CN108077256A - A kind of phthorimaea operculella lure composition and its application - Google Patents
A kind of phthorimaea operculella lure composition and its application Download PDFInfo
- Publication number
- CN108077256A CN108077256A CN201810025149.3A CN201810025149A CN108077256A CN 108077256 A CN108077256 A CN 108077256A CN 201810025149 A CN201810025149 A CN 201810025149A CN 108077256 A CN108077256 A CN 108077256A
- Authority
- CN
- China
- Prior art keywords
- phthorimaea operculella
- lure
- synergist
- sex pheromone
- operculella
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01M—CATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
- A01M7/00—Special adaptations or arrangements of liquid-spraying apparatus for purposes covered by this subclass
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
- A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
Abstract
The invention discloses a kind of phthorimaea operculella lure compositions and its application for belonging to insect sex pheromone preparing technical field.The phthorimaea operculella lure composition includes phthorimaea operculella sex pheromone and synergist, the main component of the phthorimaea operculella sex pheromone is anti-4, along 7 oleatridecadiene, 1 alcohol acetate and anti-4, along 7 tridecatriene, 1 alcohol acetate, mass ratio 4:1, the synergist is selected from plant volatiles：One or more in birch oil, butyl salicylate, salicylic acid leaf-alcohol ester.Phthorimaea operculella lure composition provided by the invention can accurately be applied to phthorimaea operculella detecting and reporting pest information, pest quarantine, mass trapping, be of great significance for comprehensive treatment phthorimaea operculella.
Description
Technical field
The present invention relates to insect sex pheromone preparing technical fields, are combined more particularly to a kind of phthorimaea operculella lure
Object and its application.
Background technology
Phthorimaea operculella Phthorimaea operculella (Zeller) also known as tobacco leaf miner, are bored with larva
Eat into a kind of oligophagy pest of cause harm potato and tobacco.In the growth period of potato and tobacco, Adult worms producting eggs are incubated at vein
Mesophyll, the terminal bud of the larva moth food host of change, seriously affects plant strain growth and cigarette quality.In potato harvest phase Adult worms producting eggs
In exposed at the potato wedge bud eye of Tu Biaochu, the potato wedge with ovum is transported to more tight to the potato harm of storage period in warehouse
Weight, the aggrieved rate of potato tubers of storage 4 months lose edible value completely up to 100%.Due to the children of phthorimaea operculella
For worm brill moth to causing harm inside host, long-term chemopreventive effects are unsatisfactory.Long-time service Agro-chemicals control potato ball
Stem moth may make pest develop immunity to drugs, kill natural enemy, polluting environment and destroy ecosystem etc..In face of applied chemistry medicament
The variety of problems brought, the mankind will be gradually converted into biological control, explore the mode of sustainable control.
In nature, phthorimaea operculella female adult pest can discharge a kind of compound for being sex pheromone after sexal maturity,
Male worm is lured to mate to produce offspring to release source orientation flight, and with release female adult pest.Insect sex attractant product is bionical height
Sci-tech product, discharges artificial synthesized sex pheromone compound by lure, and is sustained to field, lures male moth to trapper,
And male moth is killed with Physical, so as to destroy its mating, it is finally reached the purpose of prevention.But general sex pheromone can only lure
Male worm, unavoidable male worm have mated pest great outburst caused by the moving into of female adult there are multiple mating and non-process area.
It, can be to male and female with reference to sex pheromone and plant volatile according to the interaction between insect and host plant volatile
Worm is more effectively traped.Therefore, the formula rate specified between phthorimaea operculella sex pheromone and plant volatile can
Accurately it is applied to detecting and reporting pest information, pest quarantine, mass trapping, so as to reach the ideal effect of comprehensive treatment phthorimaea operculella.
The content of the invention
It is an object of the invention to provide a kind of phthorimaea operculella lure composition and its applications.
The lure composition of a kind of phthorimaea operculella provided by the invention, including phthorimaea operculella sex pheromone and association
Same agent, the phthorimaea operculella sex pheromone are trans- 4, cis- 7- oleatridecadienes -1- alcohol acetates and/or trans- 4, cis- 7-
Tridecanayl triene -1 -ol acetate, the synergist is birch oil, one kind or one kind in butyl salicylate, salicylic acid leaf-alcohol ester
More than.
Optionally, the weight ratio of the phthorimaea operculella sex pheromone and synergist is 1:(0.5~10)；The Ma Ling
Potato wedge stem moth sex pheromone is trans- 4, cis- 7- oleatridecadienes -1- alcohol acetates and trans- 4, cis- 7- tridecanayl triene -1s -ol
Acetate, mass ratio 4:1.
Preferably, the weight ratio of the phthorimaea operculella sex pheromone and synergist is 1:(1~5).
Optionally, the synergist is made of following components according to respective parts by weight：0~9 part of birch oil, butyl salicylate
0~9 part, 0~9 part of salicylic acid leaf-alcohol ester.
Preferably, the synergist is made of following components according to respective parts by weight：1~5 part of birch oil, butyl salicylate
3~7 parts, 1~5 part of salicylic acid leaf-alcohol ester.
The present invention also provides a kind of application of phthorimaea operculella lure composition, the application is included the synergist
It is applied in the lure containing phthorimaea operculella sex pheromone；Or by the synergist and phthorimaea operculella sex pheromone
It mixes in the after-applied lure to blank；Or include and the synergist is applied in the lure of blank, then the association will be contained
Lure with agent is used with the collocation of phthorimaea operculella sex pheromone.
It is prevented and/or the method for monitoring phthorimaea operculella the present invention also provides a kind of, including by above-mentioned potato tubers
Moth lure composition is applied to the spot of phthorimaea operculella.
Optionally, the dosage of the phthorimaea operculella lure composition is 0.1~10mg/m2。
Preferably, the dosage of the phthorimaea operculella lure composition is 0.5~2.5mg/m2。
Beneficial effects of the present invention：1) occupation mode is flexible, and the present invention provides phthorimaea operculella lure composition, including
Phthorimaea operculella sex pheromone and its synergist can be made synergist lure and match somebody with somebody with phthorimaea operculella sex pheromone lure core
It closes and uses, phthorimaea operculella sex pheromone solution conjunction with which agent solution can also be mixed, lure composition lure is made
It uses；Multiple components can be used alone with unrestricted choice or are used in conjunction with according to proportioning, and independence is stronger；2) with only containing
Phthorimaea operculella sex pheromone and compared without the lure of its synergist, using containing phthorimaea operculella sex pheromone and its
The lure of synergist ingredient shows stronger trapping activity in the phthorimaea operculella trapping experiments in field；3) present invention carries
The synergist ingredient of confession is cheap, can reduce the cost for making lure, suitable for popularizing.
Description of the drawings
Fig. 1 is the structure diagram of birch oil.
Fig. 2 is the structure diagram of butyl salicylate.
Fig. 3 is the structure diagram of salicylic acid leaf-alcohol ester.
Specific embodiment
The specific embodiment of the present invention is described in detail below, it is to be understood that protection scope of the present invention is not
It is restricted by specific implementation.
The present invention provides a kind of phthorimaea operculella lure composition, including phthorimaea operculella sex pheromone and collaboration
Agent；
The phthorimaea operculella sex pheromone is trans- 4, cis- 7- oleatridecadienes -1- alcohol acetates and trans- 4, cis- 7-
Tridecanayl triene -1 -ol acetate, mass ratio 4:1.
As one embodiment of the present of invention, the phthorimaea operculella lure composition is by following components according to each dead weight
Measure part composition：5 parts of phthorimaea operculella sex pheromones and 5 parts of butyl salicylates.
As one embodiment of the present of invention, the phthorimaea operculella lure composition is by following components according to each dead weight
Measure part composition：5 parts of phthorimaea operculella sex pheromones, 5 parts of birch oils (Fig. 1), 5 parts of butyl salicylates (Fig. 2) and 5 parts of salicylic acid leaves
Alcohol ester (Fig. 3).
As one embodiment of the present of invention, the phthorimaea operculella lure composition is by following components according to each dead weight
Measure part composition：5 parts of phthorimaea operculella sex pheromones, 3 parts of birch oils, 5 parts of butyl salicylates and 3 parts of salicylic acid leaf-alcohol esters.
As one embodiment of the present of invention, the phthorimaea operculella lure composition is by following components according to each dead weight
Measure part composition：5 parts of phthorimaea operculella sex pheromones, 1 part of birch oil, 2 parts of butyl salicylates and 1 part of salicylic acid leaf-alcohol ester.
The present invention also provides a kind of phthorimaea operculella lure composition in preventing and/or monitoring phthorimaea operculella
Application, specifically, the application form of phthorimaea operculella lure provided by the invention can there are many, as long as potato can be made
The agent of stem tuber moth sex pheromone conjunction with which generates synergistic effect, improves trapping activity.
In one embodiment, the application can include the synergist being applied to containing phthorimaea operculella property
In the lure of pheromones.
In another embodiment, the application can be included the synergist and phthorimaea operculella sex pheromone
Mix it is after-applied in the blank lure without phthorimaea operculella sex pheromone, being made synergist lure, then by the synergist
Lure is used cooperatively with phthorimaea operculella sex pheromone lure core.
In another embodiment, the application can include the synergist mixing after-applied arrive with sex pheromone
In blank lure.
The present invention also provides the lures containing phthorimaea operculella sex pheromone and its lure composition of synergist.
The present invention also provides the preparation method of the lure, including：It will be dripped containing the hexane solution of the synergist
It is added in the lure containing phthorimaea operculella sex pheromone, dichloromethane is added drop-wise in the lure after n-hexane volatilization,
The lure containing phthorimaea operculella sex pheromone and its synergist is made after dichloromethane volatilization.It can be lured manufactured
Core is packed into aluminium foil interior sealing, is preserved at -20 DEG C.
In another embodiment, collaboration agent solution can be added drop-wise to the sky without phthorimaea operculella sex pheromone
In white lure, synergist lure is made.The preparation method of the synergist lure can include：By containing the synergist just
Hexane solution is added drop-wise on carrier (for example, on partition of anti-mouth formula rubber stopper)；Dichloromethane is added dropwise after n-hexane volatilization
Onto the carrier, the lure containing synergist is made after dichloromethane volatilization.Manufactured synergist lure can be packed into
Aluminium foil interior sealing preserves at -20 DEG C, then is used cooperatively with phthorimaea operculella sex pheromone lure core.
The concentration of the hexane solution of the phthorimaea operculella sex pheromone can be 600 μ g/mL.The synergist
The concentration of hexane solution is 600 μ g/mL.
The present invention also provides it is a kind of prevent and/or monitoring phthorimaea operculella method, including by the present invention Ma Ling
Potato wedge stem moth lure composition is applied to the habitat of phthorimaea operculella.The dosage of the phthorimaea operculella lure composition
1.0mg/m2。
In order to further illustrate the feasibility of phthorimaea operculella lure composition provided by the invention, with reference to specific
Experiment illustrate.
In Fields of Qujing City in Yunnan Zhanyi County, big slope native soil bridge village expansion experiment carries out synergist cooperation phthorimaea operculella property letter
The trap effect experiment of the plain lure of breath.
The purity of phthorimaea operculella sex pheromone component and plant volatile component used and supplier etc. in embodiment
Information is as shown in table 1.
The relevant information of 1 phthorimaea operculella lure composition component of table
Birch oil, butyl salicylate and salicylic acid leaf-alcohol ester are each dissolved in n-hexane with the concentration of 500 μ g/mL respectively
In, 1mL is taken to be added dropwise by several times on the partition of the rubber stopper cleaned with n-hexane, by 1mL dichloromethane after n-hexane volatilization
It is added dropwise by several times, synergist lure is made after dichloromethane volatilization.By the synergist of manufactured single, two components and three components
Lure is packed into aluminium foil interior sealing, is preserved at -20 DEG C.
The preparation method of the phthorimaea operculella sex pheromone lure core is as follows：
Step 1, by phthorimaea operculella sex pheromone component trans- 4, cis- 7- oleatridecadienes -1- alcohol acetates and trans-
4, cis- 7- tridecanayl triene -1s -ol acetate, by using mass ratio as 4:1 is sufficiently mixed.
Step 2, the mixture for obtaining step 1 are dissolved in n-hexane, and the n-hexane pheromones solution concentration of preparation is 600
μg/mL。
The pheromones solution 2mL that step 2 obtains is added drop-wise in blank rubber lure, obtained Ma Ling by step 3 by several times
The dosage of the pheromones contained in potato wedge stem moth sex pheromone lure core is 1200 μ g/ lures.Horse described in lure is combined in experiment
Bell potato wedge stem moth is that the solution for obtaining step 2 about 1mL is added drop-wise in blank rubber lure by several times for sex pheromone lure core, gained
To phthorimaea operculella sex pheromone lure core on the dosage of pheromones that contains be 600 μ g/ lures.
When carrying out trapping experiments in field, synergist lure is fixed on the universal trapper epimere of moth class with thin wire
(the universal trapper of moth class is purchased from Pherobio Technology Co., Ltd.), by trapper be suspended on Potato Cultivars,
Growing way, fertilizer and water management are consistent, in flakes potato fields of the area at 10 mu or more, while coordinate phthorimaea operculella property information
Plain lure is used in conjunction with.
When carrying out trapping experiments in field, by phthorimaea operculella lure composition lure or phthorimaea operculella property information
Plain lure is fixed on the universal trapper of moth class.CK1 is without phthorimaea operculella lure composition lure or potato tubers
The blank control of moth sex pheromone lure core；The control of CK2 only phthorimaea operculella sex pheromone lure cores；X1 groups to X3 groups are single group
Divide the processing of synergist lure；X4 groups to X6 groups are the processing of the phthorimaea operculella lure composition lure containing one-component；
01 group to the 03 group processing for the phthorimaea operculella lure composition lure of the synergist containing bi-component；04 group to 10 groups is containing three
The processing of the phthorimaea operculella lure composition lure of component synergist.Each processing sets three repetitions, random alignment, phase
Two 15~30m of trapper interval of neighbour.After setting from second day, every morning records the phthorimaea operculella quantity traped
And remove it in time, persistently investigate 30 days.Result of the test is as shown in table 2.
Field synergistic effect of the 2 different component synergist of table to phthorimaea operculella sex pheromone
One pack system synergist has phthorimaea operculella attractive activity as shown in Table 2, but trap effect is significantly lower than Ma Ling
The trap effect of potato wedge stem moth sex pheromone in itself.But make after one pack system synergist is mixed with phthorimaea operculella sex pheromone
With trap effect is apparently higher than only with the trap effect of one pack system synergist in itself.The trapping amount of phthorimaea operculella is with collaboration
The increase of agent quantity and increase, synergist and sex pheromone are mixed in different formulations ratio, the trapping of sex pheromone lure core is equal
Higher than the trap effect of sex pheromone in itself, and the dosage of sex pheromone greatly reduces.
Phthorimaea operculella lure composition provided by the invention can accurately be applied to phthorimaea operculella detecting and reporting pest information, evil
Worm quarantine, mass trapping, are of great significance for comprehensive treatment phthorimaea operculella.And the phthorimaea operculella lure group
It closes object and prepares simple, using simple, condition is feasible, has very strong trapping capability, and stability is good；Meanwhile the potato tubers
Moth lure composition specificity is strong, does not generate resistance, and natural enemy is not injured, nontoxic to people and animals, environmental-friendly；Resistance is strong,
It is not afraid of wind, rainforest and solarization；Lasting period is long, and control effect can maintain 30 days or so.
Those of ordinary skills in the art should understand that：The above is only a specific embodiment of the present invention, and
The limitation present invention is not used in, within the spirit and principles of the invention, any modification, equivalent substitution, improvement and etc. done,
It should be included within protection scope of the present invention.
Claims (6)
1. a kind of phthorimaea operculella lure composition, which is characterized in that including phthorimaea operculella sex pheromone and synergist,
The phthorimaea operculella sex pheromone is trans- 4, cis- 7- oleatridecadienes -1- alcohol acetates and/or trans- 4, cis- 7- 13
Carbon triolefin -1- alcohol acetates, the synergist is birch oil, the one or more in butyl salicylate, salicylic acid leaf-alcohol ester.
A kind of 2. phthorimaea operculella lure composition according to claim 1, which is characterized in that the phthorimaea operculella
The weight ratio of sex pheromone and synergist is 1:（0.5~10）；The phthorimaea operculella sex pheromone is trans- 4, cis- 7- 13
Carbon diene -1- alcohol acetates and trans- 4, cis- 7- tridecanayl triene -1s -ol acetate, mass ratio 4:1.
3. a kind of phthorimaea operculella lure composition according to claim 1, which is characterized in that the synergist is by following
The component composition of parts by weight：0 ~ 9 part of birch oil, 0 ~ 9 part of butyl salicylate, 0 ~ 9 part of salicylic acid leaf-alcohol ester.
4. the application of the phthorimaea operculella lure composition described in claim 1, which is characterized in that the application includes will
The synergist is applied in the lure containing phthorimaea operculella sex pheromone；Or by the synergist and potato ball
Stem moth sex pheromone is mixed in the after-applied lure to blank；Or the synergist is applied in the lure of blank, then will
Lure containing the synergist is used with the collocation of phthorimaea operculella sex pheromone.
It is prevented and/or the method for monitoring phthorimaea operculella 5. a kind of, which is characterized in that including by the horse described in claim 1
Bell potato wedge stem moth lure composition is applied to the spot of phthorimaea operculella.
6. the method for preventing according to claim 5 and/or monitoring phthorimaea operculella, which is characterized in that the potato
The dosage of stem tuber moth lure composition is 0.1 ~ 10 mg/m2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810025149.3A CN108077256A (en) | 2018-01-11 | 2018-01-11 | A kind of phthorimaea operculella lure composition and its application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810025149.3A CN108077256A (en) | 2018-01-11 | 2018-01-11 | A kind of phthorimaea operculella lure composition and its application |
Publications (1)
| Publication Number | Publication Date |
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| CN108077256A true CN108077256A (en) | 2018-05-29 |
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ID=62181986
Family Applications (1)
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| CN201810025149.3A Pending CN108077256A (en) | 2018-01-11 | 2018-01-11 | A kind of phthorimaea operculella lure composition and its application |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110278950A (en) * | 2019-07-04 | 2019-09-27 | 南京新安中绿生物科技有限公司 | Phthorimaea operculella eats lure and its application |
| CN110292043A (en) * | 2019-08-02 | 2019-10-01 | 中国农业科学院植物保护研究所 | A kind of phthorimaea operculella sex attractant of system optimization and its application |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4014942A (en) * | 1975-08-06 | 1977-03-29 | Zoecon Corporation | Novel acetal |
| CN103190419A (en) * | 2013-05-01 | 2013-07-10 | 云南农业大学 | Phthorimaea operculella zell attractant |
-
2018
- 2018-01-11 CN CN201810025149.3A patent/CN108077256A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4014942A (en) * | 1975-08-06 | 1977-03-29 | Zoecon Corporation | Novel acetal |
| CN103190419A (en) * | 2013-05-01 | 2013-07-10 | 云南农业大学 | Phthorimaea operculella zell attractant |
Non-Patent Citations (1)
| Title |
|---|
| 马艳粉等: "滇杨挥发物成分对马铃薯块茎蛾产卵选择的影响", 《植物保护》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110278950A (en) * | 2019-07-04 | 2019-09-27 | 南京新安中绿生物科技有限公司 | Phthorimaea operculella eats lure and its application |
| CN110278950B (en) * | 2019-07-04 | 2022-02-22 | 南京新安中绿生物科技有限公司 | Potato tuber moth feed attractant and application thereof |
| CN110292043A (en) * | 2019-08-02 | 2019-10-01 | 中国农业科学院植物保护研究所 | A kind of phthorimaea operculella sex attractant of system optimization and its application |
| CN110292043B (en) * | 2019-08-02 | 2020-09-04 | 中国农业科学院植物保护研究所 | Sex attractant for tuber moth with optimized system and application thereof |
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