CN108020165B - Method and system for measuring thickness of non-metallic material by using terahertz waves - Google Patents

Method and system for measuring thickness of non-metallic material by using terahertz waves Download PDF

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CN108020165B
CN108020165B CN201711233541.9A CN201711233541A CN108020165B CN 108020165 B CN108020165 B CN 108020165B CN 201711233541 A CN201711233541 A CN 201711233541A CN 108020165 B CN108020165 B CN 108020165B
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terahertz
terahertz wave
metallic material
reflection signal
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俞跃
郝元
王强
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Hohai University HHU
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01BMEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B11/00Measuring arrangements characterised by the use of optical techniques
    • G01B11/02Measuring arrangements characterised by the use of optical techniques for measuring length, width or thickness
    • G01B11/06Measuring arrangements characterised by the use of optical techniques for measuring length, width or thickness for measuring thickness ; e.g. of sheet material
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/41Refractivity; Phase-affecting properties, e.g. optical path length

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Abstract

The invention provides a method and a system for measuring the thickness of a non-metallic material by utilizing terahertz waves. The method of the invention comprises the following steps: vertically irradiating the terahertz wave to the surface of the non-metal material, respectively reflecting the terahertz wave by the surface and the bottom surface of the non-metal material to form a first reflected signal and a second reflected signal, receiving the first reflected signal and the second reflected signal, and obtaining a receiving time difference delta T of the two reflected signals1(ii) a Make the terahertz wave at an angle thetaiThe terahertz waves are incident to the surface of the non-metallic material, the terahertz waves are reflected by the surface and the bottom surface of the non-metallic material to form third and fourth reflection signals respectively, the third and fourth reflection signals are received, and the receiving time difference delta T of the two reflection signals is obtained2Wherein 0 degree<θi<90 degrees; according to the difference of receiving time DeltaT1And Δ T2Obtaining the refractive index n of the non-metal material; and obtaining the thickness d of the non-metal material according to the refractive index n of the non-metal material. The method can directly measure the refractive index and the thickness of the non-metallic material, and has small measurement error and high accuracy.

Description

Method and system for measuring thickness of non-metallic material by using terahertz waves
Technical Field
The invention relates to a thickness measuring method, in particular to a method and a system for measuring the thickness of a non-metal material by utilizing terahertz waves.
Background
The terahertz wave is an electromagnetic wave with the frequency of 0.1 THz-10 THz, the wavelength of the terahertz wave is approximately 0.03 mm-3 mm, and the wave band is between the microwave and the infrared light. In recent years, the rapid development of the ultrafast laser technology provides a stable and reliable excitation light source for the generation of terahertz pulses, so that the mechanism research, detection technology and application technology of terahertz radiation are developed vigorously.
At present, the conventional thickness measurement method based on the terahertz principle is generally performed on the basis of the known refractive index of a sample, the method measures a material once to obtain a receiving time difference between two reflected signals, and then calculates the thickness of the material by combining the receiving time difference and the known refractive index, however, the method cannot measure the thickness of the material when the refractive index of the material is unknown.
In order to overcome the above-mentioned drawbacks, there is a method using inverse calculation, which obtains a receiving time difference between two reflected signals by performing one measurement on a standard sample having a known thickness, and inversely calculates a refractive index of the sample from the receiving time difference; subsequently, the thickness of the material is obtained by the receiving time difference between two reflected signals obtained by one measurement of the same sample material and the above-mentioned refractive index calculated reversely, however, the method has measurement errors caused by different materials having refractive index differences and the like.
Disclosure of Invention
The invention provides a method and a system for measuring the thickness of a non-metallic material by utilizing terahertz waves, which can directly measure the refractive index and the thickness of the non-metallic material, thereby avoiding measurement errors caused by different materials with refractive index differences and other factors and ensuring the accuracy of measurement results.
The invention provides a method for measuring the thickness of a non-metallic material by utilizing terahertz waves, wherein the non-metallic material is provided with a surface and a bottom surface, and the method comprises the following steps:
vertically irradiating the terahertz waves to the surface of the non-metallic material, respectively forming a first reflection signal and a second reflection signal by the terahertz waves reflected by the surface and the bottom of the non-metallic material, receiving the first reflection signal and the second reflection signal, and obtaining a receiving time difference delta T between the first reflection signal and the second reflection signal1
Make the terahertz wave at an angle thetaiThe terahertz waves are incident to the surface of the non-metallic material, the terahertz waves are reflected by the surface and the bottom surface of the non-metallic material to form a third reflection signal and a fourth reflection signal respectively, the third reflection signal and the fourth reflection signal are received, and a third reflection signal is obtainedReceiving time difference delta T between the transmitted signal and the fourth reflected signal2Wherein 0 degree<θi<90°;
According to the difference of receiving time DeltaT1And a reception time difference Δ T2Obtaining the refractive index n of the non-metal material;
and obtaining the thickness d of the non-metal material according to the refractive index n of the non-metal material.
The method of the invention passes through different incident angles thetaiThe method can measure the refractive index and the thickness of the same non-metal material under the condition that the refractive index of the material is unknown, can avoid measurement errors caused by the fact that different materials have refractive index differences and the like, and ensures the accuracy of a measurement result.
Specifically, at the time of the first measurement, the terahertz wave is perpendicularly incident to the surface of the non-metallic material (i.e., the angle θ)i0), at the moment, the terahertz wave is reflected by the surface of the non-metal material to form a first reflection signal; meanwhile, the terahertz wave penetrates through the surface of the non-metallic material and is reflected at the bottom surface of the non-metallic material so as to form a second reflection signal; receiving the first reflected signal and the second reflected signal and obtaining the receiving time difference Delta T of the first reflected signal and the second reflected signal1Then, the thickness of the first measurement can be obtained according to the terahertz wave propagation theory, namely:
Figure BDA0001488583850000021
in equation (1): d is the thickness of the non-metallic material; c is the speed of light in vacuum (i.e., the speed of the terahertz wave in vacuum); n is the refractive index of the non-metallic material, Δ T1Is the difference in the time of reception of the first measurement.
At the time of the second measurement, the terahertz wave is at an angle θi(0°<θi<The terahertz waves are incident to the surface of the non-metal material at 90 degrees, and at the moment, the terahertz waves are reflected by the surface of the non-metal material to form a third reflection signal; meanwhile, terahertz waves are refracted by the surface of the non-metallic materialThen the reflected light is reflected by the bottom surface of the optical fiber to form a fourth reflected signal; receiving the third reflected signal and the fourth reflected signal and obtaining the receiving time difference Delta T of the third reflected signal and the fourth reflected signal2Then, the second measurement thickness can be obtained according to the terahertz wave propagation theory, namely:
Figure BDA0001488583850000031
in equation (2): d is the thickness of the non-metallic material; c is the speed of light in vacuum; n is the refractive index of the non-metallic material, thetaiFor the second measured angle of incidence, Δ T2Is the difference in the time of receipt of the second measurement.
In view of the fact that the first and second measurements are performed on the same non-metallic material, i.e. the thickness of the first measurement is the same as the thickness of the second measurement, the refractive index n of the non-metallic material can be obtained by the above equations (1) and (2), i.e.:
Figure BDA0001488583850000032
further, substituting the above equation (3) into equation (1) can obtain the thickness d of the non-metallic material, that is:
Figure BDA0001488583850000033
in the present invention, it is understood that the non-metallic material to be measured is a material having a certain thickness; the method of the present invention has no strict requirement on the thickness uniformity of the non-metal material, and can measure the thickness of the non-metal material with uniform thickness and the thickness of a certain position on the non-metal material with non-uniform thickness.
Specifically, in determining the thickness of a non-metallic material of uniform thickness, the present invention measures the thickness at normal incidence (i.e., the first measurement) and at an angle θiThe emission distance of the terahertz wave (i.e. the distance between the emission source of the terahertz wave and the incident point) at the time of incidence (i.e. the second measurement)Off) and the position of incidence (i.e., the incidence point) on the surface of the non-metallic material are not strictly limited; preferably, the terahertz waves can be made to be incident to the same position on the surface of the non-metal material at the same emission distance, and the measurement result is more accurate.
In determining the thickness of a certain position on a non-metallic material having a non-uniform thickness, terahertz waves should be made to be incident on the same position on the surface of the non-metallic material at the same emission distance at the first measurement and the second measurement in order to accurately measure the thickness of the non-metallic material at the position.
The terahertz wave used for measurement is not strictly limited, and can be conventional terahertz wave, the frequency of the terahertz wave can be 0.1 THz-10 THz, and the wavelength of the terahertz wave can be 0.03 mm-3 mm.
The thickness of the non-metal material is not strictly limited, and the thickness of the non-metal material can be 0.5 mm-50 mm.
The invention can measure the incident angle theta of the terahertz wave in the second measurementiNot critical, provided that 0 degree is used<θi<The temperature is 90 degrees; further, the angle θiCan be 30-60 degrees.
The transmission distance of the terahertz waves is not strictly limited, and can be set to be a conventional transmission distance, for example, 10 cm-30 cm.
The invention does not strictly limit the nonmetal materials to be measured, and can be polyethylene, glass fiber, carbon fiber, silicon chip, glue layer, rubber, paperboard and the like; in addition, the present invention does not strictly limit the shape of the non-metallic material to be measured, and the non-metallic material may be in the form of a tube, a sheet, a layer, or the like.
The invention also provides a system for measuring the thickness of the non-metallic material by utilizing the terahertz waves, which comprises a terahertz wave transmitting device, a terahertz wave receiving device, a sample fixing table and a track,
the terahertz wave emitting device is arranged on the track in a sliding mode and can emit terahertz waves to the non-metal material arranged on the sample fixing table,
the terahertz wave receiving device is arranged on the track in a sliding mode and can receive terahertz wave signals reflected by the non-metal materials.
In the present invention, the terahertz-wave emitting device is used to emit terahertz waves, which may be a conventional device in the art; it is understood that the emission source of the terahertz-wave emitting device should be directed toward the sample holding stage so as to facilitate the incidence of the terahertz waves emitted by the terahertz-wave emitting device on the surface of the non-metallic material placed on the sample holding stage.
In the present invention, the terahertz-wave receiving device is used for receiving a terahertz-wave signal reflected from a non-metallic material to obtain a reception time difference between different reflected signals, which may be a conventional device in the art.
The arrangement modes of the terahertz wave transmitting device and the terahertz wave receiving device are not strictly limited; the terahertz wave transmitting device and the terahertz wave receiving device can be arranged into two independent devices or can be arranged into one integrated device; under the premise of realizing respective functions, the functions can be reasonably set according to actual conditions.
In the present invention, the sample holding stage is used to hold the non-metallic material to be measured, which may be of conventional construction in the art.
In the invention, the track is used for supporting the sliding of the terahertz wave transmitting device and the terahertz wave receiving device, thereby facilitating the terahertz waves transmitted by the terahertz wave transmitting device to be at different angles thetaiThe terahertz wave signal is incident to the surface of the non-metallic material, and meanwhile, the terahertz wave signal reflected by the non-metallic material can be well received by the terahertz wave receiving device.
It can be understood that, at the time of the first measurement, the terahertz wave transmitting device and the terahertz wave receiving device may be respectively disposed at normal positions of the non-metallic material, and at this time, the terahertz wave transmitted by the terahertz wave transmitting device can be vertically incident on the surface of the non-metallic material.
During the second measurement, the terahertz wave transmitting device and the terahertz wave receiving device can be respectively arranged on two sides of the normal of the non-metal material; in particular, the terahertz-wave receiving device can be disposed between the third reflected signal and the fourth reflected signal, thereby facilitating good reception of the third reflected signal and the fourth reflected signal at the same time.
The invention does not strictly limit the shape of the track; preferably, the track may be a circular arc track centered on the sample fixing stage. The arc-shaped track can enable terahertz waves to be incident to the same position on the surface of the non-metal material at the same emission distance during the first measurement and the second measurement, so that the thickness of the non-metal material can be measured more accurately.
Further, the arc radius (i.e., the emission distance) of the circular arc track may be set to 10cm to 30 cm.
The implementation of the invention has at least the following advantages:
1. the method disclosed by the invention is used for measuring the thickness and the refractive index of the non-metallic material based on the terahertz detection principle, and is different from the traditional terahertz thickness measurement principle that the thickness measurement can be carried out only by knowing the refractive index of the measured material.
2. The method can directly measure the refractive index and thickness information of the non-metal material, thereby avoiding measurement errors caused by different materials with refractive index difference and other factors, and having high accuracy of the measurement result.
3. The system has simple structure, can obtain the refractive index information and the thickness information of the measured material by measuring the receiving time difference twice, has simple operation of measuring twice, can avoid human errors, and has more rigorous and accurate measurement on the material.
Drawings
FIG. 1 is a schematic diagram of the system of the present invention in a first measurement;
fig. 2 is a schematic diagram of the system of the present invention in a second measurement.
Description of reference numerals:
1: a terahertz wave emitting device; 2: a terahertz wave receiving device; 3: a track; 4: a non-metallic material; 41: a surface; 42: a bottom surface.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings and the embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
In this example, a polyethylene pipe (thickness of about 3 cm) with unknown refractive index and unknown thickness is measured by the following specific method:
1. first measurement
The terahertz wave is made to be perpendicular (theta) at a transmission distance of 30cmiThe terahertz waves are incident to the surface of the polyethylene pipe at 0 DEG, and are reflected by the surface of the polyethylene pipe (namely, the outer wall of the pipe) to form a first reflection signal, and simultaneously, the terahertz waves penetrate through the surface of the polyethylene pipe and are reflected by the bottom surface (namely, the inner wall of the pipe) to form a second reflection signal.
Receiving the first reflected signal and the second reflected signal to obtain a receiving time difference delta T between the first reflected signal and the second reflected signal1
2. Second measurement
The same terahertz wave is emitted at a distance of 30cm and an incident angle of 60 degrees (theta)iIncident at the same position on the surface of the polyethylene pipe at 60 degrees, and reflecting the terahertz waves through the surface of the polyethylene pipe to form a third reflection signal; meanwhile, the terahertz wave is refracted by the surface of the polyethylene pipe and then reflected by the bottom surface of the polyethylene pipe to form a fourth reflection signal.
Receiving the third reflected signal and the fourth reflected signal to obtain a receiving time difference delta T between the third reflected signal and the fourth reflected signal2
3. Calculating refractive index
The refractive index of the polyethylene pipe is calculated according to the following formula:
Figure BDA0001488583850000061
wherein: n: a refractive index; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
4. Calculating the thickness
The thickness of the polyethylene pipe is calculated according to the following formula:
Figure BDA0001488583850000071
wherein: d: thickness; c: speed of light in vacuum; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
Example 2
In this example, a glass fiber board (with a thickness of about 2.5 mm) with unknown refractive index and unknown thickness is measured by the following specific method:
1. first measurement
The terahertz wave is made perpendicular (theta) at a transmission distance of 20cmiThe terahertz wave is incident to the surface of the glass fiber board, the terahertz wave is reflected by the surface of the glass fiber board to form a first reflection signal, and meanwhile, the terahertz wave penetrates through the surface of the glass fiber board and is reflected at the bottom surface of the glass fiber board to form a second reflection signal.
Receiving the first reflected signal and the second reflected signal to obtain a receiving time difference delta T between the first reflected signal and the second reflected signal1
2. Second measurement
The same terahertz wave is emitted at a distance of 20cm and an incident angle of 30 degrees (theta)iIncident on the same position on the surface of the glass fiber plate at 30 degrees, and the terahertz wave is reflected by the surface of the glass fiber plate to form a third reflection signal; meanwhile, the terahertz waves are folded through the surface of the glass fiber plateAfter the light is emitted, the light is reflected by the bottom surface to form a fourth reflected signal.
Receiving the third reflected signal and the fourth reflected signal to obtain a receiving time difference delta T between the third reflected signal and the fourth reflected signal2
3. Calculating refractive index
The refractive index of the glass fiber sheet was calculated according to the following formula:
Figure BDA0001488583850000072
wherein: n: a refractive index; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
4. Calculating the thickness
The thickness of the glass fiber sheet was calculated according to the following formula:
Figure BDA0001488583850000081
wherein: d: thickness; c: speed of light in vacuum; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
Example 3
In this embodiment, a silicon wafer (with a thickness of about 0.5 mm) with unknown refractive index and unknown thickness is measured by the following specific method:
1. first measurement
The terahertz wave is made perpendicular (theta) at a transmission distance of 10cmiThe terahertz wave is incident to the surface of the silicon wafer at 0 DEG, the terahertz wave is reflected by the surface of the silicon wafer to form a first reflection signal, and meanwhile, the terahertz wave penetrates through the surface of the silicon wafer and is reflected at the bottom surface of the silicon wafer to form a second reflection signal.
Receiving the first reflected signal and the second reflected signal to obtain a receiving time difference delta T between the first reflected signal and the second reflected signal1
2. Second measurement
The same terahertz wave is emitted at a distance of 10cm and an incident angle of 55 degrees (theta)iThe terahertz waves are incident to the same position on the surface of the silicon wafer at 55 degrees, and the terahertz waves are reflected by the surface of the silicon wafer to form a third reflection signal; meanwhile, the terahertz wave is refracted by the surface of the silicon wafer and then reflected by the bottom surface of the silicon wafer to form a fourth reflection signal.
Receiving the third reflected signal and the fourth reflected signal to obtain a receiving time difference delta T between the third reflected signal and the fourth reflected signal2
3. Calculating refractive index
The refractive index of the silicon wafer is calculated according to the following formula:
Figure BDA0001488583850000082
wherein: n: a refractive index; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
4. Calculating the thickness
Calculating the thickness of the silicon wafer according to the following formula:
Figure BDA0001488583850000091
wherein: d: thickness; c: speed of light in vacuum; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
Example 4
In this embodiment, a rubber sheet (with a thickness of about 1 mm) with unknown refractive index and unknown thickness is measured by the following specific method:
1. first measurement
The terahertz wave is made perpendicular (theta) at a transmission distance of 20cmiIncident at 0 deg. to the surface of the rubber sheet, the terahertz wave is reflected by the surface of the rubber sheet to form a first reflection signal, and at the same time, the terahertz wave is reflected by the surface of the rubber sheet to form a second reflection signalThe Hertz wave penetrates through the surface of the rubber sheet and is reflected on the bottom surface of the rubber sheet to form a second reflection signal.
Receiving the first reflected signal and the second reflected signal to obtain a receiving time difference delta T between the first reflected signal and the second reflected signal1
2. Second measurement
The same terahertz wave is emitted at a distance of 20cm and an incident angle of 45 degrees (theta)iThe terahertz waves are incident to the same position on the surface of the rubber sheet at 45 degrees, and the terahertz waves are reflected by the surface of the rubber sheet to form a third reflection signal; meanwhile, the terahertz wave is refracted by the surface of the rubber sheet and then reflected by the bottom surface of the rubber sheet to form a fourth reflection signal.
Receiving the third reflected signal and the fourth reflected signal to obtain a receiving time difference delta T between the third reflected signal and the fourth reflected signal2
3. Calculating refractive index
The refractive index of the rubber sheet was calculated according to the following formula:
Figure BDA0001488583850000092
wherein: n: a refractive index; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
4. Calculating the thickness
The thickness of the rubber sheet was calculated according to the following formula:
Figure BDA0001488583850000101
wherein: d: thickness; c: speed of light in vacuum; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
Example 5
In this example, the measurement is performed on a paperboard (thickness is about 10 mm) with unknown refractive index and unknown thickness by the following specific method:
1. first measurement
The terahertz wave is made perpendicular (theta) at a transmission distance of 25cmiIncident to the surface of the paperboard, the terahertz waves are reflected by the surface of the paperboard to form a first reflection signal, and meanwhile, the terahertz waves penetrate through the surface of the paperboard and are reflected at the bottom surface of the paperboard to form a second reflection signal.
Receiving the first reflected signal and the second reflected signal to obtain a receiving time difference delta T between the first reflected signal and the second reflected signal1
2. Second measurement
The same terahertz wave is emitted at a distance of 25cm and an incident angle of 35 degrees (theta)iThe terahertz waves are incident to the same position of the surface of the paperboard, and the terahertz waves are reflected by the surface of the paperboard to form a third reflection signal; meanwhile, the terahertz wave is refracted by the surface of the paperboard and then reflected by the bottom surface of the paperboard to form a fourth reflection signal.
Receiving the third reflected signal and the fourth reflected signal to obtain a receiving time difference delta T between the third reflected signal and the fourth reflected signal2
3. Calculating refractive index
The refractive index of the paperboard was calculated according to the following formula:
Figure BDA0001488583850000102
wherein: n: a refractive index; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
4. Calculating the thickness
The thickness of the paperboard is calculated according to the following formula:
Figure BDA0001488583850000111
wherein: d: thickness; c: speed of light in vacuum; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
Example 6
Referring to fig. 1 and 2, the system for measuring the thickness of a non-metallic material by using terahertz waves of the present invention includes a terahertz wave transmitting device 1, a terahertz wave receiving device 2, a sample fixing table (not shown), and a rail 3, wherein the terahertz wave transmitting device 1 is slidably disposed on the rail 3 and is capable of transmitting terahertz waves to the non-metallic material 4 disposed on the sample fixing table, and the terahertz wave receiving device 2 is slidably disposed on the rail 3 and is capable of receiving terahertz wave signals reflected from the non-metallic material 4.
In the present invention, the terahertz-wave transmitting device 1 is for transmitting terahertz waves, which may be a conventional device in the art; it is understood that the emission source of the terahertz-wave emitting device 1 should be directed toward the sample holding stage so as to facilitate the incidence of the terahertz waves emitted by the terahertz-wave emitting device 1 on the surface 41 of the non-metallic material 4 placed on the sample holding stage.
In the present invention, the terahertz-wave receiving device 2 is for receiving a terahertz-wave signal reflected from the non-metallic material 4 and acquiring a reception time difference between the two reflected signals, which may be a conventional device in the art.
The arrangement modes of the terahertz wave transmitting device 1 and the terahertz wave receiving device 2 are not strictly limited, and the terahertz wave receiving device can be arranged into two independent devices or an integrated device; under the premise of realizing respective functions, the functions can be reasonably set according to actual conditions.
In the present invention, the sample holding stage is used to hold the non-metallic material 4 to be measured, which may be of conventional construction in the art. It is understood that the non-metallic material 4 is a material having a thickness, which has a surface 41 and a bottom surface 42, and the thickness and material are not limited; the thickness of the non-metallic material 4 can be 0.5 mm-50 mm, and the non-metallic material 4 can be polyethylene, glass fiber, carbon fiber, silicon chip, colloid, rubber, paperboard and the like.
In the present invention, the rail 3 is used for supporting the terahertz wave generatorThe terahertz-wave transmitting device 1 and the terahertz-wave receiving device 2 slide, thereby facilitating the terahertz waves transmitted by the terahertz-wave transmitting device 1 to be at different angles thetaiIncident to the surface 41 of the non-metallic material 4, while facilitating the terahertz-wave receiving device 2 to satisfactorily receive the terahertz-wave signal reflected from the non-metallic material 4.
As shown in fig. 1, at the time of the first measurement, the terahertz-wave transmitting device 1 and the terahertz-wave receiving device 2 may be respectively disposed at normal positions of the non-metallic material 4, and the terahertz wave transmitted by the terahertz-wave transmitting device 1 can be vertically incident on the surface 41 of the non-metallic material 4.
As shown in fig. 2, at the time of the second measurement, the terahertz-wave transmitting device 1 and the terahertz-wave receiving device 2 may be respectively disposed on both sides of the normal line of the non-metallic material 4; specifically, the angle between the terahertz wave emitting device 1 and the normal of the nonmetal material 4 is the incident angle θiThe terahertz-wave receiving device 2 can be disposed between the third reflected signal and the fourth reflected signal, thereby facilitating good reception of the third reflected signal and the fourth reflected signal at the same time.
The invention does not impose strict restrictions on the shape of the track 3; preferably, the track 3 may be a circular arc track centered on the sample holding stage. The circular arc-shaped track enables terahertz waves to be incident to the same position on the surface 41 of the non-metallic material 4 at the same emission distance during the first measurement and the second measurement, so that the thickness of the non-metallic material 4 can be accurately measured.
Further, the arc radius (i.e., the launch distance) of the circular arc shaped track may be set to 10cm to 30 cm.
The method for measuring the thickness of the non-metallic material 4 by using the system is as follows:
1. first measurement
As shown in fig. 1, after the non-metallic material 4 is fixed on the sample fixing table, the terahertz wave transmitting device 1 and the terahertz wave receiving device 2 are disposed at or near the normal position of the non-metallic material 4, wherein the distance (i.e., the transmission distance) between the transmission source of the terahertz wave transmitting device 1 and the position of incidence on the surface 41 of the non-metallic material 4 can be set to 10cm to 30 cm.
The terahertz wave emitted by the terahertz wave emitting device 1 is perpendicular (θ)iIncident on the surface 41 of the non-metallic material 4, the terahertz wave is reflected by the surface 41 of the non-metallic material 4 to form a first reflected signal, and at the same time, the terahertz wave is transmitted through the surface 41 of the non-metallic material 4 and is reflected at the bottom surface 42 thereof to form a second reflected signal.
The terahertz wave receiving device 2 receives the first reflected signal and the second reflected signal to obtain a receiving time difference Δ T between the first reflected signal and the second reflected signal1
2. Second measurement
Subsequently, the terahertz-wave transmitting device 1 and the terahertz-wave receiving device 2 are slid on the rail 3, whereby the positions of the terahertz-wave transmitting device 1 and the terahertz-wave receiving device 2 are adjusted to both sides of the normal position of the nonmetallic material 4, respectively, wherein the angle between the set position of the terahertz-wave transmitting device 1 and the normal position of the nonmetallic material 4 is an incident angle θi(0°<θi<90°)。
The terahertz wave emitted by the terahertz wave emitting device 1 is at an incident angle θiThe terahertz waves are incident to the surface 41 of the non-metal material 4, and the terahertz waves are reflected by the surface 41 of the non-metal material 4 to form a third reflection signal; meanwhile, the terahertz wave is refracted by the surface 41 of the non-metallic material 4 and then reflected by the bottom surface 42 thereof to form a fourth reflection signal.
The terahertz wave receiving device 2 is arranged between the third reflected signal and the fourth reflected signal, and the terahertz wave receiving device 2 receives the third reflected signal and the fourth reflected signal to obtain a receiving time difference delta T between the third reflected signal and the fourth reflected signal2
3. Calculating refractive index
The refractive index of the non-metallic material 4 is calculated according to the following formula:
Figure BDA0001488583850000131
wherein: n: a refractive index; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
4. Calculating the thickness
The thickness of the non-metallic material 4 is calculated according to the following formula:
Figure BDA0001488583850000132
wherein: d: thickness; c: speed of light in vacuum; thetai: a second measured angle of incidence; delta T1: the difference in the time of receipt of the first measurement; delta T2: the difference in the time of receipt of the second measurement.
The system has simple structure, can obtain the refractive index information and the thickness information of the measured material by measuring the receiving time difference twice, has simple operation of measuring twice, can avoid human errors, and has more rigorous and accurate measurement on the material.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention.

Claims (10)

1. A method for measuring a thickness of a non-metallic material using terahertz waves, the non-metallic material having a surface and a bottom surface, the method comprising the steps of:
vertically irradiating the terahertz waves to the surface of the non-metallic material, respectively forming a first reflection signal and a second reflection signal by the terahertz waves reflected by the surface and the bottom of the non-metallic material, receiving the first reflection signal and the second reflection signal, and obtaining a receiving time difference delta T between the first reflection signal and the second reflection signal1
Make the terahertz wave at an angle thetaiThe terahertz waves are incident to the surface of the non-metallic material, the terahertz waves are reflected by the surface and the bottom surface of the non-metallic material to form a third reflection signal and a fourth reflection signal respectively, the third reflection signal and the fourth reflection signal are received, and the receiving time difference delta T between the third reflection signal and the fourth reflection signal is obtained2Wherein 0 degree<θi<90°;
According to the difference of receiving time DeltaT1And a reception time difference Δ T2Obtaining the refractive index n of the non-metal material;
and obtaining the thickness d of the non-metal material according to the refractive index n of the non-metal material.
2. The method of claim 1, wherein the refractive index n of the non-metallic material is obtained according to the following formula,
Figure FDA0002257202910000011
3. the method of claim 1, wherein the thickness d of the non-metallic material is obtained according to the following formula,
Figure FDA0002257202910000012
where c is the speed of light in vacuum.
4. A method according to any one of claims 1 to 3, wherein at said normal incidence and at an angle θiWhen the terahertz waves are incident, the terahertz waves are made to be incident to the same position on the surface of the nonmetal material at the same emission distance.
5. A method according to any of claims 1 to 3, wherein the thickness of the non-metallic material is between 0.5mm and 50 mm.
6. A method according to any one of claims 1 to 3, wherein the angle θiIs 30-60 degrees.
7. The method according to any one of claims 1 to 3, wherein the non-metallic material is selected from any one of polyethylene, glass fiber, carbon fiber, silicon wafer, glue layer, rubber and cardboard.
8. A system for measuring the thickness of a non-metallic material by using terahertz waves is characterized by comprising a terahertz wave transmitting device, a terahertz wave receiving device, a sample fixing table and a track,
the terahertz wave emitting device is arranged on the track in a sliding mode and can emit terahertz waves to the non-metal material arranged on the sample fixing table,
the terahertz wave receiving device is arranged on the track in a sliding mode and can receive terahertz wave signals reflected by the non-metallic material;
when the terahertz wave transmitting device and the terahertz wave receiving device are respectively arranged at the normal positions of the non-metal material, terahertz wave transmitted by the terahertz wave transmitting device can vertically enter the surface and the bottom surface of the non-metal material to respectively form a first reflection signal and a second reflection signal, and the terahertz wave receiving device receives the first reflection signal and the second reflection signal and obtains the receiving time difference delta T between the first reflection signal and the second reflection signal1
When the terahertz wave transmitting device and the terahertz wave receiving device are respectively arranged on two sides of the normal of the nonmetal material, the terahertz wave transmitted by the terahertz wave transmitting device is at an angle thetaiThe terahertz wave receiving device receives the third reflected signal and the fourth reflected signal and obtains a receiving time difference delta T between the third reflected signal and the fourth reflected signal2
9. The system of claim 8, wherein the track is a circular arc track centered on the sample holding stage.
10. The system of claim 9, wherein the circular arc track has a circular arc radius of 10cm to 30 cm.
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CN111536885B (en) * 2020-06-02 2022-02-25 莱仪特太赫兹(天津)科技有限公司 Double-incidence-angle type terahertz time-domain spectral coating measuring method
CN112051454B (en) * 2020-09-08 2023-11-07 中电科思仪科技股份有限公司 Method and system for detecting dielectric characteristics of material under high-temperature environment based on terahertz waves
CN113136774B (en) * 2021-04-25 2022-03-25 北京理工大学 Terahertz wave-based road icing condition inspection method

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1555479A (en) * 2001-07-13 2004-12-15 ³��ƽ Method and apparatus for increasing signal to noise ratio in a photoacoustic film thickness measurement system
EP1876438A1 (en) * 2006-07-05 2008-01-09 Dtu Determining concentration of a substance in aqueous solution by selfreferenced reflection THz spectroscopy
CN102384892A (en) * 2011-11-17 2012-03-21 江苏大学 Device and method for quickly diagnosing crop nutrition level based on polarized spectrum technology
CN102620666A (en) * 2012-03-29 2012-08-01 吴周令 Detecting system for semiconductor wafer thickness and detecting method thereof
JP5360741B2 (en) * 2008-06-13 2013-12-04 グローリー株式会社 Paper sheet inspection method and inspection apparatus using terahertz light
CN104169677A (en) * 2012-02-08 2014-11-26 霍尼韦尔阿斯卡公司 Caliper coating measurement on continuous non-uniform web using THz sensor
CN104458595A (en) * 2014-12-21 2015-03-25 华东交通大学 Device and method for spectral detection of content of proline in tomato leaves in multi-angle and in-situ manner
CN104748691A (en) * 2015-03-05 2015-07-01 江苏大学 Measurement device and method for film thickness
CN105588516A (en) * 2016-02-23 2016-05-18 天津大学 Paint film thickness measuring method based on terahertz pulse spectrum
JP2017062201A (en) * 2015-09-25 2017-03-30 株式会社Screenホールディングス Film thickness measurement device and film thickness measurement method
CN106841095A (en) * 2017-01-04 2017-06-13 北京环境特性研究所 A kind of method of use terahertz pulse measurement material parameter and material thickness

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1555479A (en) * 2001-07-13 2004-12-15 ³��ƽ Method and apparatus for increasing signal to noise ratio in a photoacoustic film thickness measurement system
EP1876438A1 (en) * 2006-07-05 2008-01-09 Dtu Determining concentration of a substance in aqueous solution by selfreferenced reflection THz spectroscopy
JP5360741B2 (en) * 2008-06-13 2013-12-04 グローリー株式会社 Paper sheet inspection method and inspection apparatus using terahertz light
CN102384892A (en) * 2011-11-17 2012-03-21 江苏大学 Device and method for quickly diagnosing crop nutrition level based on polarized spectrum technology
CN104169677A (en) * 2012-02-08 2014-11-26 霍尼韦尔阿斯卡公司 Caliper coating measurement on continuous non-uniform web using THz sensor
CN102620666A (en) * 2012-03-29 2012-08-01 吴周令 Detecting system for semiconductor wafer thickness and detecting method thereof
CN104458595A (en) * 2014-12-21 2015-03-25 华东交通大学 Device and method for spectral detection of content of proline in tomato leaves in multi-angle and in-situ manner
CN104748691A (en) * 2015-03-05 2015-07-01 江苏大学 Measurement device and method for film thickness
JP2017062201A (en) * 2015-09-25 2017-03-30 株式会社Screenホールディングス Film thickness measurement device and film thickness measurement method
CN105588516A (en) * 2016-02-23 2016-05-18 天津大学 Paint film thickness measuring method based on terahertz pulse spectrum
CN106841095A (en) * 2017-01-04 2017-06-13 北京环境特性研究所 A kind of method of use terahertz pulse measurement material parameter and material thickness

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
基于太赫兹时域光谱的胶层厚度均匀性检测;李丽娟,周明星,任娇娇;《激光与红外》;20140731;第44卷(第7期);801-804 *

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