CN107998023A - A kind of cleawhite pack liquid containing ossein and preparation method thereof - Google Patents
A kind of cleawhite pack liquid containing ossein and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of cleawhite pack liquid containing ossein, it is made of the raw material below according to parts by weight:48 parts of 3 formamide of pyridine, 9 12 parts of ursin, 24 parts of ossein, 15 19 parts of Purslane extract, 7 11 parts of extracting solution of south dodder seed, 0.5 0.9 parts of xanthans, 25 parts of niacinamide, 1.2 1.8 parts of glycerine, 2.1 2.6 parts of dipotassium glycyrrhizinate, 12 parts of hydrolecithin, 0.3 0.7 parts of tromethamine, 58 parts of triethanolamine, 95 100 parts of deionized water.The invention also discloses the preparation method of the cleawhite pack liquid containing ossein.Facial mask liquid prepared by the present invention has excellent whitening effect, is easily received by consumers in general, has important market value and social value.
Description
Technical field
The present invention relates to cosmetic technical field, is specifically a kind of cleawhite pack liquid containing ossein and its preparation side
Method.
Background technology
With the development of science and technology with the continuous improvement of living standards of the people, cosmetics are in people live in occupation of more
Carry out more consequence, this has also driven the development of cosmetic chemistry.In recent years, the kind of cosmetics is on the increase, its function
Property it is also increasingly stronger, while scientific and technological content is also higher and higher.One of the mainstream product of facial mask as cosmetics, has also obtained length
The development of foot.
The mankind use facial mask with a long history as cosmetic tool, can trace back to ancient Egypt and Chinese Tang Dynasty.Facial mask most base
This is also that most important purpose is to make up makeup removing and the still insufficient cleaning that washes one's face, and realizes other maintenances on this basis
Function, such as replenishing water and preserving moisture, whitening and anti-aging etc..The principle of facial mask, exactly using the of short duration time for being covered in face, temporarily
When the extraneous air of isolation and pollution, improve skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, make
The oxygen content of skin rises, and is conducive to skin and excludes the product of epidermal cell metabolism and the oil substances of accumulation, facial mask
In moisture penetrate into the cuticula of epidermis, skin becomes soft, and light is flexible naturally for skin.
Facial mask species currently on the market is various, but these facial masks showed on whitening effect it is not good enough, therefore market need
The good facial mask of a whitening effect.
The content of the invention
It is above-mentioned to solve it is an object of the invention to provide a kind of cleawhite pack liquid containing ossein and preparation method thereof
The problem of being proposed in background technology.
To achieve the above object, the present invention provides following technical solution:
A kind of cleawhite pack liquid containing ossein, is made of the raw material below according to parts by weight:Pyridine-3-carboxamide 4-
8 parts, 9-12 parts of ursin, 2-4 parts of ossein, 15-19 parts of Purslane extract, 7-11 parts of extracting solution of south dodder seed, xanthans
0.5-0.9 parts, 2-5 parts of niacinamide, 1.2-1.8 parts of glycerine, 2.1-2.6 parts of dipotassium glycyrrhizinate, 1-2 parts of hydrolecithin, ammonia fourth
0.3-0.7 parts of triol, 5-8 parts of triethanolamine, 95-100 parts of deionized water.
As the further scheme of the present invention:It is made of the raw material below according to parts by weight:5-7 parts of pyridine-3-carboxamide,
10-11 parts of ursin, 2.5-3.5 parts of ossein, 16-18 parts of Purslane extract, 8-10 parts of extracting solution of south dodder seed, xanthans
0.6-0.8 parts, 3-4 parts of niacinamide, 1.4-1.6 parts of glycerine, 2.2-2.5 parts of dipotassium glycyrrhizinate, 1.3-1.7 parts of hydrolecithin,
0.4-0.6 parts of tromethamine, 6-7 parts of triethanolamine, 96-98 parts of deionized water.
As further scheme of the invention:It is made of the raw material below according to parts by weight:6 parts of pyridine-3-carboxamide,
11 parts of ursin, 3 parts of ossein, 17 parts of Purslane extract, 9 parts of extracting solution of south dodder seed, 0.7 part of xanthans, niacinamide 3.5
Part, 1.5 parts of glycerine, 2.3 parts of dipotassium glycyrrhizinate, 1.5 parts of hydrolecithin, 0.5 part of tromethamine, 6 parts of triethanolamine, deionization
97 parts of water.
As further scheme of the invention:The Purslane extract is made by following methods:Purslane is taken, is washed
Only, dry, grind, add the water of 10-12 times of weight, soak 2-3h, decoct 1-2h, obtain a decoction liquor and once decoct residual
Slag, to once decoct residue in add 6-8 times of weight water, soak 1-2h, decoct 0.5h, obtain secondary decoction liquor and it is secondary decoct
Residue is boiled, a decoction liquor and secondary decoction liquor are merged, filtering, is evaporated under reduced pressure 15-20% of the concentration for original volume, obtains horse
Bitterroot extracting solution.
As further scheme of the invention:The extracting solution of south dodder seed is made by following methods:Semen Cuscutae is taken, clearly
Wash, dry, processing 30-40min is bakeed at 160-180 DEG C, grinding, then adds the water of 7-8 times of weight, soak 2-3h, decoct
1-2h is boiled, decoction liquor is obtained and decocts residue, the water of 4-5 times of weight of addition into decoction residue, ultrasonication 50-60min,
Filtering, obtains ultrasonic extract and ultrasonic wave extraction residue, and decoction liquor and ultrasonic extract are merged is evaporated under reduced pressure concentration
For the 25-30% of original volume, extracting solution of south dodder seed is obtained.
The preparation method of the cleawhite pack liquid containing ossein, step are as follows:
1) pyridine-3-carboxamide, Purslane extract and niacinamide are weighed, after merging, is put into mixer, stirring is mixed
40-50min is closed, discharging, obtains the first mixture;
2) extracting solution of south dodder seed, ursin and dipotassium glycyrrhizinate are weighed, after merging, puts into mixer, is stirred
50-60min, discharging, obtains the second mixture;
3) the first mixture and the second mixture are merged, and adds tromethamine and triethanolamine, put into together to magnetic
In power mixer, the magnetic agitation 45-50min at 50-60 DEG C, obtains the 3rd mixture;
4) deionized water, xanthans and hydrolecithin are weighed, input is into emulsification pot, the homogenization at 75-80 DEG C
10-15min, obtains mixture A;
5) emulsification pot temperature is cooled to 55-60 DEG C, adds ossein, glycerine and the 3rd mixture, continue homogenization
30-35min, discharging, obtains mixture B;
6) nature examination is carried out to mixture B, after qualified, you can.
As further scheme of the invention:The emulsification pot is vacuum emulsifying pot.
Compared with prior art, the beneficial effects of the invention are as follows:
Facial mask liquid prepared by the present invention has excellent whitening effect, and does not stimulate skin, can effectively suppress melanin
Deposition, long-time service can desalinate melanin, play obvious whitening effect, easily received by consumers in general, have weight
The market value and social value wanted.
Embodiment
Technical scheme is described in more detail with reference to embodiment.
Embodiment 1
A kind of cleawhite pack liquid containing ossein, is made of the raw material below according to parts by weight:Pyridine-3-carboxamide 4
Part, 9 parts of ursin, 2 parts of ossein, 15 parts of Purslane extract, 7 parts of extracting solution of south dodder seed, 0.5 part of xanthans, niacinamide 2
Part, 1.2 parts of glycerine, 2.1 parts of dipotassium glycyrrhizinate, 1 part of hydrolecithin, 0.3 part of tromethamine, 5 parts of triethanolamine, deionized water
95 parts.
Wherein, the Purslane extract is made by following methods:Purslane is taken, is cleaned, drying, grinds, and adds 10 times
The water of weight, soaks 2h, decocts 1h, obtains a decoction liquor and once decocts residue, and 6 times of weights are added in residue to once decocting
The water of amount, soaks 1h, decocts 0.5h, secondary decoction liquor and secondary decoction residue is obtained, by a decoction liquor and secondary decoction liquor
Merge, filtering, reduction vaporization concentration is the 15% of original volume, obtains Purslane extract.
The extracting solution of south dodder seed is made by following methods:Semen Cuscutae is taken, is cleaned, drying, the baking processing at 160 DEG C
30min, grinding, then adds the water of 7 times of weight, and immersion 2h, decocts 1h, obtains decoction liquor and decocts residue, to decoction residue
The middle water for adding 4 times of weight, ultrasonication 50min, filtering, obtains ultrasonic extract and ultrasonic wave extraction residue, will decoct
It is the 25% of original volume that boil liquid and ultrasonic extract, which merge reduction vaporization concentrations, obtains extracting solution of south dodder seed.
In the present embodiment, the preparation method of the cleawhite pack liquid containing ossein, step is as follows:
1) pyridine-3-carboxamide, Purslane extract and niacinamide are weighed, after merging, is put into mixer, stirring is mixed
40min is closed, discharging, obtains the first mixture;
2) extracting solution of south dodder seed, ursin and dipotassium glycyrrhizinate are weighed, after merging, puts into mixer, is stirred
50min, discharging, obtains the second mixture;
3) the first mixture and the second mixture are merged, and adds tromethamine and triethanolamine, put into together to magnetic
In power mixer, the magnetic agitation 45min at 50 DEG C, obtains the 3rd mixture;
4) deionized water, xanthans and hydrolecithin are weighed, input is into emulsification pot, the homogenization at 75 DEG C
10min, obtains mixture A, wherein, the emulsification pot is vacuum emulsifying pot;
5) emulsification pot temperature is cooled to 55 DEG C, adds ossein, glycerine and the 3rd mixture, continue homogenization
30min, discharging, obtains mixture B;
6) nature examination is carried out to mixture B, after qualified, you can.
Embodiment 2
A kind of cleawhite pack liquid containing ossein, is made of the raw material below according to parts by weight:Pyridine-3-carboxamide 5
Part, 10 parts of ursin, 2.5 parts of ossein, 18 parts of Purslane extract, 10 parts of extracting solution of south dodder seed, 0.8 part of xanthans, nicotinoyl
3 parts of amine, 1.4 parts of glycerine, 2.2 parts of dipotassium glycyrrhizinate, 1.7 parts of hydrolecithin, 0.6 part of tromethamine, 7 parts of triethanolamine, go
96 parts of ionized water.
Wherein, the Purslane extract is made by following methods:Purslane is taken, is cleaned, drying, grinds, and adds 11 times
The water of weight, soaks 2h, decocts 1.5h, obtains a decoction liquor and once decocts residue, and 6.5 are added to once decocting in residue
The water of times weight, soaks 1h, decocts 0.5h, obtains secondary decoction liquor and secondary decoction residue, by a decoction liquor and secondary decocts
Boil liquid merges, filtering, and reduction vaporization concentration is the 16% of original volume, obtains Purslane extract.
The extracting solution of south dodder seed is made by following methods:Semen Cuscutae is taken, is cleaned, drying, the baking processing at 165 DEG C
32min, grinding, then adds the water of 7 times of weight, soaks 2.5h, decoct 1h, obtains decoction liquor and decocts residue, residual to decocting
The water of 4 times of weight is added in slag, ultrasonication 53min, filtering, obtains ultrasonic extract and ultrasonic wave extraction residue, will
It is the 27% of original volume that decoction liquor and ultrasonic extract, which merge reduction vaporization concentrations, obtains extracting solution of south dodder seed.
In the present embodiment, the preparation method of the cleawhite pack liquid containing ossein, step is as follows:
1) pyridine-3-carboxamide, Purslane extract and niacinamide are weighed, after merging, is put into mixer, stirring is mixed
42min is closed, discharging, obtains the first mixture;
2) extracting solution of south dodder seed, ursin and dipotassium glycyrrhizinate are weighed, after merging, puts into mixer, is stirred
53min, discharging, obtains the second mixture;
3) the first mixture and the second mixture are merged, and adds tromethamine and triethanolamine, put into together to magnetic
In power mixer, the magnetic agitation 45min at 55 DEG C, obtains the 3rd mixture;
4) deionized water, xanthans and hydrolecithin are weighed, input is into emulsification pot, the homogenization at 76 DEG C
10min, obtains mixture A, wherein, the emulsification pot is vacuum emulsifying pot;
5) emulsification pot temperature is cooled to 58 DEG C, adds ossein, glycerine and the 3rd mixture, continue homogenization
30min, discharging, obtains mixture B;
6) nature examination is carried out to mixture B, after qualified, you can.
Embodiment 3
A kind of cleawhite pack liquid containing ossein, is made of the raw material below according to parts by weight:Pyridine-3-carboxamide 6
Part, 11 parts of ursin, 3 parts of ossein, 17 parts of Purslane extract, 9 parts of extracting solution of south dodder seed, 0.7 part of xanthans, niacinamide
3.5 parts, 1.5 parts of glycerine, 2.3 parts of dipotassium glycyrrhizinate, 1.5 parts of hydrolecithin, 0.5 part of tromethamine, 6 parts of triethanolamine, go
97 parts of ionized water.
Wherein, the Purslane extract is made by following methods:Purslane is taken, is cleaned, drying, grinds, and adds 11 times
The water of weight, soaks 2.5h, decocts 1.5h, obtains a decoction liquor and once decocts residue, and 7 are added to once decocting in residue
The water of times weight, soaks 1.5h, decocts 0.5h, obtains secondary decoction liquor and secondary decoction residue, by a decoction liquor and secondary
Decoction liquor merges, filtering, and reduction vaporization concentration is the 18% of original volume, obtains Purslane extract.
The extracting solution of south dodder seed is made by following methods:Semen Cuscutae is taken, is cleaned, drying, the baking processing at 170 DEG C
35min, grinding, then add 7.5 times of weight water, soak 2.5h, decoct 1.5h, obtain decoction liquor and decoct residue, to decoct
The water that 4.5 times of weight is added in residue is boiled, ultrasonication 55min, filtering, obtains ultrasonic extract and ultrasonic wave extraction is residual
Slag, it is the 28% of original volume that decoction liquor and ultrasonic extract are merged reduction vaporization concentrations, obtains extracting solution of south dodder seed.
In the present embodiment, the preparation method of the cleawhite pack liquid containing ossein, step is as follows:
1) pyridine-3-carboxamide, Purslane extract and niacinamide are weighed, after merging, is put into mixer, stirring is mixed
45min is closed, discharging, obtains the first mixture;
2) extracting solution of south dodder seed, ursin and dipotassium glycyrrhizinate are weighed, after merging, puts into mixer, is stirred
55min, discharging, obtains the second mixture;
3) the first mixture and the second mixture are merged, and adds tromethamine and triethanolamine, put into together to magnetic
In power mixer, the magnetic agitation 48min at 55 DEG C, obtains the 3rd mixture;
4) deionized water, xanthans and hydrolecithin are weighed, input is into emulsification pot, the homogenization at 77 DEG C
13min, obtains mixture A, wherein, the emulsification pot is vacuum emulsifying pot;
5) emulsification pot temperature is cooled to 57 DEG C, adds ossein, glycerine and the 3rd mixture, continue homogenization
32min, discharging, obtains mixture B;
6) nature examination is carried out to mixture B, after qualified, you can.
Embodiment 4
A kind of cleawhite pack liquid containing ossein, is made of the raw material below according to parts by weight:Pyridine-3-carboxamide 7
Part, 11 parts of ursin, 3.5 parts of ossein, 16 parts of Purslane extract, 8 parts of extracting solution of south dodder seed, 0.6 part of xanthans, niacinamide
4 parts, 1.6 parts of glycerine, 2.5 parts of dipotassium glycyrrhizinate, 1.3 parts of hydrolecithin, 0.4 part of tromethamine, 6 parts of triethanolamine, go from
Sub- 98 parts of water.
Wherein, the Purslane extract is made by following methods:Purslane is taken, is cleaned, drying, grinds, and adds 11 times
The water of weight, soaks 3h, decocts 1.5h, obtains a decoction liquor and once decocts residue, and 8 times are added in residue to once decocting
The water of weight, soak 1.5h, decoct 0.5h, obtain secondary decoction liquor and secondary decoction residue, by a decoction liquor and it is secondary decoct
Boil liquid merges, filtering, and reduction vaporization concentration is the 20% of original volume, obtains Purslane extract.
The extracting solution of south dodder seed is made by following methods:Semen Cuscutae is taken, is cleaned, drying, the baking processing at 170 DEG C
35min, grinding, then adds the water of 8 times of weight, soaks 3h, decoct 1.5h, obtains decoction liquor and decocts residue, residual to decocting
The water of 5 times of weight is added in slag, ultrasonication 57min, filtering, obtains ultrasonic extract and ultrasonic wave extraction residue, will
It is the 30% of original volume that decoction liquor and ultrasonic extract, which merge reduction vaporization concentrations, obtains extracting solution of south dodder seed.
In the present embodiment, the preparation method of the cleawhite pack liquid containing ossein, step is as follows:
1) pyridine-3-carboxamide, Purslane extract and niacinamide are weighed, after merging, is put into mixer, stirring is mixed
50min is closed, discharging, obtains the first mixture;
2) extracting solution of south dodder seed, ursin and dipotassium glycyrrhizinate are weighed, after merging, puts into mixer, is stirred
60min, discharging, obtains the second mixture;
3) the first mixture and the second mixture are merged, and adds tromethamine and triethanolamine, put into together to magnetic
In power mixer, the magnetic agitation 50min at 60 DEG C, obtains the 3rd mixture;
4) deionized water, xanthans and hydrolecithin are weighed, input is into emulsification pot, the homogenization at 80 DEG C
15min, obtains mixture A, wherein, the emulsification pot is vacuum emulsifying pot;
5) emulsification pot temperature is cooled to 60 DEG C, adds ossein, glycerine and the 3rd mixture, continue homogenization
35min, discharging, obtains mixture B;
6) nature examination is carried out to mixture B, after qualified, you can.
Embodiment 5
A kind of cleawhite pack liquid containing ossein, is made of the raw material below according to parts by weight:Pyridine-3-carboxamide 8
Part, 12 parts of ursin, 4 parts of ossein, 19 parts of Purslane extract, 11 parts of extracting solution of south dodder seed, 0.9 part of xanthans, niacinamide 5
Part, 1.8 parts of glycerine, 2.6 parts of dipotassium glycyrrhizinate, 2 parts of hydrolecithin, 0.7 part of tromethamine, 8 parts of triethanolamine, deionized water
100 parts.
Wherein, the Purslane extract is made by following methods:Purslane is taken, is cleaned, drying, grinds, and adds 12 times
The water of weight, soaks 3h, decocts 2h, obtains a decoction liquor and once decocts residue, and 8 times of weights are added in residue to once decocting
The water of amount, soaks 2h, decocts 0.5h, secondary decoction liquor and secondary decoction residue is obtained, by a decoction liquor and secondary decoction liquor
Merge, filtering, reduction vaporization concentration is the 20% of original volume, obtains Purslane extract.
The extracting solution of south dodder seed is made by following methods:Semen Cuscutae is taken, is cleaned, drying, the baking processing at 180 DEG C
40min, grinding, then adds the water of 8 times of weight, and immersion 3h, decocts 2h, obtains decoction liquor and decocts residue, to decoction residue
The middle water for adding 5 times of weight, ultrasonication 60min, filtering, obtains ultrasonic extract and ultrasonic wave extraction residue, will decoct
It is the 30% of original volume that boil liquid and ultrasonic extract, which merge reduction vaporization concentrations, obtains extracting solution of south dodder seed.
In the present embodiment, the preparation method of the cleawhite pack liquid containing ossein, step is as follows:
1) pyridine-3-carboxamide, Purslane extract and niacinamide are weighed, after merging, is put into mixer, stirring is mixed
50min is closed, discharging, obtains the first mixture;
2) extracting solution of south dodder seed, ursin and dipotassium glycyrrhizinate are weighed, after merging, puts into mixer, is stirred
60min, discharging, obtains the second mixture;
3) the first mixture and the second mixture are merged, and adds tromethamine and triethanolamine, put into together to magnetic
In power mixer, the magnetic agitation 50min at 60 DEG C, obtains the 3rd mixture;
4) deionized water, xanthans and hydrolecithin are weighed, input is into emulsification pot, the homogenization at 80 DEG C
15min, obtains mixture A, wherein, the emulsification pot is vacuum emulsifying pot;
5) emulsification pot temperature is cooled to 60 DEG C, adds ossein, glycerine and the 3rd mixture, continue homogenization
35min, discharging, obtains mixture B;
6) nature examination is carried out to mixture B, after qualified, you can.
Facial mask liquid prepared by the present invention has excellent whitening effect, and does not stimulate skin, can effectively suppress melanin
Deposition, long-time service can desalinate melanin, play obvious whitening effect, easily received by consumers in general, have weight
The market value and social value wanted.
The better embodiment of the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula, can also be on the premise of present inventive concept not be departed from the knowledge that one skilled in the relevant art possesses
Various changes can be made.
Claims (7)
1. a kind of cleawhite pack liquid containing ossein, it is characterised in that be made of the raw material below according to parts by weight:Pyridine-
4-8 parts of 3- formamides, 9-12 parts of ursin, 2-4 parts of ossein, 15-19 parts of Purslane extract, extracting solution of south dodder seed 7-11
Part, 0.5-0.9 parts of xanthans, 2-5 parts of niacinamide, 1.2-1.8 parts of glycerine, 2.1-2.6 parts of dipotassium glycyrrhizinate, hydrolecithin 1-
2 parts, 0.3-0.7 parts of tromethamine, 5-8 parts of triethanolamine, 95-100 parts of deionized water.
2. the cleawhite pack liquid according to claim 1 containing ossein, it is characterised in that by below according to parts by weight
Raw material forms:5-7 parts of pyridine-3-carboxamide, 10-11 parts of ursin, 2.5-3.5 parts of ossein, Purslane extract 16-18
Part, 8-10 parts of extracting solution of south dodder seed, 0.6-0.8 parts of xanthans, 3-4 parts of niacinamide, 1.4-1.6 parts of glycerine, dipotassium glycyrrhizinate
2.2-2.5 parts, 1.3-1.7 parts of hydrolecithin, 0.4-0.6 parts of tromethamine, 6-7 parts of triethanolamine, deionized water 96-98
Part.
3. the cleawhite pack liquid according to claim 2 containing ossein, it is characterised in that by below according to parts by weight
Raw material forms:6 parts of pyridine-3-carboxamide, 11 parts of ursin, 3 parts of ossein, 17 parts of Purslane extract, extracting solution of south dodder seed 9
Part, 0.7 part of xanthans, 3.5 parts of niacinamide, 1.5 parts of glycerine, 2.3 parts of dipotassium glycyrrhizinate, 1.5 parts of hydrolecithin, tromethamine
0.5 part, 6 parts of triethanolamine, 97 parts of deionized water.
4. the cleawhite pack liquid according to claim 1 containing ossein, it is characterised in that the Purslane extract by
Following methods are made:Purslane is taken, is cleaned, drying, grinds, and adds the water of 10-12 times of weight, soaks 2-3h, decocts 1-2h, obtains
Obtain a decoction liquor and once decoct residue, to the water for once decocting 6-8 times of weight of addition in residue, soak 1-2h, decoct
0.5h, obtains secondary decoction liquor and secondary decoction residue, and a decoction liquor and secondary decoction liquor are merged, and filters, and is evaporated under reduced pressure
The 15-20% for original volume is concentrated, obtains Purslane extract.
5. the cleawhite pack liquid according to claim 1 containing ossein, it is characterised in that the extracting solution of south dodder seed by
Following methods are made:Semen Cuscutae is taken, is cleaned, drying, bakees processing 30-40min, grinding, then adds 7- at 160-180 DEG C
The water of 8 times of weight, soaks 2-3h, decocts 1-2h, obtains decoction liquor and decocts residue, 4-5 times of weight is added in residue to decocting
Water, ultrasonication 50-60min, filtering, obtains ultrasonic extract and ultrasonic wave extraction residue, by decoction liquor and ultrasound
Ripple extracting solution merges and 25-30% of the concentration for original volume is evaporated under reduced pressure, and obtains extracting solution of south dodder seed.
A kind of 6. preparation method of cleawhite pack liquid containing ossein as described in claim 1-5 is any, it is characterised in that
Step is as follows:
1) pyridine-3-carboxamide, Purslane extract and niacinamide are weighed, after merging, puts into mixer, is stirred
40-50min, discharging, obtains the first mixture;
2) extracting solution of south dodder seed, ursin and dipotassium glycyrrhizinate are weighed, after merging, puts into mixer, is stirred 50-
60min, discharging, obtains the second mixture;
3) the first mixture and the second mixture are merged, and adds tromethamine and triethanolamine, put into magnetic force stir together
Mix in machine, the magnetic agitation 45-50min at 50-60 DEG C, obtain the 3rd mixture;
4) deionized water, xanthans and hydrolecithin are weighed, input is into emulsification pot, the homogenization 10- at 75-80 DEG C
15min, obtains mixture A;
5) emulsification pot temperature is cooled to 55-60 DEG C, adds ossein, glycerine and the 3rd mixture, continue homogenization 30-
35min, discharging, obtains mixture B;
6) nature examination is carried out to mixture B, after qualified, you can.
7. the preparation method of the cleawhite pack liquid according to claim 6 containing ossein, it is characterised in that the emulsification
Pot is vacuum emulsifying pot.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108785141A (en) * | 2018-09-14 | 2018-11-13 | 广州优刻生物科技有限公司 | A kind of beautifying liquid, preparation method and applications |
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KR20090096928A (en) * | 2008-03-10 | 2009-09-15 | 김준현 | Mask pack composition containig white clay and mackban-stone |
CN104000761A (en) * | 2014-06-12 | 2014-08-27 | 金玲 | Freckle removing and whitening facial mask solution, facial mask and production method of facial mask solution |
CN105748319A (en) * | 2016-03-02 | 2016-07-13 | 佛山市万盈化妆品有限公司 | Facial mask containing ossein |
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2017
- 2017-12-19 CN CN201711377421.6A patent/CN107998023A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20090096928A (en) * | 2008-03-10 | 2009-09-15 | 김준현 | Mask pack composition containig white clay and mackban-stone |
CN104000761A (en) * | 2014-06-12 | 2014-08-27 | 金玲 | Freckle removing and whitening facial mask solution, facial mask and production method of facial mask solution |
CN105748319A (en) * | 2016-03-02 | 2016-07-13 | 佛山市万盈化妆品有限公司 | Facial mask containing ossein |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108785141A (en) * | 2018-09-14 | 2018-11-13 | 广州优刻生物科技有限公司 | A kind of beautifying liquid, preparation method and applications |
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