CN108096089A - A kind of cosmetic composition of Gotu Kola P.E with anti-inflammatory anti-oxidant complex function and its preparation method and application - Google Patents
A kind of cosmetic composition of Gotu Kola P.E with anti-inflammatory anti-oxidant complex function and its preparation method and application Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of cosmetic compositions of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function, and count by weight percentage, formula includes following components：Gotu Kola P.E 5 10%；Trifoliate orange extract 1 5%；Gentrin Knotweed P.E 1 5%；Camomile extract 2 6%；Shrubby sophora extract 3 7%；Green-tea extract 0.5 2%；Schisandra chinens P.E 0.5 2%；Surplus is cosmetic base.The present invention extracts centella with the method for homogenate extraction, the extraction efficiency of active ingredient in centella is greatly improved, operability is good, it pollutes small, reduce production cost, the triterpene substance in centella can effectively be extracted, and retain other active components therein to greatest extent, coordinate chamomile, active ingredient in trifoliate orange, with the green-tea extract with high-efficiency antioxidant effect, Gentrin Knotweed P.E, shrubby sophora extract and Schisandra chinens P.E organically combine to reach efficient anti-inflammatory anti-oxidant compound action, and it is gentle, easily absorb, it is non-stimulated, meet requirement of the people to cosmetics safety validity, it has a extensive future.
Description
Technical field
The present invention relates to a kind of cosmetic compositions of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function.
The invention further relates to a kind of cosmetic compositions of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function
Preparation method and application.
Background technology
Centella is the drying herb of Umbelliferae Centella centella, belongs to the perennial herbaceous plant that crawls, in China
East China, south China, the Central-South and ground such as southwestern.Centella is mainly used for dispelling wind and eliminating dampness, and relaxing tendons and activating collaterals has chafing good
Therapeutic effect.Wherein triterpene substance is the principle active component of centella.
Trifoliate orange, just entitled trifoliate orange, Chinese endemic tree have cultivation the areas to the south of Yellow River basin more.It is main in the dried immature fruit of citron orange to have
Limit ingredient is Flavonoid substances, has excellent antiphlogistic effects.
Giant knotweed is the dry rhizome and root of polygonaceae plant giant knotweed, is distributed in northwest, East China, Central China, south China and southwest etc.
Ground has removing dampness through diuresis and removing jaundice, clearing heat and detoxicating, scattered silt analgesic and other effects.Containing abundant resveratrol in giant knotweed, and resveratrol has
There is good antioxidant and anti-aging to act on.
Chamomile, feverfew originate in Europe, can alleviate inflammation and the pain symptom of patient, improve the skin profit of allergy
Damp skin.
The matrine contained in kuh-seng has dermatophyte certain inhibitory action, and oxymatrine have antiallergy,
Anti-inflammatory effect；It is well known that the tea polyphenols contained in green tea, catechin, caffeine, amino acid, vitamin etc. to anti-aging, kill
Bacterium, anti-inflammatory have special-effect；Schisandra chinensis also has good inhibitory action to dermatophyte.
Anti-inflammatory anti-oxidation function unobvious are used alone in the effect of each herbal medicine is different.It is accordingly, it is desirable to provide a kind of
New technology solves the above problems.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of accumulated snow of safe and efficient anti-inflammatory anti-oxidant complex function
The cosmetic composition of careless extract using the Total Of Triterpenes in homogenate extraction centella, cooperates with trifoliate orange, chamomile it is effective
Ingredient have the function that efficiently it is anti-inflammatory, giant knotweed, Schisandra chinensis, kuh-seng cooperation green tea in active ingredient reach antioxidation, will
Anti-inflammatory and antioxidation combination in these types of plant prepares a kind of cosmetics with anti-inflammatory anti-oxidant complex function
Composition.
The present invention also technical problems to be solved are to provide a kind of accumulated snow of safe and efficient anti-inflammatory anti-oxidant complex function
The preparation method and application of the cosmetic composition of careless extract.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
A kind of cosmetic composition of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function, count by weight percentage,
Formula includes following components：
Gotu Kola P.E 5-10%；
Trifoliate orange extract 1-5%；
Gentrin Knotweed P.E 1-5%；
Camomile extract 2-6%；
Shrubby sophora extract 3-7%；
Green-tea extract 0.5-2%；
Schisandra chinens P.E 0.5-2%；
Surplus is cosmetic base.
A kind of preparation method of the cosmetic composition of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function, including
Following steps：
（1）Centella raw material is taken, the 50-60 DEG C of machine of dry, pulverize is ground into coarse powder, by 1：10-15 ratios add in solvent, flash to carry
3-5min is taken, is extracted 2 times；
（2）Trifoliate orange raw material is chosen, adds in 3-5 times of solvent, 40-60 DEG C of Microwave Extraction 20-40min, filter paper filtering, filtrate is Chinese holly
Tangerine extract；
（3）Giant knotweed raw material is weighed, adds in giant knotweed 4-8 times of solvent of raw material, 60-80 DEG C of water-bath 1-2h, filter paper filtering, filtrate is tiger
Cane extract；
（4）Chamomile raw material is chosen, adds in 3-5 times of solvent, 20-30 DEG C of ultrasonic extraction 20-40min, filter paper filters, and filtrate is
Camomile extract；
（5）Kuh-seng raw material is weighed, adds in 4-6 times of solvent, 50-60 DEG C of water-bath 1-2h, filter paper filtering, filtrate is kuh-seng extraction
Object；
（6）Green tea materials are weighed, add in 6-10 times of solvent, 60-80 DEG C of water-bath 1-2h, filter paper filtering, filtrate is green tea extraction
Object；
（7）Schisandra raw material is weighed, adds in 4-8 times of solvent, 60-80 DEG C of water-bath 1-2h, filter paper filtering, filtrate is that Schisandra chinensis carries
Take object.
By formula measure Gotu Kola P.E, trifoliate orange extract, Gentrin Knotweed P.E, camomile extract, shrubby sophora extract,
Green-tea extract, Schisandra chinens P.E and cosmetic base are fitted into after dissolving mixing in the bottle sterilized.
Solvent in step 2 is one kind in 1,3 butanediols of deionized water or joint, propylene glycol, dipropylene glycol.
A kind of application of Gotu Kola P.E in the cosmetic composition with anti-inflammatory anti-oxidant complex function is prepared.
Beneficial effects of the present invention：The preparation method of the present invention is improved using active ingredient in homogenate extraction method extraction centella
Extraction efficiency, operability is good, can effectively extract the triterpene substance in centella, and retain to greatest extent it is therein its
His active ingredient, the active ingredient in cooperation chamomile, trifoliate orange, with the green-tea extract with high-efficiency antioxidant effect, giant knotweed
Extract, shrubby sophora extract and Schisandra chinens P.E organically combine to reach efficient anti-inflammatory anti-oxidant compound action, and matter
Ground is mild, easily absorbs, non-stimulated, meets requirement of the people to cosmetics safety validity, has a extensive future.
Description of the drawings
Fig. 1 be calmness of the present invention releive liquid remove DPPH experimental result pictures.
The present invention is described in further detail With reference to embodiment.
Specific embodiment：
The preparation method of Gotu Kola P.E in the present invention, comprises the following steps：
Centella raw material is taken, the 50-60 DEG C of machine of dry, pulverize is ground into coarse powder, by 1：10-15 ratios add in solvent, homogenate extraction
3-5min is extracted 2 times；
Gotu Kola P.E made from preparation method of the present invention is being prepared with anti-inflammatory anti-oxidant compound with reference to embodiments
Application in the cosmetic composition of function is described in further details, but these embodiments are not limitation of the invention.
The compound Scavenging activity for free radical of Gotu Kola P.E is tested：
First, reagent prepares
1 3.943mgDPPH is settled to 50mL with 95% ethyl alcohol；
2 10mg or so Trolox is settled to 100mL with 95% ethyl alcohol；
3 Gotu Kola P.Es are compound.
2nd, experimental procedure
（1）3.943mgDPPH is settled to 50mL with 95% ethyl alcohol；
（2）UV schools zero, for 95% ethyl alcohol as blank sample, allocation list is as shown in table 3 below；
（3）500 μ L DPPH+1000 μ L, 95% ethyl alcohol shakes 10s, stands 10min, absorbance is surveyed twice, such as the following table 3 institute
Show.
Table 1
Table 2
Table 3
It is understood in conjunction with Fig. 1：Centella is compounded with the effect of good removing DPPH free radicals, and IC50 values are 546 μ g/mL, and
The compound content of centella is higher, and the ability for removing free radical is also stronger.
Embodiment 1-3 is the embodiment of the preparation method of cosmetic composition
Embodiment 1
A kind of preparation method of the cosmetic composition of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function, including following
Step：
（1）High-quality centella raw material is taken, 50 DEG C of machines of dry, pulverize are ground into coarse powder, by 1：10 ratios add in solvent, homogenate extraction
3min is extracted 2 times；
（2）It chooses high-quality trifoliate orange raw material and adds in 3 times of solvents, 40 DEG C of Microwave Extraction 20min, filter paper filtering, filtrate is trifoliate orange extraction
Object；
（3）It weighs giant knotweed raw material and adds in 4 times of solvents, 60 DEG C of water-bath 1h, filter paper filtering, filtrate is Gentrin Knotweed P.E；
（4）It chooses chamomile raw material and adds in 3 times of solvents, 20 DEG C of ultrasonic extraction 20min, filter paper filtering, filtrate is chamomile extraction
Object；
（5）It weighs kuh-seng raw material and adds in 4 times of solvents, 50 DEG C of water-bath 1h, filter paper filtering, filtrate is shrubby sophora extract；
（6）It weighs green tea materials and adds in 6 times of solvents, 60 DEG C of water-bath 1h, filter paper filtering, filtrate is green-tea extract；
（7）It weighs schisandra raw material and adds in 4 times of solvents, 60 DEG C of water-bath 1h, filter paper filtering, filtrate is Schisandra chinens P.E.
By formula measure Gotu Kola P.E, trifoliate orange extract, Gentrin Knotweed P.E, camomile extract, shrubby sophora extract,
Green-tea extract, Schisandra chinens P.E and cosmetic base are fitted into after dissolving mixing in the bottle sterilized.
Embodiment 2
A kind of preparation method of the cosmetic composition of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function, including following
Step：
（1）High-quality centella raw material is taken, 55 DEG C of machines of dry, pulverize are ground into coarse powder, by 1：12 ratios add in solvent, homogenate extraction
3min is extracted 2 times；
（2）It chooses high-quality trifoliate orange raw material and adds in 4 times of solvents, 50 DEG C of Microwave Extraction 30min, filter paper filtering, filtrate is trifoliate orange extraction
Object；
（3）It weighs giant knotweed raw material and adds in 6 times of solvents, 70 DEG C of water-bath 1.5h, filter paper filtering, filtrate is Gentrin Knotweed P.E；
（4）It chooses chamomile raw material and adds in 4 times of solvents, 25 DEG C of ultrasonic extraction 30min, filter paper filtering, filtrate is chamomile extraction
Object；
（5）It weighs kuh-seng raw material and adds in 5 times of solvents, 55 DEG C of water-bath 1.5h, filter paper filtering, filtrate is shrubby sophora extract；
（6）It weighs green tea materials and adds in 8 times of solvents, 70 DEG C of water-bath 1.5h, filter paper filtering, filtrate is green-tea extract；
（7）It weighs schisandra raw material and adds in 6 times of solvents, 70 DEG C of water-bath 1.5h, filter paper filtering, filtrate is Schisandra chinens P.E.
By formula measure Gotu Kola P.E, trifoliate orange extract, Gentrin Knotweed P.E, camomile extract, shrubby sophora extract,
Green-tea extract, Schisandra chinens P.E and cosmetic base are fitted into after dissolving mixing in the bottle sterilized.
Embodiment 3
A kind of preparation method of the cosmetic composition of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function, including following
Step：
（1）High-quality centella raw material is taken, 60 DEG C of machines of dry, pulverize are ground into coarse powder, by 1：15 ratios add in solvent, flash to carry
3min is taken, is extracted 2 times；
（2）It chooses high-quality trifoliate orange raw material and adds in 5 times of solvents, 60 DEG C of Microwave Extraction 40min, filter paper filtering, filtrate is trifoliate orange extraction
Object；
（3）It weighs giant knotweed raw material and adds in 8 times of solvents, 80 DEG C of water-bath 2h, filter paper filtering, filtrate is Gentrin Knotweed P.E；
（4）It chooses chamomile raw material and adds in 5 times of solvents, 30 DEG C of ultrasonic extraction 40min, filter paper filtering, filtrate is chamomile extraction
Object；
（5）It weighs kuh-seng raw material and adds in 6 times of solvents, 60 DEG C of water-bath 2h, filter paper filtering, filtrate is shrubby sophora extract；
（6）It weighs green tea materials and adds in 10 times of solvents, 80 DEG C of water-bath 2h, filter paper filtering, filtrate is green-tea extract；
（7）It weighs schisandra raw material and adds in 8 times of solvents, 80 DEG C of water-bath 2h, filter paper filtering, filtrate is Schisandra chinens P.E.
By formula measure Gotu Kola P.E, trifoliate orange extract, Gentrin Knotweed P.E, camomile extract, shrubby sophora extract,
Green-tea extract, Schisandra chinens P.E and cosmetic base are fitted into after dissolving mixing in the bottle sterilized.
Cosmetics embodiment 4-6 is as follows made of the above method：
Embodiment 4
Cosmetics with the anti-oxidant complex function of antiallergic, dosage form are Essence, and count by weight percentage, formula includes
Following components：
Gotu Kola P.E 5%；Trifoliate orange extract 2%；Gentrin Knotweed P.E 1%；Camomile extract 3%；Shrubby sophora extract 3%；It is green
Tea extraction 0.5%；Schisandra chinens P.E 0.5%；1,3 butanediols 2%；Preservative 0.5%；Surplus is deionized water.
Each component is measured by formula, is fitted at normal temperatures after mixing in the bottle sterilized.
Embodiment 5
Cosmetics with the anti-oxidant complex function of antiallergic, dosage form are elite breast, and count by weight percentage, formula includes
Following components：
A phases：Cetostearyl alcohol 1.5%；Tristerin 1%；Polyoxyethylene sorbitan monooleate 1.5%；Sorb
Sugar alcohol 0.5%；D-pantothenyl aleohol 1%；1,3 pentanediols 0.5%；
B phases：Gotu Kola P.E 7%；Trifoliate orange extract 3%；Gentrin Knotweed P.E 1%；Camomile extract 5%；Shrubby sophora extract
5%；Green-tea extract 1%；Schisandra chinens P.E 1%；1,3 butanediols 2%；Preservative 0.5%；Surplus is deionized water.
A phases and B phases are measured by formula, is dissolved respectively at a temperature of 70-80 DEG C, then mixing, is packed into the bottle sterilized
In.
Embodiment 6
Cosmetics with the anti-oxidant complex function of antiallergic, dosage form are moisturiser, and count by weight percentage, formula includes
Following components：
Gotu Kola P.E 10%；Trifoliate orange extract 5%；Gentrin Knotweed P.E 5%；Camomile extract 6%；Shrubby sophora extract 7%；
Green-tea extract 2%；Schisandra chinens P.E 2%；Surplus is cosmetic base.
The present invention extracts centella using the method for homogenate extraction, and the extraction effect of active ingredient in centella is greatly improved
Rate, operability is good, and pollution is small, reduces production cost, can effectively extract the triterpene substance in centella, and to greatest extent
Reservation other active components therein, cooperation chamomile, the active ingredient in trifoliate orange, and with the green of high-efficiency antioxidant effect
Tea extraction, Gentrin Knotweed P.E, shrubby sophora extract and Schisandra chinens P.E organically combine to reach efficient anti-inflammatory anti-oxidant
Compound action, and be gentle, easily absorb, it is non-stimulated, meet requirement of the people to cosmetics safety validity, application prospect is wide
It is wealthy.
Claims (4)
1. a kind of cosmetic composition of the Gotu Kola P.E with anti-inflammatory anti-oxidant complex function, which is characterized in that by weight
Percentage calculation is measured, formula includes following components：
Gotu Kola P.E 5-10%；
Trifoliate orange extract 1-5%；
Gentrin Knotweed P.E 1-5%；
Camomile extract 2-6%；
Shrubby sophora extract 3-7%；
Green-tea extract 0.5-2%；
Schisandra chinens P.E 0.5-2%；
Surplus is cosmetic base.
2. a kind of cosmetic combinations of Gotu Kola P.E with anti-inflammatory anti-oxidant complex function according to claim 1
The preparation method of object, which is characterized in that comprise the following steps：
（1）Centella raw material is taken, the 50-60 DEG C of machine of dry, pulverize is ground into coarse powder, by 1：10-15 ratios add in solvent, flash to carry
3-5min is taken, is extracted 2 times；
（2）Trifoliate orange raw material is chosen, adds in 3-5 times of solvent, 40-60 DEG C of Microwave Extraction 20-40min, filter paper filtering, filtrate is Chinese holly
Tangerine extract；
（3）Giant knotweed raw material is weighed, adds in giant knotweed 4-8 times of solvent of raw material, 60-80 DEG C of water-bath 1-2h, filter paper filtering, filtrate is tiger
Cane extract；
（4）Chamomile raw material is chosen, adds in 3-5 times of solvent, 20-30 DEG C of ultrasonic extraction 20-40min, filter paper filters, and filtrate is
Camomile extract；
（5）Kuh-seng raw material is weighed, adds in 4-6 times of solvent, 50-60 DEG C of water-bath 1-2h, filter paper filtering, filtrate is kuh-seng extraction
Object；
（6）Green tea materials are weighed, add in 6-10 times of solvent, 60-80 DEG C of water-bath 1-2h, filter paper filtering, filtrate is green tea extraction
Object；
（7）Schisandra raw material is weighed, adds in 4-8 times of solvent, 60-80 DEG C of water-bath 1-2h, filter paper filtering, filtrate is that Schisandra chinensis carries
Take object.
Gotu Kola P.E, trifoliate orange extract, Gentrin Knotweed P.E, camomile extract, shrubby sophora extract, green tea are measured by formula
Extract, Schisandra chinens P.E and cosmetic base are fitted into after dissolving mixing in the bottle sterilized.
3. a kind of preparation of centella cosmetic composition with anti-inflammatory anti-oxidant complex function according to claim 2
Method, it is characterised in that：Solvent in step 2 is one in 1,3 butanediols of deionized water or joint, propylene glycol, dipropylene glycol
Kind.
4. a kind of application of Gotu Kola P.E in the cosmetic composition with anti-inflammatory anti-oxidant complex function is prepared.
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| CN109363991A (en) * | 2018-11-28 | 2019-02-22 | 澳宝化妆品（惠州）有限公司 | A kind of skin care compositions of the plant extracts containing antiallergy |
| CN110859785A (en) * | 2019-12-02 | 2020-03-06 | 江苏巴帝恩生物科技有限公司 | Preparation method and application of anti-allergy compound |
| CN111904911A (en) * | 2020-08-25 | 2020-11-10 | 云南省药物研究所 | Panax notoginseng-containing plant antioxidant composition and application thereof |
| CN111904911B (en) * | 2020-08-25 | 2023-04-07 | 云南省药物研究所 | Panax notoginseng-containing plant antioxidant composition and application thereof |
| CN112656707A (en) * | 2020-12-29 | 2021-04-16 | 中华全国供销合作总社南京野生植物综合利用研究所 | Extraction method of centella asiatica polysaccharide extract, centella asiatica polysaccharide extract and application thereof |
| CN113456558A (en) * | 2021-06-16 | 2021-10-01 | 陈应荣 | Formula and preparation method of free radical-removing, antibacterial and nourishing product for skin and mucosa |
| CN113893274A (en) * | 2021-09-29 | 2022-01-07 | 怀化学院 | Preparation method of antibacterial honey mask containing centella asiatica extract |
| CN115227617A (en) * | 2022-08-09 | 2022-10-25 | 润芳可(上海)生物科技有限公司 | Skin repairing composition and preparation method and application thereof |
| CN117883500A (en) * | 2024-01-19 | 2024-04-16 | 广州腾麟生物科技有限公司 | Composition containing anti-inflammatory active ingredients and preparation method and application thereof |
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