CN107956126A - 一种真丝织物抗皱整理工艺 - Google Patents

一种真丝织物抗皱整理工艺 Download PDF

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CN107956126A
CN107956126A CN201711203508.1A CN201711203508A CN107956126A CN 107956126 A CN107956126 A CN 107956126A CN 201711203508 A CN201711203508 A CN 201711203508A CN 107956126 A CN107956126 A CN 107956126A
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silk fabric
real silk
crease finishing
finishing technique
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胡晓荣
俞娟
胡瑜
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Wuxi Haoyu Energy Saving Environmental Protection Equipment Co Ltd
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Abstract

本发明公开了一种真丝织物抗皱整理工艺，所述工艺包括真丝织物的前处理、抗皱整理液的配制及抗皱整理等步骤。本发明所述工艺整理获得的真丝织物具有良好的褶皱恢复性能和强力保留率；本发明所述工艺整理获得的真丝织物具有优异的亲水性和手感；奔赴买哪个所述工艺整理获得的真丝织物耐磨性得到提高。

Description

一种真丝织物抗皱整理工艺
技术领域
本发明属于纺织技术领域，涉及一种功能性织物的制备方法，具体为一种真丝织物抗皱整理工艺。
背景技术
由于真丝的蛋白质大分子之间不存在化学交联，当丝纤维吸水膨润时，盐键发生断裂，同时，湿态时水分子破坏了纤维大分子之间的氢键，因此当受到外力作用时，分子链很容易发生相对滑移，外力去除时，分子间又没有足够的约束力使其回复到原来的位置，这使得真丝织物湿抗皱性很差，大大影响了面料的实用效果。这是真丝织物的一个严重缺点，对丝绸的使用带来诸多不便，因此有必要对真丝织物进行抗皱整理。
现有技术中，将烯烃酸类低聚物、甲酸、催化剂、有机硅柔软剂和水的组合物用作蚕丝织物的放皱整理，采用二浸二轧，轧余率为85～90％，并将浸轧后的蚕丝织物进行预烘、烘焙、水洗、烘干制得抗皱真丝织物。该技术方案使用的抗皱整理剂原料价格低廉，不含甲醛成分，经济环保，抗皱整理工艺简单易操作，经整理后的蚕丝织物具有较好的褶皱恢复性能和强力保留率，抗皱性能良好。但是由于其具有硅油类柔软剂影响真丝面料的手感，并影响其亲水性能。
发明内容
本发明解决的技术问题：为了克服现有技术的缺陷，获得一种具有良好的褶皱恢复性能和强力保留率的真丝织物，本发明提供了一种真丝织物抗皱整理工艺。
技术方案：一种真丝织物抗皱整理工艺，所述工艺包括以下步骤：
(1)将真丝织物与质量浓度为10～15g/L亚硫酸钠水溶液混合，常温条件下反应2～5小时，反应结束后，采用去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的真丝织物置于磷酸盐缓冲液中浸泡24～48h，取出后55℃恒温烘干；
(3)将水溶性聚氨酯、壳聚糖和去离子水加到锥形瓶中，并滴加盐酸使溶液pH值为1.5～2.2，置于30～45℃水浴条件下，剧烈振荡12～20min；
(4)向步骤(3)的体系中加入柔软剂、强力保护剂、催化剂和渗透剂，在40～50℃条件下，搅拌混匀，制得抗皱整理液；
(5)将步骤(2)处理后的真丝织物浸渍于步骤(4)获得的抗皱整理液中，在37℃条件下恒温振荡反应5～24h，取出后经二浸二轧，老化干燥，水洗，常温晾干。
优选的，步骤(3)中水溶性聚氨酯与壳聚糖的质量比为11～15:1～2。
优选的，步骤(3)中所述水溶性聚氨酯的型号为Nano-PU。
优选的，步骤(3)中所述壳聚糖的平均分子量为1.6×104～1.8×104。
优选的，步骤(4)中所述柔软剂的型号为TEXILONE SP。
优选的，步骤(4)中所述强力保护剂为PEP。
优选的，步骤(4)中所述催化剂为次磷酸钠。
优选的，步骤(4)中所述渗透剂为聚氧乙烯线性烷基醚。
优选的，步骤(5)中浸轧时的浸轧速率为10-40m/min，浸轧压力为2-2.5kg/cm2，浸轧残液率为50-75％。
有益效果：(1)本发明所述工艺整理获得的真丝织物具有良好的褶皱恢复性能和强力保留率；(2)本发明所述工艺整理获得的真丝织物具有优异的亲水性和手感；(3)奔赴买哪个所述工艺整理获得的真丝织物耐磨性得到提高。
具体实施方式
实施例1
一种真丝织物抗皱整理工艺，所述工艺包括以下步骤：
(1)将真丝织物与质量浓度为10g/L亚硫酸钠水溶液混合，常温条件下反应2小时，反应结束后，采用去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的真丝织物置于磷酸盐缓冲液中浸泡24h，取出后55℃恒温烘干；
(3)将水溶性聚氨酯、壳聚糖和去离子水加到锥形瓶中，并滴加盐酸使溶液pH值为1.5，置于30℃水浴条件下，剧烈振荡12min；
(4)向步骤(3)的体系中加入柔软剂、强力保护剂、催化剂和渗透剂，在40℃条件下，搅拌混匀，制得抗皱整理液；
(5)将步骤(2)处理后的真丝织物浸渍于步骤(4)获得的抗皱整理液中，在37℃条件下恒温振荡反应5h，取出后经二浸二轧，老化干燥，水洗，常温晾干。
步骤(3)中水溶性聚氨酯与壳聚糖的质量比为11:1。
步骤(3)中所述水溶性聚氨酯的型号为Nano-PU。
步骤(3)中所述壳聚糖的平均分子量为1.6×104。
步骤(4)中所述柔软剂的型号为TEXILONE SP。
步骤(4)中所述强力保护剂为PEP。
步骤(4)中所述催化剂为次磷酸钠。
步骤(4)中所述渗透剂为聚氧乙烯线性烷基醚。
步骤(5)中浸轧时的浸轧速率为10m/min，浸轧压力为2kg/cm2，浸轧残液率为50％。
实施例2
一种真丝织物抗皱整理工艺，所述工艺包括以下步骤：
(1)将真丝织物与质量浓度为12g/L亚硫酸钠水溶液混合，常温条件下反应3.5小时，反应结束后，采用去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的真丝织物置于磷酸盐缓冲液中浸泡36h，取出后55℃恒温烘干；
(3)将水溶性聚氨酯、壳聚糖和去离子水加到锥形瓶中，并滴加盐酸使溶液pH值为2.0，置于36℃水浴条件下，剧烈振荡18min；
(4)向步骤(3)的体系中加入柔软剂、强力保护剂、催化剂和渗透剂，在45℃条件下，搅拌混匀，制得抗皱整理液；
(5)将步骤(2)处理后的真丝织物浸渍于步骤(4)获得的抗皱整理液中，在37℃条件下恒温振荡反应16h，取出后经二浸二轧，老化干燥，水洗，常温晾干。
步骤(3)中水溶性聚氨酯与壳聚糖的质量比为13:2。
步骤(3)中所述水溶性聚氨酯的型号为Nano-PU。
步骤(3)中所述壳聚糖的平均分子量为1.7×104。
步骤(4)中所述柔软剂的型号为TEXILONE SP。
步骤(4)中所述强力保护剂为PEP。
步骤(4)中所述催化剂为次磷酸钠。
步骤(4)中所述渗透剂为聚氧乙烯线性烷基醚。
步骤(5)中浸轧时的浸轧速率为26m/min，浸轧压力为2.2kg/cm2，浸轧残液率为65％。
实施例3
一种真丝织物抗皱整理工艺，所述工艺包括以下步骤：
(1)将真丝织物与质量浓度为15g/L亚硫酸钠水溶液混合，常温条件下反应5小时，反应结束后，采用去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的真丝织物置于磷酸盐缓冲液中浸泡48h，取出后55℃恒温烘干；
(3)将水溶性聚氨酯、壳聚糖和去离子水加到锥形瓶中，并滴加盐酸使溶液pH值为2.2，置于45℃水浴条件下，剧烈振荡20min；
(4)向步骤(3)的体系中加入柔软剂、强力保护剂、催化剂和渗透剂，在50℃条件下，搅拌混匀，制得抗皱整理液；
(5)将步骤(2)处理后的真丝织物浸渍于步骤(4)获得的抗皱整理液中，在37℃条件下恒温振荡反应24h，取出后经二浸二轧，老化干燥，水洗，常温晾干。
步骤(3)中水溶性聚氨酯与壳聚糖的质量比为15:2。
步骤(3)中所述水溶性聚氨酯的型号为Nano-PU。
步骤(3)中所述壳聚糖的平均分子量为1.8×104。
步骤(4)中所述柔软剂的型号为TEXILONE SP。
步骤(4)中所述强力保护剂为PEP。
步骤(4)中所述催化剂为次磷酸钠。
步骤(4)中所述渗透剂为聚氧乙烯线性烷基醚。
步骤(5)中浸轧时的浸轧速率为40m/min，浸轧压力为2.5kg/cm2，浸轧残液率为75％。
对实施例1～3所述工艺制备获得的真丝织物进行性能测试，结果如下：

Claims (9)

1.一种真丝织物抗皱整理工艺，其特征在于，所述工艺包括以下步骤：
(1)将真丝织物与质量浓度为10～15g/L亚硫酸钠水溶液混合，常温条件下反应2～5小时，反应结束后，采用去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的真丝织物置于磷酸盐缓冲液中浸泡24～48h，取出后55℃恒温烘干；
(3)将水溶性聚氨酯、壳聚糖和去离子水加到锥形瓶中，并滴加盐酸使溶液pH值为1.5～2.2，置于30～45℃水浴条件下，剧烈振荡12～20min；
(4)向步骤(3)的体系中加入柔软剂、强力保护剂、催化剂和渗透剂，在40～50℃条件下，搅拌混匀，制得抗皱整理液；
(5)将步骤(2)处理后的真丝织物浸渍于步骤(4)获得的抗皱整理液中，在37℃条件下恒温振荡反应5～24h，取出后经二浸二轧，老化干燥，水洗，常温晾干。
2.根据权利要求1所述的一种真丝织物抗皱整理工艺，其特征在于，步骤(3)中水溶性聚氨酯与壳聚糖的质量比为11～15:1～2。
3.根据权利要求1所述的一种真丝织物抗皱整理工艺，其特征在于，步骤(3)中所述水溶性聚氨酯的型号为Nano-PU。
4.根据权利要求1所述的一种真丝织物抗皱整理工艺，其特征在于，步骤(3)中所述壳聚糖的平均分子量为1.6×104～1.8×104。
5.根据权利要求1所述的一种真丝织物抗皱整理工艺，其特征在于，步骤(4)中所述柔软剂的型号为TEXILONE SP。
6.根据权利要求1所述的一种真丝织物抗皱整理工艺，其特征在于，步骤(4)中所述强力保护剂为PEP。
7.根据权利要求1所述的一种真丝织物抗皱整理工艺，其特征在于，步骤(4)中所述催化剂为次磷酸钠。
8.根据权利要求1所述的一种真丝织物抗皱整理工艺，其特征在于，步骤(4)中所述渗透剂为聚氧乙烯线性烷基醚。
9.根据权利要求1所述的一种真丝织物抗皱整理工艺，其特征在于，步骤(5)中浸轧时的浸轧速率为10-40m/min，浸轧压力为2-2.5kg/cm2，浸轧残液率为50-75％。
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