CN107915784A - A kind of intelligence dried starch homogeneously takes off branch polymerization - Google Patents

A kind of intelligence dried starch homogeneously takes off branch polymerization Download PDF

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Publication number
CN107915784A
CN107915784A CN201711365245.4A CN201711365245A CN107915784A CN 107915784 A CN107915784 A CN 107915784A CN 201711365245 A CN201711365245 A CN 201711365245A CN 107915784 A CN107915784 A CN 107915784A
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CN
China
Prior art keywords
starch
branch
polymerization
homogeneously
intelligent
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CN201711365245.4A
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Chinese (zh)
Inventor
黄继红
吕行
侯银臣
卞科
林江涛
廖爱美
赵祎
纪小国
张亚奇
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Henan University of Technology
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Henan University of Technology
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Priority to CN201711365245.4A priority Critical patent/CN107915784A/en
Publication of CN107915784A publication Critical patent/CN107915784A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B31/00Preparation of derivatives of starch
    • C08B31/02Esters
    • C08B31/04Esters of organic acids, e.g. alkenyl-succinated starch
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin

Abstract

The present invention provides a kind of intelligent dried starch homogeneously to take off branch polymerization.Using starch as raw material, homemade intelligent dry method starch is added based on deal homogeneously to take off in branch polymerization machine, vacuumize and heat in closed rotation process, the spray non-volatile organic acids of uniform atomizing at the same time, temperature is adjusted according to X-ray and differential scanning result, after starch debranching and polymerization effect reach ideal indicator, automatic slowly cools down 80 DEG C.Realize the intelligent combination of the processes such as the chain rupture of starch, de- branch, polymerization, monitoring.Compared with chemical modification under the conditions of conventional liquid, technological process is simplified, eliminates substantial amounts of chemical reagent, while any waste water will not be produced, is had laid a good foundation for the preparation of resistant starch.

Description

A kind of intelligence dried starch homogeneously takes off branch polymerization
Technical field
The invention belongs to food machinery biological technical field, and in particular to a kind of intelligence dried starch homogeneously takes off Zhi Juhe side Method.
Background technology
Starch is a kind of polycrystalline high polymer, and a part of molecules align is into loose amorphous area, another part point in its particle Crystal region that is sub then being arranged in high-sequential, crystalline texture are mainly connected by starch molecule by hydrogen bond, and crystal region accounts for The 25%~50% of grain.This design feature of starch molecule, limits the use scope of starch, such as starch crystals area molecules align Closely, water and chemical reagent etc. are not easy to touch the molecule in crystal region, cause the gelatinization point height of starch, chemical reactivity low The big and numerous hydroxyl of relative molecular weight Deng starch causes viscosity each other with hydrogen bond association into close network structure Excessive, poor fluidity.Therefore, how research changes starch granules structure, crystal region supramolecular structure and reduces starch crystals The method in area is to improve the physicochemical properties of starch, the reactivity of raising starch becomes an extremely important research class Topic.
Resistant starch is also known as resistant starch, impedance starch and indigestibility starch etc., refers in the small intestine of Healthy People The starch of absorption and its general name of decomposition product cannot be digested.From physiologically saying, RS has the physiological function similar to dietary fiber, It if do not degraded by human small intestine's enzyme, can be utilized, and have the advantages that in contrast more by large intestine microorganism:(1)Resistance is formed sediment Powder can resist the decomposition of enzyme, and release glucose is slow in vivo, has relatively low insulin response, can control blood glucose balance, Reduce hunger, particularly suitable patients with diabetes mellitus;(2)Resistant starch has the function of soluble edible fibre, can after food Increase Fecal wastes, reduce constipation, reduce the danger of colon cancer;(3)Resistant starch can reduce the amount of cholesterolemia and triglyceride, Because of the amount of cholesterol and triglyceride increase in excreta after edible resistant starch, thus there is certain antiobesity action.Eating In product processing, the functional character of resistant starch uniqueness can be utilized, produces high-quality food.Resistant starch is suitable for based on cereal The food formula of raw material is wanted, can be used to improve food processing technology, increases the brittleness of food, dilatancy and improves final products Quality.In addition, its color is white, it is added to the appearance that food is not interfered with food and will not be influenced as dietary fiber The mouthfeel of food.Resistant starch is easily ground into tiny particle, and feeling of grittiness will not be produced by being added in food, beverage.Foreign countries are Apply it in the flour products such as bread, steamed stuffed bun, snack, macaroni, biscuit.Wherein most strikingly RS is in bread Application, RS can be added in bread instead of dietary fiber, solve dietary fiber influence bread rise, poor taste the shortcomings of. Some researches show that after adding RS, the puffed degree increase of food, density declines, and brittleness is improved.By the puffing food added with RS Product are dipped into the beverages such as milk in use, though its quality softens but not collapsed because of water suction, and can maintain the long period Brittleness.Current development trend is seen, world population, still in reduced levels, does not reach much also in the consumption of dietary fiber Needed by human body requirement.It is daily 20-35g in the consumption per head that American diet fiber association is recommended, but is actually only 12- 17g, almost differs half.Even in the preferable New Zealand of situation, its consumption figure is also not reaching to the upper limit of standard requirement.Hair Up to country even in this way, the consumption per head of developing country is even more much insufficient.It can be seen from the above that resistant starch is a kind of great Physiological function potentiality, the component that can be used for manufacture high-quality food with good food processing feature, have extensive market Prospect and development potentiality.The present invention homogeneously takes off branch polymerization machine using homemade intelligent dry method starch and carries out mechanical activation to starch, Compared with chemical modification under the conditions of conventional liquid, technological process is simplified, eliminates substantial amounts of chemical reagent, while will not produce Any waste water, haves laid a good foundation for the preparation of resistant starch.
The content of the invention
It is an object of the invention to provide a kind of intelligent dried starch homogeneously to take off branch polymerization, with changing under the conditions of conventional liquid Learn modification to compare, simplify technological process, eliminate substantial amounts of chemical reagent, while any waste water will not be produced, form sediment for resistance The preparation of powder is had laid a good foundation.
A kind of mechanochemistry method that wheaten starch is modified, it is characterised in that comprise the following steps:
Step 1, by weight, 8~10 parts of Raw Wheat Starch add homemade intelligent dry method starch homogeneously de- branch polymerization machine In;
Step 2, intelligent dry method starch homogeneously takes off branch polymerization machine and is vacuumized during rotation, and uniform atomizing spray is non-waves Hair property organic acid;
Step 3, intelligent adjustment temperature and organic acid additive amount.Using in X-ray and differential scanning monitoring device starch it is de- Branch and extent of polymerization, and corresponding temperature and acid adding amount is automatically generated according to data above so that temperature and acid adding amount are realized and moved State changes, and lays the foundation for the preparation of resistant starch.
Further, it is that first homogeneously takes off branch both at home and abroad that homemade intelligence dry method starch, which homogeneously takes off branch polymerization machine, in step 1 The technique such as polymerization machine, equipment collects atomization spray acid, homogeneous, high temperature takes off, a polymerization is in quaternity, according to X-ray and differential scanning The dynamic change for realizing temperature and acid adding amount, simplify technological process.
Embodiment
A kind of mechanochemistry method that wheaten starch is modified, it is characterised in that:Comprise the following steps:
Step 1, by weight, 8~10 parts of Raw Wheat Starch add homemade intelligent dry method starch homogeneously de- branch polymerization machine In;
Step 2, intelligent dry method starch homogeneously takes off branch polymerization machine and is vacuumized during rotation, and uniform atomizing spray is non-waves Hair property organic acid;
Step 3, intelligent adjustment temperature and organic acid additive amount.Using in X-ray and differential scanning monitoring device starch it is de- Branch and extent of polymerization, and corresponding temperature and acid adding amount is automatically generated according to data above so that temperature and acid adding amount are realized and moved State changes, and lays the foundation for the preparation of resistant starch.

Claims (2)

1. a kind of intelligence dried starch homogeneously takes off branch polymerization, it is characterised in that:Comprise the following steps:
Step 1, by weight, 8~10 parts of Raw Wheat Starch add homemade intelligent dry method starch homogeneously de- branch polymerization machine In;
Step 2, intelligent dry method starch homogeneously takes off branch polymerization machine and is vacuumized during rotation, and uniform atomizing spray is non-waves Hair property organic acid;
Step 3, intelligent adjustment temperature and organic acid additive amount;
Using the de- branch and extent of polymerization of starch in X-ray and differential scanning monitoring device, and automatically generated according to data above Corresponding temperature and acid adding amount so that temperature and acid adding amount realize dynamic change, lay the foundation for the preparation of resistant starch.
2. a kind of intelligent dried starch according to claim 1 homogeneously takes off branch polymerization, it is characterised in that in step 1 certainly It is first homogeneous de- branch polymerization machine both at home and abroad that the intelligent dry method starch of system, which homogeneously takes off branch polymerization machine, equipment collection atomization spray acid, it is homogeneous, The techniques such as high temperature takes off, a polymerization realize temperature and acid adding amount in quaternity according to the real time monitoring of X-ray and differential scanning Dynamic change, simplify technological process.
CN201711365245.4A 2017-12-18 2017-12-18 A kind of intelligence dried starch homogeneously takes off branch polymerization Pending CN107915784A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711365245.4A CN107915784A (en) 2017-12-18 2017-12-18 A kind of intelligence dried starch homogeneously takes off branch polymerization

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711365245.4A CN107915784A (en) 2017-12-18 2017-12-18 A kind of intelligence dried starch homogeneously takes off branch polymerization

Publications (1)

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CN107915784A true CN107915784A (en) 2018-04-17

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CN (1) CN107915784A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1094732A (en) * 1994-04-08 1994-11-09 廖俊云 Drying process for producing acid modified starch
CN102453100A (en) * 2010-11-04 2012-05-16 廖俊云 Pure dry preparation method of acid treated starch

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1094732A (en) * 1994-04-08 1994-11-09 廖俊云 Drying process for producing acid modified starch
CN102453100A (en) * 2010-11-04 2012-05-16 廖俊云 Pure dry preparation method of acid treated starch

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Application publication date: 20180417