CN108103767A - A kind of Efficient textile slurry and preparation method thereof - Google Patents

A kind of Efficient textile slurry and preparation method thereof Download PDF

Info

Publication number
CN108103767A
CN108103767A CN201711344592.9A CN201711344592A CN108103767A CN 108103767 A CN108103767 A CN 108103767A CN 201711344592 A CN201711344592 A CN 201711344592A CN 108103767 A CN108103767 A CN 108103767A
Authority
CN
China
Prior art keywords
parts
slurry
efficient textile
textile slurry
inorganic nanoparticles
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711344592.9A
Other languages
Chinese (zh)
Inventor
储平
徐有琦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu New Lucky Polytron Technologies Inc
Original Assignee
Jiangsu New Lucky Polytron Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangsu New Lucky Polytron Technologies Inc filed Critical Jiangsu New Lucky Polytron Technologies Inc
Priority to CN201711344592.9A priority Critical patent/CN108103767A/en
Publication of CN108103767A publication Critical patent/CN108103767A/en
Pending legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/07Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
    • D06M11/11Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/07Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
    • D06M11/09Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with free halogens or interhalogen compounds
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/46Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • D06M13/148Polyalcohols, e.g. glycerol or glucose
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/368Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03Polysaccharides or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/15Proteins or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40Reduced friction resistance, lubricant properties; Sizing compositions

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a kind of Efficient textile slurry and preparation method thereof, the Efficient textile slurry is made of the raw material of following parts by weight:20 30 parts of nano SiO 2 modified starch, 35 parts of hydroxypropyl methyl cellulose, 5 10 parts of albumen slurry, 57 parts of sodium lignin sulfonate, 35 parts of inorganic nanoparticles, 13 parts of triethanolamine, 10 20 parts of ethyl alcohol, 13 parts of kaolin, 57 parts of glycerine, 13 parts of dimethicone, 35 parts of beta glucan, 30 50 parts of deionized water.The Efficient textile slurry preparation method of the present invention is relatively reasonable, adds the adhesion strength between fiber, improves the tension strength of yarn, to adapt to beat up in the hightension in weaving process, reduces broken end, improve efficiency.The Efficient textile slurry manufacturing process of the present invention is simple to operation, and low in raw material price easily obtains, and viscosity stabilization, can be gelatinized completely.

Description

A kind of Efficient textile slurry and preparation method thereof
Technical field
The invention belongs to textile Sizing Technology fields, specifically relate to a kind of Efficient textile slurry and its preparation side Method.
Background technology
Warp sizing is one of critical process in textile manufacturing.With the development of science and technology, various tencel phases After appearance, novel high speed loom is also such as emerged rapidly in large numbersBamboo shoots after a spring rain.The update of textile product, the continuous development of kind and new technology it is wide General application promotes warp sizing technology also increasingly updating, and constantly advances.Three big elements of warp sizing are that slurry, sizing are set Standby and slashing technique, three complement each other.Good sizing not only will will also lean on advanced slashing technique by good slurry and formula And equipment, and the selection of slurry plays conclusive effect with cooperation.With the development of textile industry, existing slurry is reasonably selected Material, active development new slurry, the slurry formula to study science should meet the requirement of slashing technique, energy saving again, reduce Environmental pollution reduces sizing costs, this is a highly important technical work.
Warp sizing is the key link of Textile Engineering, and the main purpose of sizing is to improve the wearability of yarn, high at present Effect spinning sizing agent is broadly divided into starch, polyvinyl alcohol, polyacrylic acid three categories slurry, at home and abroad play an important role. But at present there is also some problems, such as:Polyvinyl alcohol pulp cannot degrade, and cause serious environmental problem, Gradually substituted, viscosity is serious again for traditional polypropylene slurry, causes leasing difficult, and Starch Size viscosity fluctuation is big, paste Change poor performance.So it is badly in need of developing a kind of environmental protection, cheap, biodegradable slurry, to meet the need in slurry market It asks.
The content of the invention
It is an object of the invention to provide a kind of Efficient textile slurry and preparation method thereof, to solve in above-mentioned background technology The problem of proposition.
To achieve the above object, the present invention provides following technical solution:
A kind of Efficient textile slurry, according to parts by weight, including following components:Nano SiO 2 modified starch 20-30 Part, 3-5 parts of hydroxypropyl methyl cellulose, 5-10 parts of albumen slurry, 5-7 parts of sodium lignin sulfonate, 3-5 parts of inorganic nanoparticles, 1-3 parts of triethanolamine, 10-20 parts of ethyl alcohol, 1-3 parts of kaolin, 5-7 parts of glycerine, 1-3 parts of dimethicone, beta glucan 3-5 Part, 30-50 parts of deionized water.
Preferably, the ethyl alcohol is absolute ethyl alcohol.
Preferably, the inorganic nanoparticles pass through the inorganic nanoparticles of hydroxyl modification for surface.
Preferably, the inorganic nanoparticles are modified manometer silicon dioxide, modified calcium carbonate particle, modified titanium dioxide It is one or more than one kinds of in titanium particle.
Preferably, the inorganic nanoparticles grain size is 5-50nm.
Preferably, the preparation method of the Efficient textile slurry, specific steps include:
Step 1,30-50 parts of deionized water is added in a kettle, and rise temperature is to 40-50 DEG C;
Step 2,20-30 parts of nano SiO 2 modified starch, 3-5 parts of hydroxypropyl methyl cellulose, albumen slurry are added in 5-10 parts, 5-7 parts of sodium lignin sulfonate, stir 20-30 minutes by 500-1000 revs/min;
Step 3,3-5 parts of inorganic nanoparticles, 1-3 parts of triethanolamine, 10-20 parts of ethyl alcohol, 1-3 parts of kaolin are surpassed Sound disperses, and it is 500-1000W to disperse power, and jitter time is 20-30 minutes;
Step 4, the mixture of step 3 is poured into the mixture of step 2,500-1000 revs/min, 20-30 points of stirring Clock;
Step 5, temperature is reduced to 30-40 DEG C, adds in 5-7 parts of glycerine, 1-3 parts of dimethicone, 3-5 parts of beta glucan, It 500-1000 revs/min, stirs 20-30 minutes;
Step 6, stirring is closed down, obtains prepared liquid Efficient textile slurry;
Step 7, stand and be cooled in stirred tank liquid Efficient textile slurry and be less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows:
1st, Efficient textile slurry manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and viscosity is steady It is fixed, it can be gelatinized completely.
2nd, mutual compatibility, synergistic effect between various raw materials used in Efficient textile slurry of the invention, collectively constitute performance Excellent product.
3rd, Efficient textile slurry of the invention in application process, does not generate poisonous gas or solid matter.
4th, Efficient textile slurry preparation method of the invention is relatively reasonable, adds the adhesion strength between fiber, improves The tension strength of yarn, to adapt to beat up in the hightension in weaving process, reduces broken end, improves efficiency.
5th, Efficient textile slurry of the invention has good film forming, is easy to desizing.
6th, Efficient textile slurry anti-aging property of the invention is good, has good affinity.
7th, technique is simplified, safe operation is simple, is easy to industrialized production.
8th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of Efficient textile slurry, according to parts by weight, including following components:Nano silicon dioxide changes 20-30 parts of starch of property, 3-5 parts of hydroxypropyl methyl cellulose, 5-10 parts of albumen slurry, 5-7 parts of sodium lignin sulfonate, inorganic nano 3-5 parts of particle, 1-3 parts of triethanolamine, 10-20 parts of ethyl alcohol, 1-3 parts of kaolin, 5-7 parts of glycerine, 1-3 parts of dimethicone, β- 3-5 parts of glucan, 30-50 parts of deionized water.
The present invention also provides a kind of preparation method of Efficient textile slurry, specific steps include:
Step 1,30-50 parts of deionized water is added in a kettle, and rise temperature is to 40-50 DEG C;
Step 2,20-30 parts of nano SiO 2 modified starch, 3-5 parts of hydroxypropyl methyl cellulose, albumen slurry are added in 5-10 parts, 5-7 parts of sodium lignin sulfonate, stir 20-30 minutes by 500-1000 revs/min;
Step 3,3-5 parts of inorganic nanoparticles, 1-3 parts of triethanolamine, 10-20 parts of ethyl alcohol, 1-3 parts of kaolin are surpassed Sound disperses, and it is 500-1000W to disperse power, and jitter time is 20-30 minutes;
Step 4, the mixture of step 3 is poured into the mixture of step 2,500-1000 revs/min, 20-30 points of stirring Clock;
Step 5, temperature is reduced to 30-40 DEG C, adds in 5-7 parts of glycerine, 1-3 parts of dimethicone, 3-5 parts of beta glucan, It 500-1000 revs/min, stirs 20-30 minutes;
Step 6, stirring is closed down, obtains prepared liquid Efficient textile slurry;
Step 7, stand and be cooled in stirred tank liquid Efficient textile slurry and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of Efficient textile slurry, according to parts by weight, including following components:Nano silicon dioxide changes 20 parts of starch of property, 3 parts of hydroxypropyl methyl cellulose, 5 parts of albumen slurry, 5 parts of sodium lignin sulfonate, 3 parts of inorganic nanoparticles, three 1 part of ethanolamine, 10 parts of ethyl alcohol, 1 part of kaolin, 5 parts of glycerine, 1 part of dimethicone, 3 parts of beta glucan, 30 parts of deionized water.
The present invention also provides a kind of preparation method of Efficient textile slurry, specific steps include:
Step 1,30 parts of deionized water is added in a kettle, and rise temperature is to 40 DEG C;
Step 2,20 parts of nano SiO 2 modified starch, 3 parts of hydroxypropyl methyl cellulose, 5 parts of albumen slurry, wood are added in 5 parts of quality sodium sulfonate, stirs 30 minutes by 500 revs/min;
Step 3, by 1 part of 3 parts of inorganic nanoparticles, 1 part of triethanolamine, 10 parts of ethyl alcohol, kaolin progress ultrasonic disperse, divide It is 500W to dissipate power, and jitter time is 30 minutes;
Step 4, the mixture of step 3 is poured into the mixture of step 2,500 revs/min, stirred 20 minutes;
Step 5, temperature is reduced to 30 DEG C, 5 parts of glycerine of addition, 1 part of dimethicone, 3 parts of beta glucan, 500 revs/min Clock stirs 20 minutes;
Step 6, stirring is closed down, obtains prepared liquid Efficient textile slurry;
Step 7, stand and be cooled in stirred tank liquid Efficient textile slurry and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of Efficient textile slurry, according to parts by weight, including following components:Nano silicon dioxide changes 25 parts of starch of property, 4 parts of hydroxypropyl methyl cellulose, 8 parts of albumen slurry, 6 parts of sodium lignin sulfonate, 4 parts of inorganic nanoparticles, three 2 parts of ethanolamine, 15 parts of ethyl alcohol, 2 parts of kaolin, 6 parts of glycerine, 2 parts of dimethicone, 4 parts of beta glucan, 40 parts of deionized water.
The present invention also provides a kind of preparation method of Efficient textile slurry, specific steps include:
Step 1,40 parts of deionized water is added in a kettle, and rise temperature is to 45 DEG C;
Step 2,25 parts of nano SiO 2 modified starch, 4 parts of hydroxypropyl methyl cellulose, 8 parts of albumen slurry, wood are added in 6 parts of quality sodium sulfonate, stirs 25 minutes by 800 revs/min;
Step 3, by 2 parts of 4 parts of inorganic nanoparticles, 2 parts of triethanolamine, 15 parts of ethyl alcohol, kaolin progress ultrasonic disperses, divide It is 800W to dissipate power, and jitter time is 25 minutes;
Step 4, the mixture of step 3 is poured into the mixture of step 2,800 revs/min, stirred 25 minutes;
Step 5, temperature is reduced to 35 DEG C, 6 parts of glycerine of addition, 2 parts of dimethicone, 4 parts of beta glucan, 800 revs/min Clock stirs 25 minutes;
Step 6, stirring is closed down, obtains prepared liquid Efficient textile slurry;
Step 7, stand and be cooled in stirred tank liquid Efficient textile slurry and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of Efficient textile slurry, according to parts by weight, including following components:Nano silicon dioxide changes 30 parts of starch of property, 5 parts of hydroxypropyl methyl cellulose, 10 parts of albumen slurry, 7 parts of sodium lignin sulfonate, 5 parts of inorganic nanoparticles, 3 parts of triethanolamine, 20 parts of ethyl alcohol, 3 parts of kaolin, 7 parts of glycerine, 3 parts of dimethicone, 5 parts of beta glucan, deionized water 50 Part.
The present invention also provides a kind of preparation method of Efficient textile slurry, specific steps include:
Step 1,50 parts of deionized water is added in a kettle, and rise temperature is to 50 DEG C;
Step 2, add in 30 parts of nano SiO 2 modified starch, 5 parts of hydroxypropyl methyl cellulose, 10 parts of albumen slurry, 7 parts of sodium lignin sulfonate, stirs 30 minutes by 1000 revs/min;
Step 3, by 3 parts of 5 parts of inorganic nanoparticles, 3 parts of triethanolamine, 20 parts of ethyl alcohol, kaolin progress ultrasonic disperses, divide It is 1000W to dissipate power, and jitter time is 20 minutes;
Step 4, the mixture of step 3 is poured into the mixture of step 2,1000 revs/min, stirred 20 minutes;
Step 5, temperature is reduced to 40 DEG C, 7 parts of glycerine of addition, 3 parts of dimethicone, 5 parts of beta glucan, 1000 revs/min Clock stirs 30 minutes;
Step 6, stirring is closed down, obtains prepared liquid Efficient textile slurry;
Step 7, stand and be cooled in stirred tank liquid Efficient textile slurry and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of Efficient textile slurry, according to parts by weight, including following components:Nano silicon dioxide changes 30 parts of starch of property, 3 parts of hydroxypropyl methyl cellulose, 10 parts of albumen slurry, 7 parts of sodium lignin sulfonate, 5 parts of inorganic nanoparticles, 3 parts of triethanolamine, 20 parts of ethyl alcohol, 3 parts of kaolin, 5 parts of glycerine, 2 parts of dimethicone, 5 parts of beta glucan, deionized water 30 Part.
The present invention also provides a kind of preparation method of Efficient textile slurry, specific steps include:
Step 1,30 parts of deionized water is added in a kettle, and rise temperature is to 40 DEG C;
Step 2, add in 30 parts of nano SiO 2 modified starch, 3 parts of hydroxypropyl methyl cellulose, 10 parts of albumen slurry, 7 parts of sodium lignin sulfonate, stirs 20 minutes by 1000 revs/min;
Step 3, by 3 parts of 5 parts of inorganic nanoparticles, 3 parts of triethanolamine, 20 parts of ethyl alcohol, kaolin progress ultrasonic disperses, divide It is 1000W to dissipate power, and jitter time is 20 minutes;
Step 4, the mixture of step 3 is poured into the mixture of step 2,1000 revs/min, stirred 20 minutes;
Step 5, temperature is reduced to 35 DEG C, 5 parts of glycerine of addition, 2 parts of dimethicone, 5 parts of beta glucan, 1000 revs/min Clock stirs 30 minutes;
Step 6, stirring is closed down, obtains prepared liquid Efficient textile slurry;
Step 7, stand and be cooled in stirred tank liquid Efficient textile slurry and be less than 20 DEG C, blowing encapsulation, finished product.
Test case
The Efficient textile slurry of embodiment 1,2,3,4 is tested for the property, test result is as follows:
The above-mentioned various embodiments enumerated, under the premise of reconcilable, can be mutually combined implementation, those skilled in the art The explanation to embodiment above can be combined, as the foundation being combined to the technical characteristic in different embodiments.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of Efficient textile slurry, it is characterised in that:The Efficient textile slurry includes the raw material of following parts by weight:Nanometer 20-30 parts of SiO 2 modified starch, 3-5 parts of hydroxypropyl methyl cellulose, 5-10 parts of albumen slurry, sodium lignin sulfonate 5-7 Part, 3-5 parts of inorganic nanoparticles, 1-3 parts of triethanolamine, 10-20 parts of ethyl alcohol, 1-3 parts of kaolin, 5-7 parts of glycerine, dimethyl-silicon 1-3 parts oily, 3-5 parts of beta glucan, 30-50 parts of deionized water.
2. Efficient textile slurry according to claim 1, it is characterised in that:The ethyl alcohol is absolute ethyl alcohol.
3. Efficient textile slurry according to claim 1, it is characterised in that:The inorganic nanoparticles pass through for surface The inorganic nanoparticles of hydroxyl modification.
4. Efficient textile slurry according to claim 1, it is characterised in that:The inorganic nanoparticles are modified Nano It is one or more than one kinds of in silica, modified calcium carbonate particle, modifying titanium dioxide particle.
5. Efficient textile slurry according to claim 1, it is characterised in that:The inorganic nanoparticles grain size is 5- 50nm。
6. a kind of preparation method using Efficient textile slurry any one of the claims 1-5, it is characterised in that:Tool Body step includes:
Step 1,30-50 parts of deionized water is added in a kettle, and rise temperature is to 40-50 DEG C;
Step 2,20-30 parts of nano SiO 2 modified starch, 3-5 parts of hydroxypropyl methyl cellulose, albumen slurry 5-10 are added in Part, 5-7 parts of sodium lignin sulfonate, stir 20-30 minutes by 500-1000 revs/min;
Step 3,3-5 parts of inorganic nanoparticles, 1-3 parts of triethanolamine, 10-20 parts of ethyl alcohol, 1-3 parts of kaolin are subjected to ultrasound point It dissipates, it is 500-1000W to disperse power, and jitter time is 20-30 minutes;
Step 4, the mixture of step 3 is poured into the mixture of step 2,500-1000 revs/min, stirred 20-30 minutes;
Step 5, temperature is reduced to 30-40 DEG C, adds in 5-7 parts of glycerine, 1-3 parts of dimethicone, 3-5 parts of beta glucan, 500- It 1000 revs/min, stirs 20-30 minutes;
Step 6, stirring is closed down, obtains prepared liquid Efficient textile slurry;
Step 7, stand and be cooled in stirred tank liquid Efficient textile slurry and be less than 20 DEG C, blowing encapsulation, finished product.
CN201711344592.9A 2017-12-15 2017-12-15 A kind of Efficient textile slurry and preparation method thereof Pending CN108103767A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711344592.9A CN108103767A (en) 2017-12-15 2017-12-15 A kind of Efficient textile slurry and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711344592.9A CN108103767A (en) 2017-12-15 2017-12-15 A kind of Efficient textile slurry and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108103767A true CN108103767A (en) 2018-06-01

Family

ID=62216145

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711344592.9A Pending CN108103767A (en) 2017-12-15 2017-12-15 A kind of Efficient textile slurry and preparation method thereof

Country Status (1)

Country Link
CN (1) CN108103767A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107893331A (en) * 2017-11-29 2018-04-10 苏州润弘贸易有限公司 A kind of spinning sizing agent
CN108823981A (en) * 2018-07-04 2018-11-16 如皋市丹凤纺织有限公司 A kind of 40 count all cotton yarn special environment protection slurry production process

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103882708A (en) * 2014-04-14 2014-06-25 苏州润弘贸易有限公司 Low-pollution textile sizing agent
CN104846643A (en) * 2015-05-21 2015-08-19 青岛德翕拓创高新技术有限公司 High-efficiency environment-friendly textile sizing agent
CN104947426A (en) * 2015-06-30 2015-09-30 青岛精石通精密机械制造有限公司 Improved starch textile sizing agent
CN106032647A (en) * 2015-03-09 2016-10-19 南通市跃达针织服饰有限公司 Textile size
CN107217484A (en) * 2017-06-23 2017-09-29 太仓大唐化纤厂 A kind of environment-friendly type starch spinning sizing agent and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103882708A (en) * 2014-04-14 2014-06-25 苏州润弘贸易有限公司 Low-pollution textile sizing agent
CN106032647A (en) * 2015-03-09 2016-10-19 南通市跃达针织服饰有限公司 Textile size
CN104846643A (en) * 2015-05-21 2015-08-19 青岛德翕拓创高新技术有限公司 High-efficiency environment-friendly textile sizing agent
CN104947426A (en) * 2015-06-30 2015-09-30 青岛精石通精密机械制造有限公司 Improved starch textile sizing agent
CN107217484A (en) * 2017-06-23 2017-09-29 太仓大唐化纤厂 A kind of environment-friendly type starch spinning sizing agent and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107893331A (en) * 2017-11-29 2018-04-10 苏州润弘贸易有限公司 A kind of spinning sizing agent
CN108823981A (en) * 2018-07-04 2018-11-16 如皋市丹凤纺织有限公司 A kind of 40 count all cotton yarn special environment protection slurry production process

Similar Documents

Publication Publication Date Title
CN101597356B (en) High-performance modified nanometre-silicon dioxide/crylic acid slurry and preparation method thereof
CN111138093B (en) SiO for basalt fiber composite rib2Nanoparticle modified thermosetting impregnating compound and preparation method thereof
CN105755890B (en) The preparation method of super-hydrophobic oleophobic transparent nanofiber element paper
US20230043739A1 (en) Method for Preparing Silane Coupling Agent/Silica/Plant Fiber Composite
CN114292073B (en) Aeolian sand anti-freezing concrete capable of being printed in 3D mode and preparation method and using method thereof
CN109456745A (en) A kind of nanometer of wetting agent and its preparation method and application
CN103882708B (en) A kind of low stain spinning sizing agent
CN103882707A (en) Environment-friendly type textile sizing agent
CN108179628A (en) The preparation method and aeroge fiber composite felt of aeroge fiber composite felt and application
CN108103767A (en) A kind of Efficient textile slurry and preparation method thereof
CN105541126A (en) Resin compatible type glass fiber yarn impregnation agent, and preparation method thereof
CN107555814A (en) One kind insulation pultrusion alkali-free glass fibre yarn size
CN108977045A (en) The method of nano-cellulose dispersed graphite alkylene modified water-soluble woodwork coating
CN110219201A (en) A kind of preparation method of basalt fibre paper
CN103898752B (en) A kind of spinning sizing agent being applicable to a high COTTON FABRIC
CN103898759A (en) Textile size applicable to linen fabrics
CN108035152A (en) A kind of spinning sizing agent and preparation method thereof
CN101089258A (en) Method for preparing high strength cellulose and silicat composite fibre and prepared composite fibre
CN110282929A (en) A kind of modified rosin batholith thermal insulation mortar preparation method
CN108560262A (en) A kind of fastness to wet rubbing reinforcing agent and preparation method thereof
CN110184666A (en) Spinning head used in the manufacturing method and manufacturing process of flame retardant cellulose fiber
CN108103779A (en) A kind of environment-friendly type spinning sizing agent and preparation method thereof
CN103924447B (en) A kind of low stain spinning sizing agent preparation method
CN103882710A (en) Preparation method for environment-friendly type textile sizing agent
CN103924448B (en) A kind of spinning sizing agent preparation method being applicable to sodolin

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20180601

RJ01 Rejection of invention patent application after publication