CN108101186A - A kind of preparation method of oxidation resistant nanoparticle pottery ball - Google Patents

A kind of preparation method of oxidation resistant nanoparticle pottery ball Download PDF

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Publication number
CN108101186A
CN108101186A CN201810040691.6A CN201810040691A CN108101186A CN 108101186 A CN108101186 A CN 108101186A CN 201810040691 A CN201810040691 A CN 201810040691A CN 108101186 A CN108101186 A CN 108101186A
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China
Prior art keywords
oyster shell
preparation
oxidation resistant
pottery ball
shell particle
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Pending
Application number
CN201810040691.6A
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Chinese (zh)
Inventor
崔建中
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Zhong Hong Nano Fiber Technology Danyang Co Ltd
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Zhong Hong Nano Fiber Technology Danyang Co Ltd
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Priority to CN201810040691.6A priority Critical patent/CN108101186A/en
Publication of CN108101186A publication Critical patent/CN108101186A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/68Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • C02F1/683Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water by addition of complex-forming compounds

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention proposes a kind of preparation method of oxidation resistant nanoparticle pottery ball, and its step are as follows:(1)Oyster shell is immersed in hydrochloric acid solution after 5 10min, is cleaned up using clear water spare;(2)Oyster shell after cleaning is put into baking oven, is toasted under the irradiation of ultraviolet light;(3)Oyster shell after baking is ground into oyster shell particle after being cooled to room temperature spare;(4)Zeolite granular will be ground into after natural zeolite cleaning, drying;(5)Sinter oyster shell particle, zeolite granular, hydroxypropyl methyl cellulose, nano-titanium dioxide and nano silver into spherical shape after mixing, the pottery ball being prepared is rich in mineral matter elements such as calcium, magnesium, silicon, potassium, sodium, phosphorus, titanium, manganese, zinc, copper, and it can be used for generating mineral water, inhibit body oxidation, improve immunity of organisms.

Description

A kind of preparation method of oxidation resistant nanoparticle pottery ball
Technical field
The present invention relates to a kind of preparation method for ball of making pottery, more particularly to a kind of preparation side of oxidation resistant nanoparticle pottery ball Method.
Background technology
In recent years, due to environmental pollution, water resource wrecks seriously, and most of provinces and cities resident, which is forced to drink, passes through large size The pure water that water purifier is processed into.Water quality expert thinks, same although pure water is filtered out exceeded harmful substance is polluted When also to needed by human, beneficial trace element, minerals are dispelled.Long-term drinking be easy to cause a large amount of calcium deficiency of human body, The mineral trace elements such as potassium, magnesium, sodium cause weakness of limbs, lassitude.
Modern agriculture largely using nitrogen, phosphorus, potassium fertilizer, destroys the intrinsic element balance of human body, food chain is caused to lack, The activity of enzyme is destroyed, causes metabolic disorder.Poultry fishing cultivation producer is cultivated using antibiotic medicine, often eats this kind of food Object, drug can be accumulated in vivo, and internal germ is made to develop immunity to drugs, causes healthy hidden danger.It is dirty by the waste water of sanitary wastewater, factory The lake river water of dye cannot directly be drunk, it is necessary to be carried out biological treatment, chlorine sterilization processing to organic matter, finally be destroyed micro- Secondary element balances so that drinking water is pale tasteless, and generates a large amount of halide toxicity carcinogens.It is excessive to rely on drug, it makes one Class is absorbed in the vicious circle of immunity forfeiture.
The content of the invention
The present invention proposes a kind of preparation method of oxidation resistant nanoparticle pottery ball regarding to the issue above, is prepared Ball make pottery rich in mineral matter elements such as calcium, magnesium, silicon, potassium, sodium, phosphorus, titanium, manganese, zinc, copper, and can be used for generating mineral water, suppression Body oxidation processed, improves immunity of organisms.
Specific technical solution is as follows:
A kind of preparation method of oxidation resistant nanoparticle pottery ball, its step are as follows:
(1)Oyster shell is immersed in hydrochloric acid solution after 5-10min, is cleaned up using clear water spare;
(2)Oyster shell after cleaning is put into baking oven, is toasted under the irradiation of ultraviolet light;
(3)Oyster shell after baking is ground into that oyster shell particle is spare after being cooled to room temperature, the grain size of oyster shell particle is 0.1- 0.5mm;
(4)The zeolite granular that grain size is 0.1-0.5mm will be ground into after natural zeolite cleaning, drying;
(5)By mass percentage by oyster shell particle 25-40%, zeolite granular 25-40%, hydroxypropyl methyl cellulose 2-6%, Nano-titanium dioxide 5-12% and the nano silver of surplus sinter spherical shape into after mixing.
A kind of preparation method of above-mentioned oxidation resistant nanoparticle pottery ball, wherein, step(1)In hydrochloric acid solution quality Concentration is 2.5-5%.
A kind of preparation method of above-mentioned oxidation resistant nanoparticle pottery ball, wherein, in step(2)In, oyster shell needs to carry out Three-phase-drying for tobacco, the temperature that first segment toasts is 60-80 DEG C, time 60-80min, and the temperature of second segment baking is 120-150 DEG C, time 20-40min, the 3rd section baking temperature be 90-100 DEG C, time 10-20min.
A kind of preparation method of above-mentioned oxidation resistant nanoparticle pottery ball, wherein, step(5)In, oyster shell particle and boiling The quality parts ratio of stone particle is 1:1.
Beneficial effects of the present invention are:
The pottery ball that the present invention is prepared is rich in the mineral matter elements such as calcium, magnesium, silicon, potassium, sodium, phosphorus, titanium, manganese, zinc, copper, and can For generating mineral water, inhibit body oxidation, improve immunity of organisms.
Specific embodiment
For technical scheme is made to become apparent from clearly, below the present invention is described further, it is any to this The technical characteristic of inventive technique scheme carries out the scheme that equivalencing is drawn with conventional reasoning and each falls within the scope of the present invention.
Embodiment one
A kind of preparation method of oxidation resistant nanoparticle pottery ball, its step are as follows:
(1)Oyster shell is immersed in hydrochloric acid solution after 10min, is cleaned up using clear water spare;
(2)Oyster shell after cleaning is put into baking oven, is toasted under the irradiation of ultraviolet light;
(3)Oyster shell after baking is ground into that oyster shell particle is spare after being cooled to room temperature, the grain size of oyster shell particle is 0.15mm;
(4)The zeolite granular that grain size is 0.1mm will be ground into after natural zeolite cleaning, drying;
(5)By mass percentage by oyster shell particle 35%, zeolite granular 35%, hydroxypropyl methyl cellulose 5%, nano-silica The nano silver for changing titanium 8% and surplus sinters spherical shape into after mixing.
Step(1)In hydrochloric acid solution mass concentration be 3%.
In step(2)In, oyster shell need to carry out three-phase-drying for tobacco, and the temperature that first segment toasts is 70 DEG C, the time is 70min, the temperature that second segment toasts is 130 DEG C, time 30min, and the 3rd section of temperature toasted is 100 DEG C, the time is 15min。
Step(5)In, the quality parts ratio of oyster shell particle and zeolite granular is 1:1.
Embodiment two
A kind of preparation method of oxidation resistant nanoparticle pottery ball, its step are as follows:
(1)Oyster shell is immersed in hydrochloric acid solution after 5min, is cleaned up using clear water spare;
(2)Oyster shell after cleaning is put into baking oven, is toasted under the irradiation of ultraviolet light;
(3)Oyster shell after baking is ground into that oyster shell particle is spare after being cooled to room temperature, the grain size of oyster shell particle is 0.2mm;
(4)The zeolite granular that grain size is 0.2mm will be ground into after natural zeolite cleaning, drying;
(5)By mass percentage by oyster shell particle 40%, zeolite granular 40%, hydroxypropyl methyl cellulose 2%, nano-silica The nano silver for changing titanium 10% and surplus sinters spherical shape into after mixing.
Step(1)In hydrochloric acid solution mass concentration be 3.6%.
In step(2)In, oyster shell need to carry out three-phase-drying for tobacco, and the temperature that first segment toasts is 80 DEG C, the time is 60min, the temperature that second segment toasts is 150 DEG C, time 20min, and the 3rd section of temperature toasted is 100 DEG C, the time is 10min。
Step(5)In, the quality parts ratio of oyster shell particle and zeolite granular is 1:1.

Claims (4)

1. a kind of preparation method of oxidation resistant nanoparticle pottery ball, it is characterized in that, its step are as follows:
(1)Oyster shell is immersed in hydrochloric acid solution after 5-10min, is cleaned up using clear water spare;
(2)Oyster shell after cleaning is put into baking oven, is toasted under the irradiation of ultraviolet light;
(3)Oyster shell after baking is ground into that oyster shell particle is spare after being cooled to room temperature, the grain size of oyster shell particle is 0.1- 0.5mm;
(4)The zeolite granular that grain size is 0.1-0.5mm will be ground into after natural zeolite cleaning, drying;
(5)By mass percentage by oyster shell particle 25-40%, zeolite granular 25-40%, hydroxypropyl methyl cellulose 2-6%, Nano-titanium dioxide 5-12% and the nano silver of surplus sinter spherical shape into after mixing.
2. a kind of preparation method of oxidation resistant nanoparticle pottery ball as described in claim 1, it is characterized in that, step(1)In Hydrochloric acid solution mass concentration be 2.5-5%.
3. a kind of preparation method of oxidation resistant nanoparticle pottery ball as described in claim 1, it is characterized in that, in step(2) In, oyster shell need to carry out three-phase-drying for tobacco, and the temperature that first segment toasts is 60-80 DEG C, time 60-80min, second segment baking Temperature be 120-150 DEG C, time 20-40min, the 3rd section baking temperature be 90-100 DEG C, time 10-20min.
4. a kind of preparation method of oxidation resistant nanoparticle pottery ball as described in claim 1, it is characterized in that, step(5)In, The quality parts ratio of oyster shell particle and zeolite granular is 1:1.
CN201810040691.6A 2018-01-16 2018-01-16 A kind of preparation method of oxidation resistant nanoparticle pottery ball Pending CN108101186A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810040691.6A CN108101186A (en) 2018-01-16 2018-01-16 A kind of preparation method of oxidation resistant nanoparticle pottery ball

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Application Number Priority Date Filing Date Title
CN201810040691.6A CN108101186A (en) 2018-01-16 2018-01-16 A kind of preparation method of oxidation resistant nanoparticle pottery ball

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CN108101186A true CN108101186A (en) 2018-06-01

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010107402A1 (en) * 2009-03-17 2010-09-23 Ufuk Bakir Hemicellulose based anti-microbial anti-fog biodegradable film capable of removing undesired gases and production method thereof
CN106107414A (en) * 2016-06-24 2016-11-16 崔建中 The food fresh keeping preparation method of pottery powder
CN107512765A (en) * 2017-09-28 2017-12-26 浙江海洋大学 A kind of preparation method of modified Nano oyster shell whiting microalgae flocculant

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010107402A1 (en) * 2009-03-17 2010-09-23 Ufuk Bakir Hemicellulose based anti-microbial anti-fog biodegradable film capable of removing undesired gases and production method thereof
CN106107414A (en) * 2016-06-24 2016-11-16 崔建中 The food fresh keeping preparation method of pottery powder
CN107512765A (en) * 2017-09-28 2017-12-26 浙江海洋大学 A kind of preparation method of modified Nano oyster shell whiting microalgae flocculant

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