CN108051069B - Calibration method of X-ray nucleon balance and X-ray nucleon balance - Google Patents

Calibration method of X-ray nucleon balance and X-ray nucleon balance Download PDF

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Publication number
CN108051069B
CN108051069B CN201810017206.3A CN201810017206A CN108051069B CN 108051069 B CN108051069 B CN 108051069B CN 201810017206 A CN201810017206 A CN 201810017206A CN 108051069 B CN108051069 B CN 108051069B
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ray
tube
source
zero point
parameter
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CN108051069A (en
Inventor
王文清
任凤国
王怀群
田柏林
樊利军
李萍
张中华
任安祥
侯世亮
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Beijing Coal Mining Electric Equipment Technical Development Co ltd
Beijing University of Technology
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Beijing Coal Mining Electric Equipment Technical Development Co ltd
Beijing University of Technology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01GWEIGHING
    • G01G23/00Auxiliary devices for weighing apparatus
    • G01G23/01Testing or calibrating of weighing apparatus
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01GWEIGHING
    • G01G9/00Methods of, or apparatus for, the determination of weight, not provided for in groups G01G1/00 - G01G7/00
    • G01G9/005Methods of, or apparatus for, the determination of weight, not provided for in groups G01G1/00 - G01G7/00 using radiations, e.g. radioactive

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)

Abstract

The invention provides a calibration method of an X-ray nucleon scale and the X-ray nucleon scale. The calibration method provided by the invention is applied to an X-ray nucleon balance, and the X-ray nucleon balance comprises the following components: an X-ray source, an X-ray detector, a bracket and a weighing instrument; the method comprises the following steps: the weighing instrument acquires the X-ray energy and intensity output by the X-ray detector and the tube voltage parameter and the tube current parameter sent by the X-ray source; the weighing instrument respectively determines the offset of the tube voltage parameter and the offset of the tube current parameter according to the tube voltage parameter and the tube current parameter; the X-ray source adjusts the tube voltage parameter and the tube current parameter according to the offset of the tube voltage parameter and the offset of the tube current parameter. According to the calibration method provided by the embodiment of the invention, the X-ray detector is used as a feedback sensor for monitoring the energy and the intensity of the X-rays, and the tube voltage and the tube current of the X-ray source are controlled by feedback to keep the X-ray parameters of the X-ray source constant, so that the metering stability of the X-ray nucleon balance is improved.

Description

Calibration method of X-ray nucleon balance and X-ray nucleon balance
Technical Field
The invention relates to the technical field of weighing, in particular to a calibration method of an X-ray nucleon scale and the X-ray nucleon scale.
Background
Coal has been dominant in the energy industry structure of our country. In order to improve economic benefit, coal enterprises strengthen supervision on coal production links, generally isotope nucleon scales are installed on a crossheading belt of a stoping working face, raw coal recovery rate of a mining area is supervised in real time, and effective recovery of coal resources is ensured.
The coal mining process of the coal mine stoping face adopts a reverse method to mine coal, and the belt conveyor of the underground stoping face is shortened along with the pushing of the coal mining face, so that the belt tension is changed. The isotope nucleon balance installed on the belt conveyer adopts non-contact weighing, and the isotope nucleon balance adopts measuring materials to measure isotopes 137 Cs releases the attenuation of gamma rays to weigh the materials conveyed by the conveyor, and the metering error is not influenced by the tension change of the belt, so that the weighing device is particularly suitable for metering under the environment of a coal mine stoping belt and is widely applied. Isotope element 137 The single-energy gamma rays generated by Cs have constant attenuation coefficient, high metering precision and good linearity.
However, the radioisotope used in the above-mentioned isotope nucleon balance 137 Cs exist in a certain radiationThe problem of shot residue.
Disclosure of Invention
The invention provides a calibration method of an X-ray nucleon scale and the X-ray nucleon scale, which are used for solving the problem that the existing isotope nucleon scale has certain radiation residues.
In a first aspect, the present invention provides a method for calibrating an X-ray nucleon scale, applied to an X-ray nucleon scale, the X-ray nucleon scale comprising: an X-ray source, an X-ray detector, a bracket and a weighing instrument; wherein the X-ray source is arranged at one end of the bracket; the other end of the bracket is arranged on the X-ray detector; a belt for conveying the tested materials is arranged between the X-ray source and the X-ray detector; the X-ray detector is connected with the weighing instrument; the method comprises the following steps:
the weighing instrument acquires the energy and intensity of the X-rays output by the X-ray detector, and acquires the tube voltage parameter and the tube current parameter sent by the X-ray source;
the weighing instrument respectively determines the offset of the tube voltage parameter and the offset of the tube current parameter according to the X-ray energy and intensity, the tube voltage parameter and the tube current parameter, and sends the offset and the offset to the X-ray source;
the X-ray source adjusts the tube voltage parameter and the tube current parameter according to the offset of the tube voltage parameter and the offset of the tube current parameter.
In a second aspect, the present invention provides an X-ray nucleon balance comprising:
an X-ray source, an X-ray detector, a bracket and a weighing instrument;
wherein the X-ray source is arranged at one end of the bracket; the other end of the bracket is arranged on the X-ray detector; a belt for conveying the tested materials is arranged between the X-ray source and the X-ray detector;
the X-ray detector is connected with the weighing instrument;
the weighing instrument is used for determining the offset of the tube voltage and the tube current parameters according to the energy and the intensity of the X-ray output by the X-ray detector and acquiring the tube voltage and the tube current parameters sent by the X-ray source and sending the offset to the X-ray source;
the X-ray source is used for adjusting the tube voltage and tube current parameters according to the offset of the tube voltage and tube current parameters.
The calibration method of the X-ray nucleon balance provided by the invention uses the X-ray detector as a feedback sensor for monitoring the energy and intensity of the X-rays, and maintains the X-ray parameters of the X-ray source to be constant by controlling the tube voltage and the tube current of the X-ray source in a feedback way, so that the measurement stability of the X-ray nucleon balance is improved, and after an alternating current power supply of the X-ray source is closed, no X-rays are generated, no radiation residue problem exists, no waste source treatment problem is needed to be considered, and the environmental impact is small.
Drawings
The accompanying drawings, which are incorporated in and constitute a part of this specification, illustrate embodiments consistent with the disclosure and together with the description, serve to explain the principles of the disclosure.
FIG. 1 is a schematic view of an embodiment of an X-ray nucleon balance according to the present invention;
FIG. 2 is a flow chart of an embodiment of a method for calibrating an X-ray nucleon balance according to the present invention;
FIG. 3 is a schematic view of an embodiment of an X-ray source of an X-ray nuclear scale according to the present invention;
fig. 4 is a schematic view of an X-ray source structure of another embodiment of an X-ray nucleon balance according to the present invention.
Reference numerals illustrate:
1. an X-ray source;
2. an X-ray detector;
3. a bracket;
4. a weighing instrument;
5. an upper belt;
6. a lower belt;
7. an X-ray tube;
8. a protective sleeve;
9. a ray window.
Specific embodiments of the present disclosure have been shown by way of the above drawings and will be described in more detail below. These drawings and the written description are not intended to limit the scope of the disclosed concepts in any way, but rather to illustrate the disclosed concepts to those skilled in the art by reference to specific embodiments.
Detailed Description
Reference will now be made in detail to exemplary embodiments, examples of which are illustrated in the accompanying drawings. When the following description refers to the accompanying drawings, the same numbers in different drawings refer to the same or similar elements, unless otherwise indicated. The implementations described in the following exemplary examples are not representative of all implementations consistent with the present disclosure. Rather, they are merely examples of apparatus consistent with some aspects of the disclosure as detailed in the accompanying claims.
The terms "comprising" and "having" and any variations thereof in the description and claims of the invention and in the drawings are intended to cover a non-exclusive inclusion. For example, a process, method, system, article, or apparatus that comprises a list of steps or elements is not limited to only those listed steps or elements but may include other steps or elements not listed or inherent to such process, method, article, or apparatus.
In the existing weighing mode in the coal production link, an electronic belt scale installed on a belt conveyor generally adopts contact weighing, and the metering error is influenced by belt tension change and is not suitable for being used in places with large belt tension change; or using isotope nucleon scales, i.e. measuring material versus isotope 137 Cs releases the attenuation of gamma rays to weigh the materials conveyed by the conveyor, and the materials are weighed in a non-contact manner, so that the metering error is not influenced by the tension change of the belt, but the problem of radiation residue exists.
The inventors have studied the replacement of the X-ray source in the course of implementing the present invention 137 And the influence on the metering performance of the nucleon scale after the Cs isotope source. Combining the differences between X-rays and isotope gamma rays, it is proposed to use an X-ray detector to monitor X-ray energy (i.e.)Tube voltage) and intensity (i.e., tube current), the tube voltage and tube current of the X-ray source are controlled by feedback to keep the X-ray parameters constant, and the concept of a 'source strong zero point' of the X-ray source is provided, and the 'source strong zero point' of the X-ray source is controlled by monitoring the 'measurement zero point' of the X-ray nucleon scale, so as to realize the stability of the measurement zero point of the X-ray nucleon scale.
FIG. 1 is a schematic diagram of an embodiment of an X-ray nuclear scale according to the present invention. As shown in fig. 1, the X-ray nucleon balance provided in this embodiment includes:
an X-ray source 1, an X-ray detector 2, a bracket 3 and a weighing instrument 4;
wherein the X-ray source 1 is arranged at one end of the bracket 2; the other end of the bracket 3 is arranged on the X-ray detector 2; a belt for conveying the tested materials is arranged between the X-ray source 1 and the X-ray detector 2;
the X-ray detector 2 is connected with the weighing instrument 4;
the weighing instrument 4 is used for determining the load of the tested material according to the X-ray intensity information sent by the X-ray detector;
the weighing instrument 4 is further configured to determine an offset of the tube voltage and the tube current parameter according to the X-ray energy and the intensity output by the X-ray detector 2 and the tube voltage and the tube current parameter sent by the X-ray source 1, and send the offset to the X-ray source;
the X-ray source 1 is used for adjusting the tube voltage and tube current parameters according to the offset of the tube voltage and tube current parameters.
As shown in fig. 2, the method of the present embodiment is applied to the X-ray nucleon balance shown in fig. 1, and includes the following steps:
step 201, the weighing instrument acquires the energy and intensity of the X-ray output by the X-ray detector, and acquires the tube voltage parameter and the tube current parameter sent by the X-ray source;
step 202, the weighing instrument respectively determines the offset of the tube voltage parameter and the offset of the tube current parameter according to the X-ray energy and intensity, the tube voltage parameter and the tube current parameter, and sends the offset and the offset to the X-ray source;
step 203, the X-ray source adjusts the tube voltage parameter and the tube current parameter according to the offset of the tube voltage parameter and the offset of the tube current parameter.
Specifically, as shown in fig. 1, an X-ray source 1 and an X-ray detector 2 are disposed at two ends of a support 3, and the X-ray source is used for generating X-rays with a certain energy and stable intensity, namely emitting the X-rays; an X-ray detector for detecting the energy and intensity of the X-rays remaining after passing through the material.
An upper belt 5 for conveying the tested materials is arranged between the X-ray source 1 and the X-ray detector 3, and in other embodiments, the positions of the X-ray source 1 and the X-ray detector 3 can be interchanged, that is, the X-ray source 1 is arranged between the upper belt 5 and the lower belt 6, and the X-ray detector 3 is arranged above the bracket, which is not limited by the embodiment of the invention.
The weighing instrument 4 and the X-ray detector 3 can be connected through a wire or wireless communication, and the weighing instrument is used for determining the load of the tested material according to the X-ray intensity information sent by the X-ray detector.
When passing through the material, a part of the X-rays are absorbed by the material, and the unabsorbed X-rays penetrate through the material and reach the X-ray detector. The intensity of the X-rays after penetrating the material decays exponentially according to the following formula (1):
N=N 0 e -μF/S ……………………………………(1)
wherein: mu represents the mass absorption coefficient of the material; f represents the material load of the conveyor; s represents the width of the conveyor belt; n (N) 0 Representing the X-ray intensity at the X-ray detector when no material exists; n represents the X-ray intensity at the X-ray detector in the presence of material.
The X-ray detector has 2 roles: 1) Monitoring the energy and intensity of the X-rays, feeding back instantaneous values of tube voltage and tube current parameters of the X-ray source to a weighing instrument, and keeping the energy and intensity of the X-rays constant; 2) As a material load detection sensor on the conveyor.
Specifically, in order to keep the energy and intensity of the X-ray nucleon balance constant, in the embodiment of the present invention, the weighing instrument acquires the energy and intensity of the X-ray detector (i.e., instantaneous values of tube voltage and tube current parameters), and tube voltage parameters and tube current parameters sent by the X-ray source, and determines the offset of the tube voltage parameters and the offset of the tube current parameters according to the energy and intensity of the X-ray and the tube voltage parameters and the tube current parameters, respectively, and sends the offset and the offset to the X-ray source, so that the X-ray source adjusts the tube voltage parameters and the tube current parameters according to the offset of the tube voltage parameters and the offset of the tube current parameters, thereby increasing the stability of the X-ray energy and intensity output by the X-ray source and improving the stability of the measurement of the X-ray nucleon balance.
As shown in fig. 3, optionally, the X-ray source includes:
an X-ray tube, a high voltage power supply module, a low voltage power supply module, and a high voltage power supply control module;
the X-ray tube is electrically connected with the high-voltage power supply module and the low-voltage power supply module respectively;
the high-voltage power supply module is electrically connected with the high-voltage power supply control module;
the X-ray source is connected with the weighing instrument through wireless communication;
the X-ray detector is connected with the weighing instrument through wireless communication;
the high-voltage power supply control module is specifically used for adjusting the tube voltage and tube current parameters according to the offset of the tube voltage and tube current parameters.
In order to overcome the influence of the change of the X-ray intensity on the metering stability of the X-ray nucleon balance, the high-voltage power supply control module of the X-ray source can be utilized to share the data of the high-voltage power supply of the X-ray source with the weighing instrument through a network so as to monitor the change of the X-ray intensity.
The weighing instrument can realize the following functions: 1) Receiving output signals of an X-ray detector, namely X-ray intensity information, transmission speed of a conveyor, X-ray energy and intensity of an X-ray source (namely instantaneous values of tube voltage and tube current parameters), and receiving the tube voltage parameters and the tube current parameters sent by the X-ray source; 2) Calculating the load, flow and shift output of materials on a conveyor, and the offset of tube current and tube voltage parameters; 3) The zero voltage value (a representation of intensity information), the instantaneous value of the X-ray energy and intensity, the tube current, and the offset of the tube voltage parameters of the X-ray nucleon balance are sent to the X-ray source via a wireless or wired network.
Because the distribution of the X-ray energy is continuous, the attenuation coefficient when the X-ray energy interacts with the substance is a variable of wavelength, and in order to improve the weighing precision and linearity of the X-ray nucleon scale, the metering state and the X-ray parameters of the X-ray nucleon scale need to be tracked in real time, so that the stability and precision of the X-ray nucleon scale are greatly improved.
The stability of an X-ray nucleon balance is determined by the stability of the X-ray source, and relates to the energy and intensity of the X-rays. The tube voltage of the X-ray source determines the X-ray energy and the tube current determines the X-ray intensity.
The high-voltage power control module in the X-ray source can be utilized, the X-ray detector is used as a feedback sensor for monitoring the energy and the intensity of X-rays, and the constant of the X-ray parameters is kept through feedback control, so that the energy and the intensity of the X-rays are kept constant. The principle is as follows:
after the X-ray source transmits power, the high-voltage power supply control module is realized by controlling the high-voltage power supply module:
1) Automatically adjusting the current and the voltage of an X-ray tube according to the set X-ray source parameters (tube current and tube voltage parameters), and ensuring that the energy and the intensity of the X-rays are not influenced by the fluctuation of a power supply voltage;
2) The weighing instrument receives instantaneous values of X-ray parameters detected by the X-ray detector through a wireless network, namely X-ray energy and intensity, compares the instantaneous values of tube current and tube voltage parameters with preset tube current and tube voltage parameters (namely tube voltage parameters and tube current parameters sent by an X-ray source), determines offset, adjusts the values of the tube voltage and tube current parameters to keep the stability of the X-ray parameters, and overcomes the reduction of X-ray intensity caused by the aging of an X-ray tube.
In the above embodiment, the stability of the X-ray nucleon balance is greatly improved by tracking the parameters of the X-rays of the X-ray nucleon balance in real time and adjusting the parameters of the tube voltage and the tube current.
Optionally, the bracket comprises:
a top plate, side plates and a bottom plate;
wherein, a closed space is enclosed among the top plate, the side plates and the bottom plate;
the top plate and the bottom plate are respectively provided with an opening for transmitting X rays.
Specifically, an opening is formed in the top plate for transmitting the X-rays emitted by the X-ray source.
An opening is provided in the base plate for transmitting the X-rays remaining after passing through the material.
According to the calibration method provided by the embodiment, the X-ray detector is used as a feedback sensor for monitoring the energy and the intensity of the X-rays, the tube voltage and the tube current of the X-ray source are controlled by feedback to keep the X-ray parameters of the X-ray source constant, the measurement stability of the X-ray nucleon balance is improved, and the isotope is replaced by the X-ray source 137 The X-ray nucleon balance made of the Cs source has no X-ray generation after the alternating current power supply of the X-ray source is turned off, no radiation residue problem exists, the problem of waste source treatment is not needed to be considered, and the environmental impact is small.
On the basis of the above embodiment, optionally, in order to improve the zero point stability of the X-ray nucleon balance, the method further comprises the following steps:
the weighing instrument acquires an X-ray intensity sampling value of the X-ray detector in a calibration period when the belt runs empty;
the weighing instrument determines a measurement zero point of the X-ray nucleon scale according to the X-ray intensity sampling value; and the measurement zero point is X-ray intensity information output by the X-ray detector when the belt runs empty.
Further, the method can also comprise the following steps:
the weighing instrument respectively acquires a tube voltage parameter sampling value and a tube current parameter sampling value of the X-ray source in a calibration period when the belt runs empty;
determining a source intensity zero point corresponding to the metering zero point according to the metering zero point, the tube voltage parameter sampling value and the tube current parameter sampling value; the source strong zero point is a tube voltage parameter and a tube current parameter corresponding to the metering zero point.
Specifically, the measurement zero point is a reference of the measurement of the X-ray nucleon scale, and is an average value of the X-ray dosage rate received by the X-ray detector when no material exists on the conveyor belt and the conveyor belt runs for one circle. The measurement zero point is commonly influenced by factors such as the consistency of X-ray energy, intensity and material of the conveyor belt. The stability of the measurement zero point determines the stability of the measurement of the X-ray nucleon balance, and the measurement zero point and the source strong zero point of the X-ray source are provided for the first time, and the stability of the measurement of the X-ray nucleon balance is realized by monitoring the measurement zero point of the X-ray and the source strong zero point of the X-ray source. The principle is as follows:
during the metering process of an X-ray nucleon balance, the source intensity of the X-ray source is zero (tube voltage U 0i Tube current I 0i ) The energy and intensity of the X-ray can be changed due to the change of the X-ray, and the stability of the output value of the X-ray detector can be influenced by factors such as belt deflection, belt abrasion and the like. In order to obtain a stable weighing zero point of the belt scale, it is important to eliminate the influence of the X-ray change on the weighing zero point.
1) Determining 'measurement zero point-source strong zero point'
After the X-ray source alternating current power supply is switched on and the X-ray is stabilized, a conveyor is started to enable the belt to run idle, and signals S of the X-ray detector acquired in a calibration period (T) of belt running are recorded by a weighing instrument respectively 0i Tube voltage U of X-ray source 0i Sum tube current I 0i
Wherein: s is S 0 、U 0 、I 0 Respectively representing the metering zero point and the corresponding source strong zero point (tube voltage and tube current) of the nucleon balance;
S 0i 、U 0i 、I 0i the value of the ith sampling signal representing the metering zero point and the corresponding source intensity zero point of the nucleon balance;
n represents the number of sampling signal points in the calibration period;
t represents a calibration period;
f s representing the signal sampling frequency of the meter.
We measure the signal S of the X-ray detector when the belt is running empty 0i The "measurement zero point" of the X-ray nucleon balance is called, and the tube voltage U of the X-ray source corresponds to the moment of the "measurement zero point" 0i Tube current I 0i Known as the "source intensity zero" of the X-ray source. The high-voltage power supply control module sends the value of the 'source strong zero point' of the X-ray source to the weighing instrument through a wireless or wired network, and the weighing instrument feeds back the 'metering zero point' to the high-voltage power supply control module through the wireless network. The weighing instrument and the high-voltage power supply control module are simultaneously built with a metering zero-source strong zero array (S) 0i 、U 0i 、I 0i )。
Further, the method further comprises:
the weighing instrument determines whether the source intensity zero point belongs to a preset source intensity zero point range;
if the source intensity zero point does not belong to the preset source intensity zero point range, the weighing instrument determines the offset of the tube voltage parameter and the offset of the tube current parameter, and sends the offset of the tube voltage parameter and the offset of the tube current parameter to the X-ray source so that the X-ray source can adjust the tube voltage parameter and the tube current parameter.
Specifically, when the conveyor runs in the air, the weighing instrument acquires the signal S of the X-ray detector in real time i Comparing with zero values stored in a balance 'measurement zero point-source strong zero point' array:
1) Signal S of X-ray detector i Value and "metering zero" S 0i The error of the values being within tolerance, i.e. the signal S of the X-ray detector i The value is at the metering zero point S 0i The preset range of values is: if the tube voltage U of the X-ray source i Value, tube current I i Value and "source strong zero point" U 0i Value, I 0i The error of the value is within the tolerance, so that the zero point of the X-ray energy spectrum and the zero point of the belt scale are not changed, and the zero point of the X-ray nucleon scale is stable; if the tube voltage U of the X-ray source i Value, tube current I i Value and "source strong zero point" U 0i Value, I 0i If the error of the value exceeds the preset range, the 'intensity zero' of the X-ray source is influenced by the working conditions such as aging of the ray tube, the 'source intensity zero' needs to be measured again, and the 'source intensity zero' which is measured newly is stored in the 'metering zero-source intensity zero' array.
2) Signal S of X-ray detector i Value and "metering zero" S 0i The error in the values exceeds a preset range: if the tube voltage U of the X-ray source i Value, tube current I i Value and "source strong zero point" U 0i Value, I 0i The error of the values being within tolerance, i.e. the tube voltage U i Value, tube current I i The value is at "source strong zero point" U 0i Value, I 0i Within a preset range of values, the zero point of the X-ray nucleon balance is influenced by the working condition of the conveyor to generate deviation, the measurement zero point is required to be measured again, and the newly measured measurement zero point is stored in a measurement zero point-source strong zero point array; if the tube voltage U of the X-ray source i Value, tube current I i Value and "source strong zero point" U 0i Value, I 0i If the error of the value exceeds the preset range, the tube voltage and tube current parameters of the X-ray are indicated to deviate, the weighing instrument determines the variation of the source intensity and feeds the variation back to the high-voltage power supply control module, the tube voltage and tube current parameters of the X-ray source are adjusted, and the X-ray is keptStability, the stability of the metering zero point is ensured.
In the specific embodiment, the stability and the precision of the X-ray nucleon scale are greatly improved by tracking the metering state and the X-ray parameters of the X-ray nucleon scale in real time.
Optionally, the method further comprises:
the X-ray source shields X-rays of less than a preset energy value before emitting the X-rays.
As shown in fig. 4, the X-ray tube 7 is disposed in a protective sleeve 8;
the protective sleeve 8 is provided with a radiation window 9 for emitting X-rays.
Specifically, electrons are generated after the cathode filament of the X-ray tube 7 is heated, and the electrons fly to the anode under the acceleration action of the high-voltage electric field; the high-speed moving electrons strike the anode target surface to generate X-rays. The magnitude of the X-ray tube voltage determines the magnitude of the high voltage electric field accelerating the electrons and determines the energy E of the X-rays. Intensity of X-ray I Connected with The magnitude of (2) is proportional to the tube current i and the atomic number Z of the anode target material, and the square of the tube voltage U is proportional to the square of the tube voltage U, namely: i Connected with =k 1 iU 2 Z(k 1 Is constant and is about 1.1X10 -19 ~1.4×10 -19 )。
Optionally, in order to eliminate the influence of the X-ray hardening on the linearity of the measurement, a shielding structure is arranged at the ray window for shielding the X-rays smaller than a preset energy value.
Specifically, since the X-rays contain a series of electromagnetic waves λ of different wavelengths, the absorption coefficient μ of the same substance for the X-rays is a cubic function of the wavelengths of the contained electromagnetic waves, and is a variable. When the X-ray penetrates through the absorber with different thickness, the low-energy particles with long wavelength are absorbed by the substance along with the increase of the thickness of the absorber, the total intensity of the X-ray after the high-energy particles with short wavelength penetrate through the substance is reduced, the ratio of the high-energy particles with short wavelength is increased, and the phenomenon of hardening appears in the energy spectrum of the X-ray after transmission compared with the energy spectrum before transmission.
By adding a shielding structure such as a selective shielding material in the ray window, for example, a shielding material with the thickness of 4mm can be added, the X-rays with the energy less than 60keV can be shielded, the hardening degree of an X-ray energy spectrum is reduced, and the influence of X-ray hardening on the measurement linearity is eliminated.
In practical application, the thickness range of the shielding material can be 4-5mm.
In the specific embodiment, the selective shielding material is additionally arranged on the ray window, so that the hardening degree of the X-ray energy spectrum is reduced, and the influence of the X-ray hardening on the measurement linearity is eliminated.
As shown in fig. 1 and 3, an embodiment of the present invention further provides an X-ray nucleon balance, including:
an X-ray source, an X-ray detector, a bracket and a weighing instrument;
wherein the X-ray source is arranged at one end of the bracket; the other end of the bracket is arranged on the X-ray detector; a belt for conveying the tested materials is arranged between the X-ray source and the X-ray detector;
the X-ray detector is connected with the weighing instrument;
the weighing instrument is used for determining the offset of the tube voltage and the tube current parameters according to the X-ray energy and the intensity output by the X-ray detector and the tube voltage and the tube current parameters sent by the X-ray source and sending the offset to the X-ray source;
the X-ray source is used for adjusting the tube voltage and tube current parameters according to the offset of the tube voltage and tube current parameters.
Optionally, the weighing instrument is further used for collecting an X-ray intensity sampling value of the X-ray detector in a calibration period when the belt runs empty; determining a measurement zero point of the X-ray detector according to the X-ray intensity sampling value; the measurement zero point is the intensity information output by the X-ray detector when the belt runs empty.
Optionally, the weighing instrument is further configured to collect a tube voltage parameter sampling value and a tube current parameter sampling value of the X-ray source in a calibration period when the belt runs empty respectively; determining a source intensity zero point corresponding to the metering zero point according to the metering zero point, the tube voltage parameter sampling value and the tube current parameter sampling value; the source strong zero point is a tube voltage and tube current parameter corresponding to the metering zero point.
Optionally, the weighing instrument is specifically configured to determine whether the source intensity zero point belongs to a preset source intensity zero point range;
if the source strong zero point does not belong to the preset source strong zero point range, determining the offset of the tube voltage parameter and the offset of the tube current parameter, and sending the offset of the tube voltage parameter and the offset of the tube current parameter to the high-voltage power supply control module so that the high-voltage power supply control module can adjust the tube voltage parameter and the tube current parameter.
Optionally, the method further comprises:
the speed measuring assembly is connected with the weighing instrument; the speed measuring assembly is arranged on the conveyor of the belt and used for measuring the conveying speed of the conveyor.
Specifically, the speed measuring component can be a speed sensor, the conveying speed of the conveyor is measured, and the conveying speed is fed back to the weighing instrument, and the weighing instrument can be used for calculating data such as flow, shift yield and the like.
The nucleon balance in the above embodiment has similar technical effects and technical effects to those of the method embodiment, and will not be described herein.
Other embodiments of the disclosure will be apparent to those skilled in the art from consideration of the specification and practice of the disclosure disclosed herein. This application is intended to cover any adaptations, uses, or adaptations of the disclosure following, in general, the principles of the disclosure and including such departures from the present disclosure as come within known or customary practice within the art to which the disclosure pertains. It is intended that the specification and examples be considered as exemplary only, with a true scope and spirit of the disclosure being indicated by the following claims.
It is to be understood that the present disclosure is not limited to the precise arrangements and instrumentalities shown in the drawings, and that various modifications and changes may be effected without departing from the scope thereof. The scope of the present disclosure is limited only by the appended claims.

Claims (6)

1. A method of calibrating an X-ray nuclear scale, applied to an X-ray nuclear scale, the X-ray nuclear scale comprising: an X-ray source, an X-ray detector, a bracket and a weighing instrument; wherein the X-ray source is arranged at one end of the bracket; the other end of the bracket is arranged on the X-ray detector; a belt for conveying the tested materials is arranged between the X-ray source and the X-ray detector; the X-ray detector is connected with the weighing instrument; the method comprises the following steps:
the weighing instrument acquires the energy and intensity of the X-rays output by the X-ray detector, and acquires the tube voltage parameter and the tube current parameter sent by the X-ray source;
the weighing instrument respectively determines the offset of the tube voltage parameter and the offset of the tube current parameter according to the X-ray energy and intensity, the tube voltage parameter and the tube current parameter, and sends the offset and the offset to the X-ray source;
the X-ray source adjusts the tube voltage parameter and the tube current parameter according to the offset of the tube voltage parameter and the offset of the tube current parameter;
the method further comprises the steps of:
the weighing instrument acquires an X-ray intensity sampling value of the X-ray detector in a calibration period when the belt runs empty;
the weighing instrument determines a measurement zero point of the X-ray nucleon scale according to the X-ray intensity sampling value; the measurement zero point is X-ray intensity information output by the X-ray detector when the belt runs empty;
the weighing instrument respectively acquires a tube voltage parameter sampling value and a tube current parameter sampling value of the X-ray source in a calibration period when the belt runs empty;
determining a source intensity zero point corresponding to the metering zero point according to the metering zero point, the tube voltage parameter sampling value and the tube current parameter sampling value; the source strong zero point is a tube voltage parameter and a tube current parameter corresponding to the metering zero point.
2. The method as recited in claim 1, further comprising:
the weighing instrument determines whether the source intensity zero point belongs to a preset source intensity zero point range;
if the source intensity zero point does not belong to the preset source intensity zero point range, the weighing instrument determines the offset of the tube voltage parameter and the offset of the tube current parameter, and sends the offset of the tube voltage parameter and the offset of the tube current parameter to the X-ray source so that the X-ray source can adjust the tube voltage parameter and the tube current parameter.
3. The method as recited in claim 1, further comprising:
the X-ray source shields X-rays of less than a preset energy value before emitting the X-rays.
4. An X-ray nuclear scale, comprising:
an X-ray source, an X-ray detector, a bracket and a weighing instrument;
wherein the X-ray source is arranged at one end of the bracket; the other end of the bracket is arranged on the X-ray detector; a belt for conveying the tested materials is arranged between the X-ray source and the X-ray detector;
the X-ray detector is connected with the weighing instrument;
the weighing instrument is used for determining the offset of the tube voltage and the tube current parameters according to the energy and the intensity of the X-ray output by the X-ray detector and acquiring the tube voltage and the tube current parameters sent by the X-ray source and sending the offset to the X-ray source;
the X-ray source is used for adjusting the tube voltage and tube current parameters according to the offset of the tube voltage and tube current parameters;
the X-ray source comprises:
an X-ray tube, a high voltage power supply module, a low voltage power supply module, and a high voltage power supply control module;
the X-ray tube is electrically connected with the high-voltage power supply module and the low-voltage power supply module respectively;
the high-voltage power supply module is electrically connected with the high-voltage power supply control module;
the X-ray source is connected with the weighing instrument through wireless communication;
the X-ray detector is connected with the weighing instrument through wireless communication;
the high-voltage power supply control module is specifically used for adjusting the tube voltage and tube current parameters according to the offset of the tube voltage and tube current parameters;
the weighing instrument is also used for collecting an X-ray intensity sampling value of the X-ray detector in a calibration period when the belt runs empty; determining a measurement zero point of the X-ray detector according to the X-ray intensity sampling value; the measurement zero point is the intensity information output by the X-ray detector when the belt runs empty;
the weighing instrument is also used for respectively collecting a tube voltage parameter sampling value and a tube current parameter sampling value of the X-ray source in a calibration period when the belt runs empty; determining a source intensity zero point corresponding to the metering zero point according to the metering zero point, the tube voltage parameter sampling value and the tube current parameter sampling value; the source strong zero point is a tube voltage and tube current parameter corresponding to the metering zero point.
5. The nucleon balance of claim 4, wherein said weighing instrument is specifically configured to determine whether said source intensity zero point falls within a predetermined source intensity zero point range;
if the source strong zero point does not belong to the preset source strong zero point range, determining the offset of the tube voltage parameter and the offset of the tube current parameter, and sending the offset of the tube voltage parameter and the offset of the tube current parameter to the high-voltage power supply control module so that the high-voltage power supply control module can adjust the tube voltage parameter and the tube current parameter.
6. The nucleon balance of claim 4 wherein the balance comprises a plurality of support arms,
the X-ray tube is arranged in the protective sleeve;
the protective sleeve is provided with a ray window for emitting X rays;
and a shielding material is arranged at the ray window and used for shielding X rays with energy values smaller than the preset energy value.
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CN111239171A (en) * 2020-02-13 2020-06-05 雅化锂业(雅安)有限公司 Weighing method capable of judging materials for metallurgy
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