CN107913656B - A kind of solid-liquid reaction kettle convenient for interrupting reaction - Google Patents

A kind of solid-liquid reaction kettle convenient for interrupting reaction Download PDF

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Publication number
CN107913656B
CN107913656B CN201711163116.7A CN201711163116A CN107913656B CN 107913656 B CN107913656 B CN 107913656B CN 201711163116 A CN201711163116 A CN 201711163116A CN 107913656 B CN107913656 B CN 107913656B
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fixedly connected
autoclave body
solid
motor
inner cylinder
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CN107913656A (en
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张强
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Longnan Xin Kun inorganic New Material Co., Ltd.
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Longnan Xin Kun Inorganic New Material Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention discloses a kind of solid-liquid reaction kettles convenient for interrupting reaction, include autoclave body, pillar, feeding-in solid body mouth, drain pipe and inlet tube;The upper surface of the autoclave body is fixedly connected with first motor, the axle stretch end of first motor is fixedly connected with screw rod, the inside of autoclave body is equipped with inner cylinder, guide rod has been respectively fixedly connected at left and right sides of inner cylinder, the inner wall of autoclave body is fixedly connected with guide rail, the lower surface of autoclave body is fixedly connected with the second motor, the axle stretch end of second motor is fixedly connected with transmission shaft, drive bevel gear is fixedly connected at the top of transmission shaft, drive bevel gear is respectively arranged on the left side and the right side left rotary shaft, right spindle, reaction solution is stirred using paddle, it is uniformly mixed reaction solution, mix reaction solution using agitating plate agitation reaction solution simultaneously more uniform, further increase reaction efficiency, the present invention can according to need interrupts reaction at any time, it is convenient and efficient, substantially increase safety.

Description

A kind of solid-liquid reaction kettle convenient for interrupting reaction
Technical field
The present invention relates to a kind of field of chemical equipment, specifically a kind of solid-liquid reaction kettle convenient for interrupting reaction.
Background technique
The broad understanding of reaction kettle has the rustless steel container physically or chemically reacted, according to different process conditions demands The structure design and parameter configuration of container are carried out, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards, To realize the mixture response function of heating, evaporation that technique requires, cooling and low high speed, reaction kettle is widely used in petroleum, changes Work, rubber, pesticide, dyestuff, medicine, food, for completing the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation Pressure vessel, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.;Material generally has carbon manganese steel, stainless steel, zirconium, Ni-based conjunction Golden and other composite materials, existing frequently-used solid-liquid reaction kettle tends not to make to interrupt as needed at any time to react, if reacting Something unexpected happened in journey cannot interrupt reaction in time, be easy to happen danger.
Summary of the invention
The purpose of the present invention is to provide a kind of solid-liquid reaction kettles convenient for interrupting reaction, to solve in above-mentioned background technique The problem of proposition.
To achieve the above object, the invention provides the following technical scheme:
A kind of solid-liquid reaction kettle convenient for interrupting reaction, including autoclave body, pillar, feeding-in solid body mouth, drain pipe and inlet tube; The upper surface of the autoclave body is fixedly connected with first motor, and the axle stretch end of first motor is fixedly connected with screw rod, and screw rod passes through kettle It is protruded into autoclave body at the top of body, the inside of autoclave body is equipped with inner cylinder, and screw rod runs through inner cylinder, and connect with the bottom thread of inner cylinder, interior Cylinder is located at the lower section of feeding-in solid body mouth, has been respectively fixedly connected with guide rod at left and right sides of inner cylinder, the inner wall of autoclave body is fixedly connected There is guide rail, the other end of guide rod is embedded in guide rail, and several through-holes are distributed in the side wall of inner cylinder, and the lower surface of autoclave body is fixedly connected There is the second motor, the axle stretch end of the second motor is fixedly connected with transmission shaft, and the bottom that transmission shaft passes through autoclave body is protruded into autoclave body, passes Drive bevel gear is fixedly connected at the top of moving axis, drive bevel gear is respectively arranged on the left side and the right side left rotary shaft, right spindle, turns left Axis, right spindle one end be respectively fixedly connected with left angular wheel, right bevel gear, left angular wheel, right bevel gear respectively with initiative taper The inner wall of gear engagement, left rotary shaft, the other end of right spindle and autoclave body is rotatablely connected, fixed respectively in left rotary shaft, right spindle to connect Several agitating plates are connected to, the right side wall of autoclave body is fixedly connected with drain pipe, and valve is equipped on drain pipe, and the left side wall of autoclave body is solid Surely it is connected with inlet tube, valve is installed on inlet tube.
As a further solution of the present invention: the lower surface of the autoclave body is fixedly connected with pillar, and the lower end of pillar is arranged There is sleeve, the inside of sleeve is equipped with spring, and the upper and lower ends of spring are fixedly connected with pillar, sleeve respectively.
As the present invention further scheme: the upper surface of the autoclave body is fixedly connected with feeding-in solid body mouth, solid into Material mouth is connected to autoclave body.
As further scheme of the invention: the first motor is clockwise and anticlockwise motor.
As further scheme of the invention: being fixedly connected with paddle on the transmission shaft.
Compared with prior art, it the beneficial effects of the present invention are: solid reactant is poured into feeding-in solid body mouth, was reacting Cheng Zhong stirs reaction solution using paddle, is uniformly mixed reaction solution, while keeping reaction solution mixed using agitating plate agitation reaction solution It closes more uniform, further increases reaction efficiency, when needing to interrupt reaction, control inner cylinder is moved up, and makes solid reactant It being separated with liquid reactants, achievees the purpose that interrupt reaction, the present invention can according to need and interrupt reaction at any time, and it is convenient and efficient, Safety is substantially increased, buffer function can be played using spring, reduces the vibration generated when present invention operation.
Detailed description of the invention
Fig. 1 is the structural schematic diagram convenient for interrupting the solid-liquid reaction kettle of reaction;
Fig. 2 is the top view convenient for interrupting inner cylinder in the solid-liquid reaction kettle of reaction.
In figure: 1- autoclave body;2- pillar;3- sleeve;4- spring;5- feeding-in solid body mouth;6- first motor;7- screw rod;In 8- Cylinder;9- guide rod;10- guide rail;11- through-hole;The second motor of 12-;13- transmission shaft;14- paddle;15- drive bevel gear;16- Left angular wheel;The right bevel gear of 17-;18- left rotary shaft;19- right spindle;20- agitating plate;21- drain pipe;22- inlet tube.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Please refer to Fig. 1,2, in the embodiment of the present invention, a kind of solid-liquid reaction kettle convenient for interrupting reaction, including autoclave body 1, branch Column 2, feeding-in solid body mouth 5, drain pipe 21 and inlet tube 22, the lower surface of the autoclave body 1 are fixedly connected with pillar 2, under pillar 2 End cap is equipped with sleeve 3, and pillar 2 can slide up and down in sleeve 3, and the inside of sleeve 3 is equipped with spring 4, the upper and lower ends of spring 4 It is fixedly connected respectively with pillar 2, sleeve 3, certain cushioning effect can be played using spring 4, the upper surface of autoclave body 1 is fixed to be connected It is connected to feeding-in solid body mouth 5, first motor 6, first motor 6 is clockwise and anticlockwise motor, and feeding-in solid body mouth 5 is connected to autoclave body 1, the first electricity The axle stretch end of machine 6 is fixedly connected with screw rod 7, and the top that screw rod 7 passes through autoclave body 1 is protruded into autoclave body 1, and the inside of autoclave body 1 is equipped with interior Cylinder 8, screw rod 7 runs through inner cylinder 8, and connect with the bottom thread of inner cylinder 8, and inner cylinder 8 is located at the lower section of feeding-in solid body mouth 5, by solid Reactant puts into feeding-in solid body mouth 5, falls into inner cylinder 8, the left and right sides of inner cylinder 8 has been respectively fixedly connected with guide rod 9, autoclave body 1 Inner wall be fixedly connected with guide rail 10, in the other end insertion guide rail 10 of guide rod 9, guide rod 9 can be along about 10 guide rail Sliding to drive 7 positive and negative rotation of screw rod, and then drives inner cylinder 8 to move up and down, inner cylinder 8 by controlling 6 positive and negative rotation of first motor Side wall be distributed with several through-holes 11, the lower surface of autoclave body 1 is fixedly connected with the second motor 12, and the axle stretch end of the second motor 12 is solid Surely it is connected with transmission shaft 13, the bottom that transmission shaft 13 passes through autoclave body 1 is protruded into autoclave body 1, and stirring is fixedly connected on transmission shaft 13 Leaf 14, the top of transmission shaft 13 are fixedly connected with drive bevel gear 15, and drive bevel gear 15 is respectively arranged on the left side and the right side left-hand rotation Axis 18, right spindle 19, left rotary shaft 18, right spindle 19 one end be respectively fixedly connected with left angular wheel 16, right bevel gear 17, left cone Gear 16, right bevel gear 17 engage with drive bevel gear 15 respectively, left rotary shaft 18, right spindle 19 the other end and autoclave body 1 it is interior Wall is rotatablely connected, and several agitating plates 20 have been respectively fixedly connected in left rotary shaft 18, right spindle 19, and the second motor 12 drives when running Transmission shaft 13 rotates, and then paddle 14 is driven to rotate, and stirs reaction solution, is uniformly mixed reaction solution, when transmission shaft 13 rotates It drives drive bevel gear 15 to rotate, and then drives left rotary shaft 18, right spindle 19 to rotate by left angular wheel 16, right bevel gear 17, And left rotary shaft 18, right spindle 19 turn on the contrary, finally agitating plate 20 is driven to rotate, stirring reaction solution using agitating plate 20 makes to react Liquid mixing is more uniform, improves reaction efficiency, and the right side wall of autoclave body 1 is fixedly connected with drain pipe 21, is equipped on drain pipe 21 Valve, the left side wall of autoclave body 1 are fixedly connected with inlet tube 22, are equipped with valve on inlet tube 22.
The working principle of the invention is: solid reactant is poured into feeding-in solid body mouth 5, solid reactant is fallen into inner cylinder 8, The valve on inlet tube 22 to be opened, liquid reactants are injected in autoclave body 1, control first motor 6 is run, and drive screw rod 7 to rotate, To drive inner cylinder 8 to move down, enter liquid reactants in inner cylinder 8 by guide rod 9, occurs with solid reactant anti- It answers, starts the second motor 12, drive transmission shaft 13 to rotate when the second motor 12 is run, and then paddle 14 is driven to rotate, agitation Reaction solution is uniformly mixed reaction solution, drives drive bevel gear 15 to rotate when transmission shaft 13 rotates, and then pass through left angular wheel 16, right bevel gear 17 drives left rotary shaft 18, right spindle 19 to rotate, and left rotary shaft 18, right spindle 19 turn on the contrary, final drive is stirred The rotation of plate 20 is mixed, stirring reaction solution using agitating plate 20, to mix reaction solution more uniform, reaction efficiency is improved, when needing to interrupt When reaction, control first motor 6 is inverted, and is driven screw rod 7 to rotate backward, so that inner cylinder 8 be driven to move up, is made solid reactant It is separated with liquid reactants, achievees the purpose that interrupt reaction, the present invention can generate vibration in the process of running, and pillar 2 can be It is slided up and down in sleeve 3, buffer function can be played using spring 4, reduce vibration.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (3)

1. a kind of solid-liquid reaction kettle convenient for interrupting reaction, including autoclave body (1), pillar (2), feeding-in solid body mouth (5), drain pipe (21) and inlet tube (22);It is characterized in that, the upper surface of the autoclave body (1) is fixedly connected with first motor (6), described first Motor (6) is clockwise and anticlockwise motor, and the axle stretch end of first motor (6) is fixedly connected with screw rod (7), and screw rod (7) passes through autoclave body (1) Top is protruded into autoclave body (1), and the inside of autoclave body (1) is equipped with inner cylinder (8), and screw rod (7) runs through inner cylinder (8), and the bottom with inner cylinder (8) Portion is threadedly coupled, and inner cylinder (8) is located at the lower section of feeding-in solid body mouth (5), and inner cylinder has been respectively fixedly connected with guiding at left and right sides of (8) Bar (9), the inner wall of autoclave body (1) are fixedly connected with guide rail (10), in other end insertion guide rail (10) of guide rod (9), inner cylinder (8) Side wall be distributed with several through-holes (11), the lower surface of autoclave body (1) is fixedly connected with the second motor (12), the second motor (12) Axle stretch end is fixedly connected with transmission shaft (13), and the bottom that transmission shaft (13) passes through autoclave body (1) is protruded into autoclave body (1), transmission shaft (13) it is fixedly connected at the top of drive bevel gear (15), drive bevel gear (15) is respectively arranged on the left side and the right side left rotary shaft (18), right spindle (19), left rotary shaft (18), right spindle (19) one end be respectively fixedly connected with left angular wheel (16), right cone tooth It takes turns (17), left angular wheel (16), right bevel gear (17) engage with drive bevel gear (15) respectively, left rotary shaft (18), right spindle (19) inner wall of the other end and autoclave body (1) is rotatablely connected, and has been respectively fixedly connected in left rotary shaft (18), right spindle (19) several Agitating plate (20), the right side wall of autoclave body (1) are fixedly connected with drain pipe (21), and valve, autoclave body (1) are equipped on drain pipe (21) Left side wall be fixedly connected with inlet tube (22), valve is installed, the lower surface of the autoclave body (1) is fixed to be connected on inlet tube (22) It is connected to pillar (2), the lower end of pillar (2) is arranged with sleeve (3), and the inside of sleeve (3) is equipped with spring (4), above and below spring (4) Both ends are fixedly connected with pillar (2), sleeve (3) respectively.
2. it is according to claim 1 convenient for interrupt reaction solid-liquid reaction kettle, which is characterized in that the autoclave body (1) it is upper Surface is fixedly connected with feeding-in solid body mouth (5), and feeding-in solid body mouth (5) is connected to autoclave body (1).
3. the solid-liquid reaction kettle according to claim 1 convenient for interrupting reaction, which is characterized in that on the transmission shaft (13) It is fixedly connected with paddle (14).
CN201711163116.7A 2017-11-21 2017-11-21 A kind of solid-liquid reaction kettle convenient for interrupting reaction Active CN107913656B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108636335A (en) * 2018-05-14 2018-10-12 苏昭缄 A kind of oscillatory type solid-liquid reaction kettle with crushing function
CN108652782A (en) * 2018-05-25 2018-10-16 李辉云 A kind of animal and veterinary Baoding diagnosing and treating apparatus
CN108722331A (en) * 2018-05-30 2018-11-02 天津朝花夕拾科技有限公司 A kind of Cosmetic Manufacture reaction kettle
CN112808219A (en) * 2021-02-07 2021-05-18 山东隆信药业有限公司 Continuous asphalt production reaction kettle
CN113680094B (en) * 2021-10-27 2021-12-31 东营明德化工有限公司 Crystallization kettle with automatic screening function
CN114405431B (en) * 2022-01-22 2024-04-09 山西同杰化学试剂有限公司 Multi-connected chemical synthesis reactor

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202700527U (en) * 2012-08-01 2013-01-30 陈建发 Quantitative reaction test tube
CN205833160U (en) * 2016-07-06 2016-12-28 唐山学院 A kind of solid-liquid separation multistage screening reactor
CN206276383U (en) * 2016-12-06 2017-06-27 熊向辉 The chemical industry stirred type retort that a kind of solid-liquid raw material separately mixes
CN206492508U (en) * 2017-02-16 2017-09-15 东莞市兰宝化工新材料有限公司 A kind of automatical and efficient reactor

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202700527U (en) * 2012-08-01 2013-01-30 陈建发 Quantitative reaction test tube
CN205833160U (en) * 2016-07-06 2016-12-28 唐山学院 A kind of solid-liquid separation multistage screening reactor
CN206276383U (en) * 2016-12-06 2017-06-27 熊向辉 The chemical industry stirred type retort that a kind of solid-liquid raw material separately mixes
CN206492508U (en) * 2017-02-16 2017-09-15 东莞市兰宝化工新材料有限公司 A kind of automatical and efficient reactor

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