CN108125804A - 一种抑菌清爽型洗头膏及其制备方法 - Google Patents
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Abstract
本发明公开一种抑菌清爽型洗头膏,该洗头膏的主要成分为:ε‑聚赖氨酸、月桂醇聚醚硫酸酯钠、月桂醇硫酸酯铵盐、棕榈仁油酰胺DEA、椰油酰胺丙基甜菜碱、瓜尔胶羟丙基三甲基氯化铵、乙二醇二硬脂酸酯、氯化钠、海藻酸钠、明胶、吡咯烷酮羧酸钠、1,3‑丁二醇、乳酸薄荷酯、维生素E和水。与现有抑菌止痒洗发水相比,本发明的洗头膏抑菌范围广、能有效抑制真菌和细菌,配方温和,对头皮的无毒、无害、无刺激,能起到治疗和预防因真菌或细菌所致的头部皮肤问题。
Description
技术领域
本发明涉及一种抑菌清爽型洗头膏及其制备方法。
背景技术
随着当代社会生活节奏的加快,人们受到生活环境和生活压力的影响,很多人出现头油、头痒、头屑多等多种头皮问题,目前市场上的抑菌止痒洗发水多用硫磺、酮康唑等,这些化学物质虽然具有止痒抑菌的作用,但是对头皮刺激性较大,长期使用反而在化学成分的刺激下受到更深的伤害,加重各种头皮问题。
此外,头部真菌或细菌感染的癣症是一种常见的慢性皮肤病,其特征是出现大小不等的丘疹,红斑,表面覆盖着银白色鳞屑。头部癣症虽不直接影响生命,但是对身体健康和身心健康有直接影响。
随着生活水平不断提高,人们对头部皮肤护理方面也提出了新要求。传统方法通过化学试剂抑菌止痒只能是起到短期的缓解作用,长期来看,抑菌和止痒效果并不是很好,因此有必要提供一种抑菌范围广、有效抑制真菌和细菌,对头皮的无毒、无害、无刺激洗发膏,养护头皮,安全解决头皮问题。
发明内容
针对背景技术中提及的问题,本发明的目的之一是提供一种抑菌清爽型洗头膏。
本发明的目的之一是提供一种制备上述洗头膏的方法。
为实现上述目的,本发明提供如下技术方案:
一种抑菌清爽型洗头膏,其特征在于,所述洗头膏的主要成分为:ε-聚赖氨酸、月桂醇聚醚硫酸酯钠、月桂醇硫酸酯铵盐、棕榈仁油酰胺DEA、椰油酰胺丙基甜菜碱、瓜尔胶羟丙基三甲基氯化铵、乙二醇二硬脂酸酯、氯化钠、海藻酸钠、明胶、吡咯烷酮羧酸钠、1,3-丁二醇、乳酸薄荷酯、维生素E和水。
优选地,以每200g洗头膏计,所述各成分的含量为:ε-聚赖氨酸0.3-5g、月桂醇聚醚硫酸酯钠1-5g、月桂醇硫酸酯铵盐1-5g、棕榈仁油酰胺DEA 2-9g、椰油酰胺丙基甜菜碱3-7g、瓜尔胶羟丙基三甲基氯化铵0.5-5g、乙二醇二硬脂酸酯1-5g、氯化钠1-3g、海藻酸钠0.1-0.5g、明胶0.1-0.5g、吡咯烷酮羧酸钠2-5g、1,3-丁二醇1-7g、乳酸薄荷酯1-5g、维生素E 2-6g,用水补充足至200g。
优选地,所述洗头膏还含香精。
更优选地,每200g洗头膏计,所述洗头膏含香精2-4g。
上述洗头膏的制备方法,包括:
(1)将海藻酸钠加入水中,形成海藻酸钠凝胶液;
(2)将明胶加入水中,形成明胶凝胶液;
(3)维生素E先用乙醇溶解,再与水混合,然后除去乙醇,得到维生素E水溶液;
(4)将ε-聚赖氨酸溶于水,得到ε-聚赖氨酸溶液;
(5)将月桂醇聚醚硫酸酯钠、月桂醇硫酸酯铵盐、棕榈仁油酰胺DEA、椰油酰胺丙基甜菜碱、瓜尔胶羟丙基三甲基氯化铵、乙二醇二硬脂酸酯、氯化钠、吡咯烷酮羧酸钠、1,3-丁二醇和乳酸薄荷酯溶于水中,得到溶液I;
(6)将海藻酸钠凝胶液、明胶凝胶液、维生素E水溶液、ε-聚赖氨酸溶液和溶液I混合,补水搅拌,得到所述洗头膏。
优选地,步骤(3)采用水浴法蒸除乙醇。
优选地,在步骤(6)中加入香精。
本发明的有益效果
1、抑菌范围广、能有效抑制真菌和细菌,对头皮的无毒、无害、无刺激洗。
2、本发明温和无刺激,吡咯烷酮羧酸钠和1,3-丁二醇具有优良保湿性,提高头部皮肤抵抗力,更好地护理头部皮肤,乳酸薄荷酯清凉效果持久。
3、不仅能用于治疗头部真菌和细菌感染所致的皮肤癣症,还能用于日常预防。
4、本发明洗头膏容易制作,成本低,适合批量生产。
具体实施方式
下面将对本发明内容中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
实施例1
(1)称取海藻酸钠0.1g,加入到装有5m1蒸馏水的烧杯中,60℃水浴加热,边加热边搅拌,静置让其充分溶胀,形成海藻酸钠凝胶液,待用。
(2)称取明胶0.1g,加入到装有5m1蒸馏水的烧杯中,60℃水浴加热,边加热边搅拌,静置让其充分溶胀,形成明胶凝胶液,待用。
(3)称取维生素E 2g于无水乙醇中溶解,然后将醇溶液倒入15ml蒸馏水中搅拌,80℃恒温水浴6min除去溶液中的乙醇,冷却至室温形成维生素E水溶液,待用。
(4)称取ε-聚赖氨酸0.3g加入10ml蒸馏水中,常温条件下充分搅拌,得到ε-聚赖氨酸溶液,待用。
(5)分别称取月桂醇聚醚硫酸酯钠1g、月桂醇硫酸酯铵盐1g、棕榈仁油酰胺DEA2g、椰油酰胺丙基甜菜碱3g、瓜尔胶羟丙基三甲基氯化铵0.5g、乙二醇二硬脂酸酯1g、氯化钠1g、吡咯烷酮羧酸钠2g、1,3-丁二醇1g、乳酸薄荷酯1g,加入30ml蒸馏水中,加热使其溶解得到溶液1,待用。
(6)将海藻酸钠凝胶液、明胶凝胶液、维生素E水溶液、ε-聚赖氨酸溶液和溶液1混合,加入香精2g,补加蒸馏水至200g,充分搅拌,直到形成细腻均匀的抑菌清爽洗头膏。
实施例2
(1)称取海藻酸钠0.3g,加入到装有7m1蒸馏水的烧杯中,70℃水浴加热,边加热边搅拌,静置让其充分溶胀,形成海藻酸钠凝胶液,待用。
(2)称取明胶0.3g,加入到装有7m1蒸馏水的烧杯中,70℃水浴加热,边加热边搅拌,静置让其充分溶胀,形成明胶凝胶液,待用。
(3)称取维生素E 4g于无水乙醇中溶解,将醇溶液倒入20ml蒸馏水搅拌,85℃恒温水浴8min除去溶液中的乙醇,冷却至室温形成维生素E水溶液,待用。
(4)称取ε-聚赖氨酸2g加入13ml蒸馏水中,常温条件下充分搅拌,得到ε-聚赖氨酸溶液,待用。
(5)分别称取月桂醇聚醚硫酸酯钠3g、月桂醇硫酸酯铵盐3g、棕榈仁油酰胺DEA5g、椰油酰胺丙基甜菜碱5g、瓜尔胶羟丙基三甲基氯化铵2g、乙二醇二硬脂酸酯3g、氯化钠2g、吡咯烷酮羧酸钠3g、1,3-丁二醇4g、乳酸薄荷酯3g,加入40ml蒸馏水中,加热使其溶解得到溶液1,待用。
(6)将海藻酸钠凝胶液、明胶凝胶液、维生素E水溶液、ε-聚赖氨酸溶液和溶液1混合,加入香精3g补加蒸馏水至200g,充分搅拌,直到形成细腻均匀的抑菌清爽洗头膏。
实施例3
(1)称取海藻酸钠0.5g,加入到装有10m1蒸馏水的烧杯中,80℃水浴加热,边加热边搅拌,静置让其充分溶胀,形成海藻酸钠凝胶液,待用.
(2)称取明胶0.5g,加入到装有10m1蒸馏水的烧杯中,80℃水浴加热,边加热边搅拌,静置让其充分溶胀,形成明胶凝胶液,待用。
(3)称取维生素E 6g于无水乙醇中溶解,将醇溶液倒入25ml蒸馏水搅拌,90℃恒温水浴10min除去溶液中的乙醇,冷却至室温形成维生素E水溶液,待用。
(4)称量ε-聚赖氨酸5g加入15ml蒸馏水中,常温条件下充分搅拌,得到ε-聚赖氨酸溶液,待用。
(5)分别称取月桂醇聚醚硫酸酯钠5g、月桂醇硫酸酯铵盐5g、棕榈仁油酰胺DEA9g、椰油酰胺丙基甜菜碱7g、瓜尔胶羟丙基三甲基氯化铵5g、乙二醇二硬脂酸酯5g、氯化钠3g、吡咯烷酮羧酸钠5g、1,3-丁二醇7g、乳酸薄荷酯5g,加入50ml蒸馏水中,加热使其溶解得到溶液1,待用。
(6)将海藻酸钠凝胶液、明胶凝胶液、维生素E水溶液、ε-聚赖氨酸溶液和溶液1混合,加入香精4g加蒸馏水至200g,充分搅拌,直到形成细腻均匀的抑菌清爽洗头膏。
洗头膏抑菌性实验:
表1为上述制得的洗头膏的抑菌效果
1:实验材料:由实施例1、实施例2、实施例3制备得到的洗头膏。
2:供试菌的制备:在无菌室的超净工作台中,分别将白色念珠菌、金黄色葡萄球菌、大肠杆菌和绿脓杆菌接种至牛肉膏培养液中在28-30℃进行常规培养。
3:实验方法:
采用琼脂打孔扩散法,将添加有琼脂的牛肉膏培养基灭菌处理后倒入无菌培养皿中,待其凝固后用无菌移液管吸取100μL白色念珠菌、金黄色葡萄球菌、大肠杆菌和绿脓杆菌供试菌加到培养皿上,涂布均匀,每个菌种做三组。涂布完毕后,用外径2mm的灭菌不锈钢打孔器在培养基上打孔。分别取实施例1、实施例2、实施例3的洗头膏50μL注入孔中,空白对照组注入50μL无菌水,然后分别置于30℃下培养24h,量取抑菌圈直径(抑菌直径mm计),以3次平均值为抑菌圈直径。
由表1可知,本发明实施例制备的洗头膏对白色念珠菌的平均抑菌直径大于13.0mm,对金黄色葡萄球菌的平均抑菌直径大于12.0mm,对大肠杆菌的平均抑菌直径大于13.0mm,对绿脓杆菌的平均抑菌直径大于14.0mm,由此可知,本发明制备的洗头膏抑菌作用明显。
以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等,均应包含在本发明的保护范围之内。
Claims (7)
1.一种抑菌清爽型洗头膏,其特征在于,所述洗头膏的主要成分为:ε-聚赖氨酸、月桂醇聚醚硫酸酯钠、月桂醇硫酸酯铵盐、棕榈仁油酰胺DEA、椰油酰胺丙基甜菜碱、瓜尔胶羟丙基三甲基氯化铵、乙二醇二硬脂酸酯、氯化钠、海藻酸钠、明胶、吡咯烷酮羧酸钠、1,3-丁二醇、乳酸薄荷酯、维生素E和水。
2.根据权利要求1所述的洗头膏,其特征在于:以每200g洗头膏计,所述各成分的含量为:ε-聚赖氨酸0.3-5g、月桂醇聚醚硫酸酯钠1-5g、月桂醇硫酸酯铵盐1-5g、棕榈仁油酰胺DEA 2-9g、椰油酰胺丙基甜菜碱3-7g、瓜尔胶羟丙基三甲基氯化铵0.5-5g、乙二醇二硬脂酸酯1-5g、氯化钠1-3g、海藻酸钠0.1-0.5g、明胶0.1-0.5g、吡咯烷酮羧酸钠2-5g、1,3-丁二醇1-7g、乳酸薄荷酯1-5g、维生素E 2-6g。
3.根据权利要求1或2所述的洗头膏,其特征在于:所述洗头膏还含香精。
4.根据权利要求3所述的洗头膏,其特征在于:以每200g洗头膏计,所述洗头膏含香精2-4g。
5.权利要求1所述洗头膏的制备方法,包括:
(1)将海藻酸钠加入水中,形成海藻酸钠凝胶液;
(2)将明胶加入水中,形成明胶凝胶液;
(3)维生素E先用乙醇溶解,再与水混合,然后除去乙醇,得到维生素E水溶液;
(4)将ε-聚赖氨酸溶于水,得到ε-聚赖氨酸溶液;
(5)将月桂醇聚醚硫酸酯钠、月桂醇硫酸酯铵盐、棕榈仁油酰胺DEA、椰油酰胺丙基甜菜碱、瓜尔胶羟丙基三甲基氯化铵、乙二醇二硬脂酸酯、氯化钠、吡咯烷酮羧酸钠、1,3-丁二醇和乳酸薄荷酯溶于水中,得到溶液I;
(6)将海藻酸钠凝胶液、明胶凝胶液、维生素E水溶液、ε-聚赖氨酸溶液和溶液I混合,补水搅拌,得到所述洗头膏。
6.根据权利要求5所述的制备方法,其特征在于:步骤(3)采用水浴法蒸除乙醇。
7.根据权利要求5所述的制备方法,其特征在于:在步骤(6)中加入香精。
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