CN107913656A - A kind of solid-liquid reaction kettle easy to interruption reaction - Google Patents
A kind of solid-liquid reaction kettle easy to interruption reaction Download PDFInfo
- Publication number
- CN107913656A CN107913656A CN201711163116.7A CN201711163116A CN107913656A CN 107913656 A CN107913656 A CN 107913656A CN 201711163116 A CN201711163116 A CN 201711163116A CN 107913656 A CN107913656 A CN 107913656A
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- fixedly connected
- autoclave body
- solid
- motor
- inner cylinder
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses a kind of easy to interrupt the solid-liquid reaction kettle of reaction, autoclave body, pillar, feeding-in solid body mouth, drain pipe and inlet tube are included；The upper surface of the autoclave body is fixedly connected with the first motor, the axle stretch end of first motor is fixedly connected with screw, autoclave body is internally provided with inner cylinder, guide rod has been respectively fixedly connected with left and right sides of inner cylinder, the inner wall of autoclave body is fixedly connected with guide rail, the lower surface of autoclave body is fixedly connected with the second motor, the axle stretch end of second motor is fixedly connected with transmission shaft, drive bevel gear is fixedly connected with the top of transmission shaft, drive bevel gear is respectively arranged on the left side and the right side left rotary shaft, right spindle, reaction solution is stirred using paddle, it is uniformly mixed reaction solution, make reaction solution mixing more uniform using agitating plate agitation reaction solution at the same time, further improve reaction efficiency, the present invention can interrupt reaction at any time as needed, it is convenient and efficient, substantially increase security.
Description
Technical field
The present invention relates to a kind of field of chemical equipment, is specifically a kind of solid-liquid reaction kettle easy to interruption reaction.
Background technology
The broad understanding of reaction kettle has the rustless steel container physically or chemically reacted, according to different process conditions demands
The structure design and parameter configuration of container are carried out, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards,
To realize the heating of technological requirement, evaporation, cooling and the mixture response function of low high speed, reaction kettle is widely used in oil, changes
Work, rubber, pesticide, dyestuff, medicine, food, for completing to vulcanize, nitrifying, hydrogenating, hydrocarbonylation, polymerization, the technical process such as condensation
Pressure vessel, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.；Material generally has carbon manganese steel, stainless steel, zirconium, Ni-based conjunction
Golden and other composite materials, existing frequently-used solid-liquid reaction kettle tends not to react interruption at any time as needed, if reacting
Something unexpected happened in journey, it is impossible to interrupt reaction in time, easily cause danger.
The content of the invention
It is an object of the invention to provide a kind of easy to interrupt the solid-liquid reaction kettle of reaction, to solve in above-mentioned background technology
The problem of proposition.
To achieve the above object, the present invention provides following technical solution：
A kind of solid-liquid reaction kettle easy to interruption reaction, including autoclave body, pillar, feeding-in solid body mouth, drain pipe and inlet tube；It is described
The upper surface of autoclave body is fixedly connected with the first motor, and the axle stretch end of the first motor is fixedly connected with screw, and screw passes through autoclave body
Top is stretched into autoclave body, and autoclave body is internally provided with inner cylinder, and screw runs through inner cylinder, and is connected with the bottom thread of inner cylinder, inner cylinder position
In the lower section of feeding-in solid body mouth, guide rod is respectively fixedly connected with left and right sides of inner cylinder, the inner wall of autoclave body, which is fixedly connected with, leads
Rail, in the other end insertion guide rail of guide rod, the side wall of inner cylinder is distributed with some through holes, and the lower surface of autoclave body is fixedly connected with the
Two motors, the axle stretch end of the second motor are fixedly connected with transmission shaft, and the bottom of transmission shaft through autoclave body is stretched into autoclave body, transmission shaft
Top be fixedly connected with drive bevel gear, drive bevel gear is respectively arranged on the left side and the right side left rotary shaft, right spindle, left rotary shaft,
One end of right spindle has been respectively fixedly connected with left angular wheel, right bevel gear, left angular wheel, right bevel gear respectively with drive bevel gear
Engagement, the inner wall of left rotary shaft, the other end of right spindle and autoclave body are rotatablely connected, have been respectively fixedly connected with left rotary shaft, right spindle
Some agitating plates, the right side wall of autoclave body are fixedly connected with drain pipe, and valve is provided with drain pipe, and the left side wall of autoclave body, which is fixed, to be connected
Inlet tube is connected to, valve is installed on inlet tube.
As the further scheme of the present invention：The lower surface of the autoclave body is fixedly connected with pillar, and the lower end of pillar is arranged
There is sleeve, sleeve is internally provided with spring, and the upper and lower ends of spring are fixedly connected with pillar, sleeve respectively.
As further scheme of the invention：The upper surface of the autoclave body is fixedly connected with feeding-in solid body mouth, solid into
Material mouth is connected with autoclave body.
As further scheme of the invention：First motor is clockwise and anticlockwise motor.
As further scheme of the invention：Paddle is fixedly connected with the transmission shaft.
Compared with prior art, the beneficial effects of the invention are as follows：Solid reactant is poured into feeding-in solid body mouth, was being reacted
Cheng Zhong, stirs reaction solution using paddle, is uniformly mixed reaction solution, while mixes reaction solution using agitating plate agitation reaction solution
Conjunction is more uniform, further improves reaction efficiency, and when needing to interrupt reaction, control inner cylinder moves up, and makes solid reactant
Being separated with liquid reactants, achieve the purpose that to interrupt reaction, the present invention can interrupt reaction at any time as needed, convenient and efficient,
Security is substantially increased, cushioning effect can be played using spring, reduces vibration caused by present invention operation.
Brief description of the drawings
The structure diagram for the solid-liquid reaction kettle that Fig. 1 reacts for ease of interruption；
The top view of inner cylinder in the solid-liquid reaction kettle that Fig. 2 reacts for ease of interruption.
In figure：1- autoclave bodies；2- pillars；3- sleeves；4- springs；5- feeding-in solid body mouths；The first motors of 6-；7- screws；In 8-
Cylinder；9- guide rods；10- guide rails；11- through holes；The second motors of 12-；13- transmission shafts；14- paddles；15- drive bevel gears；16-
Left angular wheel；The right bevel gears of 17-；18- left rotary shafts；19- right spindles；20- agitating plates；21- drain pipes；22- inlet tubes.
Embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete
Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art are obtained every other without making creative work
Embodiment, belongs to the scope of protection of the invention.
Please refer to Fig.1,2, it is a kind of easy to interrupting the solid-liquid reaction kettle of reaction, including autoclave body 1, branch in the embodiment of the present invention
Column 2, feeding-in solid body mouth 5, drain pipe 21 and inlet tube 22, the lower surface of the autoclave body 1 are fixedly connected with pillar 2, under pillar 2
End cap is equipped with sleeve 3, and pillar 2 can slide up and down in sleeve 3, and sleeve 3 is internally provided with spring 4, the upper and lower ends of spring 4
It is fixedly connected respectively with pillar 2, sleeve 3, certain cushioning effect can be played using spring 4, the upper surface of autoclave body 1, which is fixed, is connected
Feeding-in solid body mouth 5, the first motor 6 are connected to, the first motor 6 is clockwise and anticlockwise motor, and feeding-in solid body mouth 5 is connected with autoclave body 1, the first electricity
The axle stretch end of machine 6 is fixedly connected with screw 7, and the top of screw 7 through autoclave body 1 is stretched into autoclave body 1, and being internally provided with for autoclave body 1 is interior
Cylinder 8, screw 7 runs through inner cylinder 8, and is connected with the bottom thread of inner cylinder 8, and inner cylinder 8 is located at the lower section of feeding-in solid body mouth 5, by solid
Reactant input feeding-in solid body mouth 5, falls into inner cylinder 8, the left and right sides of inner cylinder 8 has been respectively fixedly connected with guide rod 9, autoclave body 1
Inner wall be fixedly connected with guide rail 10, in the other end insertion guide rail 10 of guide rod 9, guide rod 9 can be along guide rail about 10
Slide, by controlling 6 rotating of the first motor, so as to drive 7 rotating of screw, and then drive inner cylinder 8 to move up and down, inner cylinder 8
Side wall some through holes 11 are distributed with, the lower surface of autoclave body 1 is fixedly connected with the second motor 12, and the axle stretch end of the second motor 12 is consolidated
Surely transmission shaft 13 is connected with, the bottom of transmission shaft 13 through autoclave body 1 is stretched into autoclave body 1, and stirring is fixedly connected with transmission shaft 13
Leaf 14, the top of transmission shaft 13 are fixedly connected with drive bevel gear 15, and drive bevel gear 15 is respectively arranged on the left side and the right side left-hand rotation
Axis 18, right spindle 19, left rotary shaft 18, one end of right spindle 19 have been respectively fixedly connected with left angular wheel 16, right bevel gear 17, left cone
Gear 16, right bevel gear 17 engage with drive bevel gear 15 respectively, left rotary shaft 18, right spindle 19 the other end and autoclave body 1 it is interior
Wall is rotatablely connected, and some agitating plates 20 have been respectively fixedly connected with left rotary shaft 18, right spindle 19, and the second motor 12 drives when running
Transmission shaft 13 rotates, and then drives paddle 14 to rotate, and stirs reaction solution, is uniformly mixed reaction solution, when transmission shaft 13 rotates
Drive drive bevel gear 15 to rotate, and then drive left rotary shaft 18, right spindle 19 to rotate by left angular wheel 16, right bevel gear 17,
And left rotary shaft 18, right spindle 19 are turned on the contrary, finally driving agitating plate 20 to rotate, stirring reaction solution using agitating plate 20 makes reaction
Liquid mixing is more uniform, improves reaction efficiency, and the right side wall of autoclave body 1 is fixedly connected with drain pipe 21, is provided with drain pipe 21
Valve, the left side wall of autoclave body 1 are fixedly connected with inlet tube 22, valve are provided with inlet tube 22.
The present invention operation principle be：Solid reactant is poured into feeding-in solid body mouth 5, solid reactant is fallen into inner cylinder 8,
The valve on inlet tube 22 to be opened, liquid reactants are injected in autoclave body 1, the first motor 6 of control is run, and drives screw 7 to rotate,
So as to drive inner cylinder 8 to move down, liquid reactants is entered by guide rod 9 in inner cylinder 8, occur with solid reactant anti-
Should, start the second motor 12, drive transmission shaft 13 to rotate when the second motor 12 is run, and then drive paddle 14 to rotate, stir
Reaction solution, is uniformly mixed reaction solution, drives drive bevel gear 15 to rotate when transmission shaft 13 rotates, and then pass through left angular wheel
16th, right bevel gear 17 drives left rotary shaft 18, right spindle 19 to rotate, and left rotary shaft 18, right spindle 19 turn on the contrary, final drive is stirred
Mix plate 20 to rotate, stirring reaction solution using agitating plate 20 makes reaction solution mixing more uniform, reaction efficiency is improved, when needing to interrupt
During reaction, the first motor 6 of control inverts, and drives screw 7 to rotate backward, so as to drive inner cylinder 8 to move up, makes solid reactant
Separated with liquid reactants, achieve the purpose that to interrupt reaction, the present invention can produce vibration in the process of running, and pillar 2 can be
Slided up and down in sleeve 3, can play cushioning effect using spring 4, reduce vibration.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.Any reference numeral in claim should not be considered as to the involved claim of limitation.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical solution, this narrating mode of specification is only that those skilled in the art should for clarity
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (4)
1. a kind of solid-liquid reaction kettle easy to interruption reaction, including autoclave body（1）, pillar（2）, feeding-in solid body mouth（5）, drain pipe
（21）And inlet tube（22）；It is characterized in that, the autoclave body（1）Upper surface be fixedly connected with the first motor（6）, the first motor
（6）Axle stretch end be fixedly connected with screw（7）, screw（7）Through autoclave body（1）Top stretch into autoclave body（1）It is interior, autoclave body（1）'s
It is internally provided with inner cylinder（8）, screw（7）Through inner cylinder（8）, and and inner cylinder（8）Bottom thread connection, inner cylinder（8）Positioned at solid
Feed inlet（5）Lower section, inner cylinder（8）The left and right sides be respectively fixedly connected with guide rod（9）, autoclave body（1）Inner wall fix connect
It is connected to guide rail（10）, guide rod（9）The other end insertion guide rail（10）It is interior, inner cylinder（8）Side wall some through holes are distributed with（11）,
Autoclave body（1）Lower surface be fixedly connected with the second motor（12）, the second motor（12）Axle stretch end be fixedly connected with transmission shaft
（13）, transmission shaft（13）Through autoclave body（1）Bottom stretch into autoclave body（1）It is interior, transmission shaft（13）Top be fixedly connected with actively
Bevel gear（15）, drive bevel gear（15）Be respectively arranged on the left side and the right side left rotary shaft（18）, right spindle（19）, left rotary shaft（18）、
Right spindle（19）One end be respectively fixedly connected with left angular wheel（16）, right bevel gear（17）, left angular wheel（16）, right bevel gear
（17）Respectively with drive bevel gear（15）Engagement, left rotary shaft（18）, right spindle（19）The other end and autoclave body（1）Inner wall rotate
Connection, left rotary shaft（18）, right spindle（19）On be respectively fixedly connected with some agitating plates（20）, autoclave body（1）Right side wall fix
It is connected with drain pipe（21）, drain pipe（21）On valve, autoclave body are installed（1）Left side wall be fixedly connected with inlet tube（22）,
Inlet tube（22）On valve, the autoclave body are installed（1）Lower surface be fixedly connected with pillar（2）, pillar（2）Lower end be arranged
There is sleeve（3）, sleeve（3）Be internally provided with spring（4）, spring（4）Upper and lower ends respectively with pillar（2）, sleeve（3）It is fixed
Connection.
2. the solid-liquid reaction kettle according to claim 1 easy to interruption reaction, it is characterised in that the autoclave body（1）It is upper
Surface is fixedly connected with feeding-in solid body mouth（5）, feeding-in solid body mouth（5）With autoclave body（1）Connection.
3. the solid-liquid reaction kettle according to claim 1 easy to interruption reaction, it is characterised in that first motor（6）
For clockwise and anticlockwise motor.
4. the solid-liquid reaction kettle according to claim 1 easy to interruption reaction, it is characterised in that the transmission shaft（13）On
It is fixedly connected with paddle（14）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711163116.7A CN107913656B (en) | 2017-11-21 | 2017-11-21 | A kind of solid-liquid reaction kettle convenient for interrupting reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711163116.7A CN107913656B (en) | 2017-11-21 | 2017-11-21 | A kind of solid-liquid reaction kettle convenient for interrupting reaction |
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| Publication Number | Publication Date |
|---|---|
| CN107913656A true CN107913656A (en) | 2018-04-17 |
| CN107913656B CN107913656B (en) | 2019-11-26 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201711163116.7A Active CN107913656B (en) | 2017-11-21 | 2017-11-21 | A kind of solid-liquid reaction kettle convenient for interrupting reaction |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108636335A (en) * | 2018-05-14 | 2018-10-12 | 苏昭缄 | A kind of oscillatory type solid-liquid reaction kettle with crushing function |
| CN108652782A (en) * | 2018-05-25 | 2018-10-16 | 李辉云 | A kind of animal and veterinary Baoding diagnosing and treating apparatus |
| CN108722331A (en) * | 2018-05-30 | 2018-11-02 | 天津朝花夕拾科技有限公司 | A kind of Cosmetic Manufacture reaction kettle |
| CN112808219A (en) * | 2021-02-07 | 2021-05-18 | 山东隆信药业有限公司 | Continuous asphalt production reaction kettle |
| CN113680094A (en) * | 2021-10-27 | 2021-11-23 | 东营明德化工有限公司 | Crystallization kettle with automatic screening function |
| CN114405431A (en) * | 2022-01-22 | 2022-04-29 | 陈健 | Multi-connected chemical synthesis reactor |
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| CN205833160U (en) * | 2016-07-06 | 2016-12-28 | 唐山学院 | A kind of solid-liquid separation multistage screening reactor |
| CN206276383U (en) * | 2016-12-06 | 2017-06-27 | 熊向辉 | The chemical industry stirred type retort that a kind of solid-liquid raw material separately mixes |
| CN206492508U (en) * | 2017-02-16 | 2017-09-15 | 东莞市兰宝化工新材料有限公司 | A kind of automatical and efficient reactor |
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| CN202700527U (en) * | 2012-08-01 | 2013-01-30 | 陈建发 | Quantitative reaction test tube |
| CN205833160U (en) * | 2016-07-06 | 2016-12-28 | 唐山学院 | A kind of solid-liquid separation multistage screening reactor |
| CN206276383U (en) * | 2016-12-06 | 2017-06-27 | 熊向辉 | The chemical industry stirred type retort that a kind of solid-liquid raw material separately mixes |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108636335A (en) * | 2018-05-14 | 2018-10-12 | 苏昭缄 | A kind of oscillatory type solid-liquid reaction kettle with crushing function |
| CN108652782A (en) * | 2018-05-25 | 2018-10-16 | 李辉云 | A kind of animal and veterinary Baoding diagnosing and treating apparatus |
| CN108722331A (en) * | 2018-05-30 | 2018-11-02 | 天津朝花夕拾科技有限公司 | A kind of Cosmetic Manufacture reaction kettle |
| CN112808219A (en) * | 2021-02-07 | 2021-05-18 | 山东隆信药业有限公司 | Continuous asphalt production reaction kettle |
| CN113680094A (en) * | 2021-10-27 | 2021-11-23 | 东营明德化工有限公司 | Crystallization kettle with automatic screening function |
| CN113680094B (en) * | 2021-10-27 | 2021-12-31 | 东营明德化工有限公司 | Crystallization kettle with automatic screening function |
| CN114405431A (en) * | 2022-01-22 | 2022-04-29 | 陈健 | Multi-connected chemical synthesis reactor |
| CN114405431B (en) * | 2022-01-22 | 2024-04-09 | 山西同杰化学试剂有限公司 | Multi-connected chemical synthesis reactor |
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Effective date of registration: 20191031 Address after: Beverly Industrial Park, 341700 Jiangxi city in Ganzhou Province, Longnan County Applicant after: Longnan Xin Kun inorganic New Material Co., Ltd. Address before: Ruida road 450000 high tech Industrial Development Zone, Henan city of Zhengzhou province No. 96 Business Center No. 1 building C260 room Applicant before: Zhengzhou integrity Information Technology Co., Ltd. |
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