CN107938423A - A kind of refractory fiber paper and preparation method thereof - Google Patents

A kind of refractory fiber paper and preparation method thereof Download PDF

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Publication number
CN107938423A
CN107938423A CN201711084331.8A CN201711084331A CN107938423A CN 107938423 A CN107938423 A CN 107938423A CN 201711084331 A CN201711084331 A CN 201711084331A CN 107938423 A CN107938423 A CN 107938423A
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CN
China
Prior art keywords
parts
paper
preparation
page
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711084331.8A
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Chinese (zh)
Inventor
周栋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yuyao Jin Chi Handicraft Co Ltd
Original Assignee
Yuyao Jin Chi Handicraft Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yuyao Jin Chi Handicraft Co Ltd filed Critical Yuyao Jin Chi Handicraft Co Ltd
Priority to CN201711084331.8A priority Critical patent/CN107938423A/en
Publication of CN107938423A publication Critical patent/CN107938423A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
    • D21F11/00—Processes for making continuous lengths of paper, or of cardboard, or of wet web for fibre board production, on paper-making machines
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21G—CALENDERS; ACCESSORIES FOR PAPER-MAKING MACHINES
    • D21G1/00—Calenders; Smoothing apparatus
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H13/00—Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
    • D21H13/36—Inorganic fibres or flakes
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H15/00—Pulp or paper, comprising fibres or web-forming material characterised by features other than their chemical constitution
    • D21H15/02—Pulp or paper, comprising fibres or web-forming material characterised by features other than their chemical constitution characterised by configuration
    • D21H15/10—Composite fibres
    • D21H15/12—Composite fibres partly organic, partly inorganic
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20—Macromolecular organic compounds
    • D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
    • D21H17/24—Polysaccharides
    • D21H17/25—Cellulose
    • D21H17/26—Ethers thereof
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20—Macromolecular organic compounds
    • D21H17/33—Synthetic macromolecular compounds
    • D21H17/46—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H17/53—Polyethers; Polyesters
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63—Inorganic compounds
    • D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
    • D21H17/68—Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/10—Coatings without pigments
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/34—Ignifugeants

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Paper (AREA)

Abstract

The invention discloses a kind of refractory fiber paper and preparation method thereof, raw material components are as follows according to weight score：30 50 parts of ceramic fibre, 10 20 parts of plant fiber, 8 15 parts of silica, 8 13 parts of composite magnesium silicate, 5 10 parts of talcum powder, 58 parts of deionized water, 5 10 parts of polyethylene glycol, 38 parts of carboxymethyl cellulose, 10 20 parts of aqueous buffing oil.Raw material of the present invention is simple and easy to get, processing method advantages of simple, and cost is low, mass produced suitable for factory, it is applied widely, it is green safe, unharmful substance, paper good toughness, tensile strength are big, transparency is high, good, anti-scratch, the anti-wiping property of guarantor's light colour retention is strong, excellent weather resistance and hard, and stability is strong, high temperature resistant, low temperature resistant, anticorrosion effect is good, and fire resisting coefficient is high, it is anti-aging, prolong the service life.

Description

A kind of refractory fiber paper and preparation method thereof
Technical field
The present invention relates to paper preparation field, is specially a kind of refractory fiber paper and preparation method thereof.
Background technology
Paper, with the increase of demand and the progress of provincial capital, produces skill as essential daily necessities in life Art is more and more ripe, and most paper still uses traditional handicraft, not only wastes trees, improves cost, and does not have fire resistance, But in the modern life, more and more for the demand of fire resisting paper, market prospects are a piece of fine, existing technical sophistication not into Ripe, product quality imperfection is of high cost.
The content of the invention
It is an object of the invention to provide a kind of refractory fiber paper and preparation method thereof, to solve to carry in above-mentioned background technology The problem of going out.
To achieve the above object, the present invention provides following technical solution：A kind of refractory fiber paper and preparation method thereof, raw material Component is as follows according to weight score：30-50 parts of ceramic fibre, 10-20 parts of plant fiber, 8-15 parts of silica, complex silicate 8-13 parts of magnesium, 5-10 parts of talcum powder, 5-8 parts of deionized water, 5-10 parts of polyethylene glycol, 3-8 parts of carboxymethyl cellulose, water-based polishing It is 10-20 parts oily.
Further improvement of the present invention is：Its preparation method is as follows：
A, ceramic fibre, plant fiber and carboxymethyl cellulose are mixed, adds deionized water and be beaten, used 2-3mm crosses sieve and sieves, and removes the laggard row of impurity and disperses, and dispersion temperature is set to 40-45 DEG C, disperses one per 10-15min It is secondary, altogether three times, water slurry is made；
B, at room temperature, silica, composite magnesium silicate, talcum powder and polyethylene glycol are mixed, in stirred Deionized water is slowly added in four times, until jelly, stir speed (S.S.) 400-500r/min；
C, the mixture in step B is added in water slurry, stirred evenly, operated using centrifuge, frequency is 3000-3500HZ, using supernatant liquor is taken after 1-2mm filter screen filtrations, is manufactured paper with pulp using clear liquid, l Water Paper page is obtained, to wet Page is squeezed and dried, and squeezing gravity is 800-1000Kg, and drying temperature is set to 150-200 DEG C；
D, hot rolling is carried out to dried page, hot-rolled temperature is set to 250-300 DEG C, to the page after hot rolling in 100- Aqueous buffing oil is sprayed under the pressure of 200kgf/cm2 and carries out press polish, bright superficial film is formed after being cooled to room temperature, obtains Product.
Compared with prior art, the beneficial effects of the invention are as follows：Raw material of the present invention is simple and easy to get, and processing method simply closes Reason, cost is low, is mass produced suitable for factory, applied widely, green safe, unharmful substance, paper good toughness, tension Intensity is big, and transparency is high, good, anti-scratch, the anti-wiping property of guarantor's light colour retention is strong, excellent weather resistance and hard, and stability is strong, high temperature resistant, low temperature resistant, resistance to Corrosive effect is good, and fire resisting coefficient is high, anti-aging, prolongs the service life.
Embodiment
The technical solution in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment Only part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this area Art personnel all other embodiments obtained without making creative work, belong to the model that the present invention protects Enclose.
Embodiment one：
A kind of refractory fiber paper and preparation method thereof, raw material components are as follows according to weight score：35 parts of ceramic fibre, plant 5 parts of fiber, 0 part of silica 1,9 parts of composite magnesium silicate, 7 parts of talcum powder, 8 parts of deionized water, 5 parts of polyethylene glycol, carboxymethyl are fine 4 parts of dimension element, 16 parts of aqueous buffing oil.
Its preparation method is as follows：
A, ceramic fibre, plant fiber and carboxymethyl cellulose are mixed, adds deionized water and be beaten, used 3mm crosses sieve and sieves, and removes the laggard row of impurity and disperses, and dispersion temperature is set to 40 DEG C, disperses once per 15min, altogether three times, Water slurry is made；
B, at room temperature, silica, composite magnesium silicate, talcum powder and polyethylene glycol are mixed, in stirred Deionized water is slowly added in four times, until jelly, stir speed (S.S.) 420r/min；
C, the mixture in step B is added in water slurry, stirred evenly, operated using centrifuge, frequency is 3100HZ, using supernatant liquor is taken after 1mm filter screen filtrations, is manufactured paper with pulp using clear liquid, obtains l Water Paper page, and l Water Paper page is carried out Squeezing and drying, squeezing gravity is 900Kg, and drying temperature is set to 200 DEG C；
D, hot rolling is carried out to dried page, hot-rolled temperature is set to 300 DEG C, to the page after hot rolling in 100kgf/cm2 Pressure under spray aqueous buffing oil and carry out press polish, be cooled to the superficial film that light is formed after room temperature, obtain product.
Embodiment two：
A kind of refractory fiber paper and preparation method thereof, raw material components are as follows according to weight score：40 parts of ceramic fibre, plant 10 parts of fiber, 8 parts of silica, 8 parts of composite magnesium silicate, 6 parts of talcum powder, 5 parts of deionized water, 6 parts of polyethylene glycol, carboxymethyl are fine 3 parts of dimension element, 12 parts of aqueous buffing oil.
Its preparation method is as follows：
A, ceramic fibre, plant fiber and carboxymethyl cellulose are mixed, adds deionized water and be beaten, used 2mm crosses sieve and sieves, and removes the laggard row of impurity and disperses, and dispersion temperature is set to 45 DEG C, disperses once per 10min, altogether three times, Water slurry is made；
B, at room temperature, silica, composite magnesium silicate, talcum powder and polyethylene glycol are mixed, in stirred Deionized water is slowly added in four times, until jelly, stir speed (S.S.) 500r/min；
C, the mixture in step B is added in water slurry, stirred evenly, operated using centrifuge, frequency is 3500HZ, using supernatant liquor is taken after 2mm filter screen filtrations, is manufactured paper with pulp using clear liquid, obtains l Water Paper page, and l Water Paper page is carried out Squeezing and drying, squeezing gravity is 1000Kg, and drying temperature is set to 150 DEG C；
D, hot rolling is carried out to dried page, hot-rolled temperature is set to 250 DEG C, to the page after hot rolling in 200kgf/cm2 Pressure under spray aqueous buffing oil and carry out press polish, be cooled to the superficial film that light is formed after room temperature, obtain product.
Embodiment three：
A kind of refractory fiber paper and preparation method thereof, raw material components are as follows according to weight score：50 parts of ceramic fibre, plant 20 parts of fiber, 5 parts of silica 1,13 parts of composite magnesium silicate, 10 parts of talcum powder, 8 parts of deionized water, 7 parts of polyethylene glycol, carboxylic first 5 parts of base cellulose, 15 parts of aqueous buffing oil.
Its preparation method is as follows：
A, ceramic fibre, plant fiber and carboxymethyl cellulose are mixed, adds deionized water and be beaten, used 2mm crosses sieve and sieves, and removes the laggard row of impurity and disperses, and dispersion temperature is set to 42 DEG C, disperses once per 15min, altogether three times, Water slurry is made；
B, at room temperature, silica, composite magnesium silicate, talcum powder and polyethylene glycol are mixed, in stirred Deionized water is slowly added in four times, until jelly, stir speed (S.S.) 450r/min；
C, the mixture in step B is added in water slurry, stirred evenly, operated using centrifuge, frequency is 3400HZ, using supernatant liquor is taken after 2mm filter screen filtrations, is manufactured paper with pulp using clear liquid, obtains l Water Paper page, and l Water Paper page is carried out Squeezing and drying, squeezing gravity is 850Kg, and drying temperature is set to 170 DEG C；
D, hot rolling is carried out to dried page, hot-rolled temperature is set to 260 DEG C, to the page after hot rolling in 190kgf/cm2 Pressure under spray aqueous buffing oil and carry out press polish, be cooled to the superficial film that light is formed after room temperature, obtain product.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of changes, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (2)

  1. A kind of 1. refractory fiber paper and preparation method thereof, it is characterised in that：Raw material components are as follows according to weight score：Ceramic fibre 30-50 parts, 10-20 parts of plant fiber, 8-15 parts of silica, 8-13 parts of composite magnesium silicate, 5-10 parts of talcum powder, deionized water 5-8 parts, 5-10 parts of polyethylene glycol, 3-8 parts of carboxymethyl cellulose, 10-20 parts of aqueous buffing oil.
  2. A kind of 2. refractory fiber paper according to claim 1 and preparation method thereof, it is characterised in that：Its preparation method is such as Under：
    A, ceramic fibre, plant fiber and carboxymethyl cellulose are mixed, adds deionized water and be beaten, using 2- 3mm crosses sieve and sieves, and removes the laggard row of impurity and disperses, and dispersion temperature is set to 40-45 DEG C, disperses once per 10-15min, Altogether three times, water slurry is made；
    B, at room temperature, silica, composite magnesium silicate, talcum powder and polyethylene glycol are mixed, divide four in stirred It is secondary to be slowly added to deionized water, until jelly, stir speed (S.S.) 400-500r/min；
    C, the mixture in step B is added in water slurry, stirred evenly, operated using centrifuge, frequency 3000- 3500HZ, using supernatant liquor is taken after 1-2mm filter screen filtrations, is manufactured paper with pulp using clear liquid, obtains l Water Paper page, to l Water Paper page into Row squeezing and drying, squeezing gravity is 800-1000Kg, and drying temperature is set to 150-200 DEG C；
    D, hot rolling is carried out to dried page, hot-rolled temperature is set to 250-300 DEG C, to the page after hot rolling in 100- Aqueous buffing oil is sprayed under the pressure of 200kgf/cm2 and carries out press polish, bright superficial film is formed after being cooled to room temperature, obtains Product.
CN201711084331.8A 2017-11-03 2017-11-03 A kind of refractory fiber paper and preparation method thereof Pending CN107938423A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711084331.8A CN107938423A (en) 2017-11-03 2017-11-03 A kind of refractory fiber paper and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201711084331.8A CN107938423A (en) 2017-11-03 2017-11-03 A kind of refractory fiber paper and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107938423A true CN107938423A (en) 2018-04-20

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112679829A (en) * 2020-12-25 2021-04-20 山东理工大学 Aluminum silicate fiber waste reinforced biomass composite material and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112679829A (en) * 2020-12-25 2021-04-20 山东理工大学 Aluminum silicate fiber waste reinforced biomass composite material and preparation method thereof

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Application publication date: 20180420