CN107950774A - A kind of feeding composite functional plants essential oil, preparation method and applications - Google Patents
A kind of feeding composite functional plants essential oil, preparation method and applications Download PDFInfo
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- CN107950774A CN107950774A CN201710283232.6A CN201710283232A CN107950774A CN 107950774 A CN107950774 A CN 107950774A CN 201710283232 A CN201710283232 A CN 201710283232A CN 107950774 A CN107950774 A CN 107950774A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/11—Aldehydes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
- A61K31/19—Carboxylic acids, e.g. valproic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/21—Esters, e.g. nitroglycerine, selenocyanates
- A61K31/215—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids
- A61K31/22—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids of acyclic acids, e.g. pravastatin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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Abstract
The invention discloses a kind of feeding composite functional plants essential oil, preparation method and applications, wherein the preparation method of feeding composite functional plants essential oil includes the following steps：Include 50 150g of composition cinnamic acid, 50 120g of origanum oil, 20 80g of Rosmarinus officinalis extract according to feeding composite functional plants essential oil described in 1Kg, 30 100g of glycerol monobutyralte, sodium butyrate 50 100,50 100g of calcium formate, 50 100g of acetic acid, 50 150g of lactic acid and surplus excipient content ratio, above-mentioned various raw materials are uniformly mixed, 20 mesh sieves is crossed and obtains feeding composite functional plants essential oil.The application of the feeding composite functional plants essential oil as additive for farm animal feed, animal and bird intestines microecological balance can be improved, improve livestock and poultry production performance, substitute antibiotics action effect, and the action character of feeding the composite functional plants essential oil combination acidulant and plants essential oil, both comprehensive advantages, effect more comprehensively, do not make pathogen develop immunity to drugs.
Description
Technical field
The present invention relates to a kind of feeding composite functional plants essential oil, and specifically, the present invention relates to a kind of feeding compound
Functional plants essential oil, preparation method and applications, belong to its feeding technical field.
Background technology
Antibiotic has been commonly used as feed addictive in feedstuff industry, it can not only prevent livestock and poultry, and
And the metabolism of livestock and poultry can be improved, survival rate and feed conversion rate are improved, promotes the growth of livestock and poultry.But with feeding antibiotic
Widely use and be continuously increased with species, cause a series of problems, such as the generation of a large amount of antibody-resistant bacterium, have impact on the mankind
Control to disease；Animal and bird intestines microecological balance is destroyed, the immunity function for causing livestock and poultry body declines, and the death rate carries
It is high；For a long time or antibiotic, which is excessively used, can cause antibiotic to be accumulated in livestock and poultry body, and the medicament residue of generation can influence animal sources
The security of food.The Ministry of Agriculture of China in 2016 puts into effect new regulation, and limitation colistine sulfate is in the use of feedstuff industry, parallel connection
The joint issue of He Duo ministries and commissions《Contain bacterial drug resistance national plan of action（2016-2020）》, future may gradually forbid it
Use of its antibiotic on food animal.Solve antibiotic added in feed caused by a series of problems except limiting and closing
Natural sciences are selected outside antibiotic, it is also necessary to constantly develop new substitute products, wherein acidulant and plants essential oil etc. becomes
Current research and using hot spot.
Fodder acidulant is the inorganic acid of one or more or the mixture of organic acid, and adding acidulant in feed can drop
The palatability for being sour power, improving feed of low feed, reduces the pH of animal and bird intestines, promotes the propagation of probiotics especially lactic acid bacteria,
The quantity of pathogenic bacteria such as Escherichia coli and salmonella is reduced, has been widely used in animal and fowl fodder production.
Plants essential oil is a kind of secondary metabolite being present in plant, be one kind make plant have peat-reek and
The native compound of color.Usually with the flower of plant, leaf, root, fruit, skin and natural gum etc. for raw material, pass through steam distillation, squeezing
And the Herbivore oil sample aromatic substance that the methods of solvent extraction extracts.Numerous studies show, plants essential oil have antibacterial,
It is anti-oxidant to wait biological characteristics.Application can suppress the growth of harmful bacteria in feed on animal productiong, promote feed intake, improve
Production performance, enhancing immunity of organism etc., and due to plants essential oil fast degradation and half-life short in vivo, do not accumulate in vivo
Characteristic, plants essential oil are considered as a kind of safe efficient, environmentally friendly novel fodder additive.
Acidulant and the plants essential oil mechanism of action are different, but effect is all embodied in the enhancement of environment to growth of animals or poultry
On, including environment and external growing environment in animal and bird intestines digestion.The acidulant and plants essential oil product applied currently on the market
Species is very much, but the product mechanism of action and function are all relatively single, it is difficult to which substitute antibiotics completely are applied in feed.
The content of the invention
The problem to be solved in the present invention is the drawbacks of overcoming above single product to use, with reference to acidulant and plants essential oil
Action character, designs a kind of both synthesis advantages, the feeding compound work(that effect does not make more comprehensively, pathogen develop immunity to drugs
Can property plants essential oil product.
To achieve these goals, present invention employs following technical solution：
A kind of feeding composite functional plants essential oil, feeding composite functional plants essential oil described in per 1Kg include：Cinnamic acid
50-150g, origanum oil 50-120g, Rosmarinus officinalis extract 20-80g, glycerol monobutyralte 30-100g, sodium butyrate 50-100, formic acid
Calcium 50-100g, acetic acid 50-100g, lactic acid 50-150g, surplus are excipient.
Preferably, mass content >=10% of the excipient in the feeding composite functional plants essential oil.
Preferably, the excipient is included in white carbon, calcium stearate, mountain flour, montmorillonite, cornstarch, defatted rice bran
At least one.
A kind of preparation method of feeding composite functional plants essential oil, includes the following steps：
S1, according to feeding composite functional plants essential oil described in 1Kg include composition cinnamic acid 50-150g, origanum oil 50-120g,
Rosmarinus officinalis extract 20-80g, glycerol monobutyralte 30-100g, sodium butyrate 50-100, calcium formate 50-100g, acetic acid 50-100g,
The ratio of the content of lactic acid 50-150g and the excipient of surplus takes each composition；
S2, mix cinnamic acid, origanum oil, Rosmarinus officinalis extract and glycerol monobutyralte in proportion, after be added in excipient, mix
Obtained mixture after closing uniformly；
S3, mix sodium butyrate, calcium formate, acetic acid and lactic acid in proportion, after be added to step（2）In mixture, it is uniformly mixed
Mixture is made afterwards；
S4, by step（3）Gained mixture is placed in mixer, stirring 1-2 it is small when after, be put into preliminary crushing in pulverizer, take
It is fine grained to be placed into after going out in micronizer and carry out separating twice, crosses 20 mesh, packs up to composite functional plant
Essential oil.
A kind of application of feeding composite functional plants essential oil, a kind of feeding composite functional plants essential oil are raised as animal
The application of feed additives, and 0.2~0.5wt ‰ that the additive amount of the feeding composite functional plants essential oil is animal feed.
The beneficial effects of the invention are as follows:The feeding composite functional plants essential oil of the present invention by addition to growth of animal and
The beneficial various nutritional ingredients of intestinal environment can be stimulated by distinctive pungent fragrance taste taste bud, enteron aisle villus cell growth and
Development and the secretion of enteron aisle digestive ferment, increase livestock and poultry feed intake, improve efficiency of feed utilization, improve breeding performonce fo animals；Promotion has
The breeding of beneficial bacteria, suppresses harmful bacteria growth, improves animal and bird intestines microorganism species balance；Strengthen animal body humoral immunity and
Cellular immune function, improves resisting respiratory tract disease ability, reduces breathing problem incidence, improves the prevention effect to Animal diseases
Fruit；Oxidation resistance is strong, can effectively prevent feedstuff oxidation acidifying corruption, and removes unnecessary free radical in vivo, improves anti-
Stress ability.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
A kind of feeding composite functional plants essential oil, includes per the feeding composite functional plants essential oils of 1Kg：Cinnamic acid
50-150g, origanum oil 50-120g, Rosmarinus officinalis extract 20-80g, glycerol monobutyralte 30-100g, sodium butyrate 50-100, formic acid
Calcium 50-100g, acetic acid 50-100g, lactic acid 50-150g, surplus are excipient.Excipient is in the feeding composite functional plant
Mass content >=10% in essential oil.Excipient includes white carbon, calcium stearate, mountain flour, montmorillonite, cornstarch, defatted rice bran
At least one of.A kind of preparation method of feeding composite functional plants essential oil, includes the following steps：
S1, according to feeding composite functional plants essential oil described in 1Kg include composition cinnamic acid 50-150g, origanum oil 50-120g,
Rosmarinus officinalis extract 20-80g, glycerol monobutyralte 30-100g, sodium butyrate 50-100, calcium formate 50-100g, acetic acid 50-100g,
The ratio of the content of lactic acid 50-150g and the excipient of surplus takes each composition；
S2, mix cinnamic acid, origanum oil, Rosmarinus officinalis extract and glycerol monobutyralte in proportion, after be added in excipient, mix
Obtained mixture after closing uniformly；
S3, mix sodium butyrate, calcium formate, acetic acid and lactic acid in proportion, after be added to step（2）In mixture, it is uniformly mixed
Mixture is made afterwards；
S4, by step（3）Gained mixture is placed in mixer, stirring 1-2 it is small when after, be put into preliminary crushing in pulverizer, take
It is fine grained to be placed into after going out in micronizer and carry out separating twice, crosses 20 mesh, packs up to composite functional plant
Essential oil.
A kind of application of feeding composite functional plants essential oil, a kind of feeding composite functional plants essential oil are raised as animal
The application of feed additives, and 0.2~0.5wt ‰ that the additive amount of the feeding composite functional plants essential oil is animal feed.
Embodiment 1
A kind of feeding composite functional plants essential oil, composition are as follows：Cinnamic acid 50g, origanum oil 60g, Rosmarinus officinalis extract 20g,
Glycerol monobutyralte 40g, sodium butyrate 50g, calcium formate 60g, acetic acid 50g, lactic acid 120g, white carbon 200g, montmorillonite 350g.
Embodiment 2
A kind of feeding composite functional plants essential oil, composition are as follows：Cinnamic acid 60g, origanum oil 80g, Rosmarinus officinalis extract 40g,
Glycerol monobutyralte 60g, sodium butyrate 80g, calcium formate 100g, acetic acid 50g, lactic acid 100g, cornstarch 100g, talcum powder 330g.
Embodiment 3
A kind of feeding composite functional plants essential oil, composition are as follows：Cinnamic acid 80g, origanum oil 90g, Rosmarinus officinalis extract 50g,
Glycerol monobutyralte 70g, sodium butyrate 80g, calcium formate 70g, acetic acid 60g, lactic acid 90g, white carbon 110g, calcium stearate 300g.
Embodiment 4
A kind of feeding composite functional plants essential oil, composition are as follows：Cinnamic acid 120g, origanum oil 100g, Rosmarinus officinalis extract
50g, glycerol monobutyralte 80g, sodium butyrate 100g, calcium formate 100g, acetic acid 100g, lactic acid 60g, defatted rice bran 100g, montmorillonite
190g。
The preparation method of feeding composite functional plants essential oil is as follows in 4 embodiments of the above, it is characterised in that：
Comprise the following steps：
（1）Each composition is taken according to component content in formula；
（2）Cinnamic acid, origanum oil, Rosmarinus officinalis extract and glycerol monobutyralte are mixed in proportion, after be added in excipient, mix
Obtained mixture after closing uniformly；
（3）Sodium butyrate, calcium formate, acetic acid and lactic acid are mixed in proportion, after be added to step（2）In mixture, it is uniformly mixed
Mixture is made afterwards；
（4）By step（3）Gained mixture is placed in mixer, stirring 1-2 it is small when after, 20 mesh are crushed in pulverizer, seal
Pack up to feeding composite functional plants essential oil.
Embodiment 5
For the feeding use functional plants essential oil that embodiment 1 is prepared as broiler chicken feed additive, additive amount is pig starter feed
0.5wt ‰.
Embodiment 6
For the feeding use functional plants essential oil that embodiment 2 is prepared as fleshy duck fodder additive, additive amount is pig starter feed
0.4wt ‰.
Embodiment 7
Using the feeding use functional plants essential oil that embodiment 3 is prepared as growing and fattening pig feed additive, additive amount is son
The 0.3wt ‰ of pannage.
Experiment
1. broiler breeding is tested
Method：The normal AA commercial generations Broiler chicks 4200 of 1 age in days health are selected, are evenly distributed to according to the consistent principle of weight
1 control group and 6 test groups, each 6 repetitions of test group, each repeat 100 chickens.Test group 1-4 adds the above 4 respectively
Feeding composite functional plants essential oil obtained by a embodiment, the feeding composite functional plant essence of the gained of embodiment 1 of test group 1
Oil, the feeding composite functional plants essential oil of the gained of embodiment 2 of test group 2, the feeding compound work(of the gained of embodiment 3 of test group 3
Energy property plants essential oil, the feeding composite functional plants essential oil of the gained of embodiment 4 of test group 4.Certain the commercially available acidulant of test group 5
Product（Main component includes formic acid, acetic acid and lactic acid）, certain the commercially available feeding essential oil product of test group 6（Main component is wild marjoram
Oil）.
Control group：Commodity complete diet pellet is fed, does not add feeder acidulant and feeding essential oil product；
Test group：Commodity complete diet pellet is fed, test group 1-4 is by the addition feeding use functional plants essential oil production of 5 adding method of embodiment
Product, test group 5 add certain commercially available acidulant 1kg/t complete diet pellet, and test group 6 adds certain commercial plant essential oil product 500g/t full price
Material.
42 days test periods, count and calculate death and culling rate, average daily feed intake, Average weight increasing a day and feedstuff-meat ratio.Result of the test is such as
Table 1 below：
Table 1
It can be seen from the data in Table 1 that 6 test group broiler chicken death and culling rates and feedstuff-meat ratio are below control group, Average weight increasing a day is high
In two control groups.Above-mentioned result of the test illustrates, invention product is added in diet than individually addition feeder acidulant and feeding plant
Thing essential oil effect on meat chicken production performance is improved is more preferable.
2. growing-finishing pig is tested
Method：The similar hybridized pig 420 of original body mass is selected, each 210 of male and female, is evenly distributed to 1 control group and 6
Test group, each test group set 3 repetitions, each to repeat 20.Test group 1-4 is added respectively to raise obtained by 4 embodiments of the above
With composite functional plants essential oil, the feeding composite functional plants essential oil of the gained of embodiment 1 of test group 1, the implementation of test group 2
The feeding composite functional plants essential oil of the gained of example 2, the feeding composite functional plants essential oil of the gained of embodiment 3 of test group 3, experiment
The feeding composite functional plants essential oil of the gained of embodiment 4 of group 4.Certain the commercially available acidulant product of test group 5（Main component includes
Formic acid, acetic acid and lactic acid）, certain the commercially available feeding essential oil product of test group 6（Main component is origanum oil）.
Control group：Commodity complete diet pellet is fed, does not add feeder acidulant and feeding essential oil product；
Test group：Commodity complete diet pellet is fed, test group 1-4 is by the addition feeding use functional plants essential oil production of 7 adding method of embodiment
Product, test group 5 add certain commercially available acidulant 1kg/t complete diet pellet, and test group 6 adds certain commercial plant essential oil product 500g/t full price
Material.
72 days test periods, statistics calculates diarrhea rate, Average weight increasing a day and feed-weight ratio, while each repetition is selected after the test
Select 2 pigs to butcher, preserved after enteron aisle Digesta samples are taken when butchering with plastic sample bag -20 DEG C of refrigerators of placement.It is dilute using tablet
Interpretation of the law counts the lactic acid bacteria in sample and Escherichia coli.Result of the test such as table 2 below.
Table 2
It can be seen from the data in Table 2 that the Escherichia coli in the diarrhea rate of test group growing-finishing pig, feed-weight ratio and enteron aisle chyme
Quantity significantly reduces compared to the control group, and lactic acid bacteria is significantly increased compared to the control group in Average weight increasing a day and enteron aisle chyme, addition
4 test groups and the commercially available acidulant of addition of invention product and 2 test group Escherichia coli of origanum oil and lactic acid bacteria have necessarily
Difference, but difference is not notable.Above-mentioned result of the test illustrates that addition product of the present invention can reduce growing and fattening diarrhea of pigs in diet
Rate, improves the production performance of growing-finishing pig, improves intestinal microecology balance, and practical application effect is better than individually adding feeding acid
Agent and origanum oil.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (5)
1. a kind of feeding composite functional plants essential oil, it is characterised in that in feeding composite functional plants essential oil described in per 1Kg
Including：Cinnamic acid 50-150g, origanum oil 50-120g, Rosmarinus officinalis extract 20-80g, glycerol monobutyralte 30-100g, sodium butyrate
50-100, calcium formate 50-100g, acetic acid 50-100g, lactic acid 50-150g, surplus are excipient.
2. a kind of feeding composite functional plants essential oil according to claim 1, it is characterised in that the excipient is in institute
State mass content >=10% in feeding composite functional plants essential oil.
3. a kind of feeding composite functional plants essential oil according to claim 1, it is characterised in that the excipient includes
At least one of white carbon, calcium stearate, mountain flour, montmorillonite, cornstarch, defatted rice bran.
4. a kind of preparation method of feeding composite functional plants essential oil, includes the following steps：
S1, according to feeding composite functional plants essential oil described in 1Kg include composition cinnamic acid 50-150g, origanum oil 50-120g,
Rosmarinus officinalis extract 20-80g, glycerol monobutyralte 30-100g, sodium butyrate 50-100, calcium formate 50-100g, acetic acid 50-100g,
The ratio of the content of lactic acid 50-150g and the excipient of surplus takes each composition；
S2, mix cinnamic acid, origanum oil, Rosmarinus officinalis extract and glycerol monobutyralte in proportion, after be added in excipient, mix
Obtained mixture after closing uniformly；
S3, mix sodium butyrate, calcium formate, acetic acid and lactic acid in proportion, after be added to step（2）In mixture, it is uniformly mixed
Mixture is made afterwards；
S4, by step（3）Gained mixture is placed in mixer, stirring 1-2 it is small when after, be put into preliminary crushing in pulverizer, take
It is fine grained to be placed into after going out in micronizer and carry out separating twice, crosses 20 mesh, packs up to composite functional plant
Essential oil.
A kind of 5. application of feeding composite functional plants essential oil, it is characterised in that：A kind of feeding composite functional plants essential oil
As the application of animal feed additive, and 0.2 that the additive amount of the feeding composite functional plants essential oil is animal feed
~0.5wt ‰.
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| CN110771729A (en) * | 2019-11-01 | 2020-02-11 | 广西壮族自治区林业科学研究院 | Feed additive containing plant essential oil and preparation method thereof |
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| WO2019243345A1 (en) * | 2018-06-22 | 2019-12-26 | Basf Se | Compositions for animals and uses thereof |
| CN112351688A (en) * | 2018-06-22 | 2021-02-09 | 巴斯夫欧洲公司 | Composition for animals and use thereof |
| JP2021528078A (en) * | 2018-06-22 | 2021-10-21 | ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ | Animal compositions and their use |
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| CN110771729A (en) * | 2019-11-01 | 2020-02-11 | 广西壮族自治区林业科学研究院 | Feed additive containing plant essential oil and preparation method thereof |
| CN111728099A (en) * | 2020-06-02 | 2020-10-02 | 湖北华扬科技发展有限公司 | Combination of a feed compound acidifier and a plant extract |
| CN114982874A (en) * | 2021-09-03 | 2022-09-02 | 唐人神集团股份有限公司 | Feed additive for improving intestinal health of broiler chickens and application thereof |
| CN114344356A (en) * | 2021-12-31 | 2022-04-15 | 福建傲农生物科技集团股份有限公司 | Bacteriostatic composite active substance microcapsule particles and preparation method and application thereof |
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