CN108113904A - Transparent essential oil gel and preparation method thereof - Google Patents
Transparent essential oil gel and preparation method thereof Download PDFInfo
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- CN108113904A CN108113904A CN201711308597.6A CN201711308597A CN108113904A CN 108113904 A CN108113904 A CN 108113904A CN 201711308597 A CN201711308597 A CN 201711308597A CN 108113904 A CN108113904 A CN 108113904A
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- essential oil
- transparent
- oil
- gel
- oil gel
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
- A61K2800/262—Transparent; Translucent
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Dermatology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of transparent essential oil gels and preparation method thereof, and the essential oil gel includes the raw material components of following weight percent:Essential oil 5 20%, grease 5 80%, emulsifier 0.5 5%, polyalcohol 1 30%, water 3%.Essential oil gel prepared by the present invention, the emulsifier sodium bacillus subtilis lipopeptide used can emulsify this highly polar grease of essential oil well, and form stable gel, be advantageously applied in aqua product, solubilizer need not additionally be added in, moreover it is possible to increase the soft and moist skin sense of product.
Description
Technical field
The invention belongs to cosmetic fields, and in particular to a kind of clear gel of emulsified refined oil and preparation method thereof.
Background technology
Essential oil in the market, which is applied in aqua product, to add in solubilizer to realize, and solubilizer on the market is to natural
The essential oil in source, the solubilising power of grease are limited, it is necessary to which aqua product could be added to by essential oil by adding in a high proportion of solubilizer
In.
It however, the skin sense of solubilizer is more sticky thick and heavy, is also easy to blister, influences very much the skin sense of entire product and makes
With sense.Common solubilizer contains PEG chains on the market at present, containing Za Zhi dioxanes in such solubilizer, is easy to cause skin
The problems such as allergy.The solubilizer price of emerging polyglycereol class is again relatively higher, makes the expensive of entire product, it is more difficult to connect
By.
Thus, it is necessary to a kind of easy to operate, safe green and highly stable essential oil gel are developed to overcome above-mentioned lack
It falls into.
The content of the invention
The defects of in order to overcome the prior art, the present invention provides one kind to have easy to operate, safe green, very steady
Fixed transparent essential oil gel and preparation method thereof.In order to overcome drawbacks described above, the technical solution adopted by the present invention is as follows:
The first aspect of the present invention provides a kind of transparent essential oil gel, by the raw material components group of following weight percent
Into:
Wherein, the emulsifier is sodium bacillus subtilis lipopeptide, from KANEKA companies.
The polyalcohol is glycerine.
The grease is selected from isohexadecane, ethylhexyl palmitate, caprylic/capric triglyceride, Nexbase 2004, hydrogen
Change polyisobutene, pentaerythrite four (thylhexoic acid) ester, saualane, avocado oil, olive oil, sunflower seed oil etc..It is preferably different
The mixture of hexadecane, olive oil and saualane.Wherein, isohexadecane is natural origin, is not the grease of synthesis source.
The essential oil is selected from Rosa Damascana, Lavender, chamomile essential oil, sweet orange oil, Rosemary Oil, fingered citron
Mandarin orange essential oil, lemon, strawflower essential oil, tea tree ethereal oil, myrrh essential oil, Peppermint essential oil etc..Preferably Bulgarian Tujue rose
(ROSA DAMASCENA) caul-fat.
Preferably, in transparent essential oil gel provided by the invention, the weight percent of water is 3%, emulsifier:It is polynary
Alcohol:Grease and essential oil:Water is 1:20:76:3.
Preferably, the transparent essential oil gel includes the raw material components of following weight percent:
The second aspect of the present invention is the preparation method for providing above-mentioned transparent essential oil gel, includes the following steps:
(A) glycerine and sodium bacillus subtilis lipopeptide are added in mixing vessel, 200rpm/min stirs 2 minutes to being uniformly mixed;
(B) Rosa Damascana and saualane, olive oil, isohexadecane are added in another mixing vessel, is uniformly mixed, obtains
To mixing oil phase;
(C) 1/3 oil phase mixed in step (B) is slowly added into the liquid mixed to step (A),
1200rpm/min is stirred 5 minutes;
(D) 1/2, the 800rpm/min that remaining oil phase is slowly added into step (C) is stirred 10 minutes;
(E) remaining oil phase is slowly added into step (D), 300rpm/min stirs 20 minutes to substantially uniformity;
(F) deionized water is added in into system, and 300rpm/min is stirred to fully transparent.
Herein, it is slowly added into and refers to slowly pouring into, so as to suitable with that can be stirred for after pouring into.
Beneficial effects of the present invention
The essential oil and natural oil of high-content, emulsifier withered grass bacterium are added in transparent essential oil gel prepared by the present invention
Lipopeptid sodium is also green fermentable sources, and entire transparent essential oil gel is made to meet the requirement of green natural, and transparent essential oil gel
Using very convenient to final products, it is added directly into final products and stirs evenly, the skin of entire product can also be made
Sense is very soft and smooth.
Figure of description
Fig. 1 is the makeup that the transparent essential oil gel of the present invention and common solubilizer Cremophor RH40 solubilising essential oil make
Figure is compared in water skin sense.
Specific embodiment
Below in conjunction with specific embodiment, the present invention will be further described.It is to be understood that following embodiment is merely to illustrate
The scope of the present invention and is not intended to limit the present invention.
In following embodiment, the commercially available acquisition of sodium bacillus subtilis lipopeptide, to be derived from KANEKA, marque is SF-S07.
The commercially available acquisition of the Rosa Damascana, to be derived from MPE companies of France, marque is Bulgarian Tujue rose (ROSA
DAMASCENA) caul-fat.
The preparation of 1 transparent essential oil gel of embodiment
Transparent essential oil gel formula (weight percent) in the present embodiment is as follows:
The preparation process of transparent essential oil gel in the present embodiment is as follows:
1st, glycerine and sodium bacillus subtilis lipopeptide are added in into suitable vessel, 200rpm/min stirs 2 minutes to being uniformly mixed;
2nd, Rosa Damascana and saualane, olive oil, isohexadecane are added in into suitable vessel, are uniformly mixed spare;
3rd, 1/3 oil phase mixed is slowly added into the liquid mixed to step 1,1200rpm/min stirs 5 points
Clock;
4th, remaining 1/2 oil phase is slowly added into, 800rpm/min is stirred 10 minutes;
5th, remaining oil phase is slowly added into, 300rpm/min stirs 20 minutes to substantially uniformity;
6th, deionized water is added in into system, and 300rpm/min stirs 5 minutes to fully transparent.
The preparation of 2 transparent essential oil gel of embodiment
The formula (weight percent) of transparent essential oil gel in the present embodiment is as follows:
The preparation process of transparent essential oil gel in the present embodiment is the same as embodiment 1.
The preparation of 3 Biofibre facial mask Essence of embodiment
Transparent essential oil gel formula (weight percent) in the present embodiment is as follows:
The preparation process of transparent essential oil gel in the present embodiment is the same as embodiment 1.
4 transparent essential oil gel stability of embodiment is tested
The transparent essential oil gel of making is fitted into 12 30mL vials, the transparent of 20mL is packed into each vial
Essential oil gel, and write corresponding label, be put into 45 DEG C, 37 DEG C, 25 DEG C, 4 DEG C, high/low temperature circulating box, 6 environment of natural light
In do stability test, each environment places 2 bottles of transparent essential oil gels, and 3 months test periods were observed weekly once.
As a result as shown in table 1 to table 6.
The transparent essential oil gel stability experiment of 1,45 DEG C of table
Sample number | First week | Second week | 3rd week | 4th week | 8th week | 12nd week |
1 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize, slightly turn yellow, no lamination |
2 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize, slightly turn yellow, no lamination |
It judges | Pass through | Pass through | Pass through | Pass through | Pass through | Pass through |
The transparent essential oil gel stability experiment of 2,37 DEG C of table
Sample number | First week | Second week | 3rd week | 4th week | 8th week | 12nd week |
1 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize, slightly turn yellow, no lamination |
2 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize, slightly turn yellow, no lamination |
It judges | Pass through | Pass through | Pass through | Pass through | Pass through | Pass through |
The transparent essential oil gel stability experiment of 3,25 DEG C of table
Sample number | First week | Second week | 3rd week | 4th week | 8th week | 12nd week |
1 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize |
2 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize |
It judges | Pass through | Pass through | Pass through | Pass through | Pass through | Pass through |
The transparent essential oil gel stability experiment of 4,4 DEG C of table
Sample number | First week | Second week | 3rd week | 4th week | 8th week | 12nd week |
1 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize |
2 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize |
It judges | Pass through | Pass through | Pass through | Pass through | Pass through | Pass through |
The transparent essential oil gel stability experiment of table 5, high/low temperature circulating box
Sample number | First week | Second week | 3rd week | 4th week | 8th week | 12nd week |
1 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize, slightly turn yellow, no lamination |
2 | Stablize | Stablize | Stablize | Stablize | Stablize | Stablize, slightly turn yellow, no lamination |
It judges | Pass through | Pass through | Pass through | Pass through | Pass through | Pass through |
The transparent essential oil gel stability experiment of table 6, natural light
The transparent essential oil gel that can be seen that making according to the test data of table 1 to table 6 is highly stable.Under hot conditions
Color slightly turns yellow, be since the natural component of essential oil causes, it is unrelated with the stability of gel in itself.
5 transparent essential oil gel skin sense of embodiment is assessed
The toner that the transparent essential oil gel and common solubilizer Cremophor RH40 solubilising essential oil of the present invention makes
Skin sense is compared.
Evaluation item includes foaming characteristic, trap, sticky sense, soft feeling and fragrance, and it is as follows to judge rule:Foaming characteristic,
Trap, sticky sense, soft feeling are carried out in the form of giving a mark, full marks ten point system, and 10 points are perfection, and 5 points are medium, and 0 point is pole
Difference.
As a result as shown in Fig. 1, table 7 and table 8.
Table 7, transparent essential oil gel skin sense assessment
Subject | Foaming characteristic | Trap | Sticky degree | Moisten degree | Pliability | Fragrance |
Tester 1 | 2 | 9 | 1 | 8 | 8 | Rose fragrance, without other peculiar smell |
Tester 2 | 2 | 9 | 1 | 8 | 9 | Rose fragrance, without other peculiar smell |
Tester 3 | 1 | 8 | 1 | 7 | 9 | Rose fragrance, without other peculiar smell |
Tester 4 | 1 | 9 | 0 | 7 | 8 | Rose fragrance, without other peculiar smell |
Tester 5 | 2 | 9 | 0 | 8 | 9 | Rose fragrance, without other peculiar smell |
Tester 6 | 2 | 9 | 1 | 8 | 8 | Rose fragrance, without other peculiar smell |
Tester 7 | 2 | 9 | 1 | 8 | 8 | Rose fragrance, without other peculiar smell |
Tester 8 | 2 | 9 | 1 | 7 | 9 | Rose fragrance, without other peculiar smell |
Tester 9 | 2 | 9 | 1 | 7 | 8 | Rose fragrance, without other peculiar smell |
Tester 10 | 2 | 9 | 1 | 8 | 9 | Rose fragrance, without other peculiar smell |
Tester 11 | 2 | 9 | 0 | 8 | 9 | Rose fragrance, without other peculiar smell |
Tester 12 | 1 | 9 | 0 | 8 | 9 | Rose fragrance, without other peculiar smell |
The toner skin sense assessment of table 8, Cremophor RH40 solubilising essential oil
Found out by the result of Fig. 1, table 7 and table 8, subject is to the toner that transparent essential oil gel makes in trap, taste
Humidity, soft feeling and fragrance are had higher rating, and the toner made using common solubilizer is relatively sticky, and skin sense is thick and heavy, and makes
Solubilizer has the characteristic odor of raw material, affects the fragrance of Rosa Damascana in itself.The transparent essence of the present invention described above
Oleogel has effects that preferable and usage experience.
Claims (10)
1. a kind of transparent essential oil gel, which is characterized in that be made of the raw material components of following weight percent:
2. transparent essential oil gel as described in claim 1, which is characterized in that the emulsifier is sodium bacillus subtilis lipopeptide.
3. transparent essential oil gel as claimed in claim 2, which is characterized in that the essential oil is selected from Rosa Damascana, lavender essence
Oil, chamomile essential oil, sweet orange oil, Rosemary Oil, Bergamot, lemon, strawflower essential oil, tea tree ethereal oil, myrrh
One or more in essential oil, Peppermint essential oil.
4. transparent essential oil gel as claimed in claim 3, which is characterized in that the polyalcohols are selected from glycerine, 1,3- fourths two
One or more in alcohol, 1,3- propylene glycol, dipropylene glycol, polyethylene glycol-8, polyethylene glycol -32, D-sorbite.
5. transparent essential oil gel as claimed in claim 4, which is characterized in that the grease is selected from isohexadecane, palmitic acid second
The own ester of base, caprylic/capric triglyceride, Nexbase 2004, Parleam, pentaerythrite four (thylhexoic acid) ester, spiny dogfish
The one or more of the liquid fats such as alkane, avocado oil, olive oil, sunflower seed oil.
6. transparent essential oil gel as claimed in claim 5, which is characterized in that the isohexadecane is natural origin, is not to close
Into the grease in source.
7. transparent essential oil gel as described in claim 1, which is characterized in that the weight percent of the water is 3%.
8. the transparent essential oil gel stated such as claim 7, which is characterized in that emulsifier:Polyalcohol:Grease and essential oil:Water is 1:
20:76:3。
9. transparent essential oil gel as claimed in claim 5, which is characterized in that by the raw material components group of following weight percent
Into:
10. the preparation method of the transparent essential oil gel described in claim 9, which is characterized in that include the following steps:
(A) glycerine and sodium bacillus subtilis lipopeptide are added in mixing vessel, 200rpm/min stirs 2 minutes to being uniformly mixed;
(B) Rosa Damascana and saualane, olive oil, isohexadecane are added in another mixing vessel, is uniformly mixed, is mixed
Oil phase;
(C) 1/3 oil phase mixed in step (B) is slowly added into the liquid mixed to step (A), 1200rpm/min
Stirring 5 minutes;
(D) 1/2, the 800rpm/min that remaining oil phase is slowly added into step (C) is stirred 10 minutes;
(E) remaining oil phase is slowly added into step (D), 300rpm/min stirs 20 minutes to substantially uniformity;
(F) deionized water is added in into system, and 300rpm/min is stirred to fully transparent.
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CN201711308597.6A CN108113904A (en) | 2017-12-11 | 2017-12-11 | Transparent essential oil gel and preparation method thereof |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110787093A (en) * | 2019-10-12 | 2020-02-14 | 广州市百好博有限公司 | Two-agent moisturizing essence and preparation method thereof |
CN110893151A (en) * | 2019-12-20 | 2020-03-20 | 广州市拉凯尔干细胞研究所 | Preparation method of phase-D emulsified cream with anti-inflammatory effect |
CN110960438A (en) * | 2019-12-23 | 2020-04-07 | 广州市拉凯尔干细胞研究所 | Skin care composition for improving skin smoothness and preparation method thereof |
CN112190504A (en) * | 2020-10-19 | 2021-01-08 | 绍兴文理学院 | Long-acting liquid gel containing rose essential oil and preparation method and application thereof |
CN114642600A (en) * | 2022-03-12 | 2022-06-21 | 广州悦荟化妆品有限公司 | Oil gel composition, non-emulsified mask liquid composition, and preparation method and use method thereof |
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TW200536561A (en) * | 2004-02-06 | 2005-11-16 | Showa Denko Kk | Method for stabilizing oil-based thickening gel composition |
JP2008069075A (en) * | 2006-09-12 | 2008-03-27 | Kracie Home Products Kk | Skin care composition |
CN101467942A (en) * | 2007-12-29 | 2009-07-01 | 天津市中宝制药有限公司 | Gel for treating acne |
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2017
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Patent Citations (3)
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TW200536561A (en) * | 2004-02-06 | 2005-11-16 | Showa Denko Kk | Method for stabilizing oil-based thickening gel composition |
JP2008069075A (en) * | 2006-09-12 | 2008-03-27 | Kracie Home Products Kk | Skin care composition |
CN101467942A (en) * | 2007-12-29 | 2009-07-01 | 天津市中宝制药有限公司 | Gel for treating acne |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110787093A (en) * | 2019-10-12 | 2020-02-14 | 广州市百好博有限公司 | Two-agent moisturizing essence and preparation method thereof |
WO2021068401A1 (en) * | 2019-10-12 | 2021-04-15 | 广州市百好博有限公司 | Two-dosage-form essence and preparation method therefor |
JP2022551856A (en) * | 2019-10-12 | 2022-12-14 | 広州市百好博有限公司 | Two-part type essence and its manufacturing method |
JP7450979B2 (en) | 2019-10-12 | 2024-03-18 | 広州市百好博有限公司 | Two-dose essence and its manufacturing method |
CN110893151A (en) * | 2019-12-20 | 2020-03-20 | 广州市拉凯尔干细胞研究所 | Preparation method of phase-D emulsified cream with anti-inflammatory effect |
CN110960438A (en) * | 2019-12-23 | 2020-04-07 | 广州市拉凯尔干细胞研究所 | Skin care composition for improving skin smoothness and preparation method thereof |
CN112190504A (en) * | 2020-10-19 | 2021-01-08 | 绍兴文理学院 | Long-acting liquid gel containing rose essential oil and preparation method and application thereof |
CN114642600A (en) * | 2022-03-12 | 2022-06-21 | 广州悦荟化妆品有限公司 | Oil gel composition, non-emulsified mask liquid composition, and preparation method and use method thereof |
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