
Take healthy rabbits 39, weight (2.0 ± 0.2) kg is randomly divided into 13 groups, every group of animal 3, before experiment for 24 hours
By rabbit skin of back both sides unhairing, check whether skin of unhairing is injured, and compromised skin is unfit to do skin irritation for 24 hours after unhairing
Experiment.The whitening foundation emulsion 3 times using embodiment 1 and comparative example 1~5 is smeared daily, it is continuous to smear 7 days, skin condition is observed,
Result of the test is shown in Table 3.
The irritation test result of 3 whitening foundation emulsion of table
"+" rabbit dermohemia, redness;" ++ " represents that congested, red and swollen phenomenon still exists, but have increase trend;"-" represents
Without congested, red and swollen phenomenon.
As shown in Table 3, the whitening foundation emulsion and the whitening foundation emulsion of comparative example 1~4 that embodiment 1 is prepared are due to addition
Physiological seawater, reduces the stimulation of functional component in foundation emulsion, improves tolerance of the skin to foundation emulsion.And comparative example
In 5 due to the use of be deionized water, there is the phenomenon that skin sensitivity in continuous smear the 5th day, illustrate provided by the invention
Whitening foundation emulsion does not have irritation to sensitive skin.
Embodiment 6
The whitening effect experiment of whitening foundation emulsion
The whitening foundation emulsion of Example 1 and comparative example 1~5 carries out skin whitening efficacy evaluation test.
Choose 130 skin healths, without cosmetic allergic contact dermatitis history, volunteer of the age between 20~35 as subject,
Arm skin is divided into 13 groups, every group of 10 people are smeared obtained using embodiment 1 and comparative example 1~5 respectively as experimental subjects
Whitening foundation emulsion.3 times a day, it is continuous to smear 60 days, skin whiteness is detected, result of the test is shown in Table 4.
The whitening result of the test of 4 whitening foundation emulsion of table
The addition of bamboo-leaves flavones, ganoderma spore polysaccharide grade beeswax contained in the whitening foundation emulsion of the present invention, effectively carries
The high whitening effect of whitening foundation emulsion.Wherein bamboo-leaves flavones have excellent tyrosinase activity inhibiting effect, efficiently anti-
Oxidation inhibits the activity of melanocyte and the generation of melanin well, while also is able to make the melanin of oxidation to restore,
Improve whitening effect.Ganoderma spore polysaccharide effectively raises the anti-oxidant of bamboo-leaves flavones while moistening effect is provided
Whitening effect plays effective collaboration antioxidation.Ganoderma spore polysaccharide and beeswax can be stablized in whitening foundation emulsion
The content of ursin and resorcinol derivatives, so as to ensure that the work(of ursin and resorcinol derivatives in whitening foundation emulsion
Effect plays, and improves whitening effect.
As shown in Table 4, after whitening foundation emulsion provided by the invention is applied to human skin, after long-time service, skin whiteness
It is gradually increased with the extension of usage time, there is apparent whitening effect.In comparative example 1 due to be added to bamboo-leaves flavones and
Ganoderma spore polysaccharide, whitening foundation emulsion obtained have preferable whitening effect, but have lacked the guarantor of beeswax relative to embodiment 1
Moisturizing effect is protected, whitening effect is not as good as embodiment 1.Bamboo-leaves flavones are added in comparative example 2, for embodiment 1, are lacked
Ganoderma spore polysaccharide and beeswax have certain whitening effect.It is added to for ganoderma spore polysaccharide in comparative example 3, relatively
For comparative example 4, the whitening effect of comparative example 3 is still better than comparative example 4.
To sum up, in whitening foundation emulsion of the invention, bamboo-leaves flavones, ganoderma spore polysaccharide and beeswax were used foundation emulsion
Collaboration skin whitening effect is played in journey, improves the whitening effect of foundation emulsion, comprehensive anti-ageing whitening is played to skin
Repairing effect.
It can be that professional and technical personnel in the field realize or use that the above embodiment, which is intended to illustrate the present invention, to above-mentioned
Embodiment is modified and be will be apparent for those skilled in the art, therefore the present invention includes but not limited to
The above embodiment, it is any to meet the claims or specification description, meet with principles disclosed herein and novelty,
The method of inventive features, technique, product, each fall within protection scope of the present invention.
Claims (10)
1. a kind of whitening foundation emulsion with anti-ageing effect, which is characterized in that comprising following weight percentage components:The leaf of bamboo is yellow
Ketone 0.01 ~ 2%, ganoderma spore polysaccharide 0.01 ~ 5%, beeswax 0.01 ~ 1%, vitamin E 0.01 ~ 5%, ursin 0.05 ~ 5%, isophthalic
Two amphyls 0.01 ~ 2%, liquid fatty 0.1 ~ 10%, surfactant 0.1% ~ 15%, polyalcohol 0.1 ~ 15%, Nano pearl powder
1 ~ 15%, chromatic timing powder 0.1 ~ 5% and surplus are physiological seawater.
2. whitening foundation emulsion according to claim 1, which is characterized in that comprising following weight percentage components:The leaf of bamboo
Flavones 0.2 ~ 1%, ganoderma spore polysaccharide 0.2 ~ 2%, beeswax 0.05 ~ 0.8%, vitamin E 0.1 ~ 4%, ursin 0.1 ~ 4%, isophthalic
Two amphyls 0.1 ~ 1%, liquid fatty 0.3 ~ 8%, surfactant 1% ~ 10%, polyalcohol 1 ~ 10%, Nano pearl powder 5 ~ 10%,
The physiological seawater of chromatic timing powder 0.5 ~ 2% and surplus.
3. whitening foundation emulsion according to claim 1 or 2, which is characterized in that the resorcinol derivatives include hexyl
The mixture of one or more of resorcinol, Symwhite-337, dimethoxy-p base -4- propyl diphenol.
4. whitening foundation emulsion according to claim 1 or 2, which is characterized in that it is sweet that the liquid fatty includes myristic acid
Grease, isopropyl myristate, Miglyol 812N, polyethylene glycol glyceryl laurate ester, glyceryl linoleate, propylene glycol
Single caprylate, two pungent capric acid propylene glycol esters, diethyl sebacate, isononyl isononanoate, propylene glycol dipelargonate and octyl group 12
The mixture of one or more of alcohol myristinate.
5. whitening foundation emulsion according to claim 1 or 2, which is characterized in that the surfactant includes the sorbierite moon
Cinnamic acid ester, Crodaret, polyoxyethylene fatty acid ester, castor oil polyoxyethylene ether and polyoxyethylene sorbitan
The mixture of one or more of alcohol fatty acid ester.
6. whitening foundation emulsion according to claim 1 or 2, which is characterized in that the polyalcohol includes polyethylene glycol, the third two
The mixture of one or more of alcohol, glycerine, 1,3 butylene glycol and 1,2- pentanediols.
7. the preparation method of any one of the claim 1-6 whitening foundation emulsions, which is characterized in that include the following steps:
A. by physiological seawater high-temperature sterilization, when greenhouse cooling is to 65-85 DEG C, beeswax is dissolved thereto;
B. after the Nano pearl powder and chromatic timing powder mixing milling, exist with the liquid fatty, surfactant and polyalcohol
80-85 DEG C is stirred 15-20 minutes;
C. the dissolving feed liquid step a obtained homogeneous together with the mixture that step b is obtained;
D. the material after homogeneous is cooled to 48-55 DEG C, adds in the bamboo-leaves flavones, ganoderma spore polysaccharide, ursin, isophthalic two
Amphyl and vitamin E, stir evenly, and are down to room temperature.
8. the preparation method of whitening foundation emulsion according to claim 7, which is characterized in that being the step of the high-temperature sterilization will
The physiological seawater is kept stirring 15-20 minutes at 90-95 DEG C.
9. the preparation method of whitening foundation emulsion according to claim 7, which is characterized in that the mixing speed of the step b is
40-50 revs/min.
10. the preparation method of whitening foundation emulsion according to claim 7, which is characterized in that homogeneous speed described in step c is
1200-1800 revs/min, homogenizing time is 3-5 minutes.
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CN114588054A (en) * | 2022-03-11 | 2022-06-07 | 广东丸美生物技术股份有限公司 | Whitening and moisturizing composition and preparation method and application thereof |
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CN114588054A (en) * | 2022-03-11 | 2022-06-07 | 广东丸美生物技术股份有限公司 | Whitening and moisturizing composition and preparation method and application thereof |
CN114588054B (en) * | 2022-03-11 | 2023-11-21 | 广东丸美生物技术股份有限公司 | Whitening and moisturizing composition and preparation method and application thereof |
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